External oil tea cake cleaning and hair nourishing liquid and preparation method thereof

Abstract

The invention relates to the field of daily chemical industry and hairdressing and hair care, in particular to an external oil tea cake cleaning and hair nourishing liquid and a preparation method thereof. The external oil-tea cake cleaning and hair nourishing liquid is prepared from 100 parts of oil-tea cakes, 20-60 parts of radix polygoni multiflori preparata, 10-30 parts of radix rehmanniae preparata, 10-30 parts of rhizoma polygonati preparata, 10-30 parts of radix rehmanniae recen, 10-30 parts of radix sophorae flavescentis, 30-100 parts of fresh ginger, 10-30 parts of Chinese soapberry fruits and 10-30 parts of senecio scandens. The hair nourishing liquid is natural and non-irritant, has obvious cleaning and hair nourishing effects, and is suitable for various hair quality and scalp types. The preparation method of the external oil tea cake cleaning and hair nourishing liquid is simple, raw materials are easy to obtain, and industrial production is facilitated.

Description

Technical Field

[0001] The invention relates to the fields of daily chemical industry and hair care, and in particular to an external oil-tea cake cleaning and nourishing hair liquid and a preparation method thereof. Background Art

[0002] There are many kinds of hair care products on the market, but most of them have problems such as excessive chemical additives, strong scalp irritation, unsatisfactory cleaning effect or poor hair care effect. Therefore, developing a natural plant hair care product that is natural, non-irritating, and has significant cleaning and hair care effects is of great significance to meet the needs of consumers. Summary of the invention

[0003] The purpose of the present invention is to provide an external oil-tea cake cleaning and nourishing hair liquid with cleaning and nourishing functions and a preparation method thereof to solve the problems existing in the above-mentioned prior art. The external oil-tea cake cleaning and nourishing hair liquid composition is natural, non-irritating, and has significant cleaning and nourishing effects.

[0004] To achieve the above object, the present invention provides the following solutions:

[0005] One of the technical schemes of the present invention is an external oil-tea cake cleaning hair care liquid composition, which comprises, by weight, 100 parts of oil-tea cakes, 20-60 parts of processed Polygonum multiflorum, 10-30 parts of prepared Rehmannia root, 10-30 parts of processed Polygonatum sibiricum, 10-30 parts of raw Rehmannia root, 10-30 parts of Sophora flavescens, 30-100 parts of ginger, 10-30 parts of Sapindus mukorossi and 10-30 parts of Senecio oleifera.

[0006] The second technical solution of the present invention is the use of the above-mentioned external-use tea cake cleansing and nourishing hair liquid composition in the preparation of cleansing and nourishing hair liquid.

[0007] The third technical solution of the present invention is a method for preparing an external oil-tea cake cleaning hair care liquid, comprising the following steps:

[0008] According to the raw material composition of the external camellia oil cake cleaning and nourishing hair liquid composition, the camellia oil cake is first crushed and then subjected to alcohol extraction, and the camellia oil cake residue is filtered to remove to obtain the camellia oil cake extract;

[0009] Then, the remaining raw materials except the oil tea cake are mixed and added into water for cooking, and after cooling, solid-liquid separation is performed by physical extrusion to obtain the remaining raw material filtrate;

[0010] Mixing the tea cake extract with the remaining raw material filtrate to obtain an extract;

[0011] A complexing agent is added to the extract to emulsify the extract to obtain the external camellia cake hair cleaning and nourishing liquid.

[0012] The fourth technical solution of the present invention is an external-use camellia cake cleaning and nourishing hair liquid prepared according to the above-mentioned preparation method.

[0013] The present invention is based on:

[0014] The whole formula is composed of oil tea cake, Polygonum multiflorum, Sophora flavescens, ginger, Sapindus mukorossi, processed Polygonatum sibiricum, Radix Rehmanniae, Radix Rehmanniae Preparata, Senecio radix etc. The external oil tea cake cleaning hair nourishing liquid composition of the present invention has the effects of cleaning hair, clearing away heat and dampness, and nourishing yin and blood, and is mainly suitable for people who are prone to hair loss, repeated hair loss, fragile hair, premature gray hair etc., and has a certain health care effect of reducing hair loss and promoting the improvement of hair quality and hair color.

[0015] "Suwen Shanggu Tianzhen Lun" says: "When a girl is seven years old, her kidney qi is strong, her teeth grow and her hair grows. ... At sixty-seven, ..., her hair starts to turn white. ... When a man is eight years old, his kidney qi is strong, his hair grows and his teeth grow. ... At sixty-eight, his yang qi is exhausted, his face becomes scorched, and his hair turns white." This shows that hair loss or graying is a natural aging phenomenon of the human body. Traditional Chinese medicine says that "blood is the residue of hair", which means that the state of hair is related to blood. The liver stores blood, and the kidney transforms blood into essence. The liver and kidney are directly related to blood. Aging and insufficient liver and kidney essence and blood are internal causes. External causes include damp heat infiltrating the skin, or wind heat stagnating in the skin, which manifests as oily scalp, sticky hair, etc. Dampness obstruction and heat stagnation both damage the yin blood of the head skin or cause poor blood circulation, causing the hair to lose blood nourishment and fall out or turn white early.

[0016] The tea cake is used as the main drug in the prescription of the present invention. The drug is recorded in the "Sui Xi Ju Diet", which has "moisturizing dryness, clearing heat, ... benefiting the head and eyes, and moistening the hair ("Concise Chinese Medicine Dictionary" explains the "sticky, greasy, and sticky"). Its sweet and bitter taste, cool nature, can clear heat to dispel evil, and moisturize to strengthen the body. The ministers are processed Polygonum multiflorum and Rehmannia glutinosa, which nourish the liver and kidney essence and blood. Polygonum multiflorum is recorded in the "Compendium of Materia Medica" and says that it "can nourish blood and benefit the liver ..., black beard and hair". The two drugs are used together to help the main drug and nourish yin and blood. ① Processed Polygonatum sibiricum and Rehmannia glutinosa are added to nourish yin and blood to help the main and minister drugs to strengthen the body and treat the root cause. ② Sophora flavescens and Cnidium monnieri are both bitter and cold in nature, clear heat and dry dampness, and can also dispel wind and stop itching. The two drugs are used together to clear damp heat to dispel evil and treat the symptoms. ③ Ginger, pungent and dispersing to move the surface, pungent and warm to promote the circulation of qi and blood, and help all the drugs to go up to nourish hair. The soapberry in the recipe is bitter and neutral. "Essentials of Herbal Medicine" states that "boiling the paste can dispel wind and reduce swelling." External use of the decoction can clear away heat and kill insects; it also has a certain foaming effect to clean the hair and the skin at the roots of the hair, helping the other drugs to work better and serving as an adjuvant. Looking at the whole recipe, the combination of the drugs has the effects of cleaning the hair, clearing away heat and dampness, and nourishing yin and blood. It is mainly suitable for people who are prone to hair loss, repeated hair loss, fragile hair, and premature gray hair.

[0017] The present invention discloses the following technical effects:

[0018] The invention provides an external oil-tea cake cleaning and nourishing hair liquid composition, which has a reasonable formula and various medicines used in combination, has the effects of cleaning hair, clearing away heat and dampness, and nourishing yin and blood, and is suitable for people who are prone to hair loss, repeated hair loss, fragile hair, premature gray hair, etc.

[0019] The present invention also provides an external oil tea cake cleaning hair care liquid, which is natural and non-irritating, has significant cleaning and hair care effects, and is suitable for hair cleaning. By adjusting the proportion of Chinese medicinal materials in the formula, hair care liquid products with different effects can be obtained to meet the diversified needs of the market.

[0020] The preparation method of the external oil-tea cake cleaning hair nourishing liquid of the invention is simple, the raw materials are easily available, and the industrial production is convenient. DETAILED DESCRIPTION

[0021] Various exemplary embodiments of the present invention will now be described in detail. This detailed description should not be considered as limiting the present invention, but should be understood as a more detailed description of certain aspects, features, and embodiments of the present invention.

[0022] It should be understood that the terms described in the present invention are only for describing a particular embodiment and are not intended to limit the present invention. In addition, for the numerical range in the present invention, it should be understood that each intermediate value between the upper and lower limits of the scope is also specifically disclosed. The intermediate value in any stated value or stated range, and each smaller range between any other stated value or intermediate value in the described range is also included in the present invention. The upper and lower limits of these smaller ranges can be independently included or excluded in the scope.

[0023] Unless otherwise indicated, all technical and scientific terms used herein have the same meanings as those generally understood by those skilled in the art. Although the present invention describes only preferred methods and materials, any methods and materials similar or equivalent to those described herein may also be used in the implementation or testing of the present invention. All documents mentioned in this specification are incorporated by reference to disclose and describe the methods and / or materials associated with the documents. In the event of a conflict with any incorporated document, the content of this specification shall prevail.

[0024] It will be apparent to those skilled in the art that various modifications and variations may be made to the specific embodiments of the present invention description without departing from the scope or spirit of the present invention. Other embodiments derived from the present invention description will be apparent to the skilled artisan. The present invention description and examples are exemplary only.

[0025] The words “include,” “including,” “have,” “contain,” etc. used in this document are open-ended terms, meaning including but not limited to.

[0026] The first aspect of the present invention provides an external oil-tea cake cleaning hair care liquid composition, which comprises, by weight, 100 parts of oil-tea cakes, 20-60 parts of processed Polygonum multiflorum, 10-30 parts of prepared Rehmannia root, 10-30 parts of processed Polygonatum sibiricum, 10-30 parts of raw Rehmannia root, 10-30 parts of Sophora flavescens, 30-100 parts of ginger, 10-30 parts of Sapindus mukorossi and 10-30 parts of Senecio oleifera.

[0027] In a preferred embodiment of the present invention, the raw materials include, by mass, 100 parts of camellia oil cake, 60 parts of processed Polygonum multiflorum, 30 parts of prepared Rehmannia root, 30 parts of processed Polygonatum sibiricum, 30 parts of raw Rehmannia root, 30 parts of Sophora flavescens, 100 parts of ginger, 30 parts of Sapindus mukorossi and 30 parts of Senecio grandiflora.

[0028] As a natural plant resource, tea cake contains rich tea polyphenols, tea saponins and other beneficial ingredients, which have antibacterial, anti-inflammatory, antipruritic and other effects, and have a good effect on the maintenance of scalp and hair. Therefore, the application of tea cake in the preparation of hair care liquid has broad application prospects.

[0029] The second aspect of the present invention provides a use of the above-mentioned external-use tea cake cleansing and nourishing hair liquid composition in the preparation of a cleansing and nourishing hair liquid.

[0030] The third aspect of the present invention provides a method for preparing an external oil-tea cake cleaning hair care liquid, comprising the following steps:

[0031] According to the raw material composition of the external camellia oil cake cleaning and nourishing hair liquid composition, the camellia oil cake is first crushed and then subjected to alcohol extraction, and the camellia oil cake residue is filtered to remove to obtain the camellia oil cake extract;

[0032] Then, the remaining raw materials except the oil tea cake are mixed and added into water for cooking, and after cooling, solid-liquid separation is performed by physical extrusion to obtain the remaining raw material filtrate;

[0033] Mixing the tea cake extract with the remaining raw material filtrate to obtain an extract;

[0034] A complexing agent is added to the extract to emulsify the extract to obtain the external camellia cake hair cleaning and nourishing liquid.

[0035] In a preferred embodiment of the present invention, the alcohol extraction uses an ethanol solution with a volume concentration of 70%-80%; the temperature of the alcohol extraction is 50°C and the time is 10 hours; the material-liquid ratio of the alcohol extraction is 1g:2mL.

[0036] In a preferred embodiment of the present invention, the cooking material-liquid ratio is 1 g:5 mL.

[0037] In a preferred embodiment of the present invention, the cooking temperature is 90-100° C. and the cooking time is 6 hours.

[0038] In a specific embodiment of the present invention, the cooking is carried out in an extraction tank, and the extraction tank adopts a full stainless steel interlayer steam heating method.

[0039] In a preferred embodiment of the present invention, the complexing agent is food-grade ethylenediaminetetraacetic acid sodium salt (disodium EDTA), and the added amount of the complexing agent is 0.05-0.2% of the mass of the extract.

[0040] In a preferred embodiment of the present invention, the emulsification conditions are as follows: disodium EDTA and the extract are added into an emulsifying pot, heated to 85-90° C., and mixed.

[0041] A fourth aspect of the present invention provides an external-use camellia cake cleansing and nourishing hair liquid prepared according to the above-mentioned preparation method.

[0042] The external oil tea cake cleaning hair nourishing liquid of the present invention has the following advantages:

[0043] (1) Natural and non-irritating: It uses natural medicinal extracts such as camellia oil cake as the main ingredients, does not contain harmful chemical additives, and is non-irritating to the scalp.

[0044] (2) Significant cleansing and hair care effects: Tea polyphenols, tea saponins and other ingredients in tea cakes can effectively cleanse the scalp, while tea seed oil and plant protein can nourish the hair and improve hair quality.

[0045] (3) Easy to prepare and preserve: The preparation process is simple, the raw materials are easily available, the product has good stability, is easy to store and use, and can provide consumers with long-lasting and effective cleaning and hair care effects.

[0046] The technical solutions described in the present invention, unless otherwise specified, are all conventional solutions in the art, and the reagents or raw materials used, unless otherwise specified, are purchased from commercial channels or have been disclosed.

[0047] The technical solutions provided by the present invention are described in detail below in conjunction with the embodiments, but they should not be construed as limiting the protection scope of the present invention.

[0048] Example 1

[0049] Step 1, prepare raw materials: by mass, the raw materials consist of 100 parts of camellia oil cakes, 60 parts of processed Polygonum multiflorum, 30 parts of prepared Rehmannia root, 30 parts of processed Polygonatum sibiricum, 30 parts of raw Rehmannia root, 30 parts of Sophora flavescens, 100 parts of ginger, 30 parts of Sapindus mukorossi and 30 parts of Senecio grandiflora.

[0050] Step 2, preparation of external camellia cake cleaning and nourishing hair liquid: crush the camellia cake according to the material-liquid ratio of 1g:2mL, add it into an ethanol aqueous solution with a volume concentration of 70%, and perform alcohol extraction at a temperature of 50°C for 10 hours, filter and remove the residue to obtain a camellia cake extract;

[0051] According to the material-liquid ratio of 1g:5mL, the remaining raw materials except the tea cake are mixed and added into deionized water and cooked at 100°C for 6 hours. After cooling, solid-liquid separation is performed by physical extrusion to obtain the remaining raw material filtrate;

[0052] The tea cake extract is mixed with the remaining raw material filtrate to obtain an extract;

[0053] Food grade disodium EDTA is added to the extract at an amount of 0.1% of the extract mass for emulsification (emulsification conditions: add disodium EDTA and the extract to an emulsifying pot, heat to 85-90° C., and mix well). After passing the test, the product is bottled and sealed for storage to obtain an external camellia cake cleansing hair care solution.

[0054] Example 2

[0055] The only difference from Example 1 is that in step 2, the volume concentration of the ethanol aqueous solution is 80%, and the remaining steps and parameters are the same as those in Example 1.

[0056] Comparative Example 1

[0057] The only difference from Example 1 is that in step 1, the amount of Rehmannia glutinosa added is 60 parts, and the addition of Rehmannia glutinosa is omitted, and the remaining steps and parameters are the same as those in Example 1.

[0058] Effect example

[0059] The effects of the external tea cake cleaning and nourishing hair liquid prepared in the examples and comparative examples were verified as follows:

[0060] 40 subjects (20 males + 20 females) were randomly selected and divided into 4 groups, each group consisting of 5 males + 5 females; all subjects had dandruff, hair loss, and gray hair, with the degree of difference not exceeding 10%. Groups 1-3 used the external oil-tea cake cleaning and hair care liquid prepared in Examples 1-2 and Comparative Example 1, respectively, and were marked as Example 1, Example 2, and Comparative Example 1, respectively; Group 4 used a common shampoo purchased on the market as a control group; the shampooing method of each group was: washing hair once every two days, leaving the shampoo on the hair and scalp for 5-10 minutes each time, and continuing to use it for 4 weeks.

[0061] 1. Observe the phenomenon and determine the effect:

[0062] Relief: After using the shampoo, dandruff is reduced, but there is no significant improvement in hair loss and dark hair;

[0063] Significant improvement: scalp itching and hair loss are eliminated, new hair grows in the areas with severe hair loss, and white hair turns black;

[0064] invalid;

[0065] The results are summarized in Table 1.

[0066] 2. Evaluate the elasticity and hair surface:

[0067] The elastic effect was evaluated by using a YG(B)001A electronic single fiber strength tester. The sample length was 5 cm, and 10% of the sample length was the fixed elongation value (L). The residual elongation value (Li) was measured by the single fiber strength tester, and then The elastic modulus R (%) of the hair at a certain elongation was calculated, where N is the number of measurements (10 times).

[0068] The results are summarized in Table 2.

[0069] Table 1

[0070] Relief (number of people) Significant improvement (number of people) Invalid (number of people) Example 1 1 9 - Example 2 2 8 - Comparative Example 1 5 5 - Control group 4 1 5

[0071] Note: “-” in the table means no.

[0072] Table 2

[0073] Elastic modulus R(%) Static friction coefficient Dynamic friction coefficient Example 1 89.14 0.1498 0.1275 Example 2 84.63 0.1524 0.1291 Comparative Example 1 71.08 0.1521 0.1243 Control group 60.82 0.2307 0.1749

[0074] The embodiments described above are only descriptions of the preferred modes of the present invention, and are not intended to limit the scope of the present invention. Without departing from the design spirit of the present invention, various modifications and improvements made to the technical solutions of the present invention by ordinary technicians in this field should all fall within the protection scope determined by the claims of the present invention.

Claims

1. An external tea cake cleaning hair care liquid composition, characterized in that: The raw materials include, by weight, 100 parts of oil-tea cake, 20-60 parts of processed Polygonum multiflorum, 10-30 parts of prepared Rehmannia root, 10-30 parts of processed Polygonatum sibiricum, 10-30 parts of raw Rehmannia root, 10-30 parts of Sophora flavescens, 30-100 parts of ginger, 10-30 parts of Sapindus mukorossi and 10-30 parts of Senecio grandiflora.

2. The external use tea cake cleaning hair care liquid composition according to claim 1, characterized in that: The raw materials include, by weight, 100 parts of camellia oil cakes, 60 parts of processed Polygonum multiflorum, 30 parts of prepared Rehmannia root, 30 parts of processed Polygonatum sibiricum, 30 parts of raw Rehmannia root, 30 parts of Sophora flavescens, 100 parts of ginger, 30 parts of Sapindus mukorossi and 30 parts of Senecio chinensis.

3. Use of the external-use tea cake cleaning and nourishing hair liquid composition as claimed in claim 1 or 2 in the preparation of cleaning and nourishing hair liquid.

4. A method for preparing an external oil-tea cake cleaning hair care liquid, characterized in that: The following steps are involved: The raw material composition of the external camellia cake cleaning and nourishing hair liquid composition according to claim 1 or 2, firstly crushing the camellia cake and then performing alcohol extraction, filtering and removing the camellia cake residue to obtain the camellia cake extract; Then, the remaining raw materials except the oil tea cake are mixed and added into water for cooking, and after cooling, solid-liquid separation is performed by physical extrusion to obtain the remaining raw material filtrate; Mixing the tea cake extract with the remaining raw material filtrate to obtain an extract; A complexing agent is added to the extract to emulsify the extract to obtain the external oil-tea cake cleaning and nourishing hair liquid.

5. The method for preparing the external oil-tea cake cleaning hair nourishing liquid according to claim 4, characterized in that: The alcohol extraction uses an ethanol solution with a volume concentration of 70%-80%; the temperature of the alcohol extraction is 50° C. and the time is 10 hours; the material-liquid ratio of the alcohol extraction is 1g:2mL.

6. The method for preparing the external oil-tea cake cleaning hair nourishing liquid according to claim 4, characterized in that: The material-liquid ratio of the cooking is 1 g:5 mL.

7. The method for preparing the external oil-tea cake cleaning hair nourishing liquid according to claim 4, characterized in that: The cooking temperature is 90-100° C. and the cooking time is 6 hours.

8. The method for preparing the external oil-tea cake cleaning hair nourishing liquid according to claim 4, characterized in that: The complexing agent is food-grade ethylenediaminetetraacetic acid sodium salt; the added amount of the complexing agent is 0.05-0.2% of the mass of the extract.

9. The method for preparing the external oil-tea cake cleaning hair nourishing liquid according to claim 4, characterized in that: The emulsification conditions are as follows: sodium ethylenediaminetetraacetic acid and the extract are added into an emulsifying pot, heated to 85-90° C., and mixed.

10. The external-use tea cake cleaning and nourishing hair liquid prepared by the preparation method according to any one of claims 4 to 9.