A reaction kettle
By setting up an insulation chamber and a dual electric heating device in the reactor, the problem of poor insulation effect is solved by utilizing the temperature difference between the insulation liquid and the material, thereby improving reaction efficiency and product quality.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- VITAYON FINE CHEM SCI & TECH CO LTD SHENZHEN
- Filing Date
- 2025-05-30
- Publication Date
- 2026-06-23
AI Technical Summary
The existing reactors have poor insulation, making it difficult to maintain the materials within the optimal temperature range, which reduces reaction efficiency and product quality.
A heat-insulating cavity is formed between the inner and outer walls of the reactor, and a dual electric heating device is installed. Heat transfer is achieved through the temperature difference between the heat-insulating liquid and the material, maintaining the material within the temperature range required for the reaction.
It improves the reaction efficiency and product quality of materials, reduces heat loss, enhances the uniformity and stability of the reaction, and extends the service life of the reactor.
Smart Images

Figure CN224388765U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of reaction vessel technology, specifically to a reaction vessel. Background Technology
[0002] A reaction vessel is a container used to realize chemical reactions. It provides specific conditions such as temperature and stirring to allow materials to undergo the desired chemical changes in a controlled environment. Reaction vessels play a crucial role in industrial production and are therefore widely used in many fields such as chemical engineering, pharmaceuticals, and food processing.
[0003] However, current reactors generally suffer from poor heat preservation, making it difficult to maintain the materials within the optimal temperature range during the reaction process. This not only reduces the reaction efficiency of the materials but also leads to a decrease in product quality and yield. Utility Model Content
[0004] This invention provides a reaction vessel that achieves excellent heat preservation. The heat from the insulating liquid can be transferred to the material, thereby compensating for the heat loss caused by heat dissipation and maintaining the material within the temperature range required for the reaction. This improves the reaction efficiency and, consequently, the quality and yield of the product. The specific technical solution of this invention is as follows:
[0005] The present invention provides a reaction vessel, comprising:
[0006] The vessel body has an inner cavity, and a heat-insulating cavity for storing heat-insulating liquid is formed between the inner wall and the outer wall of the vessel body. The heat-insulating cavity surrounds the outer periphery of the inner cavity. An inlet pipe communicating with the heat-insulating cavity is provided on the outer wall of the vessel body. A discharge valve communicating with the inner cavity and a liquid outlet valve communicating with the heat-insulating cavity are provided at the bottom of the vessel body.
[0007] A stirring device is installed on the vessel body for stirring the materials in the inner cavity;
[0008] A first electric heating device is installed in the inner cavity of the vessel body to heat the material in the inner cavity to a first preset temperature;
[0009] A second electric heating device is installed in the insulation cavity to heat the insulation liquid to a second preset temperature;
[0010] The second preset temperature is higher than the first preset temperature.
[0011] In one specific embodiment, the outer side wall and outer bottom wall of the vessel body expand outward in a direction away from the inner cavity to form the heat preservation cavity, which semi-encloses the periphery of the inner cavity.
[0012] In one specific embodiment, the second preset temperature is 5°C to 10°C higher than the first preset temperature.
[0013] In one specific embodiment, an insulation layer is provided on the cavity wall on the side away from the inner cavity of the insulation cavity.
[0014] In one specific embodiment, the reaction vessel further includes:
[0015] A first temperature sensor is disposed in the inner cavity for detecting the temperature of the material;
[0016] A second temperature sensor is installed in the insulation cavity to detect the temperature of the insulation liquid;
[0017] The control panel and power module are provided, wherein the power module is electrically connected to the first electric heating device and the second electric heating device; the control panel is connected to the first temperature sensor, the second temperature sensor and the power module respectively, for disconnecting or connecting the circuit between the power module and the first electric heating device and the second electric heating device.
[0018] In one specific embodiment, both the first electric heating device and the second electric heating device include an electric heating wire or an electric heating tube electrically connected to the power module.
[0019] In one specific embodiment, the top of the vessel body has an openable cover plate, and a sealing ring is provided at the bottom edge of the cover plate.
[0020] In one specific embodiment, the stirring device includes a rotary motor, a stirring shaft, and multiple stirring blades;
[0021] The rotary motor is located at the top of the cover plate, and the stirring shaft is located at the bottom of the cover plate. One end of the stirring shaft passes through the cover plate and is connected to the rotary motor, while the other end of the stirring shaft is connected to a plurality of stirring blades. The plurality of stirring blades are arranged at intervals along the circumference of the stirring shaft.
[0022] In one specific embodiment, a support rod is provided at the bottom of the vessel body, and a support plate is connected to the end of the support rod away from the vessel body. The support plate has screw holes.
[0023] In one specific embodiment, the reactor further includes a stepped frame, which is disposed on the side of the reactor body, and the top of the stepped frame is fixedly connected to the reactor body.
[0024] This utility model has at least the following beneficial effects:
[0025] This invention provides a reaction vessel with a heat-insulating cavity formed between the inner and outer walls of the vessel body, surrounding the cavity. The heat-insulating liquid is introduced and removed via an inlet pipe and an outlet valve, reducing heat loss from the material within the cavity and providing initial heat preservation. A stirring device ensures uniform mixing of the material within the cavity, preventing localized overheating or underheating and helping the material to approach the optimal temperature for the reaction, thus improving reaction uniformity and stability, and consequently increasing reaction efficiency and product quality. A first electric heating device heats the material within the cavity to a first preset temperature, while a second electric heating device heats the heat-insulating liquid to a second preset temperature higher than the first. This dual-heating setup creates a temperature difference between the material and the heat-insulating liquid, allowing heat to transfer from the liquid to the material, compensating for heat loss and maintaining the material within the required reaction temperature range. This improves reaction efficiency and ultimately enhances product quality and yield. Attached Figure Description
[0026] To more clearly illustrate the technical solutions in the embodiments of this application, the accompanying drawings used in the description of the embodiments will be briefly introduced below. Obviously, the accompanying drawings described below are only some embodiments of this application. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort.
[0027] Figure 1 This is a schematic diagram of the overall structure of the reactor provided in this embodiment;
[0028] Figure 2 This is a schematic cross-sectional view (AA) of the overall structure of the reactor provided in this embodiment;
[0029] Figure 3 This is a perspective view of the overall structure of the reactor provided in this embodiment;
[0030] Figure 4 A schematic diagram of the overall structure of the reactor provided for another embodiment.
[0031] Figure label:
[0032] 1-Bottle body; 11-Inner cavity; 12-Insulation cavity; 13-Feed inlet; 2-Discharge valve; 3-Liquid inlet pipe; 31-Function funnel; 4-Liquid outlet valve; 5-Stirring device; 51-Rotary motor; 52-Stirring shaft; 53-Stirring blade; 6-First electric heating device; 7-Second electric heating device; 8-Insulation layer; 9-First temperature sensor; 10-Second temperature sensor; 14-Control panel; 141-Button; 15-Cable; 16-Cover plate; 161-Sealing ring; 17-Support rod; 18-Support plate; 181-Screw hole; 19-Step frame. Detailed Implementation
[0033] Various embodiments of the present invention will be described more fully below. The present invention may have various embodiments, and adjustments and changes may be made therein. However, it should be understood that there is no intention to limit the various embodiments of the present invention to the specific embodiments disclosed herein, but rather the present invention should be understood to cover all adjustments, equivalents, and / or alternatives falling within the spirit and scope of the various embodiments of the present invention.
[0034] In the following, the terms “comprising” or “may include”, which may be used in various embodiments of the present invention, indicate the presence of the disclosed functions, operations, or elements, and do not limit the addition of one or more functions, operations, or elements. Furthermore, as used in various embodiments of the present invention, the terms “comprising,” “having,” and their cognates are intended only to indicate a specific feature, number, step, operation, element, component, or combination of the foregoing, and should not be construed as primarily excluding the presence of one or more other features, numbers, steps, operations, elements, components, or combinations of the foregoing, or the possibility of adding one or more combinations of features, numbers, steps, operations, elements, components, or combinations of the foregoing.
[0035] In various embodiments of this utility model, the expression "or" or "at least one of A and / or B" includes any combination or all combinations of the words listed simultaneously. For example, the expression "A or B" or "at least one of A and / or B" may include A, may include B, or may include both A and B.
[0036] The terms used in the various embodiments of this utility model (such as "first," "second," etc.) may modify various constituent elements in the various embodiments, but do not limit the corresponding constituent elements. For example, the above terms do not limit the order and / or importance of the elements. The above terms are only used for the purpose of distinguishing one element from other elements. For example, a first user device and a second user device refer to different user devices, although both are user devices. For example, without departing from the scope of the various embodiments of this utility model, a first element may be referred to as a second element, and similarly, a second element may be referred to as a first element.
[0037] It should be noted that, in this utility model, unless otherwise explicitly specified and defined, terms such as "installation," "connection," and "fixation" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; and they can refer to the internal connection of two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model according to the specific circumstances.
[0038] Please refer to Figures 1 to 4 An embodiment of this utility model provides a reaction vessel, comprising:
[0039] The vessel body 1 has an inner cavity 11, and a discharge valve 2 connected to the inner cavity 11 is provided at the bottom of the vessel body 1; the inner cavity 11 is a cavity used to load materials and provide a reaction chamber for the materials, and the product obtained after the reaction can be discharged from the discharge valve 2.
[0040] In an optional embodiment, the vessel body 1 is a container with double walls, and an insulating cavity 12 for storing insulating liquid is formed between the inner wall and the outer wall of the vessel body 1. The insulating cavity 12 surrounds the periphery of the inner cavity 11. That is, the inner cavity 11 is surrounded by the inner wall of the vessel body 1, while the insulating cavity 12 is located in the annular region between the inner wall and the outer wall of the vessel body 1.
[0041] The outer wall of the vessel body 1 is provided with an inlet pipe 3 that communicates with the heat preservation cavity 12, and the bottom of the vessel body 1 is provided with an outlet valve 4 that communicates with the heat preservation cavity 12.
[0042] A stirring device 5 is provided on the vessel body 1. The stirring device 5 is used to stir the material in the inner cavity 11 so that the material can be fully contacted and mixed evenly, thereby improving the reaction efficiency of the material.
[0043] The first electric heating device 6 is installed in the inner cavity 11 of the vessel body 1, and is used to heat the material in the inner cavity 11 to a first preset temperature, so that the material is maintained within the temperature range required for the reaction. The first preset temperature is adaptively set according to the type of material, and this embodiment does not specifically limit it.
[0044] The second electric heating device 7 is installed in the insulation cavity 12 and is used to heat the insulation liquid to the second preset temperature.
[0045] The second preset temperature is higher than the first preset temperature.
[0046] In this embodiment, by forming a heat-insulating cavity 12 between the inner and outer walls of the vessel body 1 and surrounding the periphery of the inner cavity 11, and by using the inlet pipe 3 and outlet valve 4 to allow the heat-insulating liquid to enter and exit, the heat loss of the material in the inner cavity 11 can be reduced, thus achieving a preliminary heat-insulating effect. The stirring device 5 can uniformly mix the material in the inner cavity 11, avoiding excessively high or low local temperatures, and helping the material to approach the optimal temperature required for the reaction as a whole, improving the uniformity and stability of the reaction, thereby improving the reaction efficiency and product quality to a certain extent. The first electric heating device 6 heats the material in the inner cavity 11 to a first preset temperature, and the second electric heating device 7 heats the heat-insulating liquid to a second preset temperature higher than the first preset temperature. The dual electric heating devices can create a temperature difference between the material and the heat-insulating liquid, allowing heat to be transferred from the heat-insulating liquid to the material, compensating for the heat loss of the material due to heat dissipation, maintaining the material within the temperature range required for the reaction, improving the reaction efficiency of the material, and thus improving the quality and yield of the product.
[0047] In an optional embodiment, the temperature difference between the material and the insulating liquid is set in the range of 5°C to 10°C, that is, the second preset temperature is 5°C to 10°C higher than the first preset temperature. This temperature difference range can effectively reduce heat loss, ensure stable temperature inside the cavity, and achieve good insulation effect; it also avoids excessive thermal stress on the vessel wall due to sudden temperature changes, thus effectively extending the service life of the vessel 1. In addition, a smaller temperature difference can prevent heat transfer from being too rapid, avoid local overheating of the material in the inner cavity 11, ensure the stability and controllability of the reaction process, and improve product quality.
[0048] In actual use, the insulating liquid is introduced into the insulating cavity 12 through the inlet pipe 3. Under the heating action of the second electric heating device 7, the insulating liquid continuously heats up and eventually reaches the second preset temperature, thereby achieving the insulating effect on the inner cavity 11. In some cases, the insulating liquid can also be heated externally first, and then introduced into the insulating cavity 12. In this case, the second electric heating device 7 may not play a heating role, but only a heat preservation role, thereby reducing the energy consumption of the reactor system.
[0049] After the reaction is complete, the outlet valve 4 can be opened to quickly discharge the high-temperature insulating liquid from the insulation chamber 12, thereby achieving rapid heat dissipation and cooling of the vessel body 1. In some cases, after the high-temperature insulating liquid is discharged, low-temperature cooling liquid can be introduced into the insulation chamber 12 through the inlet pipe 3. The low-temperature cooling liquid exchanges heat with the vessel body 1, further increasing the cooling rate of the vessel body 1, thereby improving the equipment's turnover efficiency, enabling faster production of the next batch, and also reducing the risk of injury to operators due to contact with high-temperature equipment.
[0050] Optionally, the aforementioned insulating liquid includes, but is not limited to, water, oil, and water-oil mixtures.
[0051] In one specific embodiment, please refer to Figure 1 and Figure 2 The outer walls and bottom walls of the vessel body 1 extend outwards away from the inner cavity 11 to form a heat-insulating cavity 12, which semi-encloses the outer perimeter of the inner cavity 11. Understandably, the semi-enclosed nature of the heat-insulating cavity 12 allows the heat-insulating liquid in the cavity 12 to provide heat to the inner cavity 11 from multiple directions, ensuring uniform heating of the inner cavity 11 walls and preventing localized overheating or underheating, thus guaranteeing temperature uniformity in different areas of the material within the inner cavity 11. Furthermore, the semi-enclosed nature of the heat-insulating cavity 12 increases the contact area between the heat-insulating liquid and the outer wall of the inner cavity 11, facilitating more efficient heat transfer to the inner cavity 11 and improving heat exchange efficiency.
[0052] For example, such as Figure 1 and Figure 2 As shown, the vessel body 1 can be cylindrical, with an internal hollow cavity 11. In this case, the heat preservation cavity 12 has a U-shaped cross-section in the vertical direction AA and an annular cross-section in the horizontal direction. In other cases, the vessel body 1 can also be a regular column such as a cuboid, or other irregular irregular column.
[0053] In one specific embodiment, an insulation layer 8 is also provided on the cavity wall of the insulation cavity 12 away from the inner cavity 11. The insulation layer 8 may include one or more layers of inorganic fiber insulation layer, ceramic insulation layer, and foam plastic insulation layer.
[0054] In this embodiment, by providing an insulation layer 8 on the side wall of the insulation cavity 12 away from the inner cavity 11, the insulation layer 8 will not affect the heat exchange efficiency between the insulation liquid and the material, and can also effectively reduce the heat loss of the insulation liquid, so that the insulation liquid can be more stably maintained at the second preset temperature, thereby further improving the insulation effect of the insulation liquid on the material, while reducing the energy consumption of the second electric heating device 7.
[0055] Alternatively, the inorganic fiber insulation layer may include a glass wool layer, a rock wool layer, etc.
[0056] For example, the foam insulation layer may be a polyurethane foam layer.
[0057] See Figure 3 As shown, in one specific embodiment, a first temperature sensor 9 is also provided in the inner cavity 11 for detecting the temperature of the material. A second temperature sensor 10 is also provided in the insulation cavity 12 for detecting the temperature of the insulation liquid.
[0058] In one specific embodiment, the reactor may further include: a control panel 14 and a power module (not shown in the figure), wherein the power module is electrically connected to the first electric heating device 6 and the second electric heating device 7; the control panel 14 is connected to the first temperature sensor 9, the second temperature sensor 10 and the power module respectively, and is used to disconnect or connect the circuit between the power module and the first electric heating device 6 and the second electric heating device 7.
[0059] In this embodiment, the control panel 14 is connected to the first temperature sensor 9, the second temperature sensor 10, and the power module. The control panel 14 can obtain the temperature of the material in the inner cavity 11 through the first temperature sensor 9, and the control panel 14 can obtain the temperature of the insulating liquid in the insulation cavity 12 through the second temperature sensor 10. When the temperature of the material is lower than the first preset temperature, the circuit between the power module and the first electric heating device 6 is connected, and the first electric heating device 6 continues to heat the material. When the temperature of the material is detected to reach the first preset temperature, the control panel 14 sends a control signal to the power module, causing the power module to disconnect from the first electric heating device 6, thereby stopping the first electric heating device 6 from heating the material and maintaining the material at the first preset temperature. Similarly, when the temperature of the insulation liquid is lower than the second preset temperature, the circuit between the power module and the second electric heating device 7 is connected, and the second electric heating device 7 continues to heat the insulation liquid; when the temperature of the insulation liquid is detected to reach the second preset temperature, the control panel 14 sends a control signal to the power module, causing the power module to disconnect from the electrical connection with the second electric heating device 7, thereby causing the second electric heating device 7 to stop heating the insulation liquid, so that the insulation liquid is maintained at the second preset temperature.
[0060] Therefore, this embodiment achieves automated control of material temperature and insulation liquid temperature, reducing the workload of operators and providing a better user experience. During use, the first and second preset temperatures can be set via the control panel 14.
[0061] For example, control panel 14 can be Figure 3 The button-type control panel shown may have buttons 141, such as a "heating on" button, a "heating off" button, and a "temperature adjustment" button. The control panel 14 integrates a controller, which is connected to the aforementioned buttons 141, the first temperature sensor 9, the second temperature sensor 10, and the power module. The controller may be, for example, a microcontroller chip (MCU), an application-specific integrated circuit chip (ASIC), or a field-programmable gate array chip (FPGA).
[0062] In practical applications, the power module can be integrated into the control panel 14. The controller and the power module can be connected to other components via cables 15 for signal or electrical connections. Additionally, the power module can be electrically connected to the first temperature sensor 9 and the second temperature sensor 10 to provide the necessary power for their normal operation.
[0063] In one specific embodiment, both the first electric heating device 6 and the second electric heating device 7 include an electric heating wire or an electric heating tube electrically connected to the power supply module.
[0064] For example, please refer to Figure 2 and Figure 3 The first electric heating device 6 includes an electric heating tube disposed on the wall of the inner cavity 11, and the second electric heating device 7 includes an electric heating wire disposed on the wall of the heat preservation cavity 12.
[0065] Preferably, the electric heating tube surrounds and covers the cavity wall of the inner cavity 11 around the circumference of the vessel body 1, and the electric heating wire surrounds and covers the cavity wall of the insulation cavity 12 around the circumference of the vessel body 1, thereby enabling the electric heating tube and the electric heating wire to heat the material and the insulation liquid at a higher rate, effectively improving production efficiency.
[0066] In one specific embodiment, the top of the vessel body 1 also has an openable cover plate 16, and a sealing ring 161 is provided on the bottom edge of the cover plate 16.
[0067] For example, please refer to Figure 2 and Figure 4 In this embodiment, the top of the vessel body 1 has a feed inlet 13 that communicates with the inner cavity 11. When the cover plate 16 is in the closed state, the cover plate 16 blocks the feed inlet 13, and the cover plate 16 is sealed to the edge of the feed inlet 13 through the sealing ring 161 at the bottom edge. When the reaction operation is to be carried out, the cover plate 16 can be switched to the open state, at which time the feed inlet 13 is exposed, and the operator can add materials to the inner cavity 11 of the vessel body 1 through the feed inlet 13. After the material is added, the cover plate 16 is closed again, so that the feed inlet 13 is blocked and sealed again, thereby providing a closed environment for the material reaction. The closed environment is also conducive to further improving the heat preservation effect of the material.
[0068] Optionally, the cover plate 16 can be opened by means of rotational connection, snap-fit connection, magnetic connection, etc. with the vessel body 1.
[0069] In one specific embodiment, please refer to Figure 3 The stirring device 5 may include a rotary motor 51, a stirring shaft 52, and multiple stirring blades 53.
[0070] A rotary motor 51 is located on the top of the cover plate 16, and a stirring shaft 52 is located on the bottom of the cover plate 16. One end of the stirring shaft 52 passes through the cover plate 16 and is connected to the rotary motor 51. The other end of the stirring shaft 52 is connected to multiple stirring blades 53. The multiple stirring blades 53 are arranged at intervals along the circumference of the stirring shaft 52.
[0071] In this embodiment, the stirring shaft 52 can be driven to rotate by the rotary motor 51, and the stirring shaft 52 in turn drives the stirring blades 53 on it to rotate, thereby achieving stirring of the material through the stirring blades 53. During use, since the rotary motor 51 is located on the top of the cover plate 16, the rotary motor 51 will not enter the inner cavity 11, will not cause contamination to the material, and can also effectively protect the rotary motor 51.
[0072] In one specific embodiment, a funnel 31 with its opening facing upwards is provided at the end of the liquid inlet pipe 3 away from the vessel body 1. The funnel 31 can increase the cross-sectional area of the liquid inlet, thereby facilitating the manual addition of the insulation liquid by the operator and effectively reducing the risk of the insulation liquid spilling out. This is especially important when the insulation liquid is oil, as spilling oil will be detrimental to maintaining a clean and tidy production environment.
[0073] In some cases, the end of the inlet pipe 3 away from the vessel body 1 can also be connected to an external insulation liquid conveying device. The insulation liquid conveying device can pump the insulation liquid into the insulation chamber 12 through the inlet pipe 3 to realize the automated input of the insulation liquid and further improve the automation level of the device.
[0074] In one specific embodiment, a support rod 17 is also provided at the bottom of the vessel body 1. A support plate 18 is connected to the end of the support rod 17 away from the vessel body 1. A screw hole 181 is provided on the support plate 18. In practical applications, a bolt passing through the screw hole 181 on the support plate 18 from top to bottom is provided. The bolt can be fixedly connected to an external mounting base (not shown in the figure) to achieve the fixation of the vessel body 1.
[0075] In this embodiment, by elevating the vessel body 1 with the support rod 17, direct contact between the vessel body 1 and the ground can be avoided, thereby limiting the rapid heat loss of the vessel body 1 through the contact points and improving the heat preservation performance. In addition, elevating the vessel body 1 with the support rod 17 also makes it easier for operators to operate the discharge valve 2 and liquid discharge valve 4 at the bottom of the vessel body 1, making the structure more user-friendly and easier to use.
[0076] Preferably, the support rod 17 can be configured as a telescopic support rod, thereby enabling flexible adjustment of the height of the vessel body 1 above the ground based on the telescopic movement of the support rod 17. The structure of the telescopic support rod 17 can refer to the prior art, and this embodiment does not specifically limit it.
[0077] Further, please refer to Figure 4The reactor provided in this embodiment may further include a stepped support 19, which is disposed on the side of the reactor body 1 for operators to stand on, thereby facilitating the addition of materials to the elevated reactor body 1. Furthermore, the top of the stepped support 19 is fixedly connected to the reactor body 1, thus ensuring good stability of the stepped support 19 and preventing relative sliding between the stepped support 19 and the reactor body 1, which could lead to slips and injuries to the operators. A specific structure of the stepped support 19 can be found in [reference needed]. Figure 4 .
[0078] In summary, the reaction vessel provided by this utility model, by forming a heat-insulating cavity 12 between the inner and outer walls of the vessel body 1 and surrounding the outer perimeter of the inner cavity 11, and by realizing the entry and exit of the heat-insulating liquid through the liquid inlet pipe 3 and the liquid outlet valve 4, can reduce the heat loss of the material in the inner cavity 11 and play a preliminary heat-insulating role. The stirring device 5 can make the material in the inner cavity 11 uniformly mixed, avoiding local excessively high or low temperatures, and helping the material to be closer to the optimal temperature required for the reaction as a whole, improving the uniformity and stability of the reaction, thereby improving the reaction efficiency and product quality to a certain extent. The first electric heating device 6 heats the material in the inner cavity 11 to a first preset temperature, and the second electric heating device 7 heats the heat-insulating liquid to a second preset temperature higher than the first preset temperature. The setting of the dual electric heating devices can create a temperature difference between the material and the heat-insulating liquid, so that heat is transferred from the heat-insulating liquid to the material, compensating for the heat loss of the material due to heat dissipation, maintaining the material within the temperature range required for the reaction, improving the reaction efficiency of the material, and thus improving the quality and yield of the product.
[0079] Those skilled in the art will understand that the accompanying drawings are merely schematic diagrams of a preferred embodiment, and the modules or processes shown in the drawings are not necessarily essential for implementing this utility model.
[0080] Those skilled in the art will understand that the modules in the apparatus of the implementation scenario can be distributed within the apparatus of the implementation scenario as described, or they can be located in one or more apparatuses different from this implementation scenario, with corresponding changes. The modules of the above-described implementation scenario can be combined into one module, or they can be further divided into multiple sub-modules.
[0081] The serial numbers of the above-mentioned utility models are for descriptive purposes only and do not represent the superiority or inferiority of the implementation scenarios.
[0082] The above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.
Claims
1. A reaction vessel, characterized in that, include: The vessel body has an inner cavity, and a heat-insulating cavity for storing heat-insulating liquid is formed between the inner wall and the outer wall of the vessel body. The heat-insulating cavity surrounds the outer periphery of the inner cavity. An inlet pipe communicating with the heat-insulating cavity is provided on the outer wall of the vessel body. A discharge valve communicating with the inner cavity and a liquid outlet valve communicating with the heat-insulating cavity are provided at the bottom of the vessel body. A stirring device is installed on the vessel body for stirring the materials in the inner cavity; A first electric heating device is installed in the inner cavity of the vessel body to heat the material in the inner cavity to a first preset temperature; A second electric heating device is installed in the insulation cavity to heat the insulation liquid to a second preset temperature; The second preset temperature is higher than the first preset temperature.
2. The reaction vessel according to claim 1, characterized in that, The outer side wall and outer bottom wall of the vessel body expand outward in a direction away from the inner cavity to form the heat preservation cavity, which semi-encloses the periphery of the inner cavity.
3. A reaction vessel according to claim 1, characterized in that, The second preset temperature is 5°C to 10°C higher than the first preset temperature.
4. A reaction vessel according to claim 1, characterized in that, An insulation layer is provided on the side wall of the insulation cavity away from the inner cavity.
5. A reaction vessel according to claim 1, characterized in that, The reaction vessel also includes: A first temperature sensor is disposed in the inner cavity for detecting the temperature of the material; A second temperature sensor is installed in the insulation cavity to detect the temperature of the insulation liquid; The control panel and power module are provided, wherein the power module is electrically connected to the first electric heating device and the second electric heating device; the control panel is connected to the first temperature sensor, the second temperature sensor and the power module respectively, for disconnecting or connecting the circuit between the power module and the first electric heating device and the second electric heating device.
6. A reaction vessel according to claim 5, characterized in that, Both the first electric heating device and the second electric heating device include an electric heating wire or an electric heating tube that is electrically connected to the power supply module.
7. A reaction vessel according to claim 1, characterized in that, The top of the vessel body has an openable cover, and a sealing ring is provided at the bottom edge of the cover.
8. A reaction vessel according to claim 7, characterized in that, The stirring device includes a rotary motor, a stirring shaft, and multiple stirring blades; The rotary motor is located at the top of the cover plate, and the stirring shaft is located at the bottom of the cover plate. One end of the stirring shaft passes through the cover plate and is connected to the rotary motor, while the other end of the stirring shaft is connected to a plurality of stirring blades. The plurality of stirring blades are arranged at intervals along the circumference of the stirring shaft.
9. A reaction vessel according to any one of claims 1 to 8, characterized in that, A support rod is provided at the bottom of the vessel body, and a support plate is connected to the end of the support rod away from the vessel body. A screw hole is provided on the support plate.
10. A reaction vessel according to claim 9, characterized in that, The reactor also includes a stepped frame, which is disposed on the side of the reactor body and the top of the stepped frame is fixedly connected to the reactor body.