Amorphous superfine calcium citrate production device

Abstract

The utility model belongs to the technical field of production of shaped superfine calcium citrate, and discloses an amorphous superfine calcium citrate production device which comprises a reaction kettle, a lantern ring is sleeved on the outer side of the reaction kettle, a clamping plate is embedded on the outer side of the lantern ring, a screw rod is fixedly connected to the top end of the clamping plate, a sleeve is arranged on the outer side of the screw rod in a sliding mode, and the sleeve is sleeved on the outer side of the sleeve. A rotating rod is rotatably connected to the output end of the motor; a stirring rod is fixedly connected to the bottom end of the rotating rod; a base is rotatably connected to the center position in the bottom end of the reaction kettle; a filter screen is rotatably connected to the top end of the base; the outer side of the heating wire is arranged between the reaction kettle and the filter screen, and through the scheme, the problems that calcium citrate is low in dissolving difficulty and difficult to absorb, calcium citrate particles with certain moisture are relatively high in viscosity, the processing process is tedious, and the cost is high in the processing process are solved.

Description

Technical Field

[0001] The utility model belongs to the technical field of production of shaped ultrafine calcium citrate, in particular to a production device for amorphous ultrafine calcium citrate. Background Art

[0002] Calcium is the fifth largest element in the human body. Amorphous ultrafine calcium citrate also has a high absorption rate and bioavailability, good solubility in water, is relatively easy to be absorbed by the human body, and has little irritation to the gastrointestinal tract. It is suitable for people with sensitive gastrointestinal tracts and can provide the human body with an appropriate amount of calcium. The absorption of calcium by the human body is subject to certain restrictions due to the insoluble organic calcium.

[0003] Meanwhile, patent application number 202023064186.7 discloses a granulating device for calcium citrate production, comprising a granulating device body, a raw material grinder, and a calcium flake dryer. A raw material inlet is fixedly mounted on the top of the granulating device body, and device fixing brackets are fixedly mounted around the bottom of the granulating device body. A drop pipe is fixedly mounted in the middle of the bottom of the granulating device body. This utility model, through its ingenious design, combines a raw material grinder, a raw material grinder, a fixed shaft, and a rotating shaft to conveniently solve the problem that existing granulating devices contain some large particles when granulating raw materials, making it difficult to grind the particles by chewing.

[0004] However, in the implementation of related technologies, it was found that the above-mentioned calcium citrate production granulation device has problems such as the difficulty in dissolving calcium citrate and absorbing it, the high viscosity between calcium citrate particles with a certain amount of water, the cumbersome processing process, and the high cost during the processing. Utility Model Content

[0005] In order to solve the problems raised in the above background technology, the utility model provides an amorphous ultrafine calcium citrate production device, which has the advantages of improving work efficiency by changing the previous processing method to integrate mixing, stirring and heating.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a device for producing amorphous ultrafine calcium citrate, comprising a reactor, a collar is sleeved on the outside of the reactor, a card plate is embedded on the outside of the collar, a screw rod is fixedly connected to the top end of the card plate, a sleeve is slidingly provided on the outside of the screw rod, an extension seat is fixedly connected to the top end of the sleeve, a motor is fixedly connected to the top end of the extension seat, a rotating rod is rotatably connected to the output end of the motor, a stirring rod is fixedly connected to the bottom end of the rotating rod, a base is rotatably connected to the center position of the bottom end of the reactor, a filter is rotatably connected to the top end of the base, a heating wire is attached to the outside of the filter, and the outside of the heating wire is arranged between the reactor and the filter.

[0007] Preferably, a threaded groove is provided at the top of the clamping plate, and a tightening pin is spirally connected inside the threaded groove of the clamping plate. The tightening pin passes through the interior of the clamping plate and is fixedly connected with the top of the collar.

[0008] Preferably, a drainage hole is opened on the left side of the bottom end of the reactor, and the bottom end of the drainage hole of the reactor is fixedly connected to a water collecting pipe. A discharge hole is opened on the right side of the bottom end of the reactor, and the bottom end of the discharge hole of the reactor is fixedly connected to a liquid storage tank.

[0009] Preferably, an infusion tube is fixedly connected to the outside of the liquid storage tank, and an upper cover is provided through the other end of the infusion tube, and the bottom end of the upper cover is attached to the top of the reactor.

[0010] Preferably, a discharge pipe is fixedly connected to the left side of the top of the reactor, a valve is rotatably connected inside the discharge pipe, a handle is fixedly connected to the top of the valve, and a stirring tank is fixedly connected to the left side of the discharge pipe.

[0011] Preferably, the top of the stirring tank is fixedly connected to a driving source, the output end of the driving source is rotatably connected to a stirring frame, the outer side of the stirring frame is rotatably connected to a scraper, and the outer side of the scraper is fitted to the inner wall of the stirring tank.

[0012] Preferably, the outer side of the rotating rod passes through the interior of the discharge pipe, and the stirring rod is rotatably arranged inside the filter screen.

[0013] Compared with the prior art, the beneficial effects of the present invention are as follows:

[0014] 1. The utility model reduces the reaction time by adding purified water to the slurry of calcium carbonate inside the stirring tank. By arranging the stirring tank on the upper side of the reactor, the slurry-adjusted calcium carbonate can be continuously added to the food-grade citric acid finished product solution and stirred at a constant temperature, thereby reducing the number of steps. The solution is added in an appropriate amount according to the pH value inside the reactor. Through the comprehensive control of the entire reaction process, the obtained calcium citrate has good shape and fine particle size, which is conducive to the subsequent steps.

[0015] 2. The utility model adds a solution collecting device at the bottom of the reactor, so that the separated mother liquor can be returned to the process of generating calcium hydrogen citrate for recycling. After use, the reactor is flushed by controlling the opening of the three-way pipe of the liquid storage tank, and the sewage is discharged from the inside of the water collecting pipe, which is convenient for subsequent use. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 This is a schematic diagram of the overall structure of the utility model;

[0017] Figure 2 This is a schematic diagram of the ring structure of the utility model;

[0018] Figure 3 It is the reaction kettle structure schematic view of the utility model;

[0019] Figure 4 It is the stirring tank structure schematic view of the utility model;

[0020] Figure 5 It is the stirring frame structure schematic view of the utility model.

[0021] In the drawing: 1, reaction kettle; 2, collar; 3, clamping plate; 4, screw rod; 5, sleeve; 6, extension seat; 7, motor; 8, rotating rod; 9, stirring rod; 10, filter screen; 11, heating wire; 12, base; 13, abutting pin; 14, rotating handle; 15, discharge pipe; 16, liquid delivery pipe; 17, liquid storage tank; 18, water collecting pipe; 19, valve; 20, stirring tank; 21, driving source; 22, stirring frame; 23, scraper; 24, upper cover. DETAILED DESCRIPTION

[0022] The technical solutions in the embodiments of the utility model will be clearly and completely described below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor fall within the scope of protection of the utility model.

[0023] As Figures 1 to 5 shown, the utility model provides a kind of amorphous superfine calcium citrate production device, including reaction kettle 1, the outside of reaction kettle 1 is equipped with collar 2, the outside of collar 2 is embedded with clamping plate 3, and the top of clamping plate 3 is fixedly connected with screw rod 4, when screw rod 4 rotates, sleeve 5 is slid, the top of sleeve 5 is fixedly connected with extension seat 6, the top of extension seat 6 is fixedly connected with motor 7, the output end of motor 7 is rotatably connected with rotating rod 8, the bottom of rotating rod 8 is fixedly connected with stirring rod 9, the bottom inside center position of stirring reaction kettle 1 is rotatably connected with base 12, the top of base 12 is rotatably connected with filter screen 10, and the hole of filter screen 10 is smaller, heating wire 11 is attached to the outside of filter screen 10, heating wire 11 is arranged between reaction kettle 1 and filter screen 10, for drying heating to the separated calcium citrate.

[0024] Specifically, the top of clamping plate 3 is provided with threaded groove, and abutting pin 13 is spirally connected in the threaded groove of clamping plate 3, abutting pin 13 penetrates the inside of clamping plate 3 and is fixedly connected with the top of collar 2, and is disassembled when not in use.

[0025] Furthermore, a drainage hole is opened on the left side of the bottom end of the reactor 1, and a water collecting pipe 18 is fixedly connected to the bottom end of the drainage hole of the reactor 1, which is used to collect sewage after flushing the reactor 1, and a discharge hole is opened on the right side of the bottom end of the reactor 1, and a liquid storage tank 17 is welded and fixed to the bottom end of the discharge hole of the reactor 1, and a three-way valve is added to the outside of the water collecting pipe 18 and the liquid storage tank 17, which can be opened and closed according to actual conditions.

[0026] Furthermore, the outside of the liquid storage tank 17 is fixedly connected to a liquid infusion tube 16 , and the other end of the liquid infusion tube 16 is penetrated by an upper cover 24 , and the bottom end of the upper cover 24 is attached to the top of the reactor 1 to seal the material inside the reactor 1 .

[0027] It is worth noting that a discharge pipe 15 is fixedly connected to the left side of the top of the reactor 1, and a valve 19 is rotatably connected inside the discharge pipe 15. The top of the valve 19 is fixedly connected to a handle 14, which drives the valve 19 to rotate. The slurry can be discharged from the discharge port of the valve 19, and the left side of the discharge pipe 15 is fixedly connected to a stirring tank 20.

[0028] It is worth noting that the top of the stirring tank 20 is fixedly connected to a driving source 21, the output end of the driving source 21 is rotatably connected to a stirring frame 22, the outer side of the stirring frame 22 is rotatably connected to a scraper 23, and the outer side of the scraper 23 is attached to the inner wall of the stirring tank 20 to scrape off the slurry material attached to the outside of the stirring tank 20, thereby improving the slurrying efficiency.

[0029] It is worth mentioning that the outer side of the rotating rod 8 passes through the interior of the discharge pipe 15, and the stirring rod 9 rotates inside the filter 10, which is convenient for mechanically crushing the calcium citrate and then packaging to obtain amorphous ultrafine calcium citrate.

[0030] Among them, the motor 7 and the driving source 21 are prior art and will not be described in detail. At the same time, the present invention also includes a power supply, a controller and a switch, which are not the main technical points of the present patent and will not be described in detail. The "front, back, left and right" perspectives of the present device are as follows: Figure 1 The direction shown in the figure is the reference.

[0031] Working principle:

[0032] First, the staff pours calcium carbonate into the interior of the mixing tank 20 and mixes it with purified water. The driving source 21 drives the stirring frame 22 to stir the slurry material. During the stirring process, the scraper 23 on the outside scrapes the slurry material attached to the outside of the mixing tank 20. Then, the handle 14 at the top of the discharge pipe 15 connected to the mixing tank 20 is rotated. The handle 14 drives the valve 19 to rotate, and the slurry material is discharged from the circular hole of the valve 19 and enters the interior of the reactor 1. Then, the food-grade citric acid product is dissolved with purified water to obtain a food-grade citric acid product solution. The slurry-mixed calcium carbonate is continuously added to the food-grade citric acid product solution for processing. The heating wire 11 is turned on and the motor 7 is started. The motor 7 drives the rotating rod 8 at the bottom to rotate, and the rotating rod 8 drives the stirring rod 9 to rotate. 9 rotates inside the filter 10, and the second solid-liquid separation is carried out after the reaction is completed. The base 12 drives the filter 10 to rotate, and the liquid is swung to the outside of the reactor 1 under the action of centrifugal force and flows into the inside of the liquid storage tank 17. The separated mother liquor can be returned to the process of generating calcium hydrogen citrate for recycling. The calcium citrate solid is obtained inside the filter 10, and the separated calcium citrate is dried and heated. The dried calcium citrate is mechanically crushed and then packaged to obtain amorphous ultrafine calcium citrate. When the processing is completed, the reactor 1 is rinsed, and the water flows to the water collection pipe 18. A three-way valve is added to the outside of the water collection pipe 18 and the liquid storage tank 17, which can be opened and closed according to actual conditions. After the solution flows to the liquid storage tank 17, it flows to the inside of the reactor 1 through the infusion pipe 16, which is convenient for subsequent use.

[0033] It should be noted that, in this document, relational terms such as first and second, etc., are used only to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any actual relationship or order between these entities or operations. Moreover, the terms "comprises," "comprising," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that includes a list of elements includes not only those elements but also other elements not explicitly listed, or elements inherent to such process, method, article, or apparatus.

[0034] Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations may be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A production device for amorphous ultrafine calcium citrate, comprising a reactor (1), characterized in that: The outer side of the reactor (1) is provided with a sleeve (2), the outer side of the sleeve (2) is provided with a card plate (3) in an inlaid manner, the top end of the card plate (3) is fixedly connected to a screw rod (4), the outer side of the screw rod (4) is provided with a sleeve (5) for sliding, the top end of the sleeve (5) is fixedly connected to an extension seat (6), the top end of the extension seat (6) is fixedly connected to a motor (7), the output end of the motor (7) is rotatably connected to a rotating rod (8), the bottom end of the rotating rod (8) is fixedly connected to a stirring rod (9), the bottom center position of the reactor (1) is rotatably connected to a base (12), the top end of the base (12) is rotatably connected to a filter screen (10), the outer side of the filter screen (10) is affixed with a heating wire (11), and the outer side of the heating wire (11) is provided between the reactor (1) and the filter screen (10).

2. The amorphous ultrafine calcium citrate production device according to claim 1, characterized in that: A thread groove is provided at the top of the clamping plate (3), and a tightening pin (13) is spirally connected inside the thread groove of the clamping plate (3). The tightening pin (13) passes through the interior of the clamping plate (3) and is fixedly connected to the top of the collar (2).

3. The device for producing amorphous ultrafine calcium citrate according to claim 1, characterized in that: A drainage hole is provided on the left side of the bottom end of the reactor (1), and a water collecting pipe (18) is fixedly connected to the bottom end of the drainage hole of the reactor (1). A discharge hole is provided on the right side of the bottom end of the reactor (1), and a liquid storage tank (17) is fixedly connected to the bottom end of the discharge hole of the reactor (1).

4. The device for producing amorphous ultrafine calcium citrate according to claim 3, characterized in that: The outer side of the liquid storage tank (17) is fixedly connected to a liquid infusion tube (16), and the other end of the liquid infusion tube (16) is penetrated by an upper cover (24), and the bottom end of the upper cover (24) is attached to the top of the reactor (1).

5. The device for producing amorphous ultrafine calcium citrate according to claim 3, characterized in that: A discharge pipe (15) is fixedly connected to the left side of the top of the reactor (1), a valve (19) is rotatably connected inside the discharge pipe (15), a handle (14) is fixedly connected to the top of the valve (19), and a stirring tank (20) is fixedly connected to the left side of the discharge pipe (15).

6. The device for producing amorphous ultrafine calcium citrate according to claim 5, characterized in that: The top end of the stirring tank (20) is fixedly connected to a driving source (21), the output end of the driving source (21) is rotatably connected to a stirring frame (22), the outer side of the stirring frame (22) is rotatably connected to a scraper (23), and the outer side of the scraper (23) is arranged in contact with the inner wall of the stirring tank (20).

7. The device for producing amorphous ultrafine calcium citrate according to claim 1, characterized in that: The outer side of the rotating rod (8) passes through the inside of the discharge pipe (15), and the stirring rod (9) is rotatably arranged inside the filter screen (10).

Images