Preparation method of rubber material for preparing high-/low-temperature resistant automobile pipeline rubber products

A technology for rubber materials and automobile pipelines, which is applied in the field of rubber material preparation, can solve the problems of high temperature resistance, low temperature resistance, low tensile strength changes, changes in elongation at break, cold flexural resistance, etc.

CN102825673BActive Publication Date: 2014-11-12上海天普汽车零部件有限公司
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Publication Date
2014-11-12

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Abstract

The invention discloses a preparation method of rubber material for preparing high- / low-temperature resistant automobile pipeline rubber products. The method includes (1) introducing water to cool a Banbury mixer; blending rubber material, reinforcing filler, plasticizer, activator, anti-aging agent and lubricant in the Banbury mixer; discharging under rubber temperature of below 130 DEG C; forming sheets on an open mill; and cooling to obtain master batch; and (2) inputting the master batch into the Banbury mixer; blending under uniform addition of vulcanizing agent; discharging under rubber temperature of below 90 DEG C; forming strips on the open mill; cooling and standing for aging. The produced automobile engine / transmission oil cooling pipeline rubber products have improved high- / low-temperature resistance, satisfy increasingly high requirements of automobile industry on rubber products, and accord with GM6260 M standard.
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Description

technical field

[0001] The invention relates to a method for preparing a rubber material, in particular to a method for preparing a rubber material used in automobile engine and transmission oil cooling pipes for preparing high and low temperature resistant automobile pipeline rubber products. Background technique

[0002] The high temperature (150°C) and low temperature (-40°C) resistance of rubber products such as automotive engines and transmission oil cooling pipes produced by the existing preparation method is relatively low, and cannot meet the requirements of the general GM6260M standard.

[0003] In the prior art, adopt rubber material (chlorinated polyethylene rubber) to make the test data of automobile engine and transmission oil cooling pipeline rubber products as follows:

[0004]

[0005]

[0006] From the above experimental results, it can be seen that the tensile strength change, elongation at break change and cold flex resistance of the existing automob...

Examples

preparation example Construction

[0027] The preparation method of the rubber material for preparing high and low temperature resistant automobile pipeline rubber products of the present invention comprises the following steps:

[0028] (1) Cool the internal mixer with water, put rubber raw materials, reinforcing fillers, plasticizers, active agents, anti-aging agents and lubricants into the internal mixer for internal mixing, and control the temperature of the rubber below 130°C. Glue removal, sheet release and cooling on an open rubber mixer to obtain masterbatch;

[0029] (2) Put the masterbatch into the internal mixer, add vulcanizing agent evenly for mixing, control the temperature of the glue below 90°C to discharge the glue, and make strips on the open rubber mixer, cool and leave it to mature, and obtain the raw materials for the manufacture of automobiles. High and low temperature resistant rubber materials used in products such as engine and transmission oil cooling pipes.

[0030] In the present in...

Embodiment 1

[0035] Rubber raw material: chlorinated polyethylene rubber 41.75%;

[0036] Reinforcing filler: 10.44% of quick-pressed furnace black, 14.61% of non-polluting high-definition semi-reinforcing furnace black, and 12.53% of light calcium carbonate;

[0037] Plasticizer: 4.18% dioctyl sebacate, 6.26% trioctyl trimellitate;

[0038] Vulcanizing agent: dicumyl peroxide 2.09%;

[0039] Active agent: highly active magnesium oxide 4.18%, stearic acid 0.63%, triallyl isocyanurate 1.67%;

[0040] Antiaging agent: 0.63% of 2,2,4-trimethyl-1,2-dihydroquinoline polymer, 0.63% of nickel dibutyl disulfide carbamate;

[0041] Lubricant: polyethylene wax 0.40%;

[0042] The preparation method of the rubber material for preparing high and low temperature resistant automobile pipeline rubber products of the present invention comprises the following steps:

[0043] (1) Cool the internal mixer with water, control the temperature of the internal mixer studio to <100°C, and the rotating speed: 3...

Embodiment 2

[0049] Rubber raw material: chlorinated polyethylene rubber 42.50%;

[0050] Reinforcing filler: 10.30% of quick-pressed furnace black, 14.59% of non-polluting high-definition semi-reinforcing furnace black, and 12.45% of light calcium carbonate;

[0051] Plasticizer: 3.86% dioctyl sebacate, 6.01% trioctyl trimellitate;

[0052] Vulcanizing agent: dicumyl peroxide 2.14%;

[0053] Active agent: highly active magnesium oxide 4.25%, stearic acid 0.60%, triallyl isocyanurate 1.71%;

[0054]Antiaging agent: 0.60% of 2,2,4-trimethyl-1,2-dihydroquinoline polymer, 0.60% of nickel dibutyl disulfide carbamate;

[0055] Lubricant: polyethylene wax 0.39%;

[0056] The preparation method of the rubber material for preparing high and low temperature resistant automobile pipeline rubber products of the present invention comprises the following steps:

[0057] (1) Cool the internal mixer with water, control the temperature of the internal mixer studio to <100°C, and the rotating speed: 32...