Ligands for Corrosion Stability Chromatography

By introducing multiple Staphylococcus A protein domains into the chromatographic analysis ligand and performing amino acid mutations, the problem of insufficient stability of the existing ligand in alkaline cleaning was solved, and the effect of maintaining efficient binding ability in high-concentration NaOH solution was achieved, which is suitable for low-cost and efficient purification of immunoglobulins.

CN115073568BActive Publication Date: 2025-09-16EMD MILLIPORE CORP
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Patent Information

Application Number
CN202210554191.0
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Priority Date
2008-12-24
Filing Date
2009-12-23
Publication Date
2025-09-16
Estimated Expiration
2029-12-23

AI Technical Summary

Technical Problem

Existing chromatographic analysis ligands based on Staphylococcus A protein are not stable enough when cleaned under alkaline conditions, resulting in a decrease in binding ability, affecting purification efficiency and cost.

Method used

A ligand for alkaline-stable chromatographic analysis has been developed, which contains multiple Staphylococcus A protein domains or their functional fragments. The alkaline resistance of the ligand is improved by attaching it to the resin at multiple points and performing amino acid mutations, for example, introducing a specific amino acid mutation at position 24 to enhance stability.

Benefits of technology

The stability of the ligand is significantly improved in an alkaline environment, and the efficient binding ability is maintained. It is suitable for low-cost and efficient purification of immunoglobulins and can be used for a long time in high-concentration NaOH solution without losing function.

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Abstract

The present invention relates to chromatographic ligands having improved corrosion stability, such as ligands based on immunoglobulin binding proteins, such as Staphylococcus protein A, and methods of making and using the same.
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