Polymerization ammonia introduction mixing device

Abstract

The utility model discloses a polymerization ammonia introduction mixing device, which relates to the technical field of ammonia mixing devices and comprises a hollow disc, a matched flange is mounted at the top of the hollow disc, a feed pipe and an ammonia output pipe are connected onto the side wall of the hollow disc, a discharge pipe is mounted at the bottom of the hollow disc, a gear pump is mounted on the feed pipe, and a gear pump is mounted on the ammonia output pipe. The ammonia output pipe is provided with a pressure sensor and a pressure regulating valve, the interior of the hollow disc is of a cavity structure, and one end of the feeding pipe and one end of the ammonia output pipe are located in the cavity; according to the spinning solution conveying device, spinning solution continuously enters the hollow disc through the feeding pipe, meanwhile, ammonia gas is continuously introduced through the ammonia gas output pipe, continuous mixing of the spinning solution in the conveying process is achieved, and continuous mixing of the spinning solution is achieved through the cavity structure in the hollow disc and the turbine arranged in the turbine connecting piece. The spinning solution and the ammonia gas are fully mixed in the transportation process, and the materials are further stirred and mixed through the rotation of the turbine, so that the mixing uniformity is ensured.

Description

TECHNICAL FIELD

[0001] The utility model relates to ammonia mixing device technical field, specifically is polymeric ammonia mixing device. BACKGROUND

[0002] Carbon fiber polymerization spinning dope needs to be ammoniated in the production process, the main purpose of this step is to react with the carboxyl in the resin to generate ammonium salt, this chemical reaction can significantly improve the hydrophilicity of PAN copolymer, and effectively inhibit the generation of large pores, thereby preventing the phenomenon of white loss of the yarn, however, the traditional ammoniation process has some efficiency problems.

[0003] The spinning dope generated by polymerization reaction has a large viscosity, which makes the diffusion and mixing of ammonia gas difficult, the amount of spinning dope generated per kettle is large, usually between 5 tons and 30 tons, in order to ensure that ammonia gas and spinning dope can fully react, a small amount of ammonia gas needs to be introduced, which leads to a long operation time, thereby affecting the production efficiency. UTILITY MODEL CONTENT

[0004] The utility model aims at providing polymeric ammonia mixing device to solve the problems in the above background.

[0005] In order to solve the above technical problems, the polymeric ammonia mixing device provided by the utility model comprises a hollow disc, a matching flange is installed on the top of the hollow disc, a feed pipe and an ammonia gas output pipe are connected to the sidewall of the hollow disc, a discharge pipe is installed at the bottom of the hollow disc, a gear pump is installed on the feed pipe, a pressure sensor and a pressure regulating valve are installed on the ammonia gas output pipe, the inside of the hollow disc is a cavity structure, and one end of the feed pipe and the ammonia gas output pipe is located in the cavity.

[0006] Further, a turbine connecting piece is installed at the joint of the discharge pipe and the hollow disc, and a turbine is arranged in the turbine connecting piece.

[0007] Further, flange bolts are installed at the top of the matching flange at equal intervals, bolt holes matched with the flange bolts are arranged outside the cavity in the hollow disc, and the hollow disc and the matching flange are detachably connected through the flange bolts.

[0008] Further, a flange pad is installed at the joint of the hollow disc and the matching flange.

[0009] Further, a visual window is arranged on the outer wall of the hollow disc, and the visual window is made of transparent acrylic material.

[0010] Further, a controller is installed on the outside of the hollow disc, and the output end of the controller is electrically connected with the input end of the pressure sensor, the pressure regulating valve, the gear pump and the turbine.

[0011] Compared with the prior art, the polymeric ammonia mixing device has the beneficial effects that:

[0012] 1、The polymeric ammonia mixing device has the beneficial effects that:

[0013] 2、The polymeric ammonia mixing device has the beneficial effects that: BRIEF DESCRIPTION OF DRAWINGS

[0014] Figure 1 Fig. 1 is a structural schematic view of the polymeric ammonia mixing device;

[0015] Figure 2 Fig. 2 is a structural schematic view of the polymeric ammonia mixing device in a top view;

[0016] Figure 3 Fig. 3 is a structural schematic view of the hollow disc in the polymeric ammonia mixing device;

[0017] Figure 4 Fig. 4 is a structural schematic view of the polymeric ammonia mixing device in a side view.

[0018] In the drawings:

[0019] 1、hollow disc; 2、matching flange; 3、feed pipe; 4、ammonia output pipe; 5、discharge pipe; 6、pressure sensor; 7、pressure regulating valve; 8、gear pump; 9、flange bolt; 10、turbine connecting piece; 11、turbine; 12、bolt hole; 13、flange pad; 14、visualization window. DETAILED DESCRIPTION

[0020] The technical solutions in the embodiments of the present application will be described clearly and completely below with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments in the present application, all the other embodiments obtained by those skilled in the art without creative work fall within the scope of protection of the present application.

[0021] Please refer to Figures 1-4 The present application provides a technical solution:

[0022] Please refer toFigure 1 As shown in the figure, the polymeric ammonia mixing device comprises a hollow disc 1, a matching flange 2 is installed on the top of the hollow disc 1, a feeding pipe 3 and an ammonia gas output pipe 4 are connected to the sidewall of the hollow disc 1, a discharge pipe 5 is installed at the bottom of the hollow disc 1, a gear pump 8 is installed on the feeding pipe 3, a pressure sensor 6 and a pressure regulating valve 7 are installed on the ammonia gas output pipe 4, the inside of the hollow disc 1 is a cavity structure, and one end of the feeding pipe 3 and the ammonia gas output pipe 4 is located in the cavity. In the specific implementation process, the hollow disc 1 is the core of the device, the inside of which is a cavity structure for accommodating the spinning dope entering from the feeding pipe 3 and the ammonia gas entering from the ammonia gas output pipe 4, the matching flange 2 is installed on the top of the hollow disc 1 to facilitate the connection and fixation of the device, the feeding pipe 3 is used to introduce the spinning dope into the cavity of the hollow disc 1, the gear pump 8 is used to control the flow of the spinning dope, thereby ensuring that the ratio of the ammonia gas meets the process requirements, the ammonia gas output pipe 4 is used to introduce the ammonia gas into the cavity of the hollow disc 1 to mix with the spinning dope, the pressure sensor 6 and the pressure regulating valve 7 are installed on the ammonia gas output pipe 4, the pressure sensor 6 is used to monitor the pressure of the ammonia gas in real time, and the pressure regulating valve 7 is used to adjust the flow of the ammonia gas according to the feedback of the pressure sensor 6 to ensure the mixing effect, and then the uniformly mixed spinning dope can be discharged from the device through the discharge pipe 5.

[0023] Referring to Figure 3 and Figure 4 As shown in the figure, a turbine connecting piece 10 is installed at the joint of the discharge pipe 5 and the hollow disc 1, and a turbine 11 is arranged in the turbine connecting piece 10. In the specific implementation process, the turbine 11 is arranged to further stir and mix the materials when the spinning dope flows out of the hollow disc 1 through the rotation of the turbine 11, so as to ensure that the spinning dope and the ammonia gas are more uniformly mixed.

[0024] Referring to Figure 2 and Figure 4 As shown in the figure, flange bolts 9 are installed around the top of the matching flange 2 at equal intervals, bolt holes 12 matched with the flange bolts 9 are arranged outside the cavity in the hollow disc 1, the hollow disc 1 and the matching flange 2 are detachably connected through the flange bolts 9, and a flange pad 13 is installed at the joint of the hollow disc 1 and the matching flange 2. In the specific implementation process, the hollow disc 1 can be detachably connected with the matching flange 2 through the flange bolts 9, which facilitates the assembly, disassembly and maintenance of the device, and the flange pad 13 further enhances the sealing performance of the device to prevent leakage of the materials during the mixing process.

[0025] Referring to Figure 4As shown, a visualization window 14 is provided on the outer wall of the hollow disc 1, and the visualization window 14 is made of transparent acrylic material. In the specific implementation process, through the visualization window 14, the operator can observe the mixing of spinning solution and ammonia inside the hollow disc 1 in real time. This helps to detect abnormal problems in the mixing process in a timely manner, such as uneven mixing or blockage, thereby ensuring the stability and controllability of the production process.

[0026] See Figure 1 As shown, a controller is installed on the outside of the hollow disc 1. The output of the controller is electrically connected to the pressure sensor 6, the pressure regulating valve 7, the gear pump 8, and the input of the turbine 11. In practice, the controller allows operators to easily monitor and adjust the entire mixing process. The pressure sensor 6 monitors the ammonia pressure in the ammonia feed pipe 3 in real time to ensure a stable supply of ammonia. The pressure regulating valve 7 automatically adjusts the ammonia supply pressure based on the feedback from the pressure sensor 6 to meet process requirements. The gear pump 8 precisely controls the flow rate of material through the feed pipe 3 to ensure the ratio of material to ammonia. The controller adjusts the speed of the turbine 11 to optimize the mixing effect.

[0027] Working principle:

[0028] Step 1: The spinning solution is introduced into the cavity of the hollow disc 1 through the feed pipe 3. The gear pump 8 installed on the feed pipe 3 is used to precisely control the flow rate of the spinning solution, so that the spinning solution flows into the cavity at a certain rate. This step is the basis of the mixing process. At the same time, ammonia gas is introduced into the cavity of the hollow disc 1 through the ammonia gas output pipe 4 to mix with the spinning solution. On the ammonia gas output pipe 4, the pressure sensor 6 monitors the pressure of the ammonia gas in real time to ensure a stable supply of ammonia gas. According to the feedback of the pressure sensor 6, the pressure regulating valve 7 automatically adjusts the supply pressure of ammonia gas to meet the process requirements and ensure that the ammonia gas and the spinning solution are mixed under suitable conditions.

[0029] Step 2: After the spinning solution and ammonia enter the cavity of the hollow disc 1, they begin to mix within the cavity. Because the hollow disc 1 has a hollow internal structure, it provides sufficient space for the mixing of the spinning solution and ammonia. During the mixing process, the spinning solution and ammonia come into contact with and diffuse into each other within the cavity, gradually achieving a uniform mixture. To further enhance the mixing effect, a turbine connector 10 is installed at the junction of the discharge pipe 5 and the hollow disc 1. The turbine connector 10 contains a turbine 11. When the uniformly mixed spinning solution flows out of the hollow disc 1 through the discharge pipe 5, the turbine 11 rotates accordingly, further stirring and mixing the materials. In addition, a matching flange 2 is installed on the top of the hollow disc 1, and is detachably connected to the hollow disc 1 via flange bolts 9. During operation, the operator can observe the mixing of the spinning solution and ammonia inside the hollow disc 1 in real time through the visualization window 14 on the outer wall of the hollow disc 1.

Claims

1. A polymerization ammonia mixing device, characterized in that, The device includes a hollow disc (1), with a matching flange (2) installed on the top of the hollow disc (1), a feed pipe (3) and an ammonia output pipe (4) connected to the side wall of the hollow disc (1), a discharge pipe (5) installed at the bottom of the hollow disc (1), a gear pump (8) installed on the feed pipe (3), and a pressure sensor (6) and a pressure regulating valve (7) installed on the ammonia output pipe (4). The hollow disc (1) has a cavity structure inside, and one end of the feed pipe (3) and the ammonia output pipe (4) is located inside the cavity.

2. The ammonia mixing apparatus as described in claim 1, characterized in that: A turbine connector (10) is installed at the junction of the discharge pipe (5) and the hollow disc (1), and a turbine (11) is provided inside the turbine connector (10).

3. The ammonia mixing apparatus as described in claim 2, characterized in that: The top of the matching flange (2) is equipped with flange bolts (9) at equal intervals. The hollow disc (1) has bolt holes (12) that match the flange bolts (9) on the outside of the cavity. The hollow disc (1) and the matching flange (2) are detachably connected by the flange bolts (9).

4. The ammonia mixing apparatus as described in claim 3, characterized in that: A flange gasket (13) is installed at the junction of the hollow disc (1) and the matching flange (2).

5. The ammonia mixing apparatus as described in claim 4, characterized in that: The hollow disc (1) has a visualization window (14) on its outer wall, and the visualization window (14) is made of transparent acrylic material.

6. The ammonia mixing apparatus as described in claim 5, characterized in that: A controller is installed on the outside of the hollow disk (1), and the output end of the controller is electrically connected to the input end of the pressure sensor (6), the pressure regulating valve (7), the gear pump (8), and the turbine (11).

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