Cyanomethylene tri-n-butylphosphine synthesis reactor

Abstract

The utility model relates to the technical field of production of cyano methylene tri-n-butyl phosphine, and discloses a cyano methylene tri-n-butyl phosphine synthesis reactor which comprises a tank body, a mounting hole is formed in the upper surface of the tank body, and stirring mechanisms are fixedly communicated with the inner wall of the mounting hole and the upper surface of the tank body. The bottom of the tank body is fixedly communicated with a liquid outlet pipe, and the upper surface of the tank body is fixedly communicated with a liquid inlet pipe. Through cooperation of the transverse pipe and the liquid pumping mechanism, liquid in the tank body can be automatically pumped into the transverse pipe, meanwhile, through a second electric push rod on the measuring mechanism, the measuring end of a thermometer can be automatically inserted into the transverse pipe, and the temperature of the liquid in the transverse pipe is measured through the thermometer; and through cooperation of a transverse pipe, a liquid pumping mechanism, a vertical pipe and a measuring mechanism, the synthesis reactor can automatically measure the temperature, so that the synthesis reactor is more convenient to use.

Description

Technical Field

[0001] This utility model relates to the field of cyanomethylene tri-n-butylphosphine production technology, and in particular to a cyanomethylene tri-n-butylphosphine synthesis reactor. Background Technology

[0002] Cyanomethylene tri-n-butylphosphine is an important organophosphine compound. Quaternary phosphine salts synthesized from tributylphosphine are high-performance surfactants with a wide pH adaptability and low foaming properties. They are also highly efficient, broad-spectrum, and low-toxicity bactericides. The complexes formed by cyanomethylene tri-n-butylphosphine with many transition metal elements are crucial catalysts. In the polyurethane industry, it is an excellent catalyst for the trimerization of isocyanates. Furthermore, cyanomethylene tri-n-butylphosphine can also be used as an extractant, fuel additive, and organic synthesis reagent.

[0003] Currently, the production of cyanomethylene tri-n-butylphosphine mostly involves mixing and reacting various raw materials in a synthesis reactor. Existing synthesis reactors mainly consist of a tank, inlet pipe, outlet pipe, sampling pipe, valve, and stirring mechanism. For example, Chinese Patent Publication No. CN220345842U discloses a chemical synthesis reactor with a heat preservation function. In this reactor, workers measure the temperature of the liquid by first opening the valve on the sampling pipe, then taking a sample through the sampling pipe, and finally measuring the temperature of the sample liquid with a thermometer. However, because manual sampling and temperature measurement are required, the process is quite cumbersome. Utility Model Content

[0004] The purpose of this invention is to address the shortcomings of existing technologies, such as the fact that existing synthesis reactors mainly consist of a tank, an inlet pipe, an outlet pipe, a sampling pipe, a valve, and a stirring mechanism. In these reactors, workers first open the valve on the sampling pipe to measure the temperature of the liquid inside the reactor, then take a sample through the sampling pipe and measure the temperature of the sample liquid using a thermometer. However, the manual sampling and temperature measurement by workers is cumbersome. Therefore, this invention proposes a cyanomethylene tri-n-butylphosphine synthesis reactor.

[0005] To achieve the above objectives, the present invention adopts the following technical solution:

[0006] A cyanomethylene tri-n-butylphosphine synthesis reactor includes a tank. An installation hole is provided on the upper surface of the tank. A stirring mechanism is fixedly connected to the inner wall of the installation hole and the upper surface of the tank. An outlet pipe is fixedly connected to the bottom of the tank. An inlet pipe is fixedly connected to the upper surface of the tank. Valves are fixedly connected to the top end of the inlet pipe and the bottom end of the outlet pipe. A horizontal pipe is fixedly connected to the right side of the tank. A pumping mechanism is fitted to the inner wall of the horizontal pipe. The left side of the pumping mechanism is fixedly connected to the right side of the tank. A vertical pipe is fixedly connected to the upper surface of the horizontal pipe. A measuring mechanism is fitted to the inner wall of the vertical pipe. The bottom of the measuring mechanism is fixedly connected to the upper surface of the pumping mechanism.

[0007] Preferably, the stirring mechanism includes a motor bracket, the bottom of which is fixedly connected to the upper surface of the tank, a drive motor is fixedly connected to the inner wall of the motor bracket, a rotating shaft is fixedly connected to the output end of the drive motor, bearings are fixedly connected to the surface of the rotating shaft and the inner wall of the mounting hole, and stirring blades are fixedly connected to the surface of the rotating shaft.

[0008] Preferably, the liquid extraction mechanism includes a first U-shaped plate, the left side of which is fixedly connected to the right side of the tank, a first electric push rod is fixedly connected to the right side of the inner wall of the first U-shaped plate, a first mounting plate is fixedly connected to the left end of the first electric push rod, a first piston block is fixedly connected to the left side of the first mounting plate, the surface of the first piston block is in contact with the inner wall of the liquid inlet pipe, and the upper surface of the first U-shaped plate is fixedly connected to the bottom of the measuring mechanism.

[0009] Preferably, the measuring mechanism includes a second U-shaped plate, a second electric push rod is fixedly connected to the top of the inner wall of the second U-shaped plate, a second mounting plate is fixedly connected to the bottom of the second electric push rod, a thermometer is fixedly connected to the bottom of the second mounting plate, a second piston block is adhered to the surface of the thermometer, and the surface of the second piston block is in contact with the surface of the vertical tube.

[0010] Preferably, a U-shaped column is fixedly connected to the front of the second U-shaped plate, a magnetic plate is provided on the inner wall of the U-shaped column, and a cleaning brush is fixedly connected to the back of the magnetic plate. Both the left and right sides of the cleaning brush are in contact with the inner wall of the second U-shaped plate.

[0011] Preferably, the magnetic force exerted by the magnetic plate on the U-shaped column is greater than the combined weight of the magnetic plate and the cleaning brush.

[0012] Compared with the prior art, the beneficial effects of this utility model are:

[0013] (1) This utility model can automatically draw the liquid in the tank into the horizontal tube by means of the cooperation of the horizontal tube and the liquid pumping mechanism. At the same time, the measuring end of the thermometer can be automatically inserted into the horizontal tube by means of the second electric push rod on the measuring mechanism, and the temperature of the liquid in the horizontal tube can be measured by means of the thermometer. Thus, by means of the cooperation of the horizontal tube, the liquid pumping mechanism, the vertical tube and the measuring mechanism, the synthesis reactor can automatically measure the temperature, thus making the synthesis reactor more convenient to use.

[0014] (2) This utility model can automatically reduce the cleaning brush fixed on the second U-shaped plate by the magnetic plate attracting the U-shaped column. Furthermore, when the second electric push rod controls the thermometer to move up and down, the cleaning brush can clean the reading surface of the thermometer, thereby preventing the thermometer reading from being difficult to observe due to dust sticking to the reading surface of the thermometer. Attached Figure Description

[0015] Figure 1 This is a schematic diagram of the structure of this utility model;

[0016] Figure 2 This is a top view of the tank body in this utility model;

[0017] Figure 3 This is a front view of the stirring mechanism in this utility model;

[0018] Figure 4 This is a top view of the liquid extraction mechanism in this utility model;

[0019] Figure 5 This is a front view of the measuring mechanism in this utility model;

[0020] Figure 6 for Figure 5 Sectional view at point AA;

[0021] Figure 7 This is a right view of the U-shaped column in this utility model.

[0022] In the diagram: 1. Tank body; 2. Mounting hole; 3. Stirring mechanism; 31. Motor bracket; 32. Drive motor; 33. Rotating shaft; 34. Bearing; 35. Stirring blades; 4. Discharge pipe; 5. Inlet pipe; 6. Valve; 7. Horizontal pipe; 8. Pumping mechanism; 81. First U-shaped plate; 82. First electric push rod; 83. First mounting plate; 84. First piston block; 9. Vertical pipe; 10. Measuring mechanism; 101. Second U-shaped plate; 102. Second electric push rod; 103. Second mounting plate; 104. Thermometer; 105. Second piston block; 11. U-shaped column; 12. Magnetic plate; 13. Cleaning brush. Detailed Implementation

[0023] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments.

[0024] In the description of this utility model, it should be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model.

[0025] Example 1:

[0026] Reference Figure 1-6 A cyanomethylene tri-n-butylphosphine synthesis reactor includes a tank 1. An installation hole 2 is provided on the upper surface of the tank 1. A stirring mechanism 3 is fixedly connected to the inner wall of the installation hole 2 and the upper surface of the tank 1. An outlet pipe 4 is fixedly connected to the bottom of the tank 1. An inlet pipe 5 is fixedly connected to the upper surface of the tank 1. A valve 6 is fixedly connected to the top of the inlet pipe 5 and the bottom of the outlet pipe 4. The valve 6 controls the opening and closing of the inlet pipe 5 and the outlet pipe 4. A horizontal pipe 7 is fixedly connected to the right side of the tank 1. A pumping mechanism 8 is fitted into the inner wall of the horizontal pipe 7. The left side of the pumping mechanism 8 is fixedly connected to the right side of the tank 1. A vertical pipe 9 is fixedly connected to the upper surface of the horizontal pipe 7. A measuring mechanism 10 is fitted into the inner wall of the vertical pipe 9. The bottom of the measuring mechanism 10 is fixedly connected to the upper surface of the pumping mechanism 8.

[0027] The stirring mechanism 3 includes a motor bracket 31. The bottom of the motor bracket 31 is fixedly connected to the upper surface of the tank 1. A drive motor 32 is fixedly connected to the inner wall of the motor bracket 31. A rotating shaft 33 is fixedly connected to the output end of the drive motor 32. Bearings 34 are fixedly connected to the surface of the rotating shaft 33 and the inner wall of the mounting hole 2. A stirring blade 35 is fixedly connected to the surface of the rotating shaft 33. The stirring blade 35 is driven to rotate by the drive motor 32, and the raw materials in the tank 1 can be stirred by the rotating stirring blade 35.

[0028] The liquid extraction mechanism 8 includes a first U-shaped plate 81. The left side of the first U-shaped plate 81 is fixedly connected to the right side of the tank 1. A first electric push rod 82 is fixedly connected to the right side of the inner wall of the first U-shaped plate 81. A first mounting plate 83 is fixedly connected to the left end of the first electric push rod 82. A first piston block 84 is fixedly connected to the left side of the first mounting plate 83. The surface of the first piston block 84 is in contact with the inner wall of the liquid inlet pipe 5. The upper surface of the first U-shaped plate 81 is fixedly connected to the bottom of the measuring mechanism 10. The first piston block 84 is controlled to move left and right by the first electric push rod 82. When the first piston block 84 moves to the right, the liquid in the tank 1 is drawn into the horizontal pipe 7 by the first piston block 84. When the first piston block 84 moves to the left, the liquid in the horizontal pipe 7 is pushed into the tank 1 by the first piston block 84.

[0029] The measuring mechanism 10 includes a second U-shaped plate 101. A second electric push rod 102 is fixedly connected to the top of the inner wall of the second U-shaped plate 101. A second mounting plate 103 is fixedly connected to the bottom of the second electric push rod 102. A thermometer 104 is fixedly connected to the bottom of the second mounting plate 103. A second piston block 105 is adhered to the surface of the thermometer 104. The surface of the second piston block 105 is in contact with the surface of the vertical tube 9. The thermometer 104 is moved up and down by the second electric push rod 102. The bottom of the thermometer 104 is the measuring end. When the bottom of the thermometer 104 is inserted into the horizontal tube 7, the temperature of the liquid in the horizontal tube 7 can be measured by the thermometer 104. When the thermometer 104 returns to its position, the second piston block 105 can prevent any liquid from remaining in the vertical tube 9.

[0030] Example 2:

[0031] Reference Figure 5-7 A U-shaped column 11 is fixedly connected to the front of the second U-shaped plate 101. A magnetic plate 12 is provided on the inner wall of the U-shaped column 11. A cleaning brush 13 is fixedly connected to the back of the magnetic plate 12. Both sides of the cleaning brush 13 are in contact with the inner wall of the second U-shaped plate 101. The magnetic force of the magnetic plate 12 on the U-shaped column 11 is greater than the sum of the weight of the magnetic plate 12 and the cleaning brush 13. Through the magnetic force of the magnetic plate 12 on the U-shaped column 11, the cleaning brush 13 can be automatically lowered and fixed on the second U-shaped plate 101. Furthermore, when the second electric push rod 102 controls the thermometer 104 to move up and down, the cleaning brush 13 can clean the reading surface of the thermometer 104, thereby preventing the thermometer 104 reading from being difficult to observe due to dust sticking to the reading surface of the thermometer 104.

[0032] In this invention, when using the synthesis reactor, the user first opens the valve 6 on the inlet pipe 5 and feeds the raw materials into the tank 1 through the inlet pipe 5. After the raw materials are fed in, the valve 6 is closed, and the drive motor 32 is turned on to rotate the stirring blades 35. At this time, the stirring blades 35 agitate the raw materials in the tank 1, causing the synthesis reaction of multiple raw materials in the tank 1. When it is necessary to measure the temperature of the liquid in the tank 1, the first piston block 84 is moved to the right by the first electric push rod 82, and the liquid in the tank 1 is drawn into the horizontal pipe 7 by the first piston block 84. After the piston block 84 is offset from the vertical tube 9, the bottom end of the thermometer 104 is inserted into the horizontal tube 7 by the second electric push rod 102. At this time, the temperature of the liquid in the horizontal tube 7 is measured by the thermometer 104. After the temperature measurement is completed, the thermometer 104 is returned to the initial position by the second electric push rod 102. Then, the first piston block 84 is returned to the initial position by the first electric push rod 82, and the liquid in the horizontal tube 7 is pushed into the tank 1 by the first piston block 84. After the raw material synthesis reaction is completed, the material after the synthesis reaction is discharged through the liquid outlet pipe 4 by opening the valve 6 on the liquid outlet pipe 4.

[0033] The above description is only a preferred embodiment of the present utility model, but the protection scope of the present utility model is not limited thereto. Any equivalent substitutions or changes made by those skilled in the art within the technical scope disclosed in the present utility model, based on the technical solution and the inventive concept of the present utility model, should be included within the protection scope of the present utility model.

[0034] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.

Claims

1. A cyanomethylene tri-n-butylphosphine synthesis reactor, comprising a tank (1), characterized in that, The upper surface of the tank (1) is provided with an installation hole (2). The inner wall of the installation hole (2) and the upper surface of the tank (1) are both fixedly connected to a stirring mechanism (3). The bottom of the tank (1) is fixedly connected to a liquid outlet pipe (4). The upper surface of the tank (1) is fixedly connected to a liquid inlet pipe (5). The top end of the liquid inlet pipe (5) and the bottom end of the liquid outlet pipe (4) are both fixedly connected to a valve (6). The right side of the tank (1) is fixedly connected to a horizontal pipe (7). The inner wall of the horizontal pipe (7) is fitted with a liquid extraction mechanism (8). The left side of the liquid extraction mechanism (8) is fixedly connected to the right side of the tank (1). The upper surface of the horizontal pipe (7) is fixedly connected to a vertical pipe (9). The inner wall of the vertical pipe (9) is fitted with a measuring mechanism (10). The bottom of the measuring mechanism (10) is fixedly connected to the upper surface of the liquid extraction mechanism (8).

2. The cyanomethylene tri-n-butylphosphine synthesis reactor according to claim 1, characterized in that, The stirring mechanism (3) includes a motor bracket (31), the bottom of which is fixedly connected to the upper surface of the tank (1), a drive motor (32) is fixedly connected to the inner wall of the motor bracket (31), a rotating shaft (33) is fixedly connected to the output end of the drive motor (32), a bearing (34) is fixedly connected to the surface of the rotating shaft (33) and the inner wall of the mounting hole (2), and a stirring blade (35) is fixedly connected to the surface of the rotating shaft (33).

3. The cyanomethylene tri-n-butylphosphine synthesis reactor according to claim 1, characterized in that, The liquid extraction mechanism (8) includes a first U-shaped plate (81), the left side of which is fixedly connected to the right side of the tank (1), a first electric push rod (82) is fixedly connected to the right side of the inner wall of the first U-shaped plate (81), a first mounting plate (83) is fixedly connected to the left end of the first electric push rod (82), a first piston block (84) is fixedly connected to the left side of the first mounting plate (83), the surface of the first piston block (84) is in contact with the inner wall of the liquid inlet pipe (5), and the upper surface of the first U-shaped plate (81) is fixedly connected to the bottom of the measuring mechanism (10).

4. The cyanomethylene tri-n-butylphosphine synthesis reactor according to claim 3, characterized in that, The measuring mechanism (10) includes a second U-shaped plate (101), a second electric push rod (102) is fixedly connected to the top of the inner wall of the second U-shaped plate (101), a second mounting plate (103) is fixedly connected to the bottom end of the second electric push rod (102), a thermometer (104) is fixedly connected to the bottom of the second mounting plate (103), a second piston block (105) is bonded to the surface of the thermometer (104), and the surface of the second piston block (105) is in contact with the surface of the vertical tube (9).

5. The cyanomethylene tri-n-butylphosphine synthesis reactor according to claim 4, characterized in that, A U-shaped column (11) is fixedly connected to the front of the second U-shaped plate (101). A magnetic plate (12) is provided on the inner wall of the U-shaped column (11). A cleaning brush (13) is fixedly connected to the back of the magnetic plate (12). The left and right sides of the cleaning brush (13) are in contact with the inner wall of the second U-shaped plate (101).

6. The cyanomethylene tri-n-butylphosphine synthesis reactor according to claim 5, characterized in that, The magnetic plate (12) exerts a stronger attraction on the U-shaped column (11) than the sum of the weights of the magnetic plate (12) and the cleaning brush (13).

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