A processing device for producing high-viscosity floating oil rosin and a method thereof
By setting an alternating guide plate structure of the purification cylinder and condenser in the inner cylinder and hollow cavity of the floating oil rosin processing device, the problem of poor condensation effect of the condenser is solved, the production of high viscosity floating oil rosin is realized, and the product quality is improved.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2022-11-18
- Publication Date
- 2026-03-17
AI Technical Summary
In existing processes for processing floating rosin, the condensation effect of the condenser is affected by air adhesion, resulting in low viscosity of the floating rosin. Furthermore, existing vacuum distillation equipment cannot effectively improve its viscosity.
A processing device was designed, including a purification cylinder and a condensation mechanism. The purification cylinder is equipped with an inner cylinder and a hollow chamber. The burner heats the outer wall of the inner cylinder. The air after combustion is filtered through a filter cylinder. An agitator is installed inside the inner cylinder. The condenser adopts an alternating guide plate and lifting plate structure. The cooling medium circulates and condenses, avoiding air accumulation and improving the condensation effect.
Through multiple vacuum distillations, high-viscosity floating oil rosin was produced, with excellent condensation effect, avoiding the influence of air adhesion and improving product quality.
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Figure CN115920778B_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the field of floating oil rosin processing technology, specifically to a processing apparatus and method for producing high-viscosity floating oil rosin. Background Technology
[0002] Tall rosin, also known as tall oil rosin or rosin oil resin, is derived from the wood pulping and papermaking industry. It is obtained by processing black liquor recovered from sulfate pulping. Typically, rosin is esterified with polyols such as glycerol and pentaerythritol under high temperature and in the presence of a catalyst (usually 230°C–300°C) to obtain rosin resin. To improve esterification efficiency, the catalyst usually contains esterification catalysts. To reduce the color of the rosin resin, the catalyst usually also contains decolorizing catalysts, such as organosulfur compounds. Existing tall oil rosin processing methods still produce rosin with residual moisture, resulting in a lower viscosity.
[0003] The purification of floating rosin requires the use of vacuum distillation equipment. Existing vacuum distillation equipment includes distillers, condensers, recovery tanks, vacuum pumps, etc. Among them, there are various types of condensers, and the condensation effect of the condenser directly affects the quality of floating rosin. During the circulation of the cooling medium, when air enters the condenser, the gas tends to stick to the surface of the heat exchange capillary tube, affecting the condensation effect of floating rosin. Therefore, to address the above problems, a processing device and method for producing high-viscosity floating rosin are proposed. Summary of the Invention
[0004] The present invention aims to provide a processing apparatus and method for producing high-viscosity floating rosin. The processing apparatus includes a purification cylinder with an inner cylinder inside. A hollow cavity exists between the inner cylinder and the outer wall of the purification cylinder. When the burner head in the combustion base burns, the flame burns along the outer wall of the inner cylinder, accelerating the heating of the floating rosin inside. The air after combustion enters a filter cylinder, where a filter element filters the combustion exhaust gas, achieving a good environmental protection effect. The heat exchanger chamber in the processing apparatus has alternating lower and upper guide plates. A water guide groove is provided at the top of the lower guide plate and at the bottom of the upper guide plate. The top of the heat exchanger chamber is equipped with... The device features a vertically movable lifting plate that, when lowered, fits against the top of the upper guide plate. As the lifting plate rises, the cooling medium enters the heat exchange chamber and fills it sequentially from right to left. Due to the gap between the upper guide plate and the lifting plate, the cooling medium can fill the entire heat exchange chamber, expelling the air accumulated between the upper guide plates. The air exits through the outlet pipe at the top of the heat exchange chamber. When the cooling medium level rises to the middle of the outlet pipe, it flows back into the cooling tank through the return pipe, achieving circulation of the cooling medium. This heat exchanger exhibits excellent condensation performance and effectively prevents air accumulation within the heat exchanger, which would affect the condensation of floating rosin, thus solving the problems mentioned in the background art.
[0005] To achieve the above objectives, the present invention provides the following technical solution:
[0006] A processing apparatus for producing high-viscosity floating rosin includes:
[0007] The purification cylinder has an inner cylinder inside, and a hollow cavity is provided between the inner cylinder and the outer wall of the purification cylinder. A gas pipe is provided at the top of the hollow cavity, extending out of the purification cylinder, and a filter cylinder is provided on the gas pipe. A filter element is fixedly provided on the top plate inside the filter cylinder, and the exhaust port at the top of the filter element extends upward out of the filter cylinder. An exhaust pipe connected to the inner cylinder is provided at the top of the purification cylinder.
[0008] The condensation mechanism connected to the exhaust pipe includes a heat exchanger and a cooling box. Inside the heat exchanger, from left to right, are an inlet chamber, a heat exchange chamber, and a discharge chamber. The exhaust pipe extends into the inlet chamber. A heat exchange capillary tube runs through the heat exchange chamber between the inlet chamber and the discharge chamber. Inside the heat exchange chamber, lower and upper guide plates are alternately arranged. A water guide groove is located at the top of the lower guide plate, and a water guide groove is located at the bottom of the upper guide plate. A vertically movable lifting plate is located at the top of the heat exchange chamber. After the lifting plate descends, it fits against the top of the upper guide plate. Sealing strips are provided on the edge of the lifting plate and the top edge of the upper guide plate. A water inlet pipe is provided at the bottom left end of the heat exchange chamber, which connects to the outlet of the cooling box. A circulation pump is installed on the water inlet pipe. A telescopic pipe is provided at the left end of the lifting plate, which connects to the top plate of the heat exchange chamber. A discharge pipe extending upwards out of the heat exchanger is provided at the top of the telescopic pipe. A tee is provided in the middle of the discharge pipe, and a return pipe connecting to the inlet of the cooling box is provided at the outer pipe end of the tee.
[0009] Preferably, it also includes a heating mechanism located at the bottom of the purification cylinder. The heating mechanism includes a docking cylinder and a combustion base arranged sequentially from top to bottom. A combustion head is provided on the top panel of the combustion base, and the gas pipe of the combustion head extends out of the combustion base. An electric gas flow regulating valve is provided on the gas pipe. The docking cylinder is connected to the hollow cavity.
[0010] Preferably, a purification tube extending to the left is provided on the left side panel at the bottom of the inner cylinder of the purification cylinder, and a manhole extending downward into the inner cylinder is provided on the top panel of the purification cylinder. Both the manhole and the purification tube are provided with sealing end caps.
[0011] Preferably, an installation cylinder is provided in the middle of the top panel of the purification cylinder, and a stirring shaft is provided inside the installation cylinder and rotatably connected to the inner wall of the installation cylinder through a sealed bearing. A stirrer is provided at the bottom of the stirring shaft and extends into the inner cylinder. A stirring motor is fixedly provided in the middle of the top panel of the purification cylinder, and the motor shaft of the stirring motor is connected to the stirring shaft through a coupling.
[0012] Preferably, an electric push rod is fixedly installed on the top plate of the heat exchanger, and the telescopic rod of the electric push rod is connected to the lifting plate.
[0013] Preferably, mounting slots are provided on both the front and rear side panels of the cooling box, and both the front and rear side panels of the cooling box are made of aluminum heat-conducting plates. A semiconductor cooling chip is fixedly installed inside the mounting slot, and a heat sink is installed on the hot end of the semiconductor cooling chip.
[0014] Preferably, a discharge pipe extending out of the heat exchanger is provided on the bottom right side of the discharge chamber. The discharge pipe is connected to the collection tank, and a vacuum pump is provided on the top plate of the collection tank, with the suction pipe of the vacuum pump extending into the collection tank.
[0015] A method for producing high-viscosity floating oil rosin, characterized by comprising the following steps:
[0016] S1. Add the floating rosin into the purification cylinder, turn on the electric gas flow regulating valve to introduce the mixed gas into the burner and ignite it, heat the temperature of the floating rosin inside the purification cylinder to between 250-260℃, at the same time, turn on the vacuum pump to make the inside of the purification cylinder a vacuum of 5mmHg, control the condensation temperature of the heat exchanger, collect the fraction above 180℃, and obtain fraction A.
[0017] S2. Empty the residue inside the purification cylinder, then add fraction A into the purification cylinder, add decolorizing agent and antioxidant to fraction A in sequence, and at the same time purge with protective gas. Stir the reaction with a stirrer at a temperature of 210-250℃ for 2-3 hours.
[0018] S3. After completing step S2, raise the temperature of the purification cylinder to 240-260℃, and at the same time turn on the vacuum pump to make the vacuum degree inside the purification cylinder 5mmHg, and carry out vacuum distillation to collect the fraction above 190℃ to obtain refined floating rosin.
[0019] S4. The refined floating rosin is put back into the purification cylinder, the temperature of the purification cylinder is raised to 110-180℃, and the vacuum pump is turned on to make the vacuum degree inside the purification cylinder 5mmHg. Reduced pressure distillation is carried out, and the fraction below 180℃ is collected to obtain high viscosity floating rosin.
[0020] Compared with the prior art, the beneficial effects of the present invention are:
[0021] 1. By setting up a purification cylinder, an inner cylinder is set inside the purification cylinder, and a hollow cavity is left between the inner cylinder and the outer wall of the purification cylinder. When the burner in the combustion base burns, the flame burns along the outer wall of the inner cylinder, which can accelerate the heating of the floating oil and rosin inside the inner cylinder. The air after combustion enters the filter cylinder, and the filter element set inside the filter cylinder can filter the combustion exhaust gas, which can achieve a good environmental protection effect.
[0022] 2. After high-temperature negative pressure distillation, the mixed gas released from the floating rosin is introduced into a heat exchanger for condensation. The refrigerant for the heat exchanger is supplied by a cooling box. The heat exchanger chamber is equipped with alternating lower and upper guide plates. A water guide groove is located at the top of the lower guide plate, and a water guide groove is located at the bottom of the upper guide plate. A vertically movable lifting plate is installed at the top of the heat exchange chamber. When the lifting plate descends, it contacts the top of the upper guide plate. When the lifting plate rises, the cooling medium enters the heat exchange chamber and flows from the right... The cooling medium is filled sequentially to the left. Due to the gap between the upper guide plate and the lifting plate, the cooling medium can fill the entire heat exchange chamber and discharge the air accumulated between the upper guide plates inside the heat exchange chamber to the outside of the heat exchange chamber. The air is discharged from the discharge pipe at the top of the heat exchange chamber. When the cooling medium level rises to the middle of the discharge pipe, it flows back into the cooling box from the return pipe, realizing the circulation of the cooling medium. This heat exchanger has a good condensation effect and can effectively avoid the accumulation of air in the heat exchanger, which would affect the condensation effect on floating oil and rosin.
[0023] 3. High-viscosity rosin can be obtained by purifying floating oil rosin using multiple vacuum distillations. Attached Figure Description
[0024] Figure 1 This is a schematic diagram of the overall structure of a processing device for producing high-viscosity floating oil rosin according to the present invention;
[0025] Figure 2 This is a schematic diagram of the cross-sectional structure of the purification cylinder in this invention;
[0026] Figure 3 This is a schematic diagram of the internal structure of the heat exchanger in this invention.
[0027] In the diagram: 1. Purification cylinder; 11. Impurity removal pipe; 12. Manhole; 13. Stirring motor; 131. Mounting cylinder; 132. Stirring shaft; 133. Stirrer; 134. Sealed bearing; 14. Exhaust pipe; 15. Hollow chamber; 2. Connecting cylinder; 21. Electric gas flow regulating valve; 22. Combustion base; 23. Gas pipe; 3. Filter cylinder; 31. Cleaning end cap; 32. Filter element; 33. Exhaust port; 4. Heat exchanger; 401, Inlet chamber; 402, Heat exchange chamber; 403, Discharge chamber; 404, Lower guide plate; 405, Upper guide plate; 406, Lifting plate; 407, Electric push rod; 408, Sealing strip; 41, Cooling box; 411, Mounting slot; 412, Semiconductor cooling chip; 42, Discharge pipe; 421, Telescopic pipe; 43, Return pipe; 44, Circulation pump; 5, Collection bucket; 51, Vacuum pump. Detailed Implementation
[0028] To make the objectives, technical solutions, and advantages of the present invention clearer, the present invention will be further described in detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
[0029] It should be noted that when a component is referred to as being "fixed to" or "set on" another component, it can be directly on or indirectly on that other component. When a component is referred to as being "connected to" another component, it can be directly connected to or indirectly connected to that other component.
[0030] In the description of this invention, it should be understood that the terms "length", "width", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this invention.
[0031] Furthermore, the terms "first" and "second" are used for descriptive purposes only and should not be construed as indicating or implying relative importance or implicitly specifying the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include one or more of that feature. In the description of this invention, "a plurality of" means two or more, unless otherwise explicitly specified.
[0032] To better understand the above technical solutions, the following will provide a detailed explanation of the technical solutions in conjunction with the accompanying drawings and specific embodiments.
[0033] Example:
[0034] Please see Figure 1-3 This embodiment provides a technical solution:
[0035] A processing apparatus for producing high-viscosity floating rosin includes a purification cylinder 1 and a condensation mechanism connected to an exhaust pipe 14. The purification cylinder 1 has an inner cylinder, and a hollow chamber 15 is provided between the inner cylinder and the outer wall of the purification cylinder 1. An air pipe extending out of the purification cylinder 1 is provided at the top of the hollow chamber 15, and a filter cylinder 3 is mounted on the air pipe. A filter element 32 is fixedly mounted on the top plate inside the filter cylinder 3. An exhaust port 33 at the top of the filter element 32 extends upwards out of the filter cylinder 3. An exhaust pipe 14 connecting to the inner cylinder is provided at the top of the purification cylinder 1. A purification port extending to the left is provided on the left side panel at the bottom of the inner cylinder of the purification cylinder 1. The purification cylinder 1 has a purification tube 11 outside the cylinder 1, and a manhole 12 extending downward into the inner cylinder is provided on the top panel of the purification cylinder 1. Both the manhole 12 and the purification tube 11 are provided with sealing end caps. An installation cylinder 131 is provided in the middle of the top panel of the purification cylinder 1, and a stirring shaft 132 is provided inside the installation cylinder 131 and is rotatably connected to the inner wall of the installation cylinder 131 through a sealing bearing 134. A stirrer 133 extending into the inner cylinder is provided at the bottom of the stirring shaft 132. A stirring motor 13 is fixedly provided in the middle of the top panel of the purification cylinder 1, and the motor shaft of the stirring motor 13 is connected to the stirring shaft 132 through a coupling.
[0036] Please see Figure 1 It also includes a heating mechanism located at the bottom of the purification cylinder 1. The heating mechanism includes a docking cylinder 2 and a combustion base 22 arranged sequentially from top to bottom. A combustion head is provided on the top panel of the combustion base 22, and the gas pipe 23 of the combustion head extends out of the combustion base 22. An electric gas flow regulating valve 21 is provided on the gas pipe 23. The docking cylinder 2 is connected to the hollow chamber 15. In specific use, an inner cylinder is provided inside the purification cylinder 1. A hollow chamber 15 is left between the inner cylinder and the outer wall of the purification cylinder 1. When the combustion head in the combustion base 22 burns, the flame burns along the outer wall of the inner cylinder, which can accelerate the heating of the floating oil and rosin inside the inner cylinder. The air after combustion enters the filter cylinder 1. The filter element 32 provided inside the filter cylinder 1 can filter the combustion exhaust gas, which has a good environmental protection effect.
[0037] Please see Figure 1 and Figure 3The condensation mechanism includes a heat exchanger 4 and a cooling box 41. Inside the heat exchanger 4, from left to right, are an inlet chamber 401, a heat exchange chamber 402, and a discharge chamber 403. An exhaust pipe 14 extends into the inlet chamber 401. A heat exchange capillary tube penetrating the heat exchange chamber 402 is installed between the inlet chamber 401 and the discharge chamber 403. Inside the heat exchange chamber 402, a lower guide plate 404 and an upper guide plate 405 are alternately arranged. A water guide groove is provided at the top of the lower guide plate 404, and a water guide groove is provided at the bottom of the upper guide plate 405. A vertically movable lifting plate 406 is provided at the top of the heat exchange chamber 402. After the lifting plate 406 descends, it fits against the top of the upper guide plate 405. Sealing strips 408 are provided on the edge of the lowering plate 406 and the top edge of the upper guide plate 405. A water inlet pipe is provided at the bottom left end of the heat exchange chamber 402, which is connected to the outlet of the cooling box 41. A circulating pump 44 is provided on the water inlet pipe. A telescopic pipe 421 is provided at the left end of the lifting plate 406, which is connected to the top plate of the heat exchange chamber 402. A discharge pipe 42 is provided at the top of the telescopic pipe 421, which extends upward out of the heat exchanger 4. A tee is provided in the middle of the discharge pipe 42. A return pipe 43 is provided at the outer pipe end of the tee, which is connected to the inlet of the cooling box 41. An electric push rod 407 is fixedly provided on the top plate of the heat exchanger 4. The telescopic rod of the electric push rod 407 is connected to the lifting plate 406.
[0038] In practical use, after the floating rosin undergoes high-temperature negative pressure distillation, the precipitated mixed gas is introduced into heat exchanger 4 for condensation. The refrigerant for heat exchanger 4 is provided by cooling box 41. Inside the heat exchange chamber 402 of heat exchanger 4, a lower guide plate 404 and an upper guide plate 405 are alternately arranged. A water guide groove is provided at the top of the lower guide plate 404, and a water guide groove is provided at the bottom of the upper guide plate 405. A vertically movable lifting plate 406 is provided at the top of the heat exchange chamber 402. When the lifting plate 406 descends, it contacts the top of the upper guide plate 405. When the lifting plate 406 rises, the cooling medium enters the heat exchange chamber. After 402, the cooling medium is filled sequentially from right to left. Due to the gap between the upper guide plate 405 and the lifting plate 406, the cooling medium can fill the entire heat exchange chamber 402 and discharge the air accumulated between the upper guide plates 405 in the heat exchange chamber 402. The air is discharged from the discharge pipe 42 at the top of the heat exchange chamber 402. When the cooling medium level rises to the middle of the discharge pipe 42, it flows back to the cooling box 41 through the return pipe 43, realizing the circulation of the cooling medium. This heat exchanger 4 has a good condensation effect and can effectively avoid the accumulation of air in the heat exchanger 4, which would affect the condensation effect on floating oil and rosin.
[0039] Please see Figure 1 The front and rear side panels of the cooling box 41 are provided with mounting slots 411, and the front and rear side panels of the cooling box 41 are both aluminum heat-conducting plates. A semiconductor cooling chip 412 is fixedly installed inside the mounting slot 411, and a heat sink is installed on the hot end of the semiconductor cooling chip 412.
[0040] Specifically, the cold end of the semiconductor cooling chip 412 is attached to the inner wall of the mounting groove 411 to achieve cooling of the cooling medium inside the cooling box 41.
[0041] Please see Figure 1 The bottom right side of the discharge chamber 403 is provided with a discharge pipe extending out of the heat exchanger 4. The discharge pipe is connected to the collection tank 5, and a vacuum pump 51 is provided on the top plate of the collection tank 5. The suction pipe of the vacuum pump 51 extends into the collection tank 5.
[0042] A method for producing high-viscosity floating oil rosin includes the following steps:
[0043] S1. Add the floating rosin into the purification cylinder, turn on the electric gas flow regulating valve to introduce the mixed gas into the burner and ignite it, heat the temperature of the floating rosin inside the purification cylinder to between 250-260℃, at the same time, turn on the vacuum pump to make the inside of the purification cylinder a vacuum of 5mmHg, control the condensation temperature of the heat exchanger, collect the fraction above 180℃, and obtain fraction A.
[0044] S2. Empty the residue inside the purification cylinder, then add fraction A into the purification cylinder, add a decolorizing agent and an antioxidant to fraction A in sequence, and simultaneously introduce a protective gas. Stir the reaction at 210-250℃ for 2-3 hours. The decolorizing agent is hypophosphite and / or sodium hypophosphite; the antioxidant is at least one of 2,6-di-tert-butyl-p-cresol, pentaerythritol tetrakis[β-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate], and octadecyl β-(4-hydroxyphenyl-3,5-di-tert-butyl)propionate.
[0045] Furthermore, the inert gases mentioned above include nitrogen or carbon dioxide;
[0046] S3. After completing step S2, raise the temperature of the purification cylinder to 240-260℃, and at the same time turn on the vacuum pump to make the vacuum degree inside the purification cylinder 5mmHg, and carry out vacuum distillation to collect the fraction above 190℃ to obtain refined floating rosin.
[0047] S4. The refined floating rosin is put back into the purification cylinder, the temperature of the purification cylinder is raised to 110-180℃, and the vacuum pump is turned on to make the vacuum degree inside the purification cylinder 5mmHg. Reduced pressure distillation is carried out, and the fraction below 180℃ is collected to obtain high viscosity floating rosin.
[0048] Although embodiments of the invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the invention, the scope of which is defined by the appended claims and their equivalents.
Claims
1. A processing device for the production of high viscosity floating oil rosin, characterized by: The utility model relates to a purification cylinder (1) is provided with an inner cylinder inside, and hollow chamber (15) is arranged between the inner cylinder and the outer wall of purification cylinder (1), the top of hollow chamber (15) is provided with the trachea that stretches out the outside of purification cylinder (1), and the trachea is provided with filter cylinder (3), the top plate of filter cylinder (3) is fixedly provided with filter core (32) inside, the exhaust port (33) of filter core (32) top stretches out the outside of filter cylinder (3) upwards, and the top of purification cylinder (1) is provided with the exhaust pipe (14) of connecting inner cylinder, The utility model relates to a purification cylinder (1) is provided with an inner cylinder inside, and hollow chamber (15) is arranged between the inner cylinder and the outer wall of purification cylinder (1), the top of hollow chamber (15) is provided with the trachea that stretches out the outside of purification cylinder (1), and the trachea is provided with filter cylinder (3), the top plate of filter cylinder (3) is fixedly provided with filter core (32) inside, the exhaust port (33) of filter core (32) top stretches out the outside of filter cylinder (3) upwards, and the top of purification cylinder (1) is provided with the exhaust pipe (14) of connecting inner cylinder, The utility model relates to a purification cylinder (1) is provided with an inner cylinder inside, and hollow chamber (15) is arranged between the inner cylinder and the outer wall of purification cylinder (1), the top of hollow chamber (15) is provided with the trachea that stretches out the outside of purification cylinder (1), and the trachea is provided with filter cylinder (3), the top plate of filter cylinder (3) is fixedly provided with filter core (32) inside, the exhaust port (33) of filter core (32) top stretches out the outside of filter cylinder (3) upwards, and the top of purification cylinder (1) is provided with the exhaust pipe (14) of connecting inner cylinder, The bottom right of the exhaust chamber (403) is provided with a discharge pipeline that stretches out the heat exchanger (4), the discharge pipeline is connected with a collecting barrel (5), a vacuum pump (51) is arranged on the top plate of the collecting barrel (5), and the suction pipe of the vacuum pump (51) stretches into the collecting barrel (5). 2. A processing device for producing high viscosity floating rosin according to claim 1, characterized in that: The left side panel of the bottom of the purification cylinder (1) is provided with a leftwardly extending impurity removal pipe (11) outside the purification cylinder (1), and the top panel of the purification cylinder (1) is provided with a manhole (12) extending downwardly into the inner cylinder, and the manhole (12) and the impurity removal pipe (11) are both provided with sealing end covers.
3. A processing device for producing high viscosity floating rosin according to claim 1, characterized in that: The middle part of the top panel of the purification cylinder (1) is provided with a mounting cylinder (131), and the inside of the mounting cylinder (131) is provided with a stirring shaft (132) rotatably connected with the inner wall of the mounting cylinder (131) through a sealing bearing (134), the bottom of the stirring shaft (132) is provided with a stirrer (133) extending into the inner cylinder, and the middle part of the top panel of the purification cylinder (1) is fixedly provided with a stirring motor (13), and the motor shaft of the stirring motor (13) is connected with the stirring shaft (132) through a shaft coupling.
4. The processing device for producing high viscosity tall oil rosin according to claim 1, characterized in that: The top plate of the heat exchanger (4) is fixedly provided with an electric push rod (407), and the telescopic rod of the electric push rod (407) is connected with a lifting plate (406).
5. A processing device for producing high viscosity tall oil rosin according to claim 1, characterized in that: The front and rear side panels of the cooling box (41) are both provided with mounting grooves (411), and the front and rear side panels of the cooling box (41) are both aluminum heat-conducting panels, the inside of the mounting groove (411) is fixedly provided with a semiconductor refrigeration sheet (412), and the hot end outside the semiconductor refrigeration sheet (412) is provided with a heat sink.
6. A process for the production of high viscosity floating oil rosin characterized by: The method uses the processing device of any one of claims 1-5, and comprises the following steps: S1, put the floating oil rosin into the purification cylinder, open the electric gas flow regulating valve to introduce the mixed fuel gas into the combustion head, then ignite, heat the temperature of the floating oil rosin inside the purification cylinder to 250-260℃, at the same time, open the vacuum pump to make the inside of the purification cylinder be at a vacuum degree of 5mmHg, control the condensation temperature of the heat exchanger, collect the distillate above 180℃, and obtain distillate A; S2, empty the residue inside the purification cylinder, then add the distillate A into the purification cylinder, add the decolorizing agent and antioxidant into the distillate A in sequence, at the same time, fill in the protective gas, and use the stirrer to stir for 2-3h at a temperature of 210-250℃; S3, after the step S2 is completed, increase the temperature of the purification cylinder to 240-260℃, at the same time, open the vacuum pump to make the inside of the purification cylinder be at a vacuum degree of 5mmHg, perform the reduced pressure distillation, collect the distillate above 190℃, and obtain the refined floating oil rosin; S4, put the refined floating oil rosin into the purification cylinder again, increase the temperature of the purification cylinder to 110-180℃, at the same time, open the vacuum pump to make the inside of the purification cylinder be at a vacuum degree of 5mmHg, perform the reduced pressure distillation, collect the distillate below 180℃, and obtain the high-viscosity floating oil rosin.
Citation Information
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