Storage tank for production of extractive distillation toluene mixed liquor
By introducing stirring and vibration components into the storage tank, the problems of sedimentation and stratification of the mixture were solved, achieving uniform distribution of the mixture and improving the stability of the distillation process and product quality.
Patent Information
- Application Number
- CN202520701400.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-04-14
- Publication Date
- 2026-02-17
- Estimated Expiration
- 2035-04-14
AI Technical Summary
Existing storage tanks for extractive distillation of toluene mixtures are prone to sedimentation and stratification during storage, and new raw materials are difficult to fully integrate with the original mixture, resulting in uneven concentration distribution, which affects the stability of the distillation process and product quality.
A storage tank with a stirring component and a vibration component was designed. The stirring component consists of multiple layers of stirring blades of different shapes and sizes, which are driven by a stirring shaft. Combined with the vibration component installed at the bottom of the tank, it promotes uniform mixing of the liquid and prevents sedimentation and stratification.
It effectively prevents precipitation and stratification, ensures uniform distribution of all components in the mixture, improves the stability of the distillation process and product quality, and enhances the efficiency of extractive distillation.
Smart Images

Figure CN223920161U_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The utility model relates to toluene mixed liquid technical field, specifically for a kind of storage tank for extraction rectification toluene mixed liquid production. BACKGROUND
[0002] It is known that in the complex production process of extraction rectification toluene mixed liquid, the storage tank undertakes the indispensable task, and its performance is directly related to the stability of the whole production and product quality. In the production process of extraction rectification toluene mixed liquid, the storage tank is used to store raw materials, intermediate products and finished products as a key equipment.
[0003] The existing storage tank is prone to precipitation and stratification during mixed liquid storage, which affects product quality. When new raw materials are added to the storage tank, there is no stirring device to assist, and the new raw materials and the existing mixed liquid in the tank are difficult to fully blend, which makes the concentration of each component in the mixed liquid uneven. During the next extraction rectification operation, the local concentration may be abnormal, causing unstable rectification process. UTILITY MODEL CONTENT
[0004] TECHNICAL PROBLEM SOLVED
[0005] In order to overcome the problem that the existing storage tank for extraction rectification toluene mixed liquid production does not have a stirring device, the utility model provides a storage tank for extraction rectification toluene mixed liquid production with stirring effect.
[0006] TECHNICAL SCHEME
[0007] To achieve the above purpose, the utility model provides the following technical scheme: a storage tank for extraction rectification toluene mixed liquid production, comprising:
[0008] tank body;
[0009] feed inlet, the feed inlet is opened in the top of the tank body, adopts funnel-shaped structure, large mouth end upward, small mouth end and tank body interior direct communication.
[0010] discharge port, the discharge port is opened in the bottom of the tank body, in the position close to the edge of the tank body.
[0011] stirring assembly, the stirring assembly is installed in the tank body, the stirring assembly contains stirring shaft, stirring shaft penetrates from the center position of tank body top, and is connected with driving motor above the tank body top, a plurality of stirring paddles are installed on the stirring shaft, the shape and size of each layer of stirring paddles are different, and each layer of stirring paddles is distributed along the axial direction of the stirring shaft; and
[0012] vibration assembly, the vibration assembly is installed at the bottom of the tank body.
[0013] Preferably, the multi-layer partition plates are installed inside the tank body in parallel and horizontally, and separate the tank body into multiple independent storage chambers, and a communication pipe is arranged between each storage chamber and is provided with a valve.
[0014] Further, the tank body is cylindrical, the top of the tank body is flat, and the bottom is slightly concave relative to the top.
[0015] Further, the tank body is internally provided with multiple spoilers, which are arc-shaped and uniformly distributed along the edges of the stirring paddle.
[0016] Further, the feeding port is in the form of a funnel, and a guide plate is fixedly arranged inside the feeding port and mounted on the inner wall of the feeding port.
[0017] On the basis of the foregoing, a discharge pump is arranged at the discharge port, the inlet of the discharge pump is fixedly arranged with the discharge port, the outlet of the discharge pump is connected with external equipment through a discharge pipeline, and a flow regulating valve is fixedly arranged on the discharge pipeline.
[0018] Further, on the basis of the foregoing, the vibration assembly comprises a mounting plate which is detachably arranged at the bottom of the tank body, multiple springs are fixedly arranged on the mounting plate, a vibration plate is fixedly arranged between the tops of the springs, a motor is fixedly arranged on the mounting plate, a rotating rod is fixedly arranged on the output shaft of the motor, a sliding groove is formed in the mounting plate, one end of the rotating rod is attached to the vibration plate, and the other end of the rotating rod is adapted to the sliding groove.
[0019] Further, on the basis of the foregoing, an inclined drainage plate is fixedly arranged on the top of the vibration plate, the low end of the drainage plate is close to the discharge port, and the inclined direction of the drainage plate is towards the discharge port.
[0020] Beneficial effects
[0021] The extraction rectification toluene mixture production storage tank, the multi-layer different shape and size stirring paddle of the stirring assembly can form complex and strong stirring flow field in the tank under the driving of the stirring shaft, the stirring paddle of different layers can stir the toluene mixture from different angles and depths, so that various components in the mixture are always in motion, effectively preventing the occurrence of precipitation and stratification phenomenon, thereby ensuring the stability of product quality, when new raw materials are added to the storage tank, the stirring assembly can quickly stir and mix the new raw materials with the original mixture in the tank, the synergistic effect of the multi-layer stirring paddle can quickly disperse the newly added raw materials, so that they are evenly mixed into the original mixture, ensuring that the concentration distribution of each component in the mixture is uniform, avoiding the adverse effects of uneven concentration on subsequent extraction rectification operation, the stirring assembly and the vibration assembly cooperate with each other, further enhancing the mixing effect, the vibration assembly is installed at the bottom of the tank body, and can make the tank body vibrate during work, so that the mixture in the tank flows more violently, and the stirring effect of the stirring paddle is superimposed, so that the components in the mixture are more fully mixed, which makes the concentration of the mixture more stable during the next extraction rectification operation, reduces the local concentration anomaly, thereby improving the stability of the rectification process and the efficiency and product quality of the extraction rectification. BRIEF DESCRIPTION OF DRAWINGS
[0022] Figure 1 It is a side view structure schematic diagram of the utility model;
[0023] Figure 2 It is a structure schematic diagram of the discharge pump of the utility model;
[0024] Figure 3 It is a structure schematic diagram of the guide plate of the utility model;
[0025] Figure 4 It is a structure schematic diagram of the spoiler of the utility model;
[0026] Figure 5 It is a structure schematic diagram of the stirring assembly of the utility model;
[0027] Figure 6 It is a structure schematic diagram of the vibration assembly of the utility model;
[0028] Figure 7 It is a structure schematic diagram of the motor of the utility model.
[0029] In the figure: 1, tank body; 2, feed inlet; 3, discharge outlet; 4, stirring assembly; 5, stirring shaft; 6, driving motor; 7, stirring paddle; 8, vibration assembly; 9, multi-layer partition; 10, storage chamber; 11, communication pipe; 12, valve; 13, spoiler; 14, guide plate; 15, discharge pump; 16, discharge pipeline; 17, flow regulating valve; 18, mounting plate; 19, spring; 20, vibration plate; 21, motor; 22, rotating rod; 23, sliding groove; 24, flow guide plate. DETAILED DESCRIPTION
[0030] The technical solutions in the embodiments of the utility model will be clearly and completely described below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor fall within the protection scope of the utility model.
[0031] Referring to Figures 1-7 An extraction rectification toluene mixed liquid production storage tank, including tank body 1, feed inlet 2, discharge outlet 3, stirring assembly 4 and vibration assembly 8.
[0032] The tank body 1 is cylindrical, which is beneficial to the uniform distribution and storage of the liquid in the tank. The top of the tank body 1 is relatively flat, providing a stable platform for the installation of components such as the feed inlet 2 and the driving motor 6. The bottom is slightly concave compared to the top, which helps the liquid to collect at the center of the tank body 1 bottom, facilitating the discharge operation. The tank body 1 is made of corrosion-resistant metal material, such as stainless steel, to adapt to the chemical properties of the toluene mixed liquid, prevent the tank body 1 from being corroded, and ensure the service life of the storage tank. The feed inlet 2 is provided on the top of the tank body 1 in a funnel-shaped structure, with the large end facing upwards and the small end directly communicating with the inside of the tank body 1. This design allows the toluene mixed liquid to flow more smoothly into the tank body 1, reducing the splashing and spilling of the liquid. The funnel-shaped structure also provides a certain buffering effect for the liquid, preventing it from directly impacting other components in the tank. The feed inlet 2 is fixedly provided with a guide plate 14 inside. The guide plate 14 is installed on the inner wall of the feed inlet 2. The guide plate 14 guides the toluene mixed liquid to flow uniformly into the tank body 1, preventing the liquid from concentrating in a certain area. The guide plate 14 allows the liquid to flow smoothly along the surface of the guide plate 14 into the tank body 1, promoting the preliminary mixing of the liquid in the tank. The discharge outlet 3 is provided at the bottom of the tank body 1, near the edge of the tank body 1. This position design facilitates the complete discharge of the toluene mixed liquid in the tank, avoiding liquid residue.
[0033] The stirring assembly 4 is installed in the tank body 1, and the stirring assembly 4 comprises a stirring shaft 5 which penetrates through the center of the top of the tank body 1 and is connected with the driving motor 6 above the top of the tank body 1. The stirring shaft 5 is made of high-strength metal material such as alloy steel, and the diameter and length of the stirring shaft 5 can bear the weight of the stirring blades 7 and the torque generated during rotation. The stirring shaft 5 is installed with multiple layers of stirring blades 7, and the shape and size of each layer of stirring blades 7 are different from each other. The stirring blades 7 of different shapes and sizes can generate different flow fields during stirring, thereby more effectively promoting the mixing of the toluene mixture. For example, the upper stirring blades 7 are designed as wide paddles to generate a larger stirring range to form macroscopic flow of the liquid in the tank, and the lower stirring blades 7 are designed as spiral or turbine type to generate strong shear force to promote microscopic mixing of the liquid. The stirring blades 7 are made of corrosion-resistant metal material or engineering plastic to adapt to the chemical properties of the toluene mixture. The vibration assembly 8 is installed at the bottom of the tank body 1, and the vibration assembly 8 is used to vibrate the tank body 1 during storage to prevent the solid particles or impurities in the toluene mixture from settling at the bottom of the tank body 1, thereby maintaining the uniformity of the mixture.
[0034] Firstly, referring to Figure 5 In the embodiment, a plurality of partitions 9 are further included, which are installed inside the tank body 1 in parallel and horizontally. The partitions are made of corrosion-resistant metal material or engineering plastic and are fixed in the tank body 1 by welding or other means. The horizontal and parallel installation divides the space inside the tank body 1 into a plurality of independent storage chambers 10. Each chamber is relatively independent and can store toluene mixtures in different states or stages as needed. The storage chambers 10 are fixedly provided with communication pipes 11 for connection. The communication pipes 11 are also made of corrosion-resistant material. Valves 12 installed on the communication pipes 11 are used to control the flow of the mixture between different chambers. When it is needed to mix the liquids in different chambers, the corresponding valves 12 can be opened to make the liquids flow through the communication pipes 11. When it is needed to keep the chambers independent, the valves 12 can be closed. This design increases the flexibility of the storage tank and can meet the needs of different production processes for storage and adjustment of toluene mixtures.
[0035] Then, referring to Figure 4In this embodiment, the plurality of baffles 13 fixedly arranged inside the tank body 1 are all arc-shaped and uniformly distributed along the edges of the stirring blades 7. The baffles 13 are made of corrosion-resistant metal plates or plastics and are accurately processed into arc shapes. The design of uniformly distributing the baffles 13 along the edges of the stirring blades 7 can interfere with the flow of the liquid when the stirring blades 7 rotate. When the stirring blades 7 push the liquid to flow, the baffles 13 can change the flow direction and speed of the liquid, so that the liquid forms a more complex flow field. This complex flow field helps to improve the mixing effect of the liquid and promotes the uniform distribution of each component in the toluene mixed liquid. At the same time, it can also reduce the vortex and dead angle that may occur in the stirring process of the liquid, further improving the stirring efficiency and mixing quality.
[0036] Secondly, referring to Figure 2 In this embodiment, the discharge pump 15 installed at the discharge port 3 has its inlet fixedly arranged with the discharge port 3. The discharge pump 15 is a corrosion-resistant centrifugal pump or a positive displacement pump, which is selected according to the characteristics of the toluene mixed liquid and the discharge requirements. The discharge pump 15 can provide sufficient pressure to transport the toluene mixed liquid in the tank to the external equipment, ensuring smooth discharge process. The outlet of the discharge pump 15 is connected to the external equipment through the discharge pipeline 16. The discharge pipeline 16 is made of corrosion-resistant pipeline materials, such as stainless steel pipes or polytetrafluoroethylene pipes. The flow regulating valve 17 fixedly arranged on the discharge pipeline 16 is used to control the flow size of the discharge. The operator can accurately control the discharge speed of the toluene mixed liquid by adjusting the flow regulating valve 17 according to the receiving capacity of the external equipment and the requirements of the production process, so as to ensure the stability and continuity of the production process.
[0037] Finally, referring to Figure 6 and Figure 7In the embodiment, the vibration assembly 8 comprises a mounting plate 18 which is detachably arranged at the bottom of the tank body 1, is made of metal plate, is connected with the bottom of the tank body 1 by bolt connection or other detachable manner, is convenient for installation and maintenance, the springs 19 which are uniformly and fixedly arranged on the mounting plate 18 are made of high-quality spring 19 steel, have a proper elastic coefficient, the vibration plates 20 which are fixedly arranged between the top portions of the springs 19 are provided with a proper elastic coefficient, the springs 19 play a role of buffering and transmitting vibration in the vibration process, so that the vibration plates 20 can generate stable vibration effect, the motor 21 which is fixedly arranged on the mounting plate 18 provides power for the vibration assembly 8, the rotating rod 22 which is fixedly arranged on the output shaft of the motor 21 is adapted with the sliding groove 23 which is arranged on the mounting plate 18, one end of the rotating rod 22 is attached to the vibration plate 20, the other end is adapted with the sliding groove 23 which is arranged on the mounting plate 18, when the motor 21 rotates, the rotating rod 22 rotates in the sliding groove 23, the attached surface of the rotating rod 22 and the vibration plate 20 will push the vibration plate 20 to generate vibration, by controlling the rotating speed of the motor 21, the vibration frequency and amplitude of the vibration plate 20 can be adjusted, the inclined drainage plate 24 which is fixedly arranged at the top of the vibration plate 20 is close to the discharge port 3 at the low end, the inclined direction is towards the discharge port 3, the drainage plate 24 is made of corrosion-resistant metal or plastic, the inclined design thereof can guide the toluene mixed solution at the tank bottom to flow to the discharge port 3 in the vibration process, prevent solid particles or impurities from depositing at the tank bottom, at the same time, can also accelerate the discharging process of the liquid, ensure that the liquid in the tank can be discharged more thoroughly.
[0038] Working principle:
[0039] The extraction rectification toluene mixture production storage tank, in use, first toluene mixture is added into the storage tank through the feed inlet 2, the funnel-shaped feed inlet 2 makes the mixture flow smoothly, the guide plate 14 inside the feed inlet 2 guides the mixture to be evenly dispersed into the tank body 1, avoids concentrated impact in a place in the tank, the driving motor 21 of the stirring assembly 4 is started, the motor 21 drives the stirring shaft 5 to rotate, the stirring paddle 7 of multiple layers and different shapes and sizes on the stirring shaft 5 rotates, the stirring paddle 7 of different layers is stirred from different angles and depths to toluene mixture, forms a complex stirring flow field, prevents the mixture from precipitating, stratifying, and makes the newly added raw materials and the original mixture quickly and uniformly mixed, if further enhancing the mixing effect is required, the vibration assembly 8 is started, the motor 21 of the vibration assembly 8 rotates, drives the rotating rod 22 on the output shaft to rotate in the sliding groove 23, pushes the vibration plate 20 to vibrate, the vibration plate 20 transmits vibration through the spring 19, makes the tank body 1 vibrate, promotes the mixture in the tank to flow more violently, and the stirring effect of the stirring paddle 7 is superimposed, so that the mixture components are more fully mixed, at the same time, the guide plate 24 on the top of the vibration plate 20 guides the mixture at the bottom of the tank to flow to the discharge port 3, prevents impurities from precipitating, when discharging is required, the discharge pump 15 is started, according to the receiving capacity of the external equipment and the production process requirement, the flow regulating valve 17 on the discharge pipeline 16 is adjusted, the discharge speed of toluene mixture is controlled, the mixture is conveyed to the external equipment through the discharge port 3 and the discharge pipeline 16, if the tank body 1 is provided with multiple layers of partition plates 9, and the toluene mixtures in different storage chambers 10 need to be adjusted, the valve 12 on the communication pipe 11 is opened, so that the liquid flows and mixes between the chambers, after the adjustment is completed, the valve 12 is closed.
[0040] Although the embodiments of the present application have been shown and described, it is to be understood that for the purpose of the present application, the changes, modifications, replacements and variations of the embodiments can be made by those skilled in the art without departing from the principles and spirits of the present application, and the scope of the present application is defined by the appended claims and their equivalents.
Claims
1. An extractive distillation toluene mixture production storage tank characterized by, Include: Tank body (1); Feed inlet (2) is opened in the top of the tank body (1), adopts funnel structure, large mouth end upward, small mouth end with tank body (1) inside direct communication, Discharge port (3) is opened in the bottom of the tank body (1), is located close to the edge of tank body (1) position, Stirring assembly (4) is installed in the tank body (1), the stirring assembly (4) contains stirring shaft (5), stirring shaft (5) from tank body (1) top center position penetrates, is connected with driving motor (6) above tank body (1) top, the stirring shaft (5) is installed multiple layer stirring paddle (7), the shape and size of each layer stirring paddle (7) are different, each layer stirring paddle (7) is sequentially distributed along the axial direction of stirring shaft (5);And Vibration assembly (8) is installed in the bottom of the tank body (1).
2. The storage tank for producing extractive distillation toluene mixture according to claim 1, characterized in that, Also include multiple layers of baffle (9), the multiple layers of baffle (9) are installed in the tank body (1) inside, mutually parallel and present horizontal state, the multiple layers of baffle (9) divide tank body (1) inside space into multiple independent storage chamber (10), each storage chamber (10) between fixedly provided with communication pipe (11) connection, the valve (12) is installed on the communication pipe (11).
3. The storage tank for producing extractive distillation toluene mixture according to claim 1, characterized in that, The tank body (1) is cylindrical, the top of the tank body (1) is relatively flat, the bottom is slightly concave relative to the top.
4. The storage tank for producing extractive distillation toluene mixture according to claim 1, characterized in that, The inside of the tank body (1) is fixedly provided with a plurality of spoiler (13), the spoiler (13) is arc-shaped, and is uniformly distributed along the edge of the stirring paddle (7).
5. The storage tank for producing extractive distillation toluene mixture according to claim 1, wherein, The feed inlet (2) adopts funnel structure, the feed inlet (2) is fixedly provided with a guide vane (14) inside, the guide vane (14) is installed on the inner wall of the feed inlet (2).
6. The storage tank for producing extractive distillation toluene mixture according to claim 1, wherein, The discharge port (3) is provided with a discharge pump (15), the inlet of the discharge pump (15) is fixedly provided with the discharge port (3), the outlet of the discharge pump (15) is connected with external equipment through a discharge pipeline (16), and the discharge pipeline (16) is fixedly provided with a flow regulating valve (17).
7. The storage tank for producing extractive distillation toluene mixture according to claim 1, wherein, The vibration assembly (8) includes a mounting plate (18), the mounting plate (18) is detachably arranged on the bottom of the tank body (1), the mounting plate (18) is uniformly fixedly provided with a spring (19), the top of the spring (19) is fixedly provided with a vibrating plate (20), the mounting plate (18) is fixedly provided with a motor (21), the output shaft of the motor (21) is fixedly provided with a rotating rod (22), the mounting plate (18) is provided with a sliding groove (23), one end of the rotating rod (22) is attached to the vibrating plate (20), and the other end of the rotating rod (22) is matched with the sliding groove (23).
8. The storage tank for producing extractive distillation toluene mixture according to claim 7, characterized in that, The top of the vibrating plate (20) is fixedly provided with an inclined drainage plate (24), the low end of the drainage plate (24) is close to the discharge port (3), and the inclined direction of the drainage plate (24) is towards the discharge port (3).