Material processing equipment based on ZSM-5

Abstract

The utility model discloses ZSM-5-based material processing equipment, which belongs to the technical field of biochemistry and comprises a bottom plate, a mounting box arranged on the surface of the bottom plate, a first control panel mounted on the surface of the mounting box, a charging port mounted on one side of the mounting box, a heating pot mounted on the surface of the mounting box, a first heater mounted on the surface of the heating pot, and a second heater mounted on the surface of the first heater, a heating coil is installed in the heating pot, the first heater is electrically connected with the heating coil, an electromagnetic generator is installed at the bottom of the inner wall of the heating pot, a stirring pot is arranged in the heating pot, an electromagnetic rotor is arranged in the stirring pot, and a plurality of buffer assemblies matched with the stirring pot are installed at the top of the heating pot. A sealing cover is arranged on the surface of the stirring pot. Through cooperative use of the drying oven, the second control panel, the hot air assembly, the third heater, the drying plate and the moving assembly, powder can be conveniently subjected to high-temperature treatment so that the powder can be rapidly formed, and therefore the machining efficiency is improved.

Description

TECHNICAL FIELD

[0001] The utility model relates to biochemical kind technical field, concretely relates to a material processing equipment based on ZSM 5. BACKGROUND

[0002] At present, the method of large-scale industrial production ZSM 5 zeolite molecular sieve mainly is mainly with hydrothermal synthesis method. Hydrothermal synthesis method is divided into template agent method and seed method, and the in-situ crystallization method of adding seed crystal to natural clay as raw material to synthesize molecular sieve is the most important seed method. And the traditional synthesis method exists a large amount of waste liquid solvent except that the reaction condition is rigorous, can cause environmental pollution and resource waste problem.

[0003] Therefore, the utility model discloses a green environmental protection, convenient and efficient solventless method for industrial production ZSM 5 molecular sieve. Meanwhile, in order to reduce the huge burden of waste fly ash to the environment and improve economic value, reduce the cost of synthesis zeolite raw material, the raw material of synthesizing molecular sieve uses industrial waste fly ash.

[0004] The invention patent CN201610056519.0 discloses a "molecular sieve solid phase synthesis method with controllable grain size", which uses ordinary silicon source, aluminum source, template agent and alkali source to solid phase synthesize ZSM 5. The patent uses fly ash as silicon aluminum source and does not use template agent to synthesize ZSM 5. UTILITY MODEL CONTENT

[0005] In view of the problems in the prior art, the utility model aims at providing a material processing equipment based on ZSM 5 and preparation method, which uses fly ash as silicon aluminum source, reduces the pollution caused by the synthesis of raw materials itself, and reduces the pressure on the environment caused by fly ash itself.

[0006] To solve the above problems, the utility model adopts the following technical scheme:

[0007] A ZSM-5-based material processing device, comprising a base plate, a mounting box is arranged on the surface of the base plate, a first control panel is arranged on the surface of the mounting box, a charging port is arranged on one side of the mounting box, a heating pot is arranged on the surface of the mounting box, a first heater is arranged on the surface of the heating pot, a heating coil is arranged in the heating pot, the first heater is electrically connected with the heating coil, an electromagnetic generator is arranged on the bottom of the inner wall of the heating pot, a stirring pot is arranged in the heating pot, an electromagnetic rotor is arranged in the stirring pot, a plurality of buffering assemblies adapted to the stirring pot are arranged on the top of the heating pot, a sealing cover is arranged on the surface of the stirring pot, a first supporting leg is arranged on the surface of the base plate, a heating box is arranged on the top of the first supporting leg, protective covers are arranged on both sides of the top of the heating box, two liquid guide cylinders are arranged in the heating box, a sealing ring is arranged on the top of the liquid guide cylinder, a suction filter is fixedly connected with the surface of the sealing ring, a first filter screen is arranged in the suction filter, a connecting seat is arranged on the bottom of the liquid guide cylinder, a pressurizing valve is arranged on the bottom of the connecting seat, a collecting box is arranged below the heating box and communicates with the pressurizing valve, a second supporting leg is arranged on the surface of the base plate, a grinding barrel is arranged on the surface of the second supporting leg, a second heater is arranged on the surface of the grinding barrel, a feeding hopper is arranged on the top of the grinding barrel and communicates with the grinding barrel, a screening assembly is arranged on one side of the bottom of the grinding barrel, an oven is arranged on the surface of the base plate, a second control panel is arranged on the front of the oven, a hot air assembly is arranged on the surface of one side of the oven, a third heater is arranged on the back of the oven, a plurality of moving assemblies are arranged on both sides of the inner wall of the oven, and drying plates are arranged on the inner side of the moving assemblies.

[0008] As a preferred scheme of the utility model, the buffering assembly comprises a limiting plate, a mounting cylinder, a buffering cylinder, a buffering spring and a buffering plate, the limiting plate is arranged on the surface of the heating pot, the mounting cylinder is arranged in two, the two mounting cylinders are arranged on the surface of the limiting plate, the buffering cylinder is slidably connected with the inner wall of the mounting cylinder, the buffering spring is arranged in the buffering cylinder, one end of the buffering spring is fixedly connected with the buffering cylinder, the other end of the buffering spring is fixedly connected with the mounting cylinder, the buffering plate is arranged on the surface of the buffering cylinder and slidably connected with the surface of the limiting plate.

[0009] As a preferred scheme of the utility model, the grinding assembly comprises a first rotating shaft, a second rotating shaft, a plurality of grinding teeth, a grinding plate, a first tooth plate, a second tooth plate, a protective box, a first servo motor and a rotating gear, the first rotating shaft is rotatably connected with the surface of the grinding barrel, the second rotating shaft is rotatably connected with the surface of the first rotating shaft, the grinding teeth are arranged in plurality, the plurality of grinding teeth are fixedly connected with the surface of the first rotating shaft, the grinding plate is arranged on the surface of the second rotating shaft, the first tooth plate is fixedly connected with one end of the first rotating shaft, the second tooth plate is arranged on one end of the second rotating shaft, the protective box is arranged on the surface of the grinding barrel, the first servo motor is arranged on the surface of the protective box, the rotating gear is arranged on the surface of the output shaft of the first servo motor and meshes with the first tooth plate and the second tooth plate.

[0010] As a preferred scheme of the utility model, the screening assembly includes a partition, an auxiliary hopper, a bellows, a second filter screen and a reciprocating mechanism, the auxiliary hopper is installed at the bottom of the grinding barrel, the partition is slidingly connected to the surface of the bottom of the grinding barrel, the bellows is installed at the bottom of the auxiliary hopper, the second filter screen is arranged inside the bellows, and the reciprocating mechanism is installed on the surface of the auxiliary hopper.

[0011] As a preferred scheme of the utility model, the reciprocating mechanism includes a second servo motor, a reciprocating box, an intermittent gear and a reciprocating rack, the second servo motor is installed on the surface of the auxiliary hopper, the reciprocating box is fixedly connected to the surface of the bellows, the output shaft of the second servo motor extends into the reciprocating box, the intermittent gear is fixedly connected to the surface of the output shaft of the second servo motor, the reciprocating rack is installed on the upper and lower sides of the inner wall of the reciprocating box, and the intermittent gear is engaged with the reciprocating rack on one side.

[0012] As a preferred scheme of the utility model, the hot air assembly includes a filter box, an air inlet pipe, a hot air machine, a first air guide pipe and a second air guide pipe, the filter box is installed on the surface of one side of the oven, the air inlet pipe is installed on the surface of the filter box, the hot air machine is installed on the surface of the filter box, one end of the first air guide pipe is communicated with the filter box, the other end of the first air guide pipe is communicated with the hot air machine, one end of the second air guide pipe is communicated with the hot air machine, and the other end of the second air guide pipe is communicated with the oven.

[0013] As a preferred scheme of the utility model, the moving assembly includes a first sliding rod, a second sliding rod, a third sliding rod, a first sliding groove, a first limiting column, a second sliding groove and a second limiting column, the first sliding rod is installed on the surface of the inner wall of the oven, the second sliding rod is slidingly connected to the inner wall of the first sliding rod, the third sliding rod is slidingly connected to the inner wall of the second sliding rod, the first sliding groove is arranged on the surface of the first sliding rod, the first limiting column is installed on the surface of the second sliding rod and slidingly connected to the surface of the first sliding groove, the second sliding groove is arranged on the surface of the second sliding rod, and the second limiting column is installed on the surface of the third sliding rod and slidingly connected to the second sliding groove.

[0014] Compared with the prior art, the utility model has the advantages that:

[0015] The utility model discloses a cooperation of installation box, first control panel, charging port, heating pot, first heater, heating coil, electromagnetic generator, stirring pot, electromagnetic rotor and sealing cover, and the acid of fly ash is removed conveniently, and the contact area of fly ash and hydrochloric acid is improved, through the cooperation of first support leg, heating box, protection cover, liquid guide cylinder, sealing washer, suction filter hopper, first filter screen, connecting seat, pressure valve and collection box, the mixture can be suction filtered, thereby reducing the probability that the reaction effect is influenced by too much liquid in the mixture, through the cooperation of second support leg, grinding barrel, second heater, feed hopper, grinding assembly and screening assembly, the powder can be ground and mixed with powder, TPAOH and water, and after mixing and grinding, the mixture is filtered, thereby meeting the requirement of reaction, through the cooperation of oven, second control panel, hot -blast subassembly, third heater, drying board and movement subassembly, the powder is conveniently high -temperature treatment and makes it fast forming, thereby improve processing efficiency. BRIEF DESCRIPTION OF DRAWINGS

[0016] Figure 1 It is whole perspective view of a material processing equipment based on ZSM-5 for the utility model;

[0017] Figure 2 It is the schematic diagram of first partial structure in a material processing equipment based on ZSM-5 for the utility model;

[0018] Figure 3 It is the explosion view of buffer assembly in a material processing equipment based on ZSM-5 for the utility model;

[0019] Figure 4 It is the schematic diagram of second partial structure in a material processing equipment based on ZSM-5 for the utility model;

[0020] Figure 5 It is the schematic diagram of third partial structure in a material processing equipment based on ZSM-5 for the utility model;

[0021] Figure 6 It is the first schematic diagram of grinding assembly in a material processing equipment based on ZSM-5 for the utility model;

[0022] Figure 7 It is the second schematic diagram of grinding assembly in a material processing equipment based on ZSM-5 for the utility model;

[0023] Figure 8 It is the explosion view of screening assembly in a material processing equipment based on ZSM-5 for the utility model;

[0024] Figure 9 It is the sectional view of reciprocating mechanism in a material processing equipment based on ZSM-5 for the utility model;

[0025] Figure 10 It is a schematic view of the fourth local structure in the material processing equipment based on ZSM-5;

[0026] Figure 11 It is a schematic view of the hot air assembly in the material processing equipment based on ZSM-5;

[0027] Figure 12 It is a schematic view of the moving assembly in the material processing equipment based on ZSM-5.

[0028] Mark explanation in the drawing:

[0029] 1, bottom plate; 2, installation box; 3, first control panel; 4, charging port; 5, heating pot; 6, first heater; 7, heating coil; 8, electromagnetic generator; 9, stirring pot; 10, electromagnetic rotor; 11, buffer assembly; 1101, limiting plate; 1102, installation cylinder; 1103, buffer cylinder; 1104, buffer spring; 1105, buffer plate; 12, sealing cover; 13, first supporting leg; 14, heating box; 15, protective cover; 16, liquid guide cylinder; 17, sealing ring; 18, suction filter hopper; 19, first filter screen; 20, connecting seat; 21, pressure valve; 22, collection box; 23, second supporting leg; 24, grinding barrel; 25, second heater; 26, feeding hopper; 27, grinding assembly; 2701, first rotating shaft; 2702, second rotating shaft; 2703, grinding tooth; 2704, grinding plate; 2705, first tooth plate; 2706, second tooth plate; 2707, protective box; 2708, first servo motor; 2709, rotating gear; 28, screening assembly; 2801, partition plate; 2802, auxiliary hopper; 2803, corrugated pipe; 2804, second filter screen; 2805, reciprocating mechanism; 280501, second servo motor; 280502, reciprocating box; 280503, intermittent gear; 280504, reciprocating rack; 29, oven; 30, second control panel; 31, hot air assembly; 3101, filter box; 3102, air inlet pipe; 3103, hot air machine; 3104, first air guide pipe; 3105, second air guide pipe; 32, third heater; 33, drying plate; 34, moving assembly; 3401, first sliding rod; 3402, second sliding rod; 3403, third sliding rod; 3404, first sliding groove; 3405, first limiting column; 3406, second sliding groove; 3407, second limiting column. DETAILED DESCRIPTION

[0030] The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, rather than all the embodiments of the present application. Based on the embodiments in the present application, all the other embodiments obtained by a person of ordinary skill in the art without creative work are within the protection scope of the present application.

[0031] In the description of the present application, it should be noted that the terms "upper", "lower", "inner", "outer", "top / bottom end" and the like indicate the orientation or positional relationship shown in the drawings, and are only for the convenience of describing the present application and simplifying the description, and do not indicate or imply that the devices or elements referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore cannot be understood as a limitation on the present application. In addition, the terms "first", "second" are only for the purpose of description, and cannot be understood as indicating or implying relative importance.

[0032] In the description of the present application, it should be noted that unless otherwise explicitly specified and limited, the terms "mounting", "provided with", "sleeved / connected", "connected" and the like should be understood broadly, for example, "connected" can be fixedly connected, or can be detachably connected, or integrally connected; can be mechanically connected, or can be electrically connected; can be directly connected, or can be indirectly connected through an intermediate medium; can be the communication inside two elements. For a person of ordinary skill in the art, the specific meaning of the above terms in the present application can be understood according to the specific circumstances. Embodiments

[0033] Please refer to Figures 1 to 12A kind of material processing equipment based on ZSM-5, including: base plate 1, the surface of base plate 1 is provided with mounting box 2, the surface of mounting box 2 is installed with first control panel 3, one side of mounting box 2 is installed with charging port 4, the surface of mounting box 2 is installed with heating pot 5, the surface of heating pot 5 is installed with first heater 6, heating coil 7 is installed in the inside of heating pot 5, and first heater 6 is electrically connected with heating coil 7, electromagnetic generator 8 is installed in the bottom of the inner wall of heating pot 5, stirring pot 9 is arranged in the inside of heating pot 5, electromagnetic rotor 10 is arranged in the inside of stirring pot 9, a plurality of buffering components 11 suitable for stirring pot 9 are installed on the top of heating pot 5, sealing cover 12 is arranged on the surface of stirring pot 9, first support leg 13 is arranged on the surface of base plate 1, heating box 14 is installed on the top of first support leg 13, protective cover 15 is installed on the top of heating box 14 on both sides, two liquid guide barrels 16 are installed in the inside of heating box 14, sealing ring 17 is arranged on the top of liquid guide barrel 16, filter hopper 18 is fixedly connected on the surface of sealing ring 17, first filter screen 19 is arranged in the inside of filter hopper 18, connecting seat 20 is installed on the bottom of liquid guide barrel 16, pressure valve 21 is installed on the bottom of connecting seat 20, collecting box 22 is arranged below heating box 14, and collecting box 22 is communicated with pressure valve 21, second support leg 23 is installed on the surface of base plate 1, grinding barrel 24 is installed on the surface of second support leg 23, second heater 25 is installed on the surface of grinding barrel 24, feeding hopper 26 is installed on the top of grinding barrel 24, and feeding hopper 26 is communicated with grinding barrel 24, screening assembly 28 is arranged on one side of the bottom of grinding barrel 24, oven 29 is arranged on the surface of base plate 1, second control panel 30 is installed on the front of oven 29, hot air assembly 31 is installed on the surface of one side of oven 29, third heater 32 is installed on the back of oven 29, a plurality of moving assemblies 34 are installed on both sides of the inner wall of oven 29, drying plate 33 is arranged on the inner side of moving assembly 34.

[0034] In the embodiment of the utility model, through the cooperation of installation box 2, first control panel 3, charging port 4, heating pot 5, first heater 6, heating coil 7, electromagnetic generator 8, stirring pot 9, electromagnetic rotor 10 and sealing cover 12, it is convenient to remove the impurities of fly ash by acid, and the contact area of fly ash and hydrochloric acid is improved, through the cooperation of first supporting leg 13, heating box 14, protection cover 15, liquid guide cylinder 16, sealing ring 17, suction filter hopper 18, first filter screen 19, connecting seat 20, pressure valve 21 and collection box 22, the mixture can be suction filtered, thereby reducing the probability that too much liquid in the mixture affects the reaction effect, through the cooperation of second supporting leg 23, grinding barrel 24, second heater 25, feeding hopper 26, grinding assembly 27 and screening assembly 28, the powder can be ground and mixed with TPAOH and water, and the mixture is filtered after mixing and grinding, thereby meeting the requirements of reaction, through the cooperation of oven 29, second control panel 30, hot air assembly 31, third heater 32, drying plate 33 and moving assembly 34, it is convenient to high-temperature treat the powder to make it quickly form, thereby improving the processing efficiency.

[0035] Specifically, the buffer assembly 11 includes a limiting plate 1101, a mounting cylinder 1102, a buffer cylinder 1103, a buffer spring 1104, and a buffer plate 1105. The limiting plate 1101 is installed on the surface of the heating pot 5. The mounting cylinder 1102 is provided in two, and the two mounting cylinders 1102 are installed on the surface of the limiting plate 1101. The buffer cylinder 1103 is slidingly connected to the inner wall of the mounting cylinder 1102. The buffer spring 1104 is arranged inside the buffer cylinder 1103. One end of the buffer spring 1104 is fixedly connected to the buffer cylinder 1103, and the other end of the buffer spring 1104 is fixedly connected to the mounting cylinder 1102. The buffer plate 1105 is installed on the surface of the buffer cylinder 1103, and slidingly connected to the surface of the limiting plate 1101.

[0036] In the embodiment of the utility model, through the cooperation of the limiting plate 1101, the mounting cylinder 1102, the buffer cylinder 1103, the buffer spring 1104, and the buffer plate 1105, the impact force generated when the stirring pot 9 contacts the heating pot 5 can be reduced, thereby protecting the stirring pot 9 and the heating pot 5, and improving the service life of the stirring pot 9 and the heating pot 5.

[0037] Specifically, the grinding assembly 27 comprises a first rotating shaft 2701, a second rotating shaft 2702, grinding teeth 2703, a grinding plate 2704, a first toothed plate 2705, a second toothed plate 2706, a protection box 2707, a first servo motor 2708 and a rotating gear 2709, the first rotating shaft 2701 is rotationally connected to the surface of the grinding barrel 24, the second rotating shaft 2702 is rotationally connected to the surface of the first rotating shaft 2701, the grinding teeth 2703 are provided in plurality, and the plurality of grinding teeth 2703 are fixedly connected to the surface of the first rotating shaft 2701, the grinding plate 2704 is installed on the surface of the second rotating shaft 2702, the first toothed plate 2705 is fixedly connected to one end of the first rotating shaft 2701, the second toothed plate 2706 is installed on one end of the second rotating shaft 2702, the protection box 2707 is installed on the surface of the grinding barrel 24, the first servo motor 2708 is installed on the surface of the protection box 2707, the rotating gear 2709 is installed on the surface of the output shaft of the first servo motor 2708, and the rotating gear 2709 is engaged with the first toothed plate 2705 and the second toothed plate 2706 respectively.

[0038] In the embodiment of the utility model, through the cooperation of the first rotating shaft 2701, the second rotating shaft 2702, the grinding teeth 2703, the grinding plate 2704, the first toothed plate 2705, the second toothed plate 2706, the protection box 2707, the first servo motor 2708 and the rotating gear 2709, the mixture in the grinding barrel 24 can be ground and mixed and stirred simultaneously, so that the mixing effect of the mixture is better, and subsequent processing of the mixture is facilitated.

[0039] Specifically, the screening assembly 28 comprises a partition plate 2801, an auxiliary hopper 2802, a bellows 2803, a second filter screen 2804 and a reciprocating mechanism 2805, the auxiliary hopper 2802 is installed at the bottom of the grinding barrel 24, the partition plate 2801 is slidingly connected to the surface of the bottom of the grinding barrel 24, the bellows 2803 is installed at the bottom of the auxiliary hopper 2802, the second filter screen 2804 is arranged in the interior of the bellows 2803, the reciprocating mechanism 2805 is installed on the surface of the auxiliary hopper 2802, the reciprocating mechanism 2805 comprises a second servo motor 280501, a reciprocating box 280502, an intermittent gear 280503 and reciprocating racks 280504, the second servo motor 280501 is installed on the surface of the auxiliary hopper 2802, the reciprocating box 280502 is fixedly connected to the surface of the bellows 2803, the output shaft of the second servo motor 280501 extends into the interior of the reciprocating box 280502, the intermittent gear 280503 is fixedly connected to the surface of the output shaft of the second servo motor 280501, and the reciprocating racks 280504 are installed on the upper and lower sides of the inner wall of the reciprocating box 280502, and the intermittent gear 280503 is engaged with one side of the reciprocating racks 280504.

[0040] In the embodiment of the utility model, through the partition 2801, the auxiliary hopper 2802, the bellows 2803, the second filter screen 2804 and the reciprocating mechanism 2805, the screened powder after grinding can be obtained, thereby improving the processing precision of the powder.

[0041] Specifically, the hot air assembly 31 comprises a filter box 3101, an air inlet pipe 3102, a hot air machine 3103, a hot air machine 3103, a first air guide pipe 3104 and a second air guide pipe 3105, the filter box 3101 is installed on the surface of one side of the oven 29, the air inlet pipe 3102 is installed on the surface of the filter box 3101, the hot air machine 3103 is installed on the surface of the filter box 3101, one end of the first air guide pipe 3104 is communicated with the filter box 3101, and the other end of the first air guide pipe 3104 is communicated with the hot air machine 3103, one end of the second air guide pipe 3105 is communicated with the hot air machine 3103, and the other end of the second air guide pipe 3105 is communicated with the oven 29.

[0042] In the embodiment of the utility model, the filter box 3101, the air inlet pipe 3102, the hot air machine 3103, the hot air machine 3103, the first air guide pipe 3104 and the second air guide pipe 3105 are used in cooperation, so that hot air can be conveyed in the oven 29, thereby reducing the time consumed by the internal temperature of the oven 29.

[0043] Specifically, the moving assembly 34 comprises a first sliding rod 3401, a second sliding rod 3402, a third sliding rod 3403, a first sliding groove 3404, a first limiting column 3405, a second sliding groove 3406 and a second limiting column 3407, the first sliding rod 3401 is installed on the surface of the inner wall of the oven 29, the second sliding rod 3402 is slidingly connected to the inner wall of the first sliding rod 3401, the third sliding rod 3403 is slidingly connected to the inner wall of the second sliding rod 3402, the first sliding groove 3404 is formed on the surface of the first sliding rod 3401, the first limiting column 3405 is installed on the surface of the second sliding rod 3402, and the first limiting column 3405 is slidingly connected to the surface of the first sliding groove 3404, the second sliding groove 3406 is formed on the surface of the second sliding rod 3402, and the second limiting column 3407 is installed on the surface of the third sliding rod 3403, and the second limiting column 3407 is slidingly connected to the second sliding groove 3406.

[0044] In the embodiment of the utility model, the first sliding rod 3401, the second sliding rod 3402, the third sliding rod 3403, the first sliding groove 3404, the first limiting column 3405, the second sliding groove 3406 and the second limiting column 3407 are used in cooperation, so that the drying plate 33 can be moved conveniently, thereby bringing convenience for the staff to move the drying plate 33, and the track of the drying plate 33 is limited.

[0045] A ZSM-5-based material preparation method, comprising the following steps:

[0046] S1, the concentration of hydrochloric acid 15% and fly ash together into the inside of the stirring pot 9 and the sealing cover 12 is closed, and then the first control panel 3 starts the electromagnetic generator 8, under the action of the electromagnetic generator 8, the electromagnetic rotor 10 rotates in the inside of the stirring pot 9, and the temperature of the stirring pot 9 is heated by the first heater 6 and the heating coil 7, at this time the heating temperature is 20℃, and the heating lasts for 5h, after the heating is completed;

[0047] S2, the substances in the inside of the stirring pot 9 are poured into the inside of the filter hopper 18, and then the filter is opened by starting the pressure valve 21, at this time the liquid in the substance will flow into the inside of the collection box 22 through the first filter screen 19 and the liquid guide cylinder 16, at the same time the heating box 14 will heat the filter hopper 18 and dry the substances in the inside, then the substances are put into the inside of the drying plate 33 for high temperature alkali fusion activation 18h, then deionized water is added to dissolve the active silicon aluminum components, the filter is repeated by repeating step S1, and the high-purity silicon aluminum oxide is obtained by drying, wherein the mass ratio of alkali ash is 1.5, and the high-temperature activation temperature in the oven 29 is 700℃;

[0048] S3, then the mixture with the ratio of n(SiO2):n(TPAOH):n(H2O) ≈1:0.25:3.3 is poured into the inside of the grinding barrel 24 through the feeding hopper 26, then the grinding assembly 27 is started and the powder, TPAOH and water are mixed and ground by the grinding assembly 27, and after the grinding is completed, the screened assembly 28 is used to filter the ground powder;

[0049] S4, the ground and filtered powder is poured into the polytetrafluoroethylene reaction kettle, and then the polytetrafluoroethylene reaction kettle is placed in the inside of the drying plate 33, then the drying plate 33 is moved to the inside of the oven 29 by the moving assembly 34, then the hot air assembly 31 and the third heater 32 start to work by the second control panel 30, the oven 29 temperature is set to 180, 200, 220 and 240℃, the constant temperature time is 0-60h, after constant temperature, natural cooling to room temperature, the powder is filtered and washed, and then the washed powder is put into the inside of the drying plate 33, the temperature in the inside of the oven 29 is set to 550℃, and the powder is calcined for 6h, finally the powder sample is obtained.

[0050] In the embodiment of the utility model, the utility model provides a preparation mode of ZSM-5 material, uses fly ash of industrial waste to synthesize molecular sieve in solid phase, uses industrial waste as raw material, reduces the pressure to the environment, solid phase synthesis reduces the treatment of a large amount of waste solution and thus reduces the synthesis cost, solid phase template-free synthesis ZSM-5 is a typical green crystallization route, it can avoid using organic structure directing agent, thereby avoiding calcination step and the generation of harmful gas, in solid phase synthesis, use a small part of water, reduce the large amount of waste solution generated by using traditional mode. Industrial raw material produces ZSM-5 molecular sieve due to accompanying high cost, high energy consumption, high pollution problem, the utility model uses fly ash as silicon aluminum source, not only reduces the pollution generated by the synthesis of its own raw material, but also reduces the pressure generated by fly ash to the environment.

[0051] The above is only the preferred specific embodiment of the utility model, but the protection scope of the utility model is not limited to this, any skilled person in the art in the technical range disclosed by the utility model, according to the technical scheme of the utility model and its improvement concept, equivalent replacement or change, should be covered in the protection scope of the utility model.

Claims

1. A ZSM-5 based material processing apparatus, characterized by, Include: The surface of the bottom plate (1) is provided with a mounting box (2), the surface of the mounting box (2) is provided with a first control panel (3), one side of the mounting box (2) is provided with a charging port (4), the surface of the mounting box (2) is provided with a heating pot (5), the surface of the heating pot (5) is provided with a first heater (6), the inside of the heating pot (5) is provided with a heating coil (7), and the first heater (6) is electrically connected with the heating coil (7), the bottom of the inner wall of the heating pot (5) is provided with an electromagnetic generator (8), the inside of the heating pot (5) is provided with a stirring pot (9), the inside of the stirring pot (9) is provided with an electromagnetic rotor (10), the top of the heating pot (5) is provided with a plurality of buffer assemblies (11) adapted to the stirring pot (9), the surface of the stirring pot (9) is provided with a sealing cover (12), the surface of the bottom plate (1) is provided with a first supporting leg (13), the top of the first supporting leg (13) is provided with a heating box (14), the two sides of the top of the heating box (14) are provided with a protective cover (15), the inside of the heating box (14) is provided with two liquid guide cylinders (16), the top of the liquid guide cylinder (16) is provided with a sealing ring (17), the surface of the sealing ring (17) is fixedly connected with a suction filter hopper (18), the inside of the suction filter hopper (18) is provided with a first filter screen (19), the bottom of the liquid guide cylinder (16) is provided with a connecting seat (20), the bottom of the connecting seat (20) is provided with a pressure valve (21), the lower side of the heating box (14) is provided with a collecting box (22), and the collecting box (22) is communicated with the pressure valve (21), the surface of the bottom plate (1) is provided with a second supporting leg (23), the surface of the second supporting leg (23) is provided with a grinding barrel (24), the surface of the grinding barrel (24) is provided with a second heater (25), the top of the grinding barrel (24) is provided with a feeding hopper (26), and the feeding hopper (26) is communicated with the grinding barrel (24), one side of the bottom of the grinding barrel (24) is provided with a screening assembly (28), the surface of the bottom plate (1) is provided with an oven (29), the front of the oven (29) is provided with a second control panel (30), the surface of one side of the oven (29) is provided with a hot air assembly (31), the back of the oven (29) is provided with a third heater (32), the two sides of the inner wall of the oven (29) are provided with a plurality of moving assemblies (34), and the inner side of the moving assembly (34) is provided with a drying plate (33).

2. A ZSM-5 based material processing apparatus according to claim 1, wherein, The buffer assembly (11) comprises a limiting plate (1101), a mounting cylinder (1102), a buffer cylinder (1103), a buffer spring (1104) and a buffer plate (1105), the limiting plate (1101) is installed on the surface of the heating pot (5), the mounting cylinder (1102) is provided in two, and the two mounting cylinders (1102) are installed on the surface of the limiting plate (1101), the buffer cylinder (1103) is slidably connected to the inner wall of the mounting cylinder (1102), the buffer spring (1104) is arranged in the buffer cylinder (1103), one end of the buffer spring (1104) is fixedly connected with the buffer cylinder (1103), and the other end of the buffer spring (1104) is fixedly connected with the mounting cylinder (1102), and the buffer plate (1105) is installed on the surface of the buffer cylinder (1103) and slidably connected to the surface of the limiting plate (1101).

3. A ZSM-5 based material processing apparatus according to claim 1, wherein, The grinding assembly (27) comprises a first rotating shaft (2701), a second rotating shaft (2702), a plurality of grinding teeth (2703), a grinding plate (2704), a first toothed plate (2705), a second toothed plate (2706), a protection box (2707), a first servo motor (2708) and a rotating gear (2709), the first rotating shaft (2701) is rotatably connected to the surface of the grinding barrel (24), the second rotating shaft (2702) is rotatably connected to the surface of the first rotating shaft (2701), the grinding teeth (2703) are provided in plurality, and the plurality of grinding teeth (2703) are fixedly connected to the surface of the first rotating shaft (2701), the grinding plate (2704) is installed on the surface of the second rotating shaft (2702), the first toothed plate (2705) is fixedly connected to one end of the first rotating shaft (2701), the second toothed plate (2706) is installed on one end of the second rotating shaft (2702), the protection box (2707) is installed on the surface of the grinding barrel (24), the first servo motor (2708) is installed on the surface of the protection box (2707), and the rotating gear (2709) is installed on the surface of the output shaft of the first servo motor (2708) and meshes with the first toothed plate (2705) and the second toothed plate (2706) respectively.

4. A ZSM-5 based material processing apparatus according to claim 1, wherein, The screening assembly (28) comprises a partition plate (2801), an auxiliary hopper (2802), a bellows (2803), a second filter screen (2804) and a reciprocating mechanism (2805), the auxiliary hopper (2802) is installed at the bottom of the grinding barrel (24), the partition plate (2801) is slidably connected to the surface of the bottom of the grinding barrel (24), the bellows (2803) is installed at the bottom of the auxiliary hopper (2802), the second filter screen (2804) is arranged in the bellows (2803), and the reciprocating mechanism (2805) is installed on the surface of the auxiliary hopper (2802).

5. A ZSM-5 based material processing apparatus according to claim 4, wherein, The reciprocating mechanism (2805) comprises a second servo motor (280501), a reciprocating box (280502), an intermittent gear (280503) and a reciprocating rack (280504), the second servo motor (280501) is installed on the surface of the auxiliary hopper (2802), the reciprocating box (280502) is fixedly connected to the surface of the bellows (2803), and the output shaft of the second servo motor (280501) extends into the reciprocating box (280502), the intermittent gear (280503) is fixedly connected to the surface of the output shaft of the second servo motor (280501), and the reciprocating rack (280504) is installed on the upper and lower sides of the inner wall of the reciprocating box (280502), and the intermittent gear (280503) is engaged with the reciprocating rack (280504) on one side.

6. A ZSM-5 based material processing apparatus according to claim 1, wherein, The hot air assembly (31) comprises a filter box (3101), an air inlet pipe (3102), a hot air machine (3103), a first air guide pipe (3104) and a second air guide pipe (3105), the filter box (3101) is installed on the surface of one side of the oven (29), the air inlet pipe (3102) is installed on the surface of the filter box (3101), the hot air machine (3103) is installed on the surface of the filter box (3101), one end of the first air guide pipe (3104) is communicated with the filter box (3101), the other end of the first air guide pipe (3104) is communicated with the hot air machine (3103), one end of the second air guide pipe (3105) is communicated with the hot air machine (3103), and the other end of the second air guide pipe (3105) is communicated with the oven (29).

7. A ZSM-5 based material processing apparatus according to claim 1, wherein, The moving assembly (34) comprises a first sliding rod (3401), a second sliding rod (3402), a third sliding rod (3403), a first sliding groove (3404), a first limiting column (3405), a second sliding groove (3406) and a second limiting column (3407), the first sliding rod (3401) is installed on the surface of the inner wall of the oven (29), the second sliding rod (3402) is slidingly connected to the inner wall of the first sliding rod (3401), the third sliding rod (3403) is slidingly connected to the inner wall of the second sliding rod (3402), the first sliding groove (3404) is formed in the surface of the first sliding rod (3401), the first limiting column (3405) is installed on the surface of the second sliding rod (3402), and the first limiting column (3405) is slidingly connected to the surface of the first sliding groove (3404), the second sliding groove (3406) is formed in the surface of the second sliding rod (3402), and the second limiting column (3407) is installed on the surface of the third sliding rod (3403) and slidingly connected to the second sliding groove (3406).

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