Method for manufacturing silicon nitride substrate

The production of silicon nitride substrates using a composite powder of metal silicon and silicon nitride powders, combined with sintering aids, achieves uniform nitridation, addressing rapid reaction issues and enhancing thermal conductivity and mechanical properties, thus meeting the demands of power devices.

JP7792552B1Active Publication Date: 2025-12-25JSG JAPAN CO LTD
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Patent Information

Application Number
JP2025505534
Authority / Receiving Office
JP · JP
Patent Type
Patents
Current Assignee / Owner
Priority Date
2024-07-03
Filing Date
2024-10-28
Publication Date
2025-12-25
Estimated Expiration
2044-10-28

AI Technical Summary

Technical Problem

Conventional methods for producing silicon nitride substrates face issues with rapid nitriding reactions of silicon powder, leading to heat generation, non-uniform reactions, and the inability to achieve high thermal conductivity and mechanical properties simultaneously, which are crucial for power device applications.

Method used

A method involving the use of a composite powder formed by mixing metal silicon powder and silicon nitride powder, followed by pulverization, and subsequent steps of mixing with a sintering aid and dispersion medium to form a sheet, which is then nitrided and sintered to produce a silicon nitride substrate, utilizing a mechanochemical effect to achieve uniform nitridation and prevent rapid reactions.

Benefits of technology

The method results in a silicon nitride substrate with high heat dissipation properties and excellent mechanical properties, overcoming the limitations of conventional methods by reducing production costs and ensuring uniform nitridation.

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Abstract

A method for producing a silicon nitride substrate that has high heat dissipation and excellent mechanical properties by preventing a rapid nitridation reaction of silicon and achieving a uniform nitridation reaction includes the following steps: a first step of mixing metal silicon powder and silicon nitride powder and pulverizing the mixture to form a composite powder; a second step of mixing the composite powder with a sintering aid and a dispersing medium to form a sheet-forming slurry in which the sintering aid is dispersed in the composite powder; a third step of molding the sheet-forming slurry to form a sheet; a fourth step of heating the sheet at 250 to 600°C to degrease the resin component to form a degreased sheet; a fifth step of heating the degreased sheet at 1200 to 1500°C to nitride the silicon contained in the sheet to form a nitrided sheet; and a sixth step of sintering the nitrided sheet to form a silicon nitride substrate, wherein the composite powder is formed by adsorption of metal silicon particles and silicon nitride particles.
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