Emulsifier/detergent compounds for metalworking lubricants
a technology of emulsifiers and detergents, applied in the field of emulsifiers and detergent compositions, can solve the problems of limited cooling capacity, difficult and costly disposal of chlorine, and limited cooling capacity, and achieve the effect of superior emulsification properties
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[0086] Outline of Method—The heptane sulfonic acid from the above procedure is neutralized with sodium hydroxide. The neutralized reaction mass is settled and the brine layer is removed. The neutral sodium sulfonate solution is then heated and the heptane is removed via distillation. This procedure yields a product of this invention, a sodium sulfonate.
[0087] Procedure—A known, measured and analyzed amount of heptane sulfonic acid solution is charged to a suitable vessel. Mixing is begun and water and / or methanol is added to the sulfonic acid mixture. The amount of water required is approximately five percent (5%) based upon the weight of the heptane sulfonic acid charged. Mixing is continued for 15 minutes after the water addition and, then the acid is neutralized with sodium hydroxide / water solution. The concentration of the sodium hydroxide solution is not critical and concentrations up to 50 percent (50%) sodium hydroxide can be utilized. The amount of sodium h...
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