Male article delayed spray and preparation process thereof

Abstract

The invention provides a male product delay spray and a preparation process thereof, and relates to the field of delay sprays. The preparation process of the male product delayed spray comprises the following steps: S1, preparing water and ethanol, and uniformly stirring and mixing; s2, extracting fructus cnidii, herba epimedii, flos caryophylli, pericarpium zanthoxyli, herba cistanche, herba cynomorii and piper nigrum respectively; s3, obtaining a corresponding extract according to the step S2; s4, putting the obtained extract into water and an ethanol dissolving solution; s5, increasing the stirring speed, heating, and fully dissolving and mixing; s6, stopping stirring and cooling to room temperature; and S7, performing filling. According to the invention, the plant extract is adopted as an effective component, and the special pepper kava extract is selected, so that the irritation can be obviously reduced, the delay effect can be obviously improved, and the effects of reducing the skin sensitivity of the penis and improving the sexual intercourse time can be achieved by applying the plant extract to the skin surface of the male penis.

Description

Technical Field

[0001] The invention relates to the field of delayed ejaculation sprays, in particular to a delayed ejaculation spray for men and a preparation process thereof. Background Art

[0002] With the accelerated pace of modern life and the increase in pressure, male sexual dysfunction, especially premature ejaculation, has become a common health problem among men around the world. Premature ejaculation not only affects men's physical health, but may also have a negative impact on their mental state and partner relationship.

[0003] Existing male delay products are mainly divided into two categories: one is oral medication, the other is topical medication. Oral medications often contain chemically synthesized drug ingredients. Although they can achieve a certain delay effect, since the drugs need to be absorbed through the digestive tract, the onset time is relatively slow, and they may cause a certain burden on internal organs such as the liver and gastrointestinal tract. Some drugs may cause dependence or side effects after long-term use. Topical delay sprays can quickly achieve results through local use, but most of the existing topical sprays use chemical ingredients or highly irritating drugs, which may cause skin allergies or discomfort, and even cause irritation or burning in the genital area, resulting in a poor user experience. Summary of the invention

[0004] 1. Technical issues to be resolved

[0005] In view of the deficiencies in the prior art, the present invention provides a male product delay spray and a preparation process, which solves the problem that the traditional spray may cause irritation or burning sensation to the reproductive area.

[0006] (II) Technical solution

[0007] To achieve the above objectives, the present invention is implemented through the following technical solutions:

[0008] A preparation process of a male product delay spray comprises the following steps:

[0009] S1. Prepare water and ethanol, put them into a tank and stir to mix them evenly;

[0010] S2. extracting Cnidium monnieri, Epimedium, Clove, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and Piper methysticum respectively;

[0011] S3. According to step S2, Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Piper methysticum extract are obtained respectively;

[0012] S4. The Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Kava pepper extract were dissolved in water and ethanol;

[0013] S5. Increase the stirring speed and slightly increase the temperature to allow sufficient dissolution and mixing;

[0014] S6. Stop stirring and let the temperature drop to room temperature naturally;

[0015] S7. Filling the stirred material;

[0016] Through the above technical solutions and the design of these steps, the preparation process ensures precise control of each link, which not only improves the quality and efficacy of the delayed spray, but also optimizes the production process and ensures the stability and consistency of the ingredients.

[0017] Furthermore, in step S1, the water and ethanol are both 10-30 parts, in step S3, the Cnidium monnieri extract is 0.1-1 part, the Epimedium extract is 0.1-0.5 part, the Clove extract is 0.05-0.3 part, the Zanthoxylum bungeanum extract is 1-5 parts, the Cistanche deserticola extract is 0.1-2 parts, the Cynomorium songaricum extract is 0.01-0.05 parts, and the Piper methysticum chuanxiong extract is 0.3-2.5 parts;

[0018] Through the above technical solution, precise proportioning helps to adjust the efficacy of the product according to the role and function of each ingredient, while ensuring the consistency and stability of the product efficacy.

[0019] Furthermore, in step S2, cloves and kava are extracted by steam distillation, and cnidium monnieri, epimedium, Zanthoxylum bungeanum, Cistanche deserticola, and Cynomorium songaricum are extracted by ultrasonic extraction;

[0020] The steps of extracting cloves and kava pepper are:

[0021] 1) Extrusion crushing: Take cloves or kava pepper and crush them using a single screw extruder;

[0022] 2) Boiling and mixing: Take the crushed herbs, add distilled water and soak for 0.5-1 hour, then heat and boil to dehydrate;

[0023] 3) Membrane separation: After the extract is microfiltered, it is added to an ultrafiltration membrane system for ultrafiltration, and the permeate is then added to a nanofiltration membrane for nanofiltration. An equal amount of petroleum ether is added to the concentrate and allowed to stand for crystallization;

[0024] 4) Recrystallization: Filter out the crude crystals, dissolve them in anhydrous ethanol under reflux for 2-3 times, filter them out, and dry them at low temperature to obtain the product.

[0025] The steps of extracting the Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum are:

[0026] 1) Extrusion crushing: Take dried Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and other medicinal materials and crush them with a single screw extruder;

[0027] 2) Add water and mix: Add the individual herbs and water into the ultrasonic equipment;

[0028] 3) Ultrasonic extraction: Start the ultrasonic device for extraction and filtration to obtain extracts of Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and the like.

[0029] Through the above technical scheme, by using ultrasonic extraction method for Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum, the extraction efficiency can be improved, the time can be reduced, and the concentration and quality of the extract can be improved, while using steam distillation method for Clove and Kava can effectively retain the volatile components and enhance their activity in the spray.

[0030] Further, the rotation speed in step S1 is 45-60 rpm, the rotation speed in step S5 is 50-80 rpm, and the temperature is 40° C.-45° C.;

[0031] Through the above technical solution, the rotation speed in step S1 is 300-500rpm, so that water and ethanol can be better stirred evenly and the generation of bubbles can be avoided. The rotation speed in step S5 is 50-80rpm and the temperature is 40℃-45℃, which helps to improve the dissolution rate and uniformity. At the same time, the temperature is controlled within 40℃-45℃, which can promote the dissolution of components without causing thermal degradation.

[0032] Furthermore, a male delay spray is obtained according to any one of the preparation processes described above.

[0033] (III) Beneficial effects

[0034] The present invention provides a male product delay spray and a preparation process thereof. It has the following beneficial effects:

[0035] 1. The present invention provides a male product delay spray, which contains a variety of natural plant extracts, such as cnidium monnieri, epimedium, cloves, prickly ash, etc. These ingredients are widely used in traditional medicine to improve male sexual function and prolong the duration of sexual behavior. Through precise proportioning and reasonable extraction, the active ingredients of these natural ingredients help to prolong the performance time of men in sexual life. At the same time, prickly ash has a certain stimulating effect and helps to improve sensitivity; ingredients such as Cistanche deserticola and Cynomorium songaricum help to increase blood circulation and improve erectile function.

[0036] 2. The present invention provides a preparation process of a delayed ejaculation spray for men. The preparation process of the spray adopts a variety of natural plant extracts. These plant ingredients have high biological activity and can promote the improvement of male physiological functions without producing excessive side effects. The preparation process of the spray is relatively mild and can effectively avoid irritation to the skin and genitals.

[0037] 3. The present invention provides a male product delay spray, which uses plant extracts as active ingredients and selects special kava extracts, which can significantly reduce irritation and improve delay effects. By applying to the surface of the male penis skin, it can reduce the sensitivity of the penis skin and improve the duration of sexual intercourse. DETAILED DESCRIPTION

[0038] The technical solutions in the embodiments of the present invention are described clearly and completely below. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0039] Embodiment 1:

[0040] The present invention provides a preparation process of a male product delay spray, comprising the following steps:

[0041] S1. Prepare water and ethanol, put them into a tank and stir to mix them evenly;

[0042] S2. extracting Cnidium monnieri, Epimedium, Clove, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and Piper methysticum respectively;

[0043] S3. According to step S2, Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche extract, Cynomorium songaricum extract, and Piper methysticum extract are obtained respectively;

[0044] S4. The Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Kava pepper extract were dissolved in water and ethanol;

[0045] S5. Increase the stirring speed and slightly increase the temperature to allow sufficient dissolution and mixing;

[0046] S6. Stop stirring and let the temperature drop to room temperature

[0047] S7. Filling the stirred material;

[0048] Through the design of these steps, the preparation process ensures precise control of each link, which not only improves the quality and efficacy of the delayed spray, but also optimizes the production process and ensures the stability and consistency of the ingredients.

[0049] In step S1, water and ethanol are both 10-30 parts, in step S3, the Cnidium monnieri extract is 0.1-1 part, the Epimedium extract is 0.1-0.5 part, the Clove extract is 0.05-0.3 part, the Zanthoxylum bungeanum extract is 1-5 parts, the Cistanche deserticola extract is 0.1-2 parts, the Cynomorium songaricum extract is 0.01-0.05 parts, and the Piper methysticum extract is 0.3-2.5 parts. The precise proportioning helps to adjust the efficacy of the product according to the role and efficacy of each ingredient, while ensuring the consistency and stability of the product efficacy.

[0050] In step S2, cloves and kava are extracted by steam distillation, and cnidium monnieri, epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum are extracted by ultrasonic extraction;

[0051] The steps of extracting cloves and kava pepper are:

[0052] 1) Extrusion crushing: Take cloves or kava pepper and crush them using a single screw extruder;

[0053] 2) Boiling and mixing: Take the crushed herbs, add distilled water and soak for 0.5-1 hour, then heat and boil to dehydrate;

[0054] 3) Membrane separation: After the extract is microfiltered, it is added to an ultrafiltration membrane system for ultrafiltration, and the permeate is then added to a nanofiltration membrane for nanofiltration. An equal amount of petroleum ether is added to the concentrate and allowed to stand for crystallization;

[0055] 4) Recrystallization: Filter out the crude crystals, dissolve them in anhydrous ethanol under reflux for 2-3 times, filter them out, and dry them at low temperature to obtain the product.

[0056] The steps of extracting the Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum are:

[0057] 1) Extrusion crushing: Take dried Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and other medicinal materials and crush them with a single screw extruder;

[0058] 2) Add water and mix: Add the individual herbs and water into the ultrasonic equipment;

[0059] 3) Ultrasonic extraction: Start the ultrasonic device for extraction and filtration to obtain extracts of Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and the like.

[0060] By using ultrasonic extraction method to extract cnidium monnieri, epimedium, prickly ash, cistanche deserticola and cynomorium songaricum, the extraction efficiency can be improved, the time can be reduced, and the concentration and quality of the extract can be improved. By using steam distillation method to extract cloves and kava pepper, the volatile components can be effectively retained and their activity in the spray can be enhanced. The rotation speed in step S1 is 45-60 rpm, the rotation speed in step S5 is 50-80 rpm, and the temperature is 40° C.-45° C. The rotation speed in step S1 is 45-60 rpm, so that water and ethanol can be better stirred evenly and the generation of bubbles can be avoided. The rotation speed in step S5 is 50-80 rpm and the temperature is 40° C.-45° C., so that the dissolution speed and uniformity can be improved. At the same time, the temperature is controlled within 40° C.-45° C., so that the dissolution of components can be promoted without causing thermal degradation.

[0061] The male delay spray can be obtained according to any one of the above preparation processes.

[0062] Embodiment 2:

[0063] A preparation process of a male product delay spray, specifically comprising the following steps:

[0064] Step S1: prepare 5 kg of water and ethanol, put them into a stirring tank, start stirring, set the speed to 45-60 rpm, ensure that the water and ethanol are mixed evenly, and avoid the generation of bubbles;

[0065] Step S2: extracting the fructus cnidium, herba epimedii, clove, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum, and Piper methysticum salsa, the extraction method is the same as that in Example 1, but in this example, the extraction temperature is slightly adjusted. Fructus cnidium, herba epimedii, Zanthoxylum bungeanum, Cistanche deserticola, and Cynomorium songaricum are extracted by ultrasonic extraction, the extraction temperature is 50° C., and the extraction time is extended to 30 minutes to further improve the concentration and purity of the extract, and clove and Piper methysticum are still extracted by steam distillation to retain the activity of the volatile components;

[0066] Step S3: according to step S2, respectively obtain Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum bungeanum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Piper methysticum valerianum extract, and prepare 0.1 kg of Cnidium monnieri extract, 0.08 kg of Epimedium extract, 0.04 kg of Clove extract, 0.75 kg of Zanthoxylum bungeanum extract, 0.15 kg of Cistanche deserticola extract, 0.01 kg of Cynomorium songaricum extract, and 0.2 kg of Piper methysticum valerianum extract;

[0067] Step S4: placing various extracts into water and ethanol solutions and stirring to further enhance solubility and ensure solubility and uniform distribution of each component;

[0068] Step S5: increasing the stirring speed to 70 rpm, performing mild heating, and controlling the temperature between 42° C. and 48° C., by increasing the stirring speed and temperature, promoting the full dissolution and mixing of the components, while avoiding thermal degradation of the active ingredients caused by high temperature;

[0069] Step S6: stop stirring and let stand to room temperature to ensure the stability of the solution and the consistency of the ingredients;

[0070] Step S7: Filter the stirred solution to remove impurities and suspended matter, and then fill the clarified liquid.

[0071] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A preparation process of a male product delay spray, characterized in that: The following steps are involved: S1. Prepare water and ethanol, put them into a tank and stir to mix them evenly; S2. extracting Cnidium monnieri, Epimedium, Clove, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and Piper methysticum respectively; S3. According to step S2, Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Piper methysticum extract are obtained respectively; S4. The Cnidium monnieri extract, Epimedium extract, Clove extract, Zanthoxylum extract, Cistanche deserticola extract, Cynomorium songaricum extract, and Kava pepper extract were dissolved in water and ethanol; S5. Increase the stirring speed and slightly increase the temperature to allow sufficient dissolution and mixing; S6. Stop stirring and let the temperature drop to room temperature naturally; S7. Fill the mixed material.

2. The preparation process of the delayed ejaculation spray for male products according to claim 1, characterized in that: In step S1, water and ethanol are both 10-30 parts, in step S3, the Cnidium monnieri extract is 0.1-1 part, the Epimedium extract is 0.1-0.5 part, the Clove extract is 0.05-0.3 part, the Zanthoxylum bungeanum extract is 1-5 parts, the Cistanche deserticola extract is 0.1-2 parts, the Cynomorium songaricum extract is 0.01-0.05 parts, and the Piper methysticum chuanxiong extract is 0.3-2.5 parts.

3. The preparation process of the delayed ejaculation spray for male products according to claim 1, characterized in that: In step S2, cloves and kava are extracted by steam distillation, and cnidium monnieri, epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum are extracted by ultrasonic extraction.

4. The preparation process of the delayed ejaculation spray for male products according to claim 3, characterized in that: The steps of extracting cloves and kava pepper are: 1) Extrusion crushing: Take cloves or kava pepper and crush them using a single screw extruder; 2) Boiling and mixing: Take the crushed herbs, add distilled water and soak for 0.5-1 hour, then heat and boil to dehydrate; 3) Membrane separation: After the extract is microfiltered, it is added to an ultrafiltration membrane system for ultrafiltration, and the permeate is then added to a nanofiltration membrane for nanofiltration. An equal amount of petroleum ether is added to the concentrate and allowed to stand for crystallization; 4) Recrystallization: Filter out the crude crystals, dissolve them in anhydrous ethanol under reflux for 2-3 times, filter them out, and dry them at low temperature to obtain the product.

5. The preparation process of the delayed ejaculation spray for male products according to claim 3, characterized in that: The steps of extracting the Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola and Cynomorium songaricum are: 1) Extrusion crushing: Take dried Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and other medicinal materials and crush them with a single screw extruder; 2) Add water and mix: Add the individual herbs and water into the ultrasonic equipment; 3) Ultrasonic extraction: Start the ultrasonic device for extraction and filtration to obtain extracts of Cnidium monnieri, Epimedium, Zanthoxylum bungeanum, Cistanche deserticola, Cynomorium songaricum and the like.

6. The preparation process of the delayed ejaculation spray for male products according to claim 1, characterized in that: The rotation speed in step S1 is 45-60 rpm, the rotation speed in step S5 is 50-80 rpm, and the temperature is 40° C.-45° C.

7. A male delay spray is obtained according to the preparation process described in any one of claims 1 to 4.