A hydrogen peroxide precise control dropwise adding reaction control system in a ferric phosphate preparation process

CN224686809UActive Publication Date: 2026-08-28山东锂源科技有限公司 +1
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Patent Information

Application Number
CN202521844321.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-08-28
Publication Date
2026-08-28
Estimated Expiration
2035-08-28

AI Technical Summary

Technical Problem

[0003]发明专利CN2023103471960公开了一种磷酸铁制备中的双氧水滴加装置及其使用方法,通过将氧化反应釜分为相互独立的两部分并在釜内设置若干个喷嘴,来实现双氧水的连续化滴加进料,但该方案装置繁冗,操作过程复杂,且完全依靠人工手动操作,人力消耗大,且无法保证双氧水与反应液充分混合,可能导致反应釜局部过热,具有安全隐患

Benefits of technology

[0013]有益效果:与现有技术相比,本实用新型具有如下优点:(1)通过DCS控制系统实现双氧水进料与磷酸二氢铵亚铁溶液进料的自动化联锁控制,替代人工手动操作进料,精准控制双氧水进料;(2)在DCS控制系统设置双氧水分段式精准滴加进料,并在反应釜顶端安装散布器,控制双氧水均匀分布在反应釜内,避免局部反应不均匀对产品一致性造成影响,提高双氧水的利用率,节约双氧水的使用;(3)在卸料管路上设置物料卸料防错联锁,防止双氧水漏添加或者反应未完成时卸料造成的产品性能下降。

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Abstract

The utility model discloses a hydrogen peroxide precise control drop reaction control system in the preparation process of iron phosphate, including the hydrogen peroxide tank and the reaction kettle through the pipeline connection, and is equipped with flow regulating valve and mass flowmeter on the pipeline between both, and mass flowmeter is controlled by DCS operation panel, and is equipped with the cumulative flowmeter on the feed pipe of reaction kettle, and the automatic valve is controlled by batch control instrument according to the cumulative flow of cumulative flowmeter, and then the flow regulating valve is controlled by automatic valve. The utility model discloses the automatic interlock control of hydrogen peroxide feed and ammonium dihydrogen phosphate ferrous solution feed through DCS control system, replaces manual operation feed, realizes hydrogen peroxide segmented type accurate drop feed, improves the utilization of hydrogen peroxide, and sets up material unloading mistake proof interlock on the unloading pipeline, prevents the product performance drop caused by hydrogen peroxide leak addition or unloading when the reaction is not completed.
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