Condenser for butyramide preparation

Abstract

The utility model discloses a condenser for preparing butyramide, and relates to the technical field of chemical medicine production equipment. Comprising an outer tank body, a cooling cylinder is longitudinally suspended in an inner cavity of the outer tank body, an air inlet pipe is arranged at the bottom of the outer tank body and communicated with the bottom of the cooling cylinder, an air outlet pipe is arranged on the upper portion of the outer tank body and communicated with the upper portion of the cooling cylinder, and the air outlet pipe is communicated with the side wall of the air inlet pipe. A plurality of evenly-distributed heat dissipation blades are fixedly arranged on the outer wall of the cooling cylinder in the longitudinal direction of the axis in a penetrating mode. Cooling liquid for cooling the heat dissipation blades is cooled by the cooling box B and then enters the cooling box A through the water purifying box and the cooling agent barrel again, then cyclic utilization of the cooling liquid is achieved, butyramide steam enters the cooling barrel through the air inlet pipe, heat of the butyramide steam is conducted into the cooling liquid in the inner cavity of the outer tank body through the heat dissipation blades, and the butyramide steam is cooled. And the cooled and liquefied butyramide is collected at the bottom of the cooling cylinder, so that the cooling process is simplified, and the cooling efficiency of the butyramide is improved.

Description

Technical Field

[0001] This utility model relates to the field of chemical and pharmaceutical production equipment technology, specifically a condenser for butyramide preparation. Background Technology

[0002] Butyramide is a chemical substance with the molecular formula C4H9NO. It is a colorless, leaf-shaped crystal with a melting point of 114.8℃ and a boiling point of 216℃. It is soluble in water. A condenser is a component of a refrigeration system and belongs to the category of heat exchangers. It can convert gas or vapor into liquid and transfer heat from the tubes to the air near the tubes in a rapid manner.

[0003] Patent document CN209322757U discloses a condenser for butyramide preparation, comprising a shell, a refrigerant tank, a water tank, a condensation chamber, a sodium ion exchange resin tank, an oxygen scavenger layer, a cold water pump, a spray chamber, an evaporation chamber, and a filter screen. The right inner wall of the shell is fixedly connected to the right outer wall of the condensation chamber, and the upper part of the condensation chamber on the right inner wall of the shell is fixedly connected to the right outer wall of the water tank. The left side of the water tank on the top of the base on the top outer wall of the condensation chamber is fixedly connected to the bottom of the refrigerant tank. This condenser for butyramide preparation employs a sodium ion exchange resin tank design, where sodium ions exchange calcium and magnesium ions in the cooling water to prevent scale formation when the cooling water flows over metal surfaces. The oxygen scavenger layer design removes dissolved oxygen in the cooling water, preventing metal corrosion. This equipment effectively prevents rust and scale formation, maintaining good heat exchange performance of the condenser.

[0004] Although the aforementioned patent achieves the function of preventing rust and scale in the equipment, thereby maintaining a good heat exchange effect of the condenser, it uses the method of dissolving cooling water with butyramide vapor and using an electric heating wire to heat and evaporate the cooling water into which the amide is dissolved to precipitate butyramide crystals. The efficiency of cooling and separating butyramide is low. In addition, the cooling water cannot be recycled after heating and evaporation. It is necessary to re-produce cooling water to remove oxygen and calcium and magnesium ions, which increases the production cost.

[0005] Therefore, we have made improvements to this and proposed a condenser for the preparation of butyramide. Utility Model Content

[0006] To address the shortcomings of existing technologies, this invention provides a condenser for butyramide preparation, which solves the problems of low efficiency in cooling and separating butyramide and the inability to recycle cooling water in existing technologies.

[0007] To achieve the above objectives, this utility model is implemented through the following technical solution: a condenser for preparing butyramide, comprising an outer tank, a cooling cylinder suspended longitudinally in the inner cavity of the outer tank, an air inlet pipe at the bottom of the outer tank, the air inlet pipe being connected to the bottom of the cooling cylinder, an air outlet pipe at the top of the outer tank, the air outlet pipe being connected to the top of the cooling cylinder, and the air outlet pipe being connected to the side wall of the air inlet pipe;

[0008] The outer wall of the cooling cylinder is provided with a plurality of evenly distributed heat dissipation blades that are fixedly installed longitudinally along its axis.

[0009] The inner cavity of the outer tank is filled with flowing coolant.

[0010] As a preferred embodiment, the side wall of the air inlet pipe is connected to a material conveying pipe, the material conveying pipe is equipped with a solenoid valve A, the air outlet pipe is equipped with a solenoid valve B, and the air outlet pipe is equipped with a pressure valve, which is located below the solenoid valve B.

[0011] As a preferred embodiment, a clean water tank is fixedly installed on the upper outer wall of the outer tank. A coolant cylinder is connected to the bottom of the clean water tank. A cooling tank A is connected to the bottom of the coolant cylinder. A water pump A is connected to one side of the bottom of the cooling tank A. A pipe of the water pump A is connected to an annular connecting disc. The annular connecting disc is located in the upper part of the inner cavity of the outer tank. The outer wall of the inner ring of the annular connecting disc is fixedly fitted with the outer wall of the air outlet pipe. A plurality of evenly distributed nozzles are provided on the lower surface of the annular connecting disc. The heads of the nozzles are oriented towards the heat dissipation blades.

[0012] As a preferred embodiment, a cooling box B is fixedly installed on the upper outer wall of the outer tank, and a water pump B is connected to the bottom of the cooling box B. The water pump B is connected to a pipe at the bottom of the side wall of the outer tank.

[0013] As a preferred embodiment, the bottom of the side wall of the outer tank is provided with a discharge pipe, which is connected to the bottom of the side wall of the cooling cylinder. The discharge pipe located outside the outer tank is equipped with a valve A.

[0014] As a preferred embodiment, the upper part of the side wall of the cooling tank B is connected to the upper part of the side wall of the clean water tank.

[0015] As a preferred embodiment, the upper part of the water purification tank is connected to a filling pipe, a water filling pipe, and a chemical filling pipe.

[0016] As a preferred embodiment, the lower part of the side wall of the water tank is provided with a material exchange pipe, and the material exchange pipe is provided with a sealing cover.

[0017] As a preferred embodiment, a mesh plate is provided at the connection between the coolant cylinder and the clean water tank, and a coolant pipe is connected to the upper side wall of the coolant cylinder, with valve B provided on the coolant pipe.

[0018] As a preferred embodiment, the upper part of the cooling box B is connected to an exhaust valve.

[0019] This utility model has the following beneficial effects:

[0020] The coolant for cooling the heat dissipation blades is drawn from the bottom of the outer tank into the cooling tank. After being cooled by the cooling tank B, it passes through the clean water tank and the coolant cylinder again before entering the cooling tank A, thus realizing the recycling of the coolant.

[0021] Butyramide vapor enters the cooling cylinder through the inlet pipe. The heat dissipation blades transfer the heat of the butyramide vapor to the coolant in the inner cavity of the outer tank. The cooled and liquefied butyramide collects at the bottom of the cooling cylinder, which simplifies the cooling process and thus improves the cooling efficiency of butyramide.

[0022] Of course, any product implementing this utility model does not necessarily need to achieve all of the advantages described above at the same time. Attached Figure Description

[0023] Figure 1 This is a schematic diagram of the structure of a condenser for preparing butyramide according to the present invention;

[0024] Figure 2 This is a schematic cross-sectional view of a condenser for preparing butyramide according to the present invention.

[0025] In the diagram, 1. Outer tank; 2. Cooling cylinder; 3. Inlet pipe; 4. Outlet pipe; 5. Heat dissipation fins; 6. Feeding pipe; 7. Solenoid valve A; 8. Solenoid valve B; 9. Pressure valve; 10. Clean water tank; 11. Coolant cylinder; 12. Cooling tank A; 13. Water pump A; 14. Annular connecting disc; 15. Nozzle; 16. Cooling tank B; 17. Water pump B; 18. Discharge pipe; 19. Valve A; 20. Filling pipe; 21. Water filling pipe; 22. Chemical pipe; 23. Material changing pipe; 24. Sealing cap; 25. Coolant pipe; 26. Valve B; 27. Exhaust valve. Detailed Implementation

[0026] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0027] In the description of this utility model, it should be understood that the terms "opening", "upper", "lower", "thickness", "top", "middle", "length", "inner", "around" and other terms indicating orientation or positional relationship are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the components or elements referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model.

[0028] Please refer to the examples. Figures 1 to 2 This utility model provides a technical solution: a condenser for preparing butyramide, including an outer tank 1, a cooling cylinder 2 suspended longitudinally in the inner cavity of the outer tank 1, an air inlet pipe 3 at the bottom of the outer tank 1, the air inlet pipe 3 being connected to the bottom of the cooling cylinder 2, an air outlet pipe 4 at the top of the outer tank 1, the air outlet pipe 4 being connected to the top of the cooling cylinder 2, and the air outlet pipe 4 being connected to the side wall of the air inlet pipe 3.

[0029] The outer wall of the cooling cylinder 2 is provided with a plurality of evenly distributed heat dissipation blades 5 that are fixedly installed longitudinally along its axis;

[0030] The inner cavity of the outer tank 1 is filled with flowing coolant.

[0031] The side wall of the air inlet pipe 3 is connected to a material conveying pipe 6, the material conveying pipe 6 is equipped with a solenoid valve A7, the air outlet pipe 4 is equipped with a solenoid valve B8, and the air outlet pipe 4 is equipped with a pressure valve 9, which is located below the solenoid valve B8.

[0032] A clean water tank 10 is fixedly installed on the upper outer wall of the outer tank 1. A coolant cylinder 11 is connected to the bottom of the clean water tank 10. The water tank 10 and the coolant cylinder 11 are sealed by a water inlet switch. A cooling box A12 is connected to the bottom of the coolant cylinder 11. A water pump A13 is connected to the bottom of one side of the cooling box A12. A pipe of the water pump A13 is connected to an annular connecting plate 14. The annular connecting plate 14 is located in the upper part of the inner cavity of the outer tank 1. The outer wall of the inner ring of the annular connecting plate 14 is fixedly fitted with the outer wall of the air outlet pipe 4. A plurality of evenly distributed nozzles 15 are provided on the lower surface of the annular connecting plate 14. The heads of the nozzles 15 are facing the heat dissipation blades 5.

[0033] A cooling box B16 is fixedly installed on the upper outer wall of the outer tank 1. A water pump B17 is connected to the bottom of the cooling box B16. The water pump B17 is connected to the bottom pipe of the side wall of the outer tank 1.

[0034] The outer tank 1 is provided with a discharge pipe 18 at the bottom of its side wall. The discharge pipe 18 is connected to the bottom of the side wall of the cooling cylinder 2. The discharge pipe 18 located outside the outer tank 1 is provided with a valve A19.

[0035] The upper part of the side wall of the cooling box B16 is connected to the upper part of the side wall of the clean water box 10.

[0036] The upper part of the water purification tank 10 is connected to a filling pipe 20, a water filling pipe 21, and a medicine pipe 22.

[0037] The lower part of the side wall of the water tank 10 is provided with a material exchange pipe 23, and the material exchange pipe 23 is provided with a sealing cover 24.

[0038] A mesh plate is provided at the position where the coolant cylinder 11 is connected to the clean water tank 10, and a coolant pipe 25 is connected to the upper side wall of the coolant cylinder 11, and a valve B26 is provided on the coolant pipe 25.

[0039] The upper part of the cooling box B16 is connected to an exhaust valve 27.

[0040] The working principle of this utility model:

[0041] Sodium ion exchange resin is filled into the water tank 10 through the filling pipe 20. An oxygen remover is added to the water tank 10 through the reagent pipe 22. Clean water is injected into the water tank 10 through the water inlet pipe. After the sodium ion exchange resin and the oxygen remover have treated the clean water, the water inlet switch is opened, and valve B26 is opened at the same time. Coolant is introduced into the coolant pipe 25, and water pump A13 is turned on. The coolant, which consists of coolant and treated clean water, enters the cooling tank A12 and fills the inner cavity of the outer tank 1. The above steps are repeated several times until the coolant completely fills the inner cavity of the outer tank 1. Then water pump B17 is turned on to draw the coolant from the bottom of the outer tank 1 into the cooling tank B16. After being cooled by the cooling tank B16, the coolant passes through the water tank 10 and the coolant cylinder 11 again and enters the cooling tank A12, thereby realizing the recycling of the coolant.

[0042] At the same time, butyramide vapor is introduced into the feed pipe 6. The butyramide vapor enters the cooling cylinder 2 through the air inlet pipe 3. The heat dissipation blades 5 transfer the heat of the butyramide vapor to the coolant in the inner cavity of the outer tank 1. The cooled and liquefied butyramide is collected at the bottom of the cooling cylinder 2, which simplifies the cooling process and improves the cooling efficiency of butyramide.

[0043] The remaining gas is recirculated into the cooling cylinder 2 through the air outlet pipe 4 and the air inlet pipe 3. The air pressure valve 9 detects the air pressure in the cooling cylinder 2. When the air pressure in the cooling cylinder 2 reaches the preset air pressure, the solenoid valves A7 and B8 are closed. After standing for a period of time until the air pressure in the cooling cylinder 2 no longer changes, the air pressure valve 9 discharges the air pressure in the cooling cylinder 2, and the valve A19 is opened. The butyramide liquid in the cooling cylinder 2 is discharged through the discharge pipe 18.

[0044] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.

[0045] The preferred embodiments of this utility model disclosed above are merely illustrative of the present utility model. These preferred embodiments do not exhaustively describe all details, nor do they limit the utility model to the specific implementations described. Clearly, many modifications and variations can be made based on the content of this specification. This specification selects and specifically describes these embodiments to better explain the principles and practical applications of this utility model, thereby enabling those skilled in the art to better understand and utilize it. This utility model is limited only by the claims and their full scope and equivalents.

Claims

1. A condenser for the preparation of butyramide, characterized in that: The outer tank (1) is provided with a cooling cylinder (2) suspended longitudinally in the inner cavity of the outer tank (1). An air inlet pipe (3) is provided at the bottom of the outer tank (1), and the air inlet pipe (3) is connected to the bottom of the cooling cylinder (2). An air outlet pipe (4) is provided at the top of the outer tank (1), and the air outlet pipe (4) is connected to the top of the cooling cylinder (2). The air outlet pipe (4) is connected to the side wall of the air inlet pipe (3). The outer wall of the cooling cylinder (2) is provided with a plurality of uniformly distributed heat dissipation blades (5) that are fixedly installed longitudinally along its axis. The inner cavity of the outer tank (1) is filled with flowing coolant.

2. The condenser for butyramide preparation according to claim 1, characterized in that: The side wall of the air inlet pipe (3) is connected to a material conveying pipe (6), the material conveying pipe (6) is equipped with a solenoid valve A (7), the air outlet pipe (4) is equipped with a solenoid valve B (8), the air outlet pipe (4) is equipped with a pressure valve (9), and the pressure valve (9) is located below the solenoid valve B (8).

3. A condenser for butyramide preparation according to claim 1, characterized in that: The upper outer wall of the outer tank (1) is fixedly provided with a clean water tank (10), the bottom of the clean water tank (10) is connected to a coolant cylinder (11), the bottom of the coolant cylinder (11) is connected to a cooling box A (12), the bottom of one side of the cooling box A (12) is connected to a water pump A (13), the water pump A (13) is connected to an annular connecting plate (14) through a pipe, the annular connecting plate (14) is located in the upper part of the inner cavity of the outer tank (1), the inner ring outer wall of the annular connecting plate (14) is fixedly fitted with the outer wall of the air outlet pipe (4), and the lower surface of the annular connecting plate (14) is provided with multiple evenly distributed nozzles (15), the head of the nozzles (15) is facing the heat dissipation blades (5).

4. A condenser for butyramide preparation according to claim 3, characterized in that: The upper outer wall of the outer tank (1) is fixedly provided with a cooling box B (16), and the bottom of the cooling box B (16) is connected to a water pump B (17). The water pump B (17) is connected to the bottom pipe of the side wall of the outer tank (1).

5. A condenser for preparing butyramide according to claim 1, characterized in that: The outer tank (1) has a discharge pipe (18) at the bottom of its side wall. The discharge pipe (18) is connected to the bottom of the side wall of the cooling cylinder (2). The discharge pipe (18) located outside the outer tank (1) is equipped with a valve A (19).

6. A condenser for butyramide preparation according to claim 4, characterized in that: The upper part of the side wall of the cooling box B (16) is connected to the upper part of the side wall of the water purification box (10).

7. A condenser for butyramide preparation according to claim 3, characterized in that: The upper part of the water purification tank (10) is connected to a filling pipe (20), a water filling pipe (21), and a medicine pipe (22).

8. A condenser for butyramide preparation according to claim 3, characterized in that: The lower side wall of the water tank (10) is provided with a material exchange pipe (23), and the material exchange pipe (23) is provided with a sealing cover (24).

9. A condenser for butyramide preparation according to claim 3, characterized in that: A mesh plate is provided at the connection between the coolant cylinder (11) and the clean water tank (10). A coolant pipe (25) is connected to the upper side wall of the coolant cylinder (11), and a valve B (26) is provided on the coolant pipe (25).

10. A condenser for preparing butyramide according to claim 4, characterized in that: The upper part of the cooling box B (16) is connected to an exhaust valve (27).

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