Negative pressure distillation detergent concentration device

By using heat transfer oil heating and inert gas decompression, combined with stirring and separation, the problem of incomplete removal of impurities in detergent in existing technologies has been solved, achieving a highly efficient detergent concentration process and improving product purity.

CN223760431UActive Publication Date: 2026-01-06LINYI BAIXING DAILY CHEMICAL CO LTD
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Patent Information

Application Number
CN202423203787.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-12-25
Publication Date
2026-01-06
Estimated Expiration
2034-12-25

AI Technical Summary

Technical Problem

In existing technologies, negative pressure distillation detergent concentration devices are not very effective in removing soluble impurities, which affects the quality of detergent.

Method used

The tank is heated uniformly with heat transfer oil, and inert gas is injected into the gas box to reduce pressure. Combined with stirring by the stirring shaft and separation by the separator, the useful components are separated from the impurities. The useful components are refluxed through the reflux pipe to lower the boiling point of the volatile components so that they can be evaporated and separated at low temperature.

Benefits of technology

It achieves effective evaporation and separation of useful components and impurities in dishwashing liquid at low temperatures, thereby improving the purity and quality of dishwashing liquid.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a negative pressure distillation detergent concentration device, which comprises a support frame, a gas tank and a tank body are fixedly connected in the support frame, a heating rod is arranged in the tank body, an isolation cavity is arranged in the tank body, heat conduction oil is filled in the isolation cavity, and the heat conduction oil is filled in the isolation cavity. A condenser and a separator are fixedly installed on the upper surface of the supporting frame, an outlet of the condenser is fixedly connected with the separator through a second connecting pipe, and the separator is fixedly connected with the tank body through a backflow pipe. Through the structure, the interior of the tank body is uniformly heated through the heating rod and the heat-conducting oil, and the pressure is reduced after inert gas is injected through the gas tank, so that the boiling point of volatile components in detergent can be reduced while the pressure in the distillation tank is kept stable, and substances can be evaporated at a relatively low temperature; and finally, impurities are separated through the separator and enter the tank body through the return pipe.
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Description

Technical Field

[0001] This utility model relates to the technical field, and in particular to a negative pressure distillation detergent concentration device. Background Technology

[0002] Negative pressure distillation detergent concentration equipment is a specialized device for detergent production. It combines negative pressure distillation and concentration technologies. This device can perform distillation at lower temperatures and pressures, thereby effectively extracting and concentrating the active ingredients in detergent while avoiding damage to the materials caused by high temperatures. For example, a Chinese patent discloses a detergent concentration tank with application number CN201820206870.8. It utilizes the weight difference caused by density differences to eliminate non-detergent liquid impurities, ensuring the purity of the detergent product. However, its effect on removing soluble impurities is not significant, resulting in some impurities remaining inside the detergent that cannot be removed. This has certain limitations and affects the quality of the detergent. Utility Model Content

[0003] The purpose of this utility model is to at least solve one of the technical problems existing in the prior art, and to provide a negative pressure distillation detergent concentration device. The device uses heat transfer oil to make the inside of the tank uniformly heated, and then reduces the pressure after injecting inert gas through the gas box. This can maintain the pressure stability inside the distillation tank while lowering the boiling point of the volatile components in the detergent, so that the substances can evaporate at a lower temperature. Finally, the useful components are separated from the impurities by the separator, and then enter the tank through the reflux pipe.

[0004] This utility model also provides a negative pressure distillation detergent concentration device, comprising: a support frame, an air box and a tank are fixedly connected inside the support frame, a feed pipe is fixedly connected to the inlet of the tank, a heating rod is installed inside the tank, an air inlet pipe is fixedly connected to the outlet of the air box, the end of the air inlet pipe away from the air box is fixedly connected to the tank, an exhaust valve is installed at the connection between the air inlet pipe and the tank, a pressure reducing pump is fixedly connected inside the support frame, and the input end of the pressure reducing pump is fixedly connected to the tank; a motor, a right-angle plate is fixedly connected to the outside of the motor, the lower surface of the right-angle plate is fixedly connected to the support frame, a stirring shaft is fixedly connected to the output end of the motor, a condenser and a separator are fixedly installed on the upper surface of the support frame, a first connecting pipe is fixedly connected to the outlet at the top of the tank, the end of the first connecting pipe away from the tank is fixedly connected to the condenser, the outlet of the condenser is fixedly connected to the separator through a second connecting pipe, and the separator is fixedly connected to the tank through a return pipe. The heat transfer oil ensures uniform heating inside the tank, and the pressure is reduced after injecting inert gas through the gas box. This maintains stable pressure inside the distillation tank while lowering the boiling point of volatile components in the detergent, allowing the substance to evaporate at a lower temperature. Finally, the substance is separated from impurities by a separator and then enters the tank through a reflux pipe.

[0005] According to the negative pressure distillation detergent concentration device of this utility model, the tank body is provided with an isolation chamber, and the heating rod is located inside the isolation chamber. The heating rod is fixed by the isolation chamber to ensure a safer and more efficient heating process, while avoiding direct contact between the heating rod and the substances inside the tank.

[0006] According to the present invention, a negative pressure distillation detergent concentration device is provided, wherein the isolation chamber is filled with heat-conducting oil, which is evenly distributed around the tank. This improves heat transfer efficiency and heat storage effect, ensuring that the detergent raw materials inside the tank are continuously and evenly heated.

[0007] According to the present invention, a negative pressure distillation detergent concentration device is provided inside the tank, and the pressure sensor is electrically connected to an exhaust valve. The device monitors the pressure of the gas inside the tank in real time and controls the opening or closing of the exhaust valve based on the pressure reading to ensure that the pressure inside the tank remains within a safe range.

[0008] According to the present invention, a negative pressure distillation detergent concentration device is provided, wherein the end of the stirring shaft away from the motor passes through the interior of the tank and is rotatably connected to the tank, and a sealing element is provided at the connection between the stirring shaft and the tank. This prevents material leakage from the tank and the entry of external impurities into the tank, while ensuring the normal rotation of the stirring shaft.

[0009] According to the present invention, a negative pressure distillation detergent concentration device is provided at the connection between the pressure reducing pump and the tank, and a discharge port is provided at the bottom of the tank, with a discharge valve at the discharge port. The flow of material is controlled so that the concentrated raw material inside the tank is discharged through the discharge port.

[0010] According to the present invention, a negative pressure distillation detergent concentration device is provided at the outlet of the separator, and the lower surface of the processing tank is fixedly connected to a support frame. Impurities separated by the separator are stored for further processing.

[0011] According to the negative pressure distillation detergent concentration device of this utility model, the motor is provided with a protective shell, and the lower surface of the protective shell is fixedly connected to a right-angle plate. The protective shell protects the motor and prevents the external environment from affecting the motor.

[0012] Beneficial effects: Compared with the existing technology, this new negative pressure distillation detergent concentration device uses heat transfer oil to make the inside of the tank uniformly heated, and then reduces the pressure after injecting inert gas through the gas box. This can maintain the pressure stability inside the distillation tank while lowering the boiling point of the volatile components in the detergent, allowing the substances to evaporate at a lower temperature. Finally, the substances are separated from impurities by a separator and then enter the tank through a reflux pipe. Attached Figure Description

[0013] The present invention will be further described below with reference to the accompanying drawings and embodiments;

[0014] Figure 1 This is a complete structural diagram of the negative pressure distillation detergent concentration device of this utility model;

[0015] Figure 2 This is a side view of the negative pressure distillation detergent concentration device of this utility model;

[0016] Figure 3 This is a cross-sectional view of the negative pressure distillation detergent concentration device of this utility model;

[0017] Figure 4 This is a structural diagram of the condenser and tank of the negative pressure distillation detergent concentration device of this utility model;

[0018] Figure 5 This utility model relates to a negative pressure distillation detergent concentration device. Figure 3 Partial structural diagram of point A in the middle.

[0019] Legend:

[0020] 1. Support frame; 2. Air box; 3. Tank body; 4. Feed pipe; 5. Heating rod; 6. Air inlet pipe; 7. Exhaust valve; 9. Pressure reducing pump; 10. Motor; 11. Right angle plate; 12. Stirring shaft; 13. Condenser; 14. Separator; 15. First connecting pipe; 16. Second connecting pipe; 17. Return pipe; 18. Isolation chamber; 19. Pressure sensor; 20. Seal; 21. Control valve; 22. Discharge port; 23. Discharge valve; 24. Processing tank; 25. Protective shell. Detailed Implementation

[0021] This section will describe in detail the specific embodiments of the present utility model. The preferred embodiments of the present utility model are shown in the accompanying drawings. The purpose of the drawings is to supplement the textual description with graphics, so that people can intuitively and vividly understand each technical feature and the overall technical solution of the present utility model, but they should not be construed as limiting the scope of protection of the present utility model.

[0022] Reference Figure 1-5 This utility model provides a negative pressure distillation detergent concentration device, which includes: a support frame 1, a gas box 2 and a tank 3 fixedly connected inside the support frame 1, a feed pipe 4 fixedly connected to the inlet of the tank 3 to feed the raw material into the tank 3, a heating rod 5 installed inside the tank 3 to uniformly heat the inside of the tank 3 through a ring structure, an air inlet pipe 6 fixedly connected to the outlet of the gas box 2, the gas box 2 being filled with inert gas and transported through the air inlet pipe 6, the end of the air inlet pipe 6 away from the gas box 2 being fixedly connected to the tank 3, an exhaust valve 7 being installed at the connection between the air inlet pipe 6 and the tank 3 to adjust the gas flow rate accordingly, and a pressure reducing pump 9 fixedly connected inside the support frame 1 to lower the boiling point of the volatile components in the detergent, the input end of the pressure reducing pump 9 being fixedly connected to the tank 3;

[0023] The motor 10 is externally fixedly connected to a right-angle plate 11 for fixation. A protective shell 25 is provided on the outside of the motor 10 for protection. The lower surface of the protective shell 25 is fixedly connected to the right-angle plate 11, and the lower surface of the right-angle plate 11 is fixedly connected to the support frame 1. A stirring shaft 12 is fixedly connected to the output end of the motor 10, allowing the detergent raw material to be evenly heated during stirring. The end of the stirring shaft 12 away from the motor 10 passes through the interior of the tank 3 and is rotatably connected to the tank 3. A seal 20 is provided at the connection between the stirring shaft 12 and the tank 3 to prevent leakage of the internal raw material during stirring. A [missing information - likely a device or component] is fixedly installed on the upper surface of the support frame 1. The condenser 13 and separator 14 separate impurities from useful components in the raw material. The outlet at the top of the tank 3 is fixedly connected to the first connecting pipe 15, through which the distilled volatile substances are sent to the condenser 13 for cooling. The end of the first connecting pipe 15 away from the tank 3 is fixedly connected to the condenser 13. The outlet of the condenser 13 is fixedly connected to the separator 14 through the second connecting pipe 16. The separator 14 is fixedly connected to the tank 3 through the return pipe 17, through which the useful components after impurity removal are sent back to the interior of the tank 3. The outlet of the separator 14 is provided with a processing box 24, and the lower surface of the processing box 24 is fixedly connected to the support frame 1.

[0024] The tank body 3 has an isolation chamber 18 inside, the heating rod 5 is located inside the isolation chamber 18, the isolation chamber 18 is filled with heat transfer oil, the heat transfer oil is evenly distributed around the tank body 3, the tank body 3 has a pressure sensor 19 inside, the pressure sensor 19 is electrically connected to the exhaust valve 7, the pressure reducing pump 9 is connected to the tank body 3 with a control valve 21, the bottom of the tank body 3 has a discharge port 22, the discharge port 22 is equipped with a discharge valve 23.

[0025] Working principle: First, the exhaust valve 7 is opened, and the inert gas inside the air box 2 is sent into the tank 3 through the air inlet pipe 6. This removes the air inside the tank 3 and prevents oxygen and other impurities from affecting the subsequent process. Then, the pressure reducing pump 9 is started to put the tank 3 into a negative pressure state, which can lower the boiling point of the detergent raw material liquid. Under the action of negative pressure, the detergent raw material enters the tank 3 through the feed pipe 4. The heating rod 5 is started to heat the heat transfer oil inside the isolation chamber 18, so that the inside of the tank 3 is uniformly heated by the heat transfer oil, which can heat the detergent raw material. At the same time, the motor 10 is started to drive the stirring shaft 12 to stir the detergent raw material, so that it can be heated evenly. During this process, volatile substances are distilled and enter the condenser 13 for cooling through the first connecting pipe 15. Then, the useful components in the detergent are separated from other impurities through the separator 14. Subsequently, the useful components are transported back to the tank 3 through the return pipe 17, and the impurity components enter the processing tank 24 for storage.

[0026] The embodiments of the present utility model have been described in detail above with reference to the accompanying drawings. However, the present utility model is not limited to the above embodiments. Within the scope of knowledge possessed by those skilled in the art, various changes can be made without departing from the spirit of the present utility model.

Claims

1. A negative pressure distillation of a detergent concentrate device, characterized by, Include: Support frame (1), the inside of the support frame (1) is fixedly connected with gas tank (2) and tank body (3), the inlet of the tank body (3) is fixedly connected with feed pipe (4), the inside of the tank body (3) is provided with heating rod (5), the outlet of the gas tank (2) is fixedly communicated with air inlet pipe (6), the end of the air inlet pipe (6) away from the gas tank (2) is fixedly connected with the tank body (3), the connection part of the air inlet pipe (6) and the tank body (3) is provided with exhaust valve (7), the inside of the support frame (1) is fixedly connected with pressure reducing pump (9), the input end of the pressure reducing pump (9) is fixedly connected with the tank body (3); Electric motor (10), the outside of the electric motor (10) is fixedly connected with right angle plate (11), the lower surface of the right angle plate (11) is fixedly connected with support frame (1), the output end of the electric motor (10) is fixedly connected with stirring shaft (12), the upper surface of the support frame (1) is fixedly installed with condenser (13) and separator (14), the outlet of the tank body (3) top is fixedly communicated with first connecting pipe (15), the end of the first connecting pipe (15) away from the tank body (3) is fixedly connected with the condenser (13), the outlet of the condenser (13) is fixedly connected with the separator (14) through second connecting pipe (16), the separator (14) is fixedly connected with the tank body (3) through backflow pipe (17).

2. A negative pressure distillation detergent concentrate apparatus as claimed in claim 1, wherein, The inside of the tank body (3) is provided with isolation cavity (18), and the heating rod (5) is located in the inside of the isolation cavity (18).

3. A negative pressure distillation of cleaning concentrate device according to claim 2, wherein, The inside of the isolation cavity (18) is filled with heat conducting oil, and the heat conducting oil is uniformly distributed around the tank body (3).

4. A negative pressure distillation detergent concentrate apparatus as claimed in claim 1, wherein, The inside of the tank body (3) is provided with pressure sensor (19), and the pressure sensor (19) is electrically connected with the exhaust valve (7).

5. A negative pressure distillation of cleaning concentrate device according to claim 1, wherein, The end of the stirring shaft (12) away from the electric motor (10) penetrates the inside of the tank body (3) and is rotatably connected with the tank body (3), and a sealing element (20) is arranged at the connection part of the stirring shaft (12) and the tank body (3).

6. A negative pressure distillation of cleaning concentrate device according to claim 1, wherein, The connection part of the pressure reducing pump (9) and the tank body (3) is provided with control valve (21), the bottom of the tank body (3) is provided with discharge port (22), and the discharge port (22) is provided with discharge valve (23).

7. A negative pressure distillation of cleaning concentrate device according to claim 1, wherein, The outlet of the separator (14) is provided with treatment box (24), and the lower surface of the treatment box (24) is fixedly connected with the support frame (1).

8. A negative pressure distillation of cleaning concentrate device according to claim 1, wherein, The outside of the electric motor (10) is provided with protective shell (25), and the lower surface of the protective shell (25) is fixedly connected with the right angle plate (11).

Citation Information

Patent Citations

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