Nanoparticle assembly reaction system
By using a combination of inclined stirring blades and wave-shaped guide rails in the nanoparticle assembly reaction system, vertical periodic shear force is provided, which solves the problem of uneven mixing of nanoparticle raw materials in hydrothermal reaction, realizes the circulation flow and efficient mixing of inner and outer layers, and improves production quality.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-05-26
- Publication Date
- 2026-03-27
AI Technical Summary
In existing nanoparticle assembly reactors, the vertical mobility of nanoparticle raw materials is poor during hydrothermal reactions, resulting in poor mixing effects, especially limited interaction between inner and outer layers.
The system employs a combination of inclined stirring blades and corrugated guide rails to provide vertical periodic shear force, enabling the nanoparticle raw materials to circulate in both the inner and outer layers within the hydrothermal reaction chamber. The inclined stirring blades exert an oblique force through the cooperation of a motor-driven rotating shaft and stirring rod, thereby improving the mixing effect.
This significantly improves the production quality of nanoparticles, enabling uniform mixing and circulation of nanoparticle raw materials within the hydrothermal reaction chamber, thereby enhancing production efficiency.
Smart Images
Figure CN224040968U_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The utility model relates to nanometer particle assembly technical field, concretely is a kind of nanometer particle assembly reaction system. BACKGROUND
[0002] Nanometer particle assembly reaction refers to arranging, combining nanometer scale particles according to specific mode by physical, chemical or biological method, and forming assembly body with specific structure, function and property, and nanometer particle assembly reaction system is important equipment for producing nanometer particle;
[0003] The existing nanometer particle assembly reaction kettle, in hydrothermal reaction area, realizes the stirring mixing of nanometer particle raw material by the stirring blade of uniaxial unidirectional rotation, and then assists the mutual contact between various nanometer particle raw materials in hydrothermal reaction, this mode can only realize the movement of various nanometer particle raw materials in horizontal direction, in vertical direction, various nanometer particle raw materials are poor in activity, and the interaction of various nanometer particle raw materials in inner and outer layers of hydrothermal reaction area is limited, thereby affecting the stirring mixing effect of various nanometer particle raw materials in hydrothermal reaction area. UTILITY MODEL CONTENT
[0004] The utility model solves the technical problems of overcoming the defects of the prior art, and provides a nanometer particle assembly reaction system, which provides periodic shear force in the vertical direction when performing horizontal stirring and mixing of nanometer particle raw materials, realizes the inner and outer double-layer circulation flow of nanometer particle raw materials in the hydrothermal reaction bin under the oblique force of oblique stirring blade, greatly improves the production quality of nanometer particles, and can effectively solve the problems in the background art.
[0005] To achieve the above object, the utility model provides the following technical scheme: a nanometer particle assembly reaction system, comprising a support frame, a hydrothermal reaction bin is arranged at the upper end of the support frame, a mixing bin is arranged at the middle part of the support frame, and a discharge bin is arranged at the lower end of the support frame, and further comprising a stirring mechanism.
[0006] The stirring mechanism comprises a rotating shaft, a fixed cylinder, a cross rod, a stirring rod and an inclined stirring blade, the rotating shaft is rotationally connected to the center position of the top wall of the hydrothermal reaction bin, the upper end of the outer surface of the rotating shaft is fixedly connected with the fixed cylinder, the middle part of the outer arc surface of the fixed cylinder is provided with three evenly distributed cross rods, the three cross rods are fixedly connected with a connecting ring, the upper end of the inside of the hydrothermal reaction bin is fixedly connected with a partition plate, the middle part of the rotating shaft is rotationally connected to the inside of the partition plate, the inside of the partition plate is provided with evenly distributed sliding openings, the inside of the sliding openings is slidably connected with the stirring rods, the upper surface of the partition plate and the upper end of the outer surface of the stirring rods are fixedly connected with rubber sealing sleeves, the end of the cross rod away from the central axis of the rotating shaft is fixedly connected with the upper end of the radially adjacent stirring rod, the middle part of the stirring rod is fixedly connected with evenly distributed inclined stirring blades, the lower end of the outer surface of the rotating shaft is fixedly connected with evenly distributed inclined plates, vertical periodic shear force is provided when the transverse stirring and mixing of the nanoparticle raw materials are carried out, under the action of the inclined force of the inclined stirring blades, the inside and outside double-layer circulation flow of the nanoparticle raw materials in the hydrothermal reaction bin is realized, and the production quality of the nanoparticles is greatly improved.
[0007] Further, the right end of the front side surface of the support frame is provided with a PLC controller, the input end of the PLC controller is electrically connected with an external power supply, and various electrical appliances are controlled.
[0008] Further, the stirring mechanism further comprises a motor one, a wave-shaped guide rail and a sliding ball, the motor one is arranged at the upper end of the hydrothermal reaction bin, the lower end of the output shaft of the motor one is fixedly connected with the upper end of the rotating shaft, the wave-shaped guide rail is arranged at the middle part of the outer arc surface of the fixed cylinder, the inside of the wave-shaped guide rail is slidably connected with three sliding balls, the sliding ball is fixedly connected with the end of the radially adjacent cross rod close to the central axis of the rotating shaft, the input end of the motor one is electrically connected with the output end of the PLC controller, and the vertical periodic movement of the stirring rod is realized.
[0009] Further, the upper end of the mixing bin is provided with a driving bin, the inside of the driving bin is rotationally connected with a rotating shaft, the rotating shaft extends to the inside of the mixing bin, the driving bin and the mixing bin are rotationally connected with a rotating drum, the rotating shaft is located in the inside of the rotating drum, the lower end of the outer surface of the rotating drum is fixedly connected with a stirring frame, the lower end of the outer surface of the rotating shaft is fixedly connected with evenly distributed stirring blades, the upper end of the mixing bin is provided with a motor two, the motor two is located in the inside of the driving bin, the rear end of the output shaft of the motor two is fixedly connected with a driving bevel gear, the upper end of the outer surface of the rotating drum is fixedly connected with a driven bevel gear one, the upper end of the outer surface of the rotating shaft is fixedly connected with a driven bevel gear two, the driven bevel gear one and the driven bevel gear two are meshingly connected with the driving bevel gear, the input end of the motor two is electrically connected with the output end of the PLC controller, and driving force is provided for the stirring work in the inside of the hydrothermal reaction bin.
[0010] Further, the outer arc surfaces of the hydrothermal reaction bin and the mixing bin are provided with heating bins, the heating bins are provided with spiral heaters, input ends of the heaters are electrically connected with output ends of the PLC controller, front ends of the hydrothermal reaction bin and the mixing bin are provided with temperature sensors, right ends of the hydrothermal reaction bin and the mixing bin are provided with pressure sensors, and the temperature sensors and the pressure sensors are bidirectionally electrically connected with the PLC controller, so that heat is provided for the production of nanoparticles and the temperature and the pressure in the production environment of the nanoparticles are detected.
[0011] Further, the lower end of the hydrothermal reaction bin and the upper end of the mixing bin are communicated through a connecting pipe one, the lower end of the mixing bin and the upper end of the discharge bin are communicated through a connecting pipe two, middle parts of the connecting pipe one and the connecting pipe two are provided with electromagnetic valves, the rear end of the hydrothermal reaction bin is provided with an air outlet pipe, a middle part of the air outlet pipe is provided with an electric exhaust valve, the right end of the hydrothermal reaction bin is provided with three feeding pipes, the front end of the hydrothermal reaction bin is provided with a water inlet pipe, and input ends of the two electromagnetic valves and the electric exhaust valve are electrically connected with output ends of the PLC controller, so that channels are provided for the movement of the nanoparticle materials.
[0012] Further, the inside of the discharge bin is rotatably connected with a rotating rod, the outer surface of the rotating rod is provided with spiral leaves, the front end of the discharge bin is provided with a motor three, the rear end of the output shaft of the motor three is fixedly connected with the front end of the rotating rod, the rear end of the discharge bin is provided with a discharge port, and the input end of the motor three is electrically connected with the output end of the PLC controller, so that the discharge of the nanoparticles is realized.
[0013] Compared with the prior art, the nanoparticle assembly reaction system has the following advantages:
[0014] The motor drives the rotating shaft to rotate, so that the inclined plate in rotation stirs and mixes the nanoparticle raw materials in the hydrothermal reaction bin, the three stirring rods move vertically and periodically under the action of the wave-shaped guide rail, vertical and periodic shearing force is provided for the horizontal stirring and mixing of the nanoparticle raw materials, the nanoparticle raw materials realize inner and outer double-layer circulation flow in the hydrothermal reaction bin under the oblique force of the inclined stirring piece, and the production quality of the nanoparticles is greatly improved. BRIEF DESCRIPTION OF DRAWINGS
[0015] Figure 1 It is a structural schematic view of the utility model;
[0016] Figure 2 It is a sectional view of the inside of the utility model;
[0017] Figure 3 It is a sectional view of the upper side of the utility model;
[0018] Figure 4 It is an enlarged structural schematic view of position A of the utility model;
[0019] Figure 5 It is the enlarged structure schematic view of B place of the utility model;
[0020] Figure 6 It is the enlarged structure schematic view of C place of the utility model.
[0021] In the figure: 1 support frame, 2 hydrothermal reaction bin, 3 mixing bin, 4 drive bin, 5 stirring mechanism, 51 motor one, 52 rotating shaft, 53 fixed cylinder, 54 cross bar, 55 wave-shaped guide rail, 56 sliding ball, 57 stirring rod, 58 oblique stirring piece, 6 heating bin, 7 rotating drum, 8 rotating shaft, 9 motor two, 10 stirring frame, 11 discharge bin, 12 rotating rod, 13 motor three, 14 electromagnetic valve, 15 feed pipe, 16 water inlet pipe, 17 electric exhaust valve, 18 pressure sensor, 19 temperature sensor, 20 PLC controller, 21 heater, 22 rubber sealing sleeve. DETAILED DESCRIPTION
[0022] The technical scheme in the embodiments of the utility model will be described clearly and completely below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor fall within the scope of protection of the utility model.
[0023] Please refer to Figures 1-6 The embodiment provides a kind of technical scheme: a kind of nanoparticle assembly reaction system, including support frame 1, the upper end of support frame 1 is provided with hydrothermal reaction bin 2, the middle part of support frame 1 is provided with mixing bin 3, the lower end of support frame 1 is provided with discharge bin 11, the right end of the front surface of support frame 1 is provided with PLC controller 20, the input end of PLC controller 20 is electrically connected with external power supply, it further includes stirring mechanism 5;
[0024] The stirring mechanism 5 comprises a rotating shaft 52, a fixed cylinder 53, a cross rod 54, a stirring rod 57 and an inclined stirring blade 58. The rotating shaft 52 is rotationally connected to the center of the top wall of the hydrothermal reaction chamber 2. The upper end of the outer surface of the rotating shaft 52 is fixedly connected with the fixed cylinder 53. The middle part of the outer arc surface of the fixed cylinder 53 is provided with three evenly distributed cross rods 54. The three cross rods 54 are fixedly connected with a connecting ring. The upper end inside the hydrothermal reaction chamber 2 is fixedly connected with a partition plate. The middle part of the rotating shaft 52 is rotationally connected with the inside of the partition plate. The inside of the partition plate is provided with evenly distributed sliding ports. The inside of the sliding ports is slidably connected with the stirring rods 57. The upper surface of the partition plate and the upper end of the outer surface of the stirring rods 57 are fixedly connected with rubber sealing sleeves 22. The rubber sealing sleeves 22 can be elastically deformed in the vertical position change process of the stirring rods 57. The rubber sealing sleeves 22 can ensure the sealing of the sliding ports, avoid the leakage of raw materials, and ensure the sealing of the sliding ports. The end of the cross rod 54 away from the central axis of the rotating shaft 52 is fixedly connected with the upper end of the radially adjacent stirring rod 57. The middle part of the stirring rod 57 is fixedly connected with evenly distributed inclined stirring blades 58. The lower end of the outer surface of the rotating shaft 51 is fixedly connected with evenly distributed inclined plates. The stirring mechanism 5 further comprises a motor one 51, a wave-shaped guide rail 55 and a sliding ball 56. The motor one 51 is arranged at the upper end of the hydrothermal reaction chamber 2. The lower end of the output shaft of the motor one 51 is fixedly connected with the upper end of the rotating shaft 52. The wave-shaped guide rail 55 is arranged at the middle part of the outer arc surface of the fixed cylinder 53. The inside of the wave-shaped guide rail 55 is slidably connected with three sliding balls 56. The sliding balls 56 are fixedly connected with the end of the radially adjacent cross rod 54 close to the central axis of the rotating shaft 52. The input end of the motor one 51 is electrically connected with the output end of the PLC controller 20. The operation of the motor one 51 is realized through the PLC controller 20. The output shaft of the motor one 51 drives the rotating shaft 52 to rotate. The rotating shaft 52 drives the evenly distributed inclined plates to rotate, realizing the stirring and mixing of the nano-particle raw materials in the hydrothermal reaction chamber 2. At the same time, the rotating shaft 52 drives the fixed cylinder 53 to rotate. The fixed cylinder 53 drives the wave-shaped guide rail 55 to rotate, so that the sliding balls 56 slide in the wave-shaped guide rail 55. The sliding balls 56 drive the corresponding stirring rods 57 to move vertically and periodically through the radially adjacent cross rods 54. At the same time, the three stirring rods 57 are guaranteed to move vertically and periodically under the connection of the connecting ring. The stirring rods 57 drive the evenly distributed inclined stirring blades 58 to move vertically and periodically. The vertical and periodic shearing force is provided when the nano-particle raw materials are stirred and mixed horizontally. Under the inclined force of the inclined stirring blades 58, the nano-particle raw materials move upward under the action of the upward movement of the inclined stirring blades 58, and the nano-particle raw materials move away from the center of the hydrothermal reaction chamber 2 under the action of the downward movement of the inclined stirring blades 58, realizing the internal and external double-layer circulation flow of the nano-particle raw materials in the hydrothermal reaction chamber, greatly improving the mixing effect of the nano-particle raw materials.
[0025] The upper end of the mixing bin 3 is provided with a driving bin 4, a rotating shaft 8 is rotatably connected in the driving bin 4, the rotating shaft 8 extends to the inside of the mixing bin 3, a rotating drum 7 is rotatably connected between the driving bin 4 and the mixing bin 3, the rotating shaft 8 is located in the inside of the rotating drum 7, a stirring frame 10 is fixedly connected to the lower end of the outer surface of the rotating drum 7, a plurality of stirring blades are fixedly connected to the lower end of the outer surface of the rotating shaft 8, the upper end of the mixing bin 3 is provided with a motor 2 9, the motor 2 9 is located in the inside of the driving bin 4, the rear end of the output shaft of the motor 2 9 is fixedly connected with a driving bevel gear, a driven bevel gear one is fixedly connected to the upper end of the outer surface of the rotating drum 7, a driven bevel gear two is fixedly connected to the upper end of the outer surface of the rotating shaft 8, the driven bevel gear one and the driven bevel gear two are meshingly connected with the driving bevel gear, the input end of the motor 2 9 is electrically connected with the output end of the PLC controller 20, the PLC controller 20 realizes the operation of the motor 2 9, the output shaft of the motor 2 9 drives the driving bevel gear to rotate, the driving bevel gear drives the driven bevel gear one to rotate, the driven bevel gear one drives the rotating drum 7 to rotate, the rotating drum 7 drives the stirring frame to rotate clockwise, at the same time, the driving bevel gear drives the driven bevel gear two to rotate, the driven bevel gear two drives the rotating shaft 8 to rotate, the rotating shaft 8 drives the plurality of stirring blades to rotate counterclockwise, the assembly of the accelerant and the silicon dioxide nanoparticle precursor is fully contacted, and the nanoparticle assembly is realized.
[0026] The outer arc surfaces of the hydrothermal reaction bin 2 and the mixing bin 3 are provided with heating bins 6, the heating bins 6 are provided with spiral heaters 21, the input ends of the heaters 21 are electrically connected with the output end of the PLC controller 20, the front ends of the hydrothermal reaction bin 2 and the mixing bin 3 are provided with temperature sensors 19, the right ends of the hydrothermal reaction bin 2 and the mixing bin 3 are provided with pressure sensors 18, and the temperature sensors 19 and the pressure sensors 18 are bidirectionally electrically connected with the PLC controller 20.
[0027] The lower end of the hydrothermal reaction bin 2 and the upper end of the mixing bin 3 are communicated through a connecting pipe one, the lower end of the mixing bin 3 and the upper end of the discharge bin 11 are communicated through a connecting pipe two, the middle part of the connecting pipe one and the connecting pipe two are provided with electromagnetic valves 14, the rear end of the hydrothermal reaction bin 2 is provided with an air outlet pipe, the middle part of the air outlet pipe is provided with an electric exhaust valve 17, the right end of the hydrothermal reaction bin 2 is provided with three feeding pipes 15, the front end of the hydrothermal reaction bin 2 is provided with a water inlet pipe 16, the two electromagnetic valves 14 and the electric exhaust valve 17 are electrically connected with the output end of the PLC controller 20, the PLC controller 20 realizes the operation of the heater 21 on the upper side, provides heat for the hydrothermal reaction of the nano-particle raw material, increases the temperature of the hydrothermal reaction bin 2 to a set value of 120-180 DEG C, and keeps for a certain time of 6-12 hours, carries out the hydrothermal reaction, generates the silica nano-particle precursor, at the same time, the PLC controller 20 realizes the operation of the temperature sensor 19 and the pressure sensor 18 on the upper side, the temperature sensor 19 monitors the temperature inside the hydrothermal reaction bin 2 through the reflection of infrared rays, at the same time, when the gas pressure acts on the sensitive element (usually a silicon diaphragm) of the pressure sensor 18, the diaphragm will be deformed, causing the resistance value of the pressure resistance element on the diaphragm to change, the size of the gas pressure can be known by measuring the change of the resistance value, realizing the real-time monitoring of the gas pressure inside the hydrothermal reaction bin 2, when the temperature and pressure inside the hydrothermal reaction bin 2 reach a certain degree, the PLC controller 20 realizes the operation of the electric exhaust valve 17, and carries out exhaust.
[0028] The inside of the discharge bin 11 is rotatably connected with a rotating rod 12, the outer surface of the rotating rod 12 is provided with a spiral blade, the front end of the discharge bin 11 is provided with a motor three 13, the rear end of the output shaft of the motor three 13 is fixedly connected with the front end of the rotating rod 12, the rear end of the discharge bin 11 is provided with a discharge port, the input end of the motor three 13 is electrically connected with the output end of the PLC controller 20, the PLC controller 20 realizes the operation of the motor three 13, the output shaft of the motor three 13 drives the rotating rod 12 to rotate, and then drives the spiral blade to rotate, realizing the spiral conveying of the nano-particles at the rear end of the assembly, and the nano-particles at the rear end of the assembly are removed through the discharge port.
[0029] The working principle of the nanometer particle assembly reaction system is as follows: in working, personnel first place the hydrothermal reaction bin 2 and the mixing bin 3 and other mechanisms stably on a horizontal working area through the support frame 1, after stable placement, personnel inject a certain proportion of silicon source, alkali source and solvent into the inside of the hydrothermal reaction bin 2 through the feeding pipe 15 and the water inlet pipe 16, then realize the rotation of the motor one 51 through the PLC controller 20, the output shaft of the motor one 51 rotates to drive the rotating shaft 52 to rotate, the rotating shaft 52 rotates to drive the uniformly distributed inclined plates to rotate, realize the stirring and mixing of the nanometer particle raw materials in the inside of the hydrothermal reaction bin 2, at the same time, the rotating shaft 52 rotates to drive the fixed cylinder 53 to rotate, the fixed cylinder 53 rotates to drive the wave-shaped guide rail 55 to rotate, then make the sliding balls 56 slide in the inside of the wave-shaped guide rail 55, the sliding balls 56 drive the corresponding stirring rods 57 to move vertically and periodically through the radially adjacent cross rods 54, at the same time, the synchronous movement of the three stirring rods 57 in the vertical direction is ensured under the connecting effect of the connecting ring, the stirring rods 57 drive the uniformly distributed inclined stirring blades 58 to move vertically and periodically, provide vertical and periodic shearing force when the nanometer particle raw materials are stirred and mixed horizontally, under the oblique force of the inclined stirring blades 58, the nanometer particle raw materials are guided to move to the direction close to the center of the hydrothermal reaction bin 2 in the process that the inclined stirring blades 58 move upwards and drive the nanometer particle raw materials to move upwards, the nanometer particle raw materials are guided to move to the direction away from the center of the hydrothermal reaction bin 2 in the process that the inclined stirring blades 58 move downwards and drive the nanometer particle raw materials to move downwards, realize the inner and outer double-layer circulation flow of the nanometer particle raw materials in the inside of the hydrothermal reaction bin, greatly improve the mixing effect of the nanometer particle raw materials, at the same time, the PLC controller 20 realizes the operation of the heater 21 on the upper side, provides heat for the hydrothermal reaction of the nanometer particle raw materials, increases the temperature of the hydrothermal reaction bin 2 to the set value 120-180 DEG C, and keeps for a certain time 6-12 hours, carries out the hydrothermal reaction, generates the silicon dioxide nanometer particle precursor, at the same time, the PLC controller 20 realizes the operation of the temperature sensor 19 and the pressure sensor 18 on the upper side, the temperature sensor 19 monitors the temperature in the inside of the hydrothermal reaction bin 2 through the reflection of infrared rays, at the same time, when the gas pressure acts on the sensitive element (usually silicon diaphragm) of the pressure sensor 18, the diaphragm is deformed, the resistance value of the pressure resistance element on the diaphragm is changed, the size of the gas pressure can be known through the measurement of the resistance value change, realize the real-time monitoring of the gas pressure in the inside of the hydrothermal reaction bin 2, when the temperature and pressure in the inside of the hydrothermal reaction bin 2 reach a certain degree, the PLC controller 20 realizes the operation of the electric exhaust valve 17, carries out exhaust, after the hydrothermal reaction is finished, the PLC controller 20 realizes the opening of the electromagnetic valve 14 on the upper side, the silicon dioxide nanometer particle precursor enters the inside of the mixing bin 3 through the connecting pipe one, at the same time, the assembly promoting agent is added into the inside of the mixing bin 3, then the PLC controller 20 realizes the rotation of the motor two 9, the output shaft of the motor two 9 rotates to drive the driving helical gear to rotate, the driving helical gear rotates to drive the driven helical gear one to rotate,The driving bevel gear rotates to drive the rotating drum 7 to rotate, the rotating drum 7 rotates to drive the stirring frame to rotate clockwise, meanwhile, the driving bevel gear rotates to drive the driven bevel gear two to rotate, the driven bevel gear two rotates to drive the rotating shaft 8 to rotate, the rotating shaft 8 rotates to drive the uniformly distributed stirring blades to rotate counterclockwise, the assembly accelerant and the silicon dioxide nanoparticles precursor are fully contacted, the nanoparticles are assembled, then the PLC controller 20 opens the electromagnetic valve 14 at the lower side, the nanoparticles at the rear end after assembly enter the discharge bin 11 through the connecting pipe two, then the PLC controller 20 drives the motor three 13 to rotate, the output shaft of the motor three 13 rotates to drive the rotating rod 12 to rotate, further drives the spiral blade to rotate, realizes the spiral conveying of the nanoparticles at the rear end after assembly, and the nanoparticles at the rear end after assembly are removed through the discharge port.
[0030] It is worth noting that the PLC controller 20 disclosed in the above embodiment controls the motor one 51, the motor two 9, the motor three 13, the electromagnetic valve 14, the electric exhaust valve 17, the pressure sensor 18, the temperature sensor 19 and the heater 21 to work, which all adopt the method commonly used in the prior art.
[0031] The above is only an embodiment of the present application, and does not limit the patent range of the present application, and any equivalent structure or equivalent process conversion, or direct or indirect application in other related technical fields, which is included in the patent protection range of the present application.
Claims
1. A nanoparticle assembly reaction system, comprising a support frame (1), the upper end of the support frame (1) is provided with a hydrothermal reaction bin (2), the middle part of the support frame (1) is provided with a mixing bin (3), and the lower end of the support frame (1) is provided with a discharge bin (11), characterized in that: Also include stirring mechanism (5); The stirring mechanism (5) comprises a rotating shaft (52), a fixed cylinder (53), a cross rod (54), a stirring rod (57) and an inclined stirring blade (58), the rotating shaft (52) is rotatably connected to the central position of the top wall of the hydrothermal reaction bin (2), the upper end of the outer surface of the rotating shaft (52) is fixedly connected with the fixed cylinder (53), the outer arc surface of the fixed cylinder (53) is provided with three evenly distributed cross rods (54), the three cross rods (54) are fixedly connected with a connecting ring, the upper end of the inner portion of the hydrothermal reaction bin (2) is fixedly connected with a partition plate, the middle portion of the rotating shaft (52) is rotatably connected with the inner portion of the partition plate, the inner portion of the partition plate is provided with evenly distributed sliding ports, the inner portion of the sliding port is slidably connected with the stirring rod (57), the upper surface of the partition plate and the upper end of the outer surface of the stirring rod (57) are fixedly connected with rubber sealing sleeves (22), the end of the cross rod (54) away from the central axis of the rotating shaft (52) is fixedly connected with the upper end of the radially adjacent stirring rod (57), the middle portion of the stirring rod (57) is fixedly connected with evenly distributed inclined stirring blades (58), and the lower end of the outer surface of the rotating shaft (52) is fixedly connected with evenly distributed inclined plates.
2. The nanoparticle assembly reaction system of claim 1, wherein: The right end of the front surface of the support frame (1) is provided with a PLC controller (20), and the input end of the PLC controller (20) is electrically connected with an external power supply.
3. The nanoparticle assembly reaction system of claim 2, wherein: The stirring mechanism (5) further comprises a motor one (51), a wave-shaped guide rail (55) and a sliding ball (56), the motor one (51) is arranged at the upper end of the hydrothermal reaction bin (2), the lower end of the output shaft of the motor one (51) is fixedly connected with the upper end of the rotating shaft (52), the wave-shaped guide rail (55) is arranged at the middle portion of the outer arc surface of the fixed cylinder (53), the inner portion of the wave-shaped guide rail (55) is slidably connected with three sliding balls (56), the sliding ball (56) is fixedly connected with the end of the radially adjacent cross rod (54) close to the central axis of the rotating shaft (52), and the input end of the motor one (51) is electrically connected with the output end of the PLC controller (20).
4. The nanoparticle assembly reaction system of claim 2, wherein: The upper end of the mixing bin (3) is provided with a driving bin (4), the inner portion of the driving bin (4) is rotatably connected with a rotating shaft (8), the rotating shaft (8) extends into the inner portion of the mixing bin (3), the driving bin (4) and the mixing bin (3) are rotatably connected with a rotating drum (7), the rotating shaft (8) is located in the inner portion of the rotating drum (7), the lower end of the outer surface of the rotating drum (7) is fixedly connected with a stirring frame (10), the lower end of the outer surface of the rotating shaft (8) is fixedly connected with evenly distributed stirring blades, the upper end of the mixing bin (3) is provided with a motor two (9), the motor two (9) is located in the inner portion of the driving bin (4), the rear end of the output shaft of the motor two (9) is fixedly connected with a driving bevel gear, the upper end of the outer surface of the rotating drum (7) is fixedly connected with a driven bevel gear one, the upper end of the outer surface of the rotating shaft (8) is fixedly connected with a driven bevel gear two, and the driven bevel gear one and the driven bevel gear two are meshingly connected with the driving bevel gear, and the input end of the motor two (9) is electrically connected with the output end of the PLC controller (20).
5. The nanoparticle assembly reaction system of claim 2, wherein: The outer arc surfaces of the hydrothermal reaction bin (2) and the mixing bin (3) are provided with heating bins (6), the heating bins (6) are provided with spiral heaters (21), the input ends of the heaters (21) are electrically connected with the output end of the PLC controller (20), the front ends of the hydrothermal reaction bin (2) and the mixing bin (3) are provided with temperature sensors (19), the right ends of the hydrothermal reaction bin (2) and the mixing bin (3) are provided with pressure sensors (18), and the temperature sensors (19) and the pressure sensors (18) are bidirectionally electrically connected with the PLC controller (20).
6. The nanoparticle assembly reaction system of claim 2, wherein: The lower end of the hydrothermal reaction bin (2) and the upper end of the mixing bin (3) are communicated through a connecting pipe one, the lower end of the mixing bin (3) and the upper end of the discharging bin (11) are communicated through a connecting pipe two, the middle parts of the connecting pipe one and the connecting pipe two are provided with electromagnetic valves (14), the rear end of the hydrothermal reaction bin (2) is provided with an air outlet pipe, the middle part of the air outlet pipe is provided with an electric exhaust valve (17), the right end of the hydrothermal reaction bin (2) is provided with three feeding pipes (15), the front end of the hydrothermal reaction bin (2) is provided with a water inlet pipe (16), and the two electromagnetic valves (14) and the electric exhaust valve (17) are electrically connected with the output end of the PLC controller (20).
7. The nanoparticle assembly reaction system of claim 2, wherein: The inside of the discharging bin (11) is rotatably connected with a rotating rod (12), the outer surface of the rotating rod (12) is provided with spiral leaves, the front end of the discharging bin (11) is provided with a motor three (13), the rear end of the output shaft of the motor three (13) is fixedly connected with the front end of the rotating rod (12), the rear end of the discharging bin (11) is provided with a discharging opening, and the input end of the motor three (13) is electrically connected with the output end of the PLC controller (20).