Device for preparing hypochlorous acid through multistage reaction

Abstract

The utility model provides a device for preparing hypochlorous acid through multistage reaction, and relates to the technical field of hypochlorous acid preparation. The device for preparing hypochlorous acid through multi-stage reaction comprises a first reaction bin, and an electrolysis mechanism is installed in the first reaction bin. Considering the problem of hypochlorous acid preparation, a sodium chloride solution is conveyed into the first reaction bin through the feeding port, the sodium chloride solution is electrolyzed by utilizing a plurality of positive electrode plates and negative electrode plates, and meanwhile, the sodium chloride solution is stirred by cooperating with an internal stirring rod, so that the sodium chloride solution can fully react; secondly, the electrolyzed mixed solution is conveyed into a second reaction bin through a pump body, it is ensured that the second reaction bin reaches proper reaction conditions through a temperature control mechanism, a pH value sensor and an acid injection opening, further reaction of chlorine, water and sodium hydroxide is promoted, and at the moment, the hypochlorous acid content in the solution is remarkably increased; and compared with traditional preparation only through electrolysis, the yield is higher.

Description

TECHNICAL FIELD

[0001] The application relates to the technical field of hypochlorous acid preparation, in particular to a device for preparing hypochlorous acid through multistage reaction. BACKGROUND

[0002] Hypochlorous acid (HClO) is a chlorine-containing oxygen acid with strong oxidizing properties. This property makes it an extremely effective disinfectant that can quickly destroy the cell walls, cell membranes, and internal protein and nucleic acid structures of bacteria, viruses, and other microorganisms, thereby achieving the purpose of sterilization and disinfection. In the medical and health field, hypochlorous acid is widely used for hospital environment disinfection, medical instrument disinfection, and wound care. Its mild and efficient disinfection characteristics can effectively kill pathogens and reduce irritation to human tissues, which is helpful for wound healing. In the food industry, hypochlorous acid can be used for cleaning and disinfection of food processing equipment and sterilization of food raw materials, which can effectively inhibit microbial growth, prolong the shelf life of food, and ensure food safety. In addition, in the drinking water treatment, sewage treatment, and livestock breeding industries, hypochlorous acid also plays an important role in removing harmful microorganisms and pollutants in water and improving water quality to provide safety protection for people's production and life.

[0003] Currently, the preparation methods of hypochlorous acid mainly include chemical method and electrolysis method. For the electrolysis method, hypochlorous acid is prepared by electrolyzing sodium chloride (NaCl) solution. This method is relatively environmentally friendly, but the traditional single-stage electrolysis device has many problems. Due to insufficient reaction, the yield of hypochlorous acid is low, and the generated product often contains many impurities such as unreacted raw materials and by-product, which limits the application range and effect of hypochlorous acid to some extent. CONTENT OF THE INVENTION

[0004] The application provides a device for preparing hypochlorous acid through multistage reaction to solve the problem of hypochlorous acid preparation.

[0005] The application provides a device for preparing hypochlorous acid through multistage reaction, which comprises a first reaction bin, an electrolysis mechanism is installed in the inside of the first reaction bin, a motor box is fixedly connected to the top of the first reaction bin, a stirring mechanism is installed in the inside of the motor box, a flow pipe is formed in the bottom of the first reaction bin, a pump body is through connection at the end of the flow pipe, a second reaction bin is through connection at the output end of the pump body through a pipeline, the electrolysis mechanism comprises a plurality of positive electrode sheets which are installed in the inside of the first reaction bin, a storage battery is electrically connected to one side of the positive electrode sheet through a power line, and a negative electrode sheet is electrically connected to the other side of the positive electrode sheet through a power line; the stirring mechanism comprises a driving motor which is installed in the inside of the motor box, and a stirring rod is fixedly connected to the output end of the driving motor.

[0006] Preferably, the top of the first reaction bin is provided with a feeding port, and one side of the feeding port is provided with a gas vent.

[0007] Preferably, the inside of the second reaction bin is provided with a cavity, and the inside of the cavity is provided with a temperature control mechanism.

[0008] Preferably, the temperature control mechanism comprises a heating net installed in the cavity, one side of the heating net is electrically connected with a temperature controller through a power line, and the other side of the heating net is electrically connected with a battery pack through a power line.

[0009] Preferably, the top of the second reaction bin is provided with a temperature sensor, one side of the temperature sensor is provided with a pH sensor, one side of the pH sensor is provided with an acid injection port, and the inside of the acid injection port is provided with a sealing plug.

[0010] Preferably, the bottom of the second reaction bin is provided with a drainage pipe, and the end of the drainage pipe is connected with a filter chamber in a penetrating manner.

[0011] Preferably, the inside of the filter chamber is provided with two sliding grooves, one of the sliding grooves is slidably connected with a filter screen, and the other of the sliding grooves is slidably connected with an activated carbon layer.

[0012] Beneficial effects:

[0013] Considering the problem of hypochlorous acid preparation, the sodium chloride solution is conveyed into the first reaction bin through the feeding port, and the sodium chloride solution is electrolyzed by using a plurality of positive electrode sheets and negative electrode sheets, and is stirred by using the internal stirring rod, so that the reaction can be fully carried out. Secondly, the mixed solution after electrolysis is conveyed into the second reaction bin by using the pump body, and the second reaction bin reaches the appropriate reaction condition by using the temperature control mechanism, the pH sensor and the acid injection port, so as to promote the further reaction of chlorine, water and sodium hydroxide. At this time, the content of hypochlorous acid in the solution has been significantly improved. Compared with the traditional preparation method only using electrolysis, the yield is higher.

[0014] The above description is only a summary of the technical scheme of the embodiments of the present application. In order to more clearly understand the technical means of the embodiments of the present application, the embodiments of the present application can be implemented according to the content of the specification, and in order to make the above and other purposes, characteristics and advantages of the embodiments of the present application more obvious and easy to understand, the following specific embodiments of the present application are described. BRIEF DESCRIPTION OF DRAWINGS

[0015] In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings needed to be used in the embodiment description will be briefly introduced as follows. Obviously, the drawings described in the following are some embodiments of the present application, and for those skilled in the art, other drawings can also be obtained without creative labor on the basis of these drawings.

[0016] Figure 1 It is a whole structure schematic view of the device for preparing hypochlorous acid by multistage reaction of the utility model.

[0017] Figure 2 It is a stirring mechanism structure schematic view of the device for preparing hypochlorous acid by multistage reaction of the utility model.

[0018] Figure 3 It is a temperature control mechanism structure schematic view of the device for preparing hypochlorous acid by multistage reaction of the utility model.

[0019] Figure 4 It is a filter chamber structure schematic view of the device for preparing hypochlorous acid by multistage reaction of the utility model.

[0020] Explanation of reference signs:

[0021] 1, first reaction bin;2, electrolysis mechanism;201, positive electrode sheet;202, storage battery;203, negative electrode sheet;3, motor box;4, stirring mechanism;401, driving motor;402, stirring rod;5, flow pipe;6, pump body;7, second reaction bin;8, feeding port;9, air release port;10, temperature control mechanism;1001, heating net;1002, temperature controller;1003, battery pack;11, temperature sensor;12, pH sensor;13, acid injection port;14, drainage pipe;15, filter chamber;16, filter screen;17, activated carbon layer. DETAILED DESCRIPTION

[0022] In order to make the purpose, technical solutions and advantages of the embodiments of the present application more clear, the technical solutions in the embodiments of the present application will be described clearly and completely in the following with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are some embodiments of the present application, but not all the embodiments. Based on the embodiments in the present application, all other embodiments obtained by those skilled in the art without creative labor are within the protection scope of the present application.

[0023] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs; the terminology used in the description herein is for describing particular embodiments only and is not intended to be limiting of the application; the use herein of terms such as "comprise", "have" and "include" or their conjugates herein, are used in their open ended, non-limiting sense to encompass the items listed or the equivalents thereof.

[0024] Reference herein to "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment can be included in at least one embodiment of the application. The appearances of the phrase "in an embodiment" in various places in the specification are not necessarily all referring to the same embodiment, nor are they necessarily mutually exclusive of one another.

[0025] The positional words appearing in the following description are the directions shown in the drawings, and are not intended to limit the specific structure of the application. For example, in the description of the application, the terms "center", "lengthwise", "transverse", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", "axial", "radial", "circumferential" and the like indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, and are only for the convenience of describing the application and simplifying the description, and are not intended to indicate or imply that the devices or elements referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore cannot be understood as limiting the application.

[0026] In the description of the application, it should be noted that, unless otherwise specified and limited, the terms "mounting", "connection", "connection" should be understood broadly, for example, the "connection" or "connection" of mechanical structure can mean physical connection, for example, physical connection can be fixed connection, for example, fixed connection by fixing member, for example, fixed connection by screw, bolt or other fixing member; physical connection can also be detachable connection, for example, mutual clamping or clamping connection; physical connection can also be integrally connected, for example, welding, bonding or integrally formed connection. For those skilled in the art, the specific meaning of the above terms in the application can be understood according to the specific circumstances.

[0027] In order to enable those skilled in the art to better understand the scheme of the present application, the technical solutions in the embodiments of the present application will be described clearly and completely in conjunction with the drawings.

[0028] The utility model provides a kind of Figures 1-4The device for preparing hypochlorous acid by multi-stage reaction shown comprises a first reaction bin 1, an electrolysis mechanism 2 is arranged in the first reaction bin 1, a motor box 3 is fixedly connected to the top of the first reaction bin 1, a stirring mechanism 4 is arranged in the motor box 3, a flow pipe 5 is arranged at the bottom of the first reaction bin 1, a pump body 6 is connected to the end of the flow pipe 5, a second reaction bin 7 is connected to the output end of the pump body 6 through a pipeline, the electrolysis mechanism 2 comprises a plurality of positive electrode sheets 201 arranged in the first reaction bin 1, a storage battery 202 is electrically connected to one side of the positive electrode sheet 201 through a power line, and a negative electrode sheet 203 is electrically connected to the other side of the positive electrode sheet 201 through a power line; the stirring mechanism 4 comprises a driving motor 401 arranged in the motor box 3, and a stirring rod 402 is fixedly connected to the output end of the driving motor 401.

[0029] The top of the first reaction bin 1 is provided with a feeding port 8, and the feeding port 8 is provided with a gas vent 9.

[0030] The gas vent 9 is arranged to play a role of exhausting.

[0031] The second reaction bin 7 is internally provided with a cavity, and a temperature control mechanism 10 is arranged in the cavity.

[0032] The temperature control mechanism 10 is arranged to ensure that the temperature in the second reaction bin 7 reaches a suitable temperature.

[0033] The temperature control mechanism 10 comprises a heating net 1001 arranged in the cavity, a temperature controller 1002 is electrically connected to one side of the heating net 1001 through a power line, and a battery pack 1003 is electrically connected to the other side of the heating net 1001 through a power line.

[0034] The battery pack 1003 is arranged to play a role of continuous power supply.

[0035] The second reaction bin 7 is provided with a temperature sensor 11 at the top, an acid-base value sensor 12 is arranged at one side of the temperature sensor 11, an acid injection port 13 is arranged at one side of the acid-base value sensor 12, and a sealing plug is arranged in the acid injection port 13.

[0036] The sealing plug is arranged to play a role of sealing the acid injection port 13.

[0037] The second reaction bin 7 is provided with a drainage pipe 14 at the bottom, and a filter chamber 15 is connected to the end of the drainage pipe 14.

[0038] The drainage pipe 14 is arranged to play a role of conveying liquid.

[0039] The inside of the filtering chamber 15 is provided with two chutes, one of which is slidably connected with the filter screen 16, and the other is slidably connected with the activated carbon layer 17.

[0040] The filter screen 16 is arranged to purify the reacted liquid.

[0041] Working principle: when the device is used, the sodium chloride solution is electrolyzed in the first reaction bin 1, and the mixed solution after electrolysis is delivered to the inside of the second reaction bin 7 by the pump body 6 at the bottom for secondary reaction. The temperature control mechanism 10, the temperature sensor 11, the acid-base sensor 12 and the acid injection port 13 arranged in the second reaction bin 7 promote the further reaction of chlorine, water and sodium hydroxide, and finally the generated hypochlorous acid solution enters the inside of the filtering chamber 15 through the drainage pipe 14 for purification treatment.

[0042] The above-described embodiments are only used to illustrate the technical solutions of the present application, rather than limit them. Although the present application has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that they can still modify the technical solutions recorded in the foregoing embodiments, or make equivalent replacements for some technical features. Such modifications or replacements do not make the essence of the corresponding technical solutions deviate from the spirit and scope of the technical solutions of the embodiments of the present application.

Claims

1. An apparatus for preparing hypochlorous acid through a multi-stage reaction, comprising a first reaction chamber (1), characterized in that: An electrolysis mechanism (2) is installed inside the first reaction chamber (1). A motor housing (3) is fixedly connected to the top of the first reaction chamber (1). A stirring mechanism (4) is installed inside the motor housing (3). A flow pipe (5) is opened at the bottom of the first reaction chamber (1). A pump body (6) is connected through the end of the flow pipe (5). The output end of the pump body (6) is connected through a pipe to a second reaction chamber (7). The electrolysis mechanism (2) includes a plurality of positive electrode plates (201) installed inside the first reaction chamber (1). One side of the positive electrode plate (201) is electrically connected to a battery (202) via a power line, and the other side of the positive electrode plate (201) is electrically connected to a negative electrode plate (203) via a power line. The stirring mechanism (4) includes a drive motor (401) installed inside the motor housing (3), and the output end of the drive motor (401) is fixedly connected to a stirring rod (402).

2. The apparatus for preparing hypochlorous acid through a multi-stage reaction according to claim 1, characterized in that: The first reaction chamber (1) has a feeding port (8) at the top, and a vent (9) is installed on one side of the feeding port (8).

3. The apparatus for preparing hypochlorous acid through a multi-stage reaction according to claim 1, characterized in that: The second reaction chamber (7) has an internal cavity, and a temperature control mechanism (10) is installed inside the cavity.

4. The apparatus for preparing hypochlorous acid via a multi-stage reaction according to claim 3, characterized in that: The temperature control mechanism (10) includes a heating grid (1001) installed inside the cavity. One side of the heating grid (1001) is electrically connected to a temperature controller (1002) via a power line, and the other side of the heating grid (1001) is electrically connected to a battery pack (1003) via a power line.

5. The apparatus for preparing hypochlorous acid via a multi-stage reaction according to claim 1, characterized in that: A temperature sensor (11) is installed on the top of the second reaction chamber (7). A pH sensor (12) is installed on one side of the temperature sensor (11). An acid injection port (13) is opened on one side of the pH sensor (12). A sealing plug is installed inside the acid injection port (13).

6. The apparatus for preparing hypochlorous acid through a multi-stage reaction according to claim 1, characterized in that: The bottom of the second reaction chamber (7) is provided with a drainage pipe (14), and the end of the drainage pipe (14) is connected to a filter chamber (15).

7. The apparatus for preparing hypochlorous acid through a multi-stage reaction according to claim 6, characterized in that: The filter chamber (15) has two slids inside, one of which is slidably connected to a filter screen (16), and the other is slidably connected to an activated carbon layer (17).

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