Regulating reaction tubular structure for preparing carboranes

Abstract

The utility model provides a kind of preparation carborane's adjusting reaction pipe shape change structure, belong to the technical field of preparation carborane, this preparation carborane's adjusting reaction pipe shape change structure includes bottom plate, heating box and feeding hopper, heating box is installed at bottom plate top, and feeding hopper is set at bottom plate top;When heating box and moving box body heat to reaction pipeline, reaction pipeline will occur axial deformation, reaction pipeline will push moving box body and conveying mechanism to move, to be able to very good offset axial deformation to the influence of reaction pipeline, the structure stability of reaction pipeline itself has been improved, the axial deformation of reverse pipeline has been reasonably controlled, after deformation elimination, reaction pipeline will drive moving box body and conveying mechanism to reset, do not affect subsequent use.

Description

Technical Field

[0001] This invention belongs to the field of carborane preparation technology, specifically relating to a structure for adjusting the deformation of a reaction tube in the preparation of carborane. Background Technology

[0002] In the field of carborane preparation technology, the reaction tube is a key component for the carborane preparation reaction. However, in the actual preparation process, the reaction tube needs to operate at a high temperature environment, and there are gradual heating and cooling operations. Due to the physical property of thermal expansion and contraction, the reaction tube will inevitably undergo axial deformation, which, according to actual observations, can reach 2-3 cm.

[0003] If this axial deformation cannot be properly controlled or eliminated, it will seriously affect the structural stability of the reaction tube itself. Over time, this may lead to problems such as damage to the reaction tube, and will also interfere with the normal operation of the entire carborane preparation device, thereby affecting the preparation efficiency and quality of carborane and bringing many adverse factors to the production of carborane. Utility Model Content

[0004] The purpose of this invention is to provide a structure for adjusting the deformation of the reaction tube in the preparation of carborane, aiming to solve the problem that the axial deformation of the reaction tube is difficult to control or eliminate in the prior art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a structure for adjusting the deformation of a reaction tube for preparing carborane, comprising: a base plate, a heating box, and a feeding hopper, wherein the heating box is installed on the top of the base plate, and the feeding hopper is disposed on the top of the base plate;

[0006] A support frame is installed on the side wall of the base plate. The top of the support frame is equipped with sliding rails at intervals. A movable box is slidably installed on the top of the base plate. A reaction pipe is installed inside the movable box. The reaction pipe extends into the heating box. One end of the reaction pipe is connected to the inner wall of the heating box, and the other end of the reaction pipe is connected to the inside of the movable box.

[0007] The bottom of the feeding hopper is equipped with a conveying mechanism, which is slidably mounted on a slide rail. The conveying mechanism is used to transport the material inside the feeding hopper to the inside of the reaction pipe. When the reaction pipe deforms, the reaction pipe can push the moving box and the conveying mechanism to move left and right.

[0008] As a preferred embodiment of the present invention, for adjusting the deformation of the reaction tube in the preparation of carborane, a feed pipe is installed on the outer wall of the reaction pipe inside the movable housing. The inside of the feed pipe is connected to the inside of the reaction pipe, the top of the feed pipe extends out of the movable housing, and the feed pipe is connected to the conveying mechanism.

[0009] As a preferred embodiment of the present invention for adjusting the deformation of the reaction tube in the preparation of carborane, the conveying mechanism includes a conveying pipe, a fixed frame, an auger rod, and a conveying motor. The fixed frame is slidably mounted on a slide rail. The conveying pipe is installed at one end of the fixed frame facing the moving box. The auger rod is rotatably installed inside the conveying pipe. The conveying pipe is connected to the inside of the feeding hopper and the inside of the feeding pipe. The conveying motor is mounted on the fixed frame, and the output end of the conveying motor is connected to the auger rod.

[0010] As a structure for adjusting the deformation of the reaction tube in the preparation of carborane according to the present invention, preferably, a slider is installed at the bottom of the fixing frame, and the slider is slidably disposed on the slide rail.

[0011] As a preferred embodiment of the present invention, for adjusting the deformation of the reaction tube in the preparation of carborane, the support frame includes a support base and a support column. The support column is installed on the ground, the support base is located on the top of the support column, and the slide rail is located on the support base.

[0012] As a preferred embodiment of the present invention for adjusting the deformation of the reaction tube in the preparation of carborane, the bottom plate is provided with guide rails spaced apart at the front and rear, guide blocks are slidably provided on the guide rails, the guide blocks are connected to the bottom of the movable box, and a fixing column is provided at the bottom of the bottom plate.

[0013] Compared with the prior art, the beneficial effects of this utility model are:

[0014] The modified reaction tube deformation structure for preparing carboranes involves heating the reaction tube by a heating chamber and a moving chamber. This causes axial deformation of the reaction tube, which in turn moves the moving chamber and conveying mechanism. This effectively counteracts the impact of axial deformation on the reaction tube, improving its structural stability. The axial deformation of the reverse tube is thus properly controlled. After the deformation is eliminated, the reaction tube resets, moving the chamber and conveying mechanism without affecting subsequent use. Attached Figure Description

[0015] The accompanying drawings are provided to further illustrate the present invention and form part of the specification. They are used together with the embodiments of the present invention to explain the present invention, but do not constitute a limitation thereof. In the drawings:

[0016] Figure 1 This is a three-dimensional structural diagram of a specific embodiment of the present utility model;

[0017] Figure 2 This is a side view of a specific embodiment of the present invention;

[0018] Figure 3 for Figure 2 A schematic diagram of the cross-sectional structure of AA.

[0019] In the diagram: 10. Base plate; 11. Heating box; 12. Feeding hopper; 13. Slide rail; 14. Moving box; 15. Reaction pipe; 16. Feeding pipe; 17. Fixed column; 2. Support frame; 21. Support column; 22. Support base; 23. Guide rail; 231. Guide block; 3. Conveying mechanism; 31. Conveying pipe; 32. Fixed frame; 33. Screw rod; 34. Conveying motor; 35. Sliding block. Detailed Implementation

[0020] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0021] Please see Figure 1-3 The present invention provides the following technical solution: a structure for adjusting the deformation of a reaction tube for preparing carborane, comprising: a base plate 10, a heating box 11 and a feeding hopper 12, wherein the heating box 11 is installed on the top of the base plate 10, the feeding hopper 12 is located on the top of the base plate 10, and the top of the feeding hopper 12 is provided with a feed inlet (not shown in the figure), through which the material is fed into the feeding hopper 12, and a fixing column 17 is installed at the bottom of the base plate 10, the fixing column 17 being installed on the ground.

[0022] A support frame 2 is installed on the side wall of the base plate 10. The support frame 2 includes a support column 21 and a support base 22. The support column 21 is installed on the ground at intervals, and the support base 22 is installed on the support column 21. The slide rail 13 is set on the support base 22.

[0023] The bottom of the feeding hopper 12 is provided with a conveying mechanism 3, which is slidably mounted on the slide rail 13. The conveying mechanism 3 can move left and right on the slide rail 13. The top of the bottom plate 10 is provided with a movable box 14, and a reaction pipe 15 is installed inside the movable box 14. The reaction pipe 15 extends into the heating box 11. One end of the reaction pipe 15 is connected to the inner wall of the heating box 11, and the other end of the reaction pipe 15 is connected to the inside of the movable box 14.

[0024] When the reaction pipe 15 undergoes axial deformation, it can push the movable box 14 to move towards the support frame 2. The bottom plate 10 is equipped with guide rails 23 at intervals at the top front and back. Guide blocks 231 are slidably provided on the guide rails 23. The guide blocks 231 are connected to the bottom of the movable box 14. The movable box 14 can slide on the guide rails 23 through the guide blocks 231.

[0025] A feed pipe 16 is installed on the outer wall of the reaction pipe 15 located inside the movable housing 14. The inside of the feed pipe 16 is connected to the inside of the reaction pipe 15. The top of the feed pipe 16 extends out of the movable housing 14. The feed pipe 16 is connected to the conveying mechanism 3. The conveying mechanism 3 is used to transport the material inside the hopper 12 to the inside of the feed pipe 16, and then into the inside of the reaction pipe 15 through the feed pipe 16. The heating box 11 and the movable housing 14 heat the reaction pipe 15 (this is the prior art and will not be described in detail here).

[0026] The conveying mechanism 3 includes a conveying pipe 31, a fixed frame 32, an auger rod 33, and a conveying motor 34. The fixed frame 32 is slidably mounted on the slide rail 13. A slider 35 is installed at the bottom of the fixed frame 32. The slider 35 is slidably mounted on the slide rail 13. The fixed frame 32 can move left and right on the slide rail 13 through the slider 35. The heating box 11 and the moving box 14 heat the reaction pipe 15. The reaction pipe 15 will have an axial deformation of 2-3cm. The reaction pipe 15 will push the moving box 14 and the fixed frame 32 to move left and right 2-3cm on the guide rail 23 and the slide rail 13.

[0027] The conveying pipe 31 is installed at one end of the fixed frame 32 facing the movable box 14. The auger rod 33 is rotatably installed inside the conveying pipe 31. The conveying pipe 31 is connected to the inside of the feeding hopper 12 and the inside of the feeding pipe 16. The conveying motor 34 is installed on the fixed frame 32. The output end of the conveying motor 34 is connected to the auger rod 33. The material in the feeding hopper 12 falls into the conveying pipe 31. The conveying motor 34 drives the auger rod 33 to rotate. The auger rod 33 conveys the material inside the conveying pipe 31 to the inside of the feeding pipe 16.

[0028] Please see Figure 1-3 Working principle: When in use, the operator puts the material into the feeding hopper 12. The material inside the feeding hopper 12 falls into the conveying pipe 31. The conveying motor 34 starts and drives the auger rod 33 to rotate. The auger rod 33 moves the material inside the conveying pipe 31 to the feeding pipe 16. The material inside the feeding pipe 16 falls into the reaction pipe 15.

[0029] The heating box 11 and the movable box 14 heat the reaction pipe 15, causing the reaction pipe 15 to undergo axial deformation. Since the heating box 11 is fixedly installed on the top of the base plate 10, the reaction pipe 15 pushes the movable box 14 to move on the guide rail 23. The reaction pipe 15 drives the conveying mechanism 3 to move on the slide rail 13 through the feed pipe 16.

[0030] It will be apparent to those skilled in the art that this invention is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or essential characteristics of this invention. Therefore, the embodiments should be considered illustrative and non-limiting in all respects, and the scope of this invention is defined by the appended claims and not by the foregoing description. Thus, all variations falling within the meaning and scope of equivalents of the claims are intended to be included within this invention. No reference numerals in the claims should be construed as limiting the scope of the claims.

Claims

1. A method for adjusting the deformation structure of a reaction tube in the preparation of carboranes, comprising: The system consists of a base plate, a heating box, and a feeding hopper. The heating box is installed on top of the base plate, and the feeding hopper is located on top of the base plate. The feature is that a support frame is installed on the side wall of the base plate, and a slide rail is provided at intervals at the top of the support frame. A movable box is slidably provided on the top of the base plate. A reaction pipe is installed inside the movable box. The reaction pipe extends into the heating box. One end of the reaction pipe is connected to the inner wall of the heating box, and the other end of the reaction pipe is connected to the inside of the movable box. The bottom of the feeding hopper is equipped with a conveying mechanism, which is slidably mounted on a slide rail. The conveying mechanism is used to transport the material inside the feeding hopper to the inside of the reaction pipe. When the reaction pipe deforms, the reaction pipe can push the moving box and the conveying mechanism to move left and right.

2. The method for adjusting the deformation of the reaction tube in the preparation of carborane according to claim 1, characterized in that: A feed pipe is installed on the outer wall of the reaction pipe inside the movable housing. The inside of the feed pipe is connected to the inside of the reaction pipe. The top of the feed pipe extends outside the movable housing and is connected to the conveying mechanism.

3. The method for adjusting the deformation of the reaction tube in the preparation of carborane according to claim 2, characterized in that: The conveying mechanism includes a conveying pipe, a fixed frame, an auger rod, and a conveying motor. The fixed frame is slidably mounted on a slide rail. The conveying pipe is installed at one end of the fixed frame facing the movable housing. The auger rod is rotatably installed inside the conveying pipe. The conveying pipe is connected to the inside of the feeding hopper and the inside of the feeding pipe. The conveying motor is mounted on the fixed frame, and the output end of the conveying motor is connected to the auger rod.

4. The method for adjusting the deformation of the reaction tube in the preparation of carborane according to claim 3, characterized in that: The bottom of the fixing frame is equipped with a slider, which is slidably mounted on a slide rail.

5. A modified reaction tube structure for preparing carborane according to any one of claims 1-4, characterized in that: The support frame includes a support base and a support column. The support column is installed on the ground, the support base is located on the top of the support column, and the slide rail is installed on the support base.

6. A method for adjusting the deformation of a reaction tube for preparing carborane according to any one of claims 1-4, characterized in that: The bottom plate is equipped with guide rails at intervals on the front and back, and guide blocks are slidably mounted on the guide rails. The guide blocks are connected to the bottom of the movable box, and a fixing column is provided at the bottom of the bottom plate.

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