Daily chemical essence and preparation method thereof

Abstract

The invention relates to the technical field of essence, and particularly discloses daily chemical essence and a preparation method thereof.The daily chemical essence is prepared from, by mass, 35-50 parts of fixative; 45-70 parts of a composite perfume; 5.6-16 parts of compound vegetable oil; the compound spice is a compound of carrageenal, Shumule, methyl dihydrojasmonate and commisinone; the compound vegetable oil is compounded by frankincense oil, cypress oil, lemon oil, guaiacol, patchouli oil, sweet orange oil and vetiver oil. The invention has the advantage of reducing the harm of daily chemical essence to human body.

Description

Technical Field

[0001] The present invention relates to the field of flavors, in particular to a daily chemical flavor and a preparation method thereof. Background Art

[0002] As a key fragrance enhancer for daily chemical products, the quality and composition of daily chemical fragrances are of great concern. Currently, most daily chemical fragrances on the market are made entirely from synthetic raw materials. While these fragrances can quickly create rich aromas at a manageable cost, they also have significant drawbacks. Some chemical residues can be absorbed through the skin through daily use, causing irritation and potential damage. At the same time, consumer demand for natural, green daily chemical products is exploding, and fragrances made solely from synthetic raw materials are unable to meet this demand. Therefore, there is room for improvement. Summary of the Invention

[0003] In order to reduce the harm of daily chemical fragrances to the human body, the present application provides a daily chemical fragrance and a preparation method thereof.

[0004] In the first aspect, the present application provides a daily chemical fragrance, which adopts the following technical solution: A daily chemical flavor, comprising the following components in parts by weight: 35-50 parts of fixative; 45-70 parts of compound spices; 5.6-16 parts of compound vegetable oil; The compound fragrance is a mixture of caramel aldehyde, sulphur aldehyde, methyl dihydrojasmonate and cashmeran ketone; The composite vegetable oil is a compound of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil and vetiver oil.

[0005] By adopting the above technical scheme, the pure woody fougere fragrance is precisely formulated by compounding the compound spices of caramel aldehyde, shumoufu, methyl dihydrojasmonate and cashmeran ketone. By compounding the compound plant oils of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil and vetiver oil, the unique aroma layer of fruity, floral and woody fragrances is restored. It is unique among the many daily chemical fragrances, meets consumers' demand for personalized and high-quality fragrance, and enriches the fragrance category of natural daily chemical fragrances.

[0006] And because of the addition of compound vegetable oil, it can significantly reduce irritation, making it less likely for daily chemical fragrances to cause skin irritation after contact with the skin, thereby reducing the damage to the skin caused by daily chemical fragrances. In addition, compound vegetable oil can have a significant soothing effect, which can help the skin relax and make the skin more comfortable and healthy.

[0007] Since the use of chemical synthetic raw materials is reduced, environmental pollution and other problems caused by chemical synthetic raw materials are reduced to a certain extent, making daily chemical fragrances more environmentally friendly.

[0008] Preferably, in the composite vegetable oil, the mass ratio of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil and vetiver oil is 5-10:0.1-1:0.1-1:0.1-1:0.1-1:0.1-1:0.1-1.

[0009] By adopting the above technical solution and specifically selecting the mass ratios of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil, the effect of restoring the unique aroma layers of fruity, floral, and woody aromas interwoven with each other is better, and the effects of reducing irritation and soothing the skin brought about by the specific proportions of the plant oils are more significant, which is more beneficial to human health.

[0010] Preferably, in the composite fragrance, the mass ratio of caramel aldehyde, schumofuran, methyl dihydrojasmonate, and cashmeran ketone is 5-10:5-10:30-40:5-10.

[0011] By adopting the above technical solution and specifically selecting the mass ratio of caramel aldehyde, schumofo, methyl dihydrojasmonate and cashmeran ketone, the effect of accurately blending the pure woody fougere fragrance is better and the aroma is more realistic.

[0012] Preferably, the fixative is a compound of ambergris ketone and cyclopentadecenolide.

[0013] By adopting the above technical solution and specifically selecting ambergris ketone and cyclopentadecenolide as the fixative, the fixative effect is better and the product quality is better.

[0014] Preferably, in the fixative, the mass ratio of ambergris ketone to cyclopentadecenolide is 30-40:5-10.

[0015] By adopting the above technical solution and specifically selecting the mass ratio of ambergris ketone and cyclopentadecenolide, the fragrance fixing effect is more significant and the quality of the essence is better.

[0016] In a second aspect, the present application provides a method for preparing a daily chemical fragrance, which adopts the following technical solution: A method for preparing the above-mentioned daily chemical fragrance comprises the following steps: Step 1) frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed to obtain a composite vegetable oil; Step 2) karafenaldehyde, shumufu, methyl dihydrojasmonate, and cashmeran ketone are mixed to obtain a composite fragrance, and the composite fragrance is then added to the composite vegetable oil and mixed uniformly to obtain a premix; Step 3), adding a fixative to the premix and mixing evenly to obtain a daily chemical essence.

[0017] By adopting the above technical solution, the prepared daily chemical fragrance has a pure woody fougère fragrance and restores the unique aroma layering of fruity, floral and woody aromas, which can well meet consumers' demand for personalized and high-quality fragrance.

[0018] Preferably, in step 1), frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed at 88-92°C.

[0019] By adopting the above technical solution, frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed at 88-92°C, so that the active ingredients in the plant oils cooperate with each other at high temperature, thereby exerting significant synergistic effects, making it more significant to reduce the irritation of the fragrance and provide skin soothing effects.

[0020] Preferably, in step 1), frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed at 88-92° C. for 55-65 minutes.

[0021] By adopting the above technical solution and mixing at 88-92° C. for 55-65 minutes, the synergistic effect of the active ingredients in each vegetable oil is improved, the irritation of the fragrance is reduced, and the skin soothing effect is better.

[0022] In summary, this application has the following beneficial effects: 1. This application uses a compound fragrance of caramel aldehyde, shumufu, methyl dihydrojasmonate, and cashmeran to accurately formulate a pure woody fougère fragrance, and uses a compound plant oil of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil to restore a unique aroma layer of fruity, floral, and woody fragrances. It is unique among many daily chemical fragrances, meets consumers' demand for personalized, high-quality fragrances, and enriches the fragrance category of natural daily chemical fragrances.

[0023] 2. In this application, it is preferred to add compound vegetable oil. Under the action of the compound vegetable oil, it can significantly reduce the irritation, so that the daily chemical fragrance is not likely to cause skin irritation after contacting the skin, thereby reducing the situation where the daily chemical fragrance causes skin damage. In addition, the compound vegetable oil can have a significant soothing effect, which can help the skin relax and make the skin more comfortable and healthy.

[0024] 3. In the present application, the specific mass ratios of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are preferably selected to restore the unique aroma layering of fruity, floral, and woody aromas. Moreover, the effects of reducing irritation and soothing the skin brought about by the combination of the plant oils in specific proportions are more significant, which is more beneficial to human health. DETAILED DESCRIPTION

[0025] The present application is further described in detail below with reference to the embodiments.

[0026] Example 1 A daily chemical essence, wherein the preparation method of the daily chemical essence comprises the following steps: Step 1) 5 kg of frankincense oil, 0.1 kg of cypress oil, 0.1 kg of lemon oil, 0.1 kg of guaiac oil, 0.1 kg of patchouli oil, 0.1 kg of sweet orange oil, and 0.1 kg of vetiver oil are placed in a stirred tank, heated and kept at 88° C., at a speed of 60 r / min, stirred for 55 minutes, and cooled to room temperature to obtain a composite vegetable oil; Step 2), 5kg of caramel aldehyde, 5kg of schumofu, 30kg of methyl dihydrojasmonate, and 5kg of cashmeran ketone are put into another stirred tank, the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a composite fragrance, and then all the composite fragrances are added to the composite vegetable oil in step 1), the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a premix.

[0027] Step 3), add 30kg of ambergris ketone and 5kg of cyclopentadecenolide to the premix, rotate at 80r / min, stir for 20min, mix evenly, and obtain daily chemical essence.

[0028] Frankincense oil was purchased from Wuhan Kanos Technology Co., Ltd.

[0029] Cypress oil was purchased from Jiangxi Chuanhui Herbal Biotechnology Co., Ltd.

[0030] Lemon oil was purchased from Wuhan Proloff Biotechnology Co., Ltd.

[0031] Guaiac wood oil was purchased from Wuhan Lanabai Pharmaceutical Chemical Co., Ltd.

[0032] Patchouli oil was purchased from Hunan Honghua Jinjia Ecological Environment Engineering Co., Ltd.

[0033] Sweet orange oil was purchased from Hubei Xingdongcheng Chemical Co., Ltd.

[0034] Vetiver oil was purchased from Shanghai Jiulin Industrial Co., Ltd.

[0035] Kara flower aldehyde was purchased from Hubei Zhonglong Kangsheng Fine Chemical Co., Ltd.

[0036] Shu Moufu purchased Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0037] Methyl dihydrojasmonate was purchased from Wuhan Jixin Yibang Biotechnology Co., Ltd.

[0038] Cashmeran ketone was purchased from Hubei Kemaidi Chemical Co., Ltd.

[0039] Ambergris ketone was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0040] Cyclopentadecenolide was purchased from Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0041] Example 2 A daily chemical essence, wherein the preparation method of the daily chemical essence comprises the following steps: Step 1) 7.5 kg of frankincense oil, 0.5 kg of cypress oil, 0.5 kg of lemon oil, 0.5 kg of guaiac oil, 0.5 kg of patchouli oil, 0.5 kg of sweet orange oil, and 0.5 kg of vetiver oil are placed in a stirred tank, heated and kept at 90° C., at a speed of 60 r / min, stirred for 60 minutes, and cooled to room temperature to obtain a composite vegetable oil; Step 2), 7.5kg of caramel aldehyde, 7.5kg of schumofu, 35kg of methyl dihydrojasmonate, and 7.5kg of cashmeran ketone are put into another stirred tank, the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a composite fragrance, and then all the composite fragrances are added to the composite vegetable oil in step 1), the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a premix.

[0042] Step 3), add 35kg of ambergris ketone and 7.5kg of cyclopentadecenolide to the premix, rotate at 80r / min, stir for 20min, mix evenly, and obtain daily chemical essence.

[0043] Frankincense oil was purchased from Wuhan Kanos Technology Co., Ltd.

[0044] Cypress oil was purchased from Jiangxi Chuanhui Herbal Biotechnology Co., Ltd.

[0045] Lemon oil was purchased from Wuhan Proloff Biotechnology Co., Ltd.

[0046] Guaiac wood oil was purchased from Wuhan Lanabai Pharmaceutical Chemical Co., Ltd.

[0047] Patchouli oil was purchased from Hunan Honghua Jinjia Ecological Environment Engineering Co., Ltd.

[0048] Sweet orange oil was purchased from Hubei Xingdongcheng Chemical Co., Ltd.

[0049] Vetiver oil was purchased from Shanghai Jiulin Industrial Co., Ltd.

[0050] Kara flower aldehyde was purchased from Hubei Zhonglong Kangsheng Fine Chemical Co., Ltd.

[0051] Shu Moufu purchased Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0052] Methyl dihydrojasmonate was purchased from Wuhan Jixin Yibang Biotechnology Co., Ltd.

[0053] Cashmeran ketone was purchased from Hubei Kemaidi Chemical Co., Ltd.

[0054] Ambergris ketone was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0055] Cyclopentadecenolide was purchased from Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0056] Example 3 A daily chemical essence, wherein the preparation method of the daily chemical essence comprises the following steps: Step 1) 10 kg of frankincense oil, 1 kg of cypress oil, 1 kg of lemon oil, 1 kg of guaiac oil, 1 kg of patchouli oil, 1 kg of sweet orange oil, and 1 kg of vetiver oil are placed in a stirred tank, heated and kept at 92° C., at a speed of 60 r / min, stirred for 65 minutes, and cooled to room temperature to obtain a composite vegetable oil; Step 2), 10kg of caramel aldehyde, 10kg of shumufu, 40kg of methyl dihydrojasmonate, and 10kg of cashmeran ketone are put into another stirred tank, the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a composite fragrance, and then all the composite fragrance is added to the composite vegetable oil in step 1), the speed is 120r / min, stirred for 15min, and mixed evenly to obtain a premix.

[0057] Step 3), add 40kg of ambergris ketone and 10kg of cyclopentadecenolide to the premix, rotate at 80r / min, stir for 20min, mix evenly, and obtain daily chemical essence.

[0058] Frankincense oil was purchased from Wuhan Kanos Technology Co., Ltd.

[0059] Cypress oil was purchased from Jiangxi Chuanhui Herbal Biotechnology Co., Ltd.

[0060] Lemon oil was purchased from Wuhan Proloff Biotechnology Co., Ltd.

[0061] Guaiac wood oil was purchased from Wuhan Lanabai Pharmaceutical Chemical Co., Ltd.

[0062] Patchouli oil was purchased from Hunan Honghua Jinjia Ecological Environment Engineering Co., Ltd.

[0063] Sweet orange oil was purchased from Hubei Xingdongcheng Chemical Co., Ltd.

[0064] Vetiver oil was purchased from Shanghai Jiulin Industrial Co., Ltd.

[0065] Kara flower aldehyde was purchased from Hubei Zhonglong Kangsheng Fine Chemical Co., Ltd.

[0066] Shu Moufu purchased Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0067] Methyl dihydrojasmonate was purchased from Wuhan Jixin Yibang Biotechnology Co., Ltd.

[0068] Cashmeran ketone was purchased from Hubei Kemaidi Chemical Co., Ltd.

[0069] Ambergris ketone was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.

[0070] Cyclopentadecenolide was purchased from Hubei Xinjiecheng Chemical Technology Co., Ltd.

[0071] Comparative Example 1 A daily chemical essence, compared with Example 2, the only difference is: Replace frankincense oil with an equal amount of rice bran oil.

[0072] Rice bran oil was purchased from Jianmin Natural Spice Oil Factory in Jishui County.

[0073] Comparative Example 2 A daily chemical essence, compared with Example 2, the only difference is: Replace cypress oil with hazelnut oil in equal amounts.

[0074] Hazelnut oil was purchased from the Hongxing Natural Medicinal Spice Oil Factory in Jishui County.

[0075] Comparative Example 3 A daily chemical essence, compared with Example 2, the only difference is: Replace lemon oil with an equal amount of peony seed oil.

[0076] Peony seed oil was purchased from Jianmin Natural Spice Oil Factory in Jishui County.

[0077] Comparative Example 4 A daily chemical essence, compared with Example 2, the only difference is: Replace guaiac wood oil with an equal amount of perilla seed oil.

[0078] Perilla seed oil was purchased from Hubei Xinghengye Technology Co., Ltd.

[0079] Comparative Example 5 A daily chemical essence, compared with Example 2, the only difference is: Replace the patchouli oil with an equal amount of sea buckthorn oil.

[0080] Sea buckthorn oil was purchased from Yikang Natural Spice Oil Refinery in Jishui County.

[0081] Comparative Example 6 A daily chemical essence, compared with Example 2, the only difference is: Replace the sweet orange oil with an equal amount of black pepper oil.

[0082] Black pepper oil was purchased from Ji'an Zhongda Natural Plant Spice Co., Ltd.

[0083] Comparative Example 7 A daily chemical essence, compared with Example 2, the only difference is: Replace vetiver oil with an equal amount of oregano oil.

[0084] Oregano oil was purchased from Hubei Weideli Chemical Reagent Co., Ltd.

[0085] Comparative Example 8 A daily chemical essence, compared with Example 2, the only difference is: Replace frankincense oil with an equal amount of rice bran oil, replace cypress oil with an equal amount of hazelnut oil, replace lemon oil with an equal amount of peony seed oil, replace guaiac wood oil with an equal amount of perilla seed oil, replace patchouli oil with an equal amount of sea buckthorn oil, replace sweet orange oil with an equal amount of black pepper oil, and replace vetiver oil with an equal amount of oregano oil.

[0086] Rice bran oil was purchased from Jianmin Natural Spice Oil Factory in Jishui County.

[0087] Hazelnut oil was purchased from the Hongxing Natural Medicinal Spice Oil Factory in Jishui County.

[0088] Peony seed oil was purchased from Jianmin Natural Spice Oil Factory in Jishui County.

[0089] Perilla seed oil was purchased from Hubei Xinghengye Technology Co., Ltd.

[0090] Sea buckthorn oil was purchased from Yikang Natural Spice Oil Refinery in Jishui County.

[0091] Black pepper oil was purchased from Ji'an Zhongda Natural Plant Spice Co., Ltd.

[0092] Oregano oil was purchased from Hubei Weideli Chemical Reagent Co., Ltd.

[0093] Experiment 1 According to T / JSRH 003-2023 "Hyaluronidase Inhibition Method for Anti-allergic Activity Test of Cosmetic Raw Materials", the hyaluronidase inhibition rate (%) of the test samples prepared from the daily chemical fragrances of each embodiment and comparative example was tested.

[0094] Test sample: 1g daily chemical essence, 99g white mineral oil, mix well.

[0095] Experiment 2 Chicken embryo test: The irritation score IS of the daily chemical fragrances of each embodiment and comparative example was tested according to SNT 2329-2009 "Chicken embryo chorioallantoic membrane test for eye irritation / corrosion of cosmetics".

[0096] IS<1: non-irritating.

[0097] 1≤IS<5: mild irritation.

[0098] 5≤IS<9: moderate irritation.

[0099] IS ≥ 10: Strong irritant / corrosive.

[0100] The specific experimental data of Experiment 1-2 are shown in Table 1 Table 1 According to the data comparison of each embodiment and comparative example in Table 1, it can be seen that the irritation of each embodiment is significantly lower than that of each comparative example, and the hyaluronidase inhibition rate of each embodiment is significantly higher than that of each comparative example. It can be seen that adding a composite plant oil of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil to the chemically synthesized flavor can not only further improve the richness of the flavor, but also reduce the irritation of the flavor, and have a certain soothing effect, reducing the impact of long-term use on human skin. Although other plant extracts are added to the comparative examples, although they can also improve the richness of the flavor, the effects of reducing irritation and providing skin soothing effect are relatively general, significantly worse than those of the embodiments. Long-term use can easily cause damage to human skin.

[0101] This specific embodiment is merely an explanation of the present application and is not a limitation of the present application. After reading this specification, those skilled in the art may make non-creative modifications to the present embodiment as needed, but as long as they are within the scope of the claims of the present application, they are protected by the patent law.

Claims

1. A daily chemical fragrance, characterized by: The composition includes the following parts by weight: 35-50 parts of fixative; 45-70 parts of compound spices; 5.6-16 parts of compound vegetable oil; The compound fragrance is a mixture of caramel aldehyde, sulphur, methyl dihydrojasmonate and cashmeran ketone; The composite vegetable oil is a compound of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil and vetiver oil.

2. A daily chemical fragrance according to claim 1, characterized in that: In the composite vegetable oil, the mass ratio of frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil and vetiver oil is 5-10: 0.1-1：0.1-1：0.1-1：0.1-1：0.1-1：0.1-1。 3. A daily chemical fragrance according to claim 2, characterized in that: In the composite fragrance, the mass ratio of caramel aldehyde, schumofuran, methyl dihydrojasmonate and cashmeran ketone is 5-10:5-10:30-40:5-10.

4. A daily chemical fragrance according to any one of claims 1 to 3, characterized in that: The fixative is a compound of ambergris ketone and cyclopentadecenolide.

5. A daily chemical fragrance according to claim 4, characterized in that: In the fixative, the mass ratio of ambergris ketone to cyclopentadecenolide is 30-40:5-10.

6. A method for preparing a daily chemical flavor according to any one of claims 1 to 5, characterized in that: The following steps are involved: Step 1) frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed to obtain a composite vegetable oil; Step 2) mixing caramel aldehyde, shumufu, methyl dihydrojasmonate, and cashmeran ketone to obtain a composite fragrance, and then adding the composite fragrance to the composite vegetable oil and mixing uniformly to obtain a premix; Step 3) Add a fixative to the premix and mix well to obtain a daily fragrance.

7. The method for preparing a daily chemical fragrance according to claim 6, wherein: In the step 1), frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed at 88-92°C.

8. The method for preparing a daily chemical fragrance according to claim 7, wherein: In the step 1), frankincense oil, cypress oil, lemon oil, guaiac oil, patchouli oil, sweet orange oil, and vetiver oil are mixed at 88-92° C. for 55-65 minutes.

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