Constant-temperature reaction kettle for synthesizing cyproconazole

Abstract

The utility model discloses a constant-temperature reaction kettle for synthesizing cyproconazole, which belongs to the technical field of chemical solvent preparation equipment, and is characterized by comprising a constant-temperature reaction kettle body, a constant-temperature control channel arranged on the left side of the constant-temperature reaction kettle body, and an auxiliary mechanism arranged on the left side of the constant-temperature reaction kettle body, the auxiliary mechanism comprises a bearing assembly and an auxiliary cleaning assembly, the bearing assembly is arranged on the left side of the constant-temperature reaction kettle, the auxiliary cleaning assembly is arranged at the top of the bearing assembly, and the bearing assembly and the auxiliary cleaning assembly are arranged so that the bearing assembly can be communicated with a temperature control jacket output pipe arranged outside the constant-temperature reaction kettle body; and the bearing assembly can quickly prepare a cleaning solution to dissolve and clean a scale layer formed on the inner wall of the temperature control jacket, and meanwhile, the auxiliary cleaning assembly can continuously output airflow into the temperature control jacket through the bearing assembly, so that strong convection is generated in the temperature control jacket, and the cleaning effect of the cleaning solution is enhanced.

Description

Technical Field

[0001] This utility model relates to the field of chemical solvent preparation equipment technology, and in particular to a constant temperature reaction vessel for synthesizing cycloprozac. Background Technology

[0002] A constant-temperature reactor is a container for physical or chemical reactions, and it has its own temperature control system to control the reaction temperature.

[0003] In the production of cyproconazole, if the powder introduced contains particulate matter, it may not be fully crushed, resulting in insufficient mixing and wasting raw materials.

[0004] An existing patent (publication number: CN218359255U) discloses a cyproconazole synthesis apparatus, relating to the field of chemical solvent preparation technology. The apparatus includes a main body with an inlet on one side of its top and a motor on the other side. The motor is driven by an output shaft to a rotation and translation device, including a screw. A nut is threaded onto the outer side of the screw, and a hollow sleeve is fixedly connected to the bottom of the nut. Limiting blocks are located on both sides of the nut, and a movable rod is fixedly connected to the top of each limiting block. A stirring plate is fixedly connected to the outer side of the hollow sleeve. In this cyproconazole synthesis apparatus, when raw material is added through the inlet, starting the motor causes the movable rod to move up and down. This, combined with the limiting blocks and the screw, causes the nut to rotate and move the hollow sleeve up and down. The stirring plate, crushing blocks, and curved blocks further crush large particles of raw material, resulting in more thorough mixing and improved synthesis efficiency.

[0005] To address the aforementioned problems, existing patents offer solutions. However, existing constant-temperature reactors generally consist of a reactor body, a temperature control jacket, a stirring device, and a temperature control system. During use, temperature control is directly achieved through the temperature control jacket. However, during use, impurities in the medium may deposit and form scale on the inner wall of the jacket. This scale increases thermal resistance and affects heat transfer efficiency. Furthermore, the medium within the jacket may contain corrosive components, increasing the risk of jacket corrosion, leading to equipment malfunctions and safety accidents. The presence of scale also prevents the heating or cooling process from proceeding at the expected speed and intensity, interfering with the temperature sensor's signal feedback and causing the temperature controller to inaccurately adjust the heating or cooling devices. Existing patents fail to address these issues, thus hindering user convenience.

[0006] Therefore, a constant-temperature reaction vessel for synthesizing cycloprozac is proposed. Utility Model Content

[0007] The purpose of this invention is to provide a constant-temperature reactor for synthesizing cyproconazole, addressing the problem that existing constant-temperature reactors generally consist of a reactor body, a temperature control jacket, a stirring device, and a temperature control system. During use, the temperature is directly controlled through the temperature control jacket. However, during operation, impurities in the medium may deposit and form scale on the inner wall of the jacket. This scale increases thermal resistance and affects heat transfer efficiency. Furthermore, the medium within the jacket may contain corrosive components, increasing the risk of jacket corrosion, leading to equipment malfunctions and safety accidents. The presence of scale also prevents heating or cooling from proceeding at the expected speed and intensity, interfering with the temperature sensor's signal feedback and causing the temperature controller to inaccurately adjust the heating or cooling devices. Existing patents cannot solve this problem, thus hindering user convenience.

[0008] To achieve the above objectives, the present invention provides the following technical solution: a constant temperature reactor for synthesizing cycloproconazole, comprising a constant temperature reactor body, a constant temperature control channel provided on the left side of the constant temperature reactor body, and an auxiliary mechanism provided on the left side of the constant temperature reactor body, the auxiliary mechanism comprising a support component and an auxiliary cleaning component, the support component being provided on the left side of the constant temperature reactor, and the auxiliary cleaning component being provided on top of the support component;

[0009] The supporting assembly includes a supporting pipe, a water output pipe, an electric stirring tank, a support frame, and a control pipe. The supporting pipe is connected to the left side of the constant temperature control channel, the water output pipe is connected to the left side of the top of the supporting pipe, the electric stirring tank is set at the top of the supporting pipe, the support frame is bolted to the bottom of the outside of the electric stirring tank, and the control pipe is connected to the bottom of the electric stirring tank.

[0010] Preferably, the auxiliary cleaning component includes an air compressor disposed at the bottom of the carrier pipe, and a pipe limiting bracket disposed at the top of the air compressor, the top of which is fixedly connected to the rear side of the carrier pipe.

[0011] Preferably, a vent pipe is provided on the right side of the top of the air compressor, and the bottom of the vent pipe is connected to the top right side of the constant temperature reaction vessel body.

[0012] Preferably, the top of the air compressor is provided with a controllable airflow output pipe, the top of the controllable airflow output pipe is connected to the output end of the top of the air compressor, and a metal mesh plate is fixedly connected to the bottom of the inner side of the controllable airflow output pipe.

[0013] Preferably, the top of the constant temperature reactor is provided with an auxiliary component, the auxiliary component including a bent pipe connected to the top of the vent pipe, a sealing valve being provided at the bottom of the bent pipe, and the right side of the sealing valve being connected to the inside of the vent pipe.

[0014] Preferably, a closed sleeve is snapped onto the top of the inner side of the bent tube, and the closed sleeve is cylindrical in shape.

[0015] Preferably, flanges are provided on both sides of the bearing pipe, and a throttling valve is provided on the inner side of the water output pipe.

[0016] Preferably, the bottom of the electric mixing tank is close to the top of the support tube, the inner side of the support frame is close to the surface of the support tube, and the bottom of the control tube is connected to the top of the support tube.

[0017] Preferably, the inner side of the pipe limiting bracket is arc-shaped, and the inner side of the pipe limiting bracket is close to the surface of the air compressor output channel.

[0018] Preferably, a metal splash guard is fixedly connected to the bottom of the inner side of the vent pipe, and the vent pipe is inclined.

[0019] Compared with the prior art, the beneficial effects of this utility model are:

[0020] 1. By setting up a support component, when using the constant temperature reactor for synthesizing cyclopropiconol, the user can combine the support component with the constant temperature control channel so that the support component can be connected to the output pipe of the temperature control jacket set outside the constant temperature reactor body. This allows the support component to quickly produce cleaning fluid and input it into the temperature control jacket to dissolve and clean the scale layer formed on the inner wall of the temperature control jacket.

[0021] 2. This application, by setting up an auxiliary cleaning component, allows the user to combine the auxiliary cleaning component with the support component when using the thermostatic reactor for synthesizing cycloprozac. This allows the auxiliary cleaning component to continuously output airflow into the temperature control jacket through the support component, thereby generating strong convection inside the temperature control jacket. This enhances the contact and friction between the cleaning fluid and the inner wall of the jacket. For stubborn dirt adhering to the inner wall of the jacket, the agitation of the air bubbles can loosen it, making it easier to be dissolved or washed away by the cleaning fluid. This prevents the scale layer from increasing thermal resistance and affecting heat transfer efficiency. At the same time, it avoids the scale layer containing corrosive components from corroding the jacket, leading to equipment failure and safety accidents. Furthermore, removing the presence of scale layer prevents the heating or cooling process from not proceeding at the expected speed and intensity, ensuring normal signal feedback from the temperature sensor so that the temperature controller can accurately adjust the heating or cooling of the thermostatic reactor body. Attached Figure Description

[0022] Figure 1 This is an overall structural diagram of a constant-temperature reaction vessel for synthesizing cycloprozacol according to this utility model;

[0023] Figure 2 This is a schematic diagram of the auxiliary mechanism in this utility model;

[0024] Figure 3 This is a schematic diagram of the structure of the load-bearing component in this utility model;

[0025] Figure 4 This is a schematic diagram of the auxiliary cleaning component in this utility model;

[0026] Figure 5 This is a schematic diagram of the auxiliary components in this utility model.

[0027] In the diagram, 1. Constant temperature reactor body; 2. Constant temperature control channel; 3. Auxiliary mechanism; 301. Bearing component; 301a. Bearing pipe; 301b. Water output pipe; 301c. Electric stirring tank; 301d. Support frame; 301e. Control pipe; 302. Auxiliary cleaning component; 302a. Air compressor; 302b. Pipe limiting frame; 302c. Vent pipe; 302d. Controllable airflow output pipe; 4. Auxiliary component; 401. Bending pipe; 402. Closing valve; 403. Closing sleeve. Detailed Implementation

[0028] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0029] Please see Figure 1-5 A constant temperature reactor for synthesizing cycloproconazole includes a constant temperature reactor body 1, a constant temperature control channel 2 is provided on the left side of the constant temperature reactor body 1, and an auxiliary mechanism 3 is provided on the left side of the constant temperature reactor body 1. The auxiliary mechanism 3 includes a support component 301 and an auxiliary cleaning component 302. The support component 301 is located on the left side of the constant temperature reactor, and the auxiliary cleaning component 302 is located on top of the support component 301.

[0030] The supporting component 301 includes a supporting pipe 301a, a water output pipe 301b, an electric stirring tank 301c, a support frame 301d, and a control pipe 301e. The supporting pipe 301a is connected to the left side of the constant temperature control channel 2, the water output pipe 301b is connected to the left side of the top of the supporting pipe 301a, the electric stirring tank 301c is set at the top of the supporting pipe 301a, the support frame 301d is bolted to the bottom of the outside of the electric stirring tank 301c, and the control pipe 301e is connected to the bottom of the electric stirring tank 301c.

[0031] In this embodiment: by setting up a carrier pipe 301a, a water output pipe 301b, an electric stirring tank 301c, a support frame 301d, and a control pipe 301e, when using this constant temperature reactor for synthesizing cycloprozac, due to the long-term use of the temperature control jacket to control the temperature of the constant temperature reactor body 1, dirt accumulates on the inner wall of the temperature control jacket. This allows the user to quickly prepare a cleaning agent using the electric stirring tank 301c supported by the support frame 301d, and then input it into the carrier pipe 301a and the constant temperature control channel 2 through the control pipe 301e. Afterwards, the water input through the water output pipe 301b is sent into the temperature control jacket outside the constant temperature reactor body 1, so that the dirt on the surface of the constant temperature reactor body 1 and the inner wall of the temperature control jacket is soaked in the cleaning liquid to dissolve and clean the scale layer formed on the inner wall of the temperature control jacket.

[0032] Specifically, such as Figure 2 , Figure 4 As shown, the auxiliary cleaning component 302 includes an air compressor 302a disposed at the bottom of the carrier pipe 301a, and a pipe limiting bracket 302b disposed on the top of the air compressor 302a. The top of the pipe limiting bracket 302b is fixedly connected to the rear side of the carrier pipe 301a.

[0033] Specifically, such as Figure 2 , Figure 4 As shown, an air vent pipe 302c is provided on the right side of the top of the air compressor 302a, and the bottom of the air vent pipe 302c is connected to the top right side of the constant temperature reactor body 1.

[0034] Specifically, such as Figure 2 , Figure 4 As shown, the top of the air compressor 302a is provided with a controllable airflow output pipe 302d, the top of the controllable airflow output pipe 302d is connected to the output end of the top of the air compressor 302a, and a metal mesh plate is fixedly connected to the bottom of the inner side of the controllable airflow output pipe 302d.

[0035] In this embodiment: by setting up an air compressor 302a, a pipe limiting frame 302b, a vent pipe 302c, and a controllable airflow output pipe 302d, when using the isothermal reactor for synthesizing cycloprozacol, the user can use the air compressor 302a to output compressed airflow and open the vent pipe 302c connected to the right side of the isothermal reactor body 1. Then, the airflow is delivered through the air compressor 302a output pipe limited inside the pipe limiting frame 302b. Afterward, the airflow input into the controllable airflow output pipe 302d can enter the support pipe 301a, so that the air compressor 302a can continuously output airflow into the temperature control jacket through the support pipe 301a, thereby generating strong convection inside the temperature control jacket. The vent pipe 302c can continuously discharge excess gas, thereby making the airflow output by the air compressor 302a form a cycle.

[0036] Specifically, such as Figure 5 As shown, an auxiliary component 4 is provided on the top of the constant temperature reactor. The auxiliary component 4 includes a bent pipe 401 connected to the top of the vent pipe 302c. A shut-off valve 402 is provided at the bottom of the bent pipe 401. The right side of the shut-off valve 402 is connected to the inside of the vent pipe 302c.

[0037] Specifically, such as Figure 5 As shown, a closed sleeve 403 is snapped into the top of the inner side of the bent tube 401, and the closed sleeve 403 is cylindrical in shape.

[0038] In this embodiment: by setting up a bending pipe 401, a sealing valve 402 and a sealing sleeve 403, the bending pipe 401, the sealing valve 402 and the sealing sleeve 403 cooperate with each other to seal the vent pipe 302c and control the internal flow of the vent pipe 302c.

[0039] Specifically, such as Figure 3 As shown, flanges are provided on both sides of the bearing pipe 301a, and a throttle valve is provided on the inner side of the water output pipe 301b.

[0040] Specifically, such as Figure 3 As shown, the bottom of the electric mixing tank 301c is close to the top of the support tube 301a, the inner side of the support frame 301d is close to the surface of the support tube 301a, and the bottom of the control tube 301e is connected to the top of the support tube 301a.

[0041] Specifically, such as Figure 4 As shown, the inner side of the pipe limiting bracket 302b is arc-shaped, and the inner side of the pipe limiting bracket 302b is close to the surface of the output channel of the air compressor 302a.

[0042] Specifically, such as Figure 4 As shown, a metal splash guard is fixedly connected to the bottom of the inner side of the vent pipe 302c, and the vent pipe 302c is inclined.

[0043] In this embodiment: by setting up a support pipe 301a, a water output pipe 301b, an electric mixing tank 301c, a support frame 301d, a control pipe 301e, a pipe limiting frame 302b, and a vent pipe 302c, the support pipe 301a, the water output pipe 301b, the electric mixing tank 301c, the support frame 301d, the control pipe 301e, the pipe limiting frame 302b, and the vent pipe 302c cooperate with each other to quickly produce cleaning agent and input it into the constant temperature control channel 2. At the same time, it can restrict the output pipe of the air compressor 302a and discharge excess gas inside the constant temperature control channel 2.

[0044] Working principle: First, it is used in the synthesis of cyproconazole. When using this thermostatic reactor for cyproconazole synthesis, due to prolonged use of the temperature control jacket to control the temperature of the reactor body 1, dirt accumulates on the inner wall of the temperature control jacket. Therefore, the user can quickly prepare a cleaning agent using the electric stirring tank 301c supported by the support frame 301d. This cleaning agent is then introduced into the support pipe 301a and the thermostatic control channel 2 through the control pipe 301e. Water is then introduced through the water output pipe 301b and sent into the temperature control jacket outside the reactor body 1. This allows the cleaning liquid to soak the dirt on the surface of the reactor body 1 and the inner wall of the temperature control jacket, dissolving and cleaning the temperature control jacket. The scale layer formed on the inner wall of the jacket can be removed. At the same time, the user can use the air compressor 302a to output compressed airflow and open the vent pipe 302c connected to the right side of the constant temperature reactor body 1. Then, the airflow is transported through the air compressor 302a output pipe restricted inside the pipe limiting frame 302b. After that, the airflow inside the controllable airflow output pipe 302d can enter the bearing pipe 301a, so that the air compressor 302a can continuously output airflow into the temperature control jacket through the bearing pipe 301a, thereby generating strong convection inside the temperature control jacket. The vent pipe 302c can continuously discharge excess gas, thereby making the airflow output by the air compressor 302a form a cycle.

[0045] The above are merely preferred embodiments of the present utility model and are not intended to limit the present utility model. Any modifications, equivalent substitutions, and improvements made within the scope of the present utility model should be included within the protection scope of the present utility model.

Claims

1. A constant-temperature reactor for synthesizing cyproconazole, comprising a constant-temperature reactor body (1), wherein a constant-temperature control channel (2) is provided on the left side of the constant-temperature reactor body (1), characterized in that: An auxiliary mechanism (3) is provided on the left side of the constant temperature reactor body (1). The auxiliary mechanism (3) includes a support component (301) and an auxiliary cleaning component (302). The support component (301) is located on the left side of the constant temperature reactor, and the auxiliary cleaning component (302) is located on the top of the support component (301). The supporting assembly (301) includes a supporting pipe (301a), a water output pipe (301b), an electric stirring tank (301c), a support frame (301d), and a control pipe (301e). The supporting pipe (301a) is connected to the left side of the constant temperature control channel (2). The water output pipe (301b) is connected to the left side of the top of the supporting pipe (301a). The electric stirring tank (301c) is located at the top of the supporting pipe (301a). The support frame (301d) is bolted to the bottom of the outside of the electric stirring tank (301c). The control pipe (301e) is connected to the bottom of the electric stirring tank (301c).

2. The isothermal reactor for synthesizing cyproconazole according to claim 1, characterized in that: The auxiliary cleaning component (302) includes an air compressor (302a) disposed at the bottom of the support pipe (301a), and a pipe limiting bracket (302b) disposed at the top of the air compressor (302a), the top of the pipe limiting bracket (302b) being fixedly connected to the rear side of the support pipe (301a).

3. The isothermal reactor for synthesizing cyproconazole according to claim 2, characterized in that: A vent pipe (302c) is provided on the right side of the top of the air compressor (302a), and the bottom of the vent pipe (302c) is connected to the top right side of the constant temperature reactor body (1).

4. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 3, characterized in that: The air compressor (302a) is provided with a controllable airflow output pipe (302d) at its top. The top of the controllable airflow output pipe (302d) is connected to the output end of the top of the air compressor (302a). A metal mesh plate is fixedly connected to the bottom of the inner side of the controllable airflow output pipe (302d).

5. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 1, characterized in that: The constant temperature reactor is provided with an auxiliary component (4) at the top. The auxiliary component (4) includes a bent pipe (401) connected to the top of the vent pipe (302c). A shut-off valve (402) is provided at the bottom of the bent pipe (401). The right side of the shut-off valve (402) is connected to the inside of the vent pipe (302c).

6. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 5, characterized in that: The top of the inner side of the bent tube (401) is fitted with a closed sleeve (403), and the closed sleeve (403) is cylindrical in shape.

7. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 1, characterized in that: Flanges are provided on both sides of the bearing pipe (301a), and a throttling valve is provided on the inner side of the water output pipe (301b).

8. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 1, characterized in that: The bottom of the electric mixing tank (301c) is close to the top of the support tube (301a), the inner side of the support frame (301d) is close to the surface of the support tube (301a), and the bottom of the control tube (301e) is connected to the top of the support tube (301a).

9. The isothermal reactor for synthesizing cyproconazole according to claim 2, characterized in that: The inner side of the pipe limiting bracket (302b) is arc-shaped, and the inner side of the pipe limiting bracket (302b) is close to the surface of the air compressor (302a) output channel.

10. The isothermal reactor for synthesizing cycloprozac alcohol according to claim 3, characterized in that: A metal splash guard is fixedly connected to the bottom of the inner side of the vent pipe (302c), and the vent pipe (302c) is inclined.

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