Automatic water washing reactor system and control method thereof

Abstract

The present invention provides an automated water-washing reactor system and a control method thereof. The automated water-washing reactor system comprises a reactor, a slurry premixing module, a slurry feeding module, an alkaline substance feeding module, a pure water feeding module, a coating material feeding module, a stirring module, an iron removal module, a heating module, a discharging module and a control module. The control module is provided in the automated water-washing reactor to monitor and control the reaction process, record and store real-time data of the reaction, compare the real-time monitored data with process preset values, control each other module through the control module, and obtain control parameter data of the optimal batch by comparing the quality of products of different batches. Optimal control parameters and optimal process data are obtained through data iteration.

Description

Technical Field

[0001] The present invention relates to the technical field of automatic water washing reactors, and in particular to an automatic water washing reactor system and a control method thereof. Background Art

[0002] Lithium batteries offer high energy density, long life, and are lightweight and portable. They are widely used in mobile devices, electric vehicles, drones, solar energy storage, and other fields. With the development of renewable energy and smart grids, lithium batteries will become even more important in the future. Lithium batteries primarily consist of anode materials, cathode materials, separators, electrolytes, and battery casings. The cathode material is the decisive factor in the electrochemical performance of lithium batteries, directly determining their energy density and safety, and thus affecting their overall performance.

[0003] High-nickel ternary cathode has become the most promising choice for lithium battery cathode materials in the future due to its high specific capacity. However, the existing automated water washing reactor for water washing and coating high-nickel ternary cathode materials relies on the operator's experience to complete the entire water washing and coating process. Due to the subjectivity of experience, the performance of high-nickel ternary cathode materials processed by different operators is unstable. Summary of the Invention

[0004] The present invention discloses an automated water washing reactor system, which solves the problem that the existing automated water washing reactor for water washing and coating high-nickel ternary positive electrode materials relies on the experience of the operator, resulting in unstable performance of the processed high-nickel ternary positive electrode materials. It realizes the automation and intelligence of the water washing reaction process, realizes the monitoring and control of the entire process of water washing and coating of high-nickel ternary positive electrode materials, and effectively improves the water washing and coating effect of high-nickel ternary positive electrode materials.

[0005] To achieve the above object, the technical solution of the present invention is specifically implemented as follows:

[0006] On the one hand, the present invention discloses an automatic water washing reactor system, comprising a reactor, a slurry premixing module, a slurry feeding module, an alkaline substance feeding module, a pure water feeding module, a coating material feeding module, a stirring module, an iron removal module, a heating module, a discharging module and a control module, wherein a temperature sensor, a pressure sensor and a pH sensor are provided in the reactor, wherein the temperature sensor is used to monitor the temperature value in the reactor in real time and transmit the temperature value to the control module; the pressure sensor is used to monitor the pressure value in the reactor in real time and transmit the pressure value to the control module; the pH sensor is used to monitor the pH value in the reactor in real time and transmit the pH value to the control module. The slurry premixing module is used to complete the ratio of high nickel ternary powder and pure water according to the process requirements and formula ratio; the slurry feeding module is used to add the premixed slurry mixed by the slurry premixing module into the reactor, and monitor the weight of the slurry fed into the reactor in real time, and transmit the monitored weight of the slurry fed into the reactor to the control module; the alkaline substance feeding module is used to add the required alkaline substance into the reactor, and monitor the weight of the alkaline substance and the pH value of the alkaline substance in real time, and transmit the monitored weight of the alkaline substance and the pH value of the alkaline substance to the control module; the pure water feeding module is used to add the required pure water into the reactor, The weight of the pure water and the pH value of the pure water are monitored in real time, and the weight of the pure water and the pH value of the pure water monitored in real time are transmitted to the control module; the coating material feeding module is used to add the coating material into the reactor, and monitor the weight of the coating material put into the reactor in real time, and transmit the monitored weight of the coating material put into the reactor to the control module; the stirring module achieves better mixing and coating of the slurry in the reactor through a certain stirring speed; the iron removal module is used to remove ferromagnetic substances in the slurry; the heating module is used to heat the slurry in the reactor; the unloading module is used to complete the unloading; the control module is used to record and store the alkaline substance feeding module The weight of the alkaline substance and the pH value of the alkaline substance sent, and the delivery time of the alkaline substance delivery module is controlled according to the process preset data; the weight of the pure water delivered by the pure water delivery module and the pH value of the pure water are recorded and stored, and the obtained weight of the pure water delivered and the pH value of the pure water delivered are compared with the process preset data to control the delivery time of the pure water delivery module; the weight of the slurry delivered into the reactor sent by the slurry delivery module is recorded and stored, and the delivery time of the slurry delivery module is controlled according to the process preset data; the weight of the coating material delivered into the reactor by the coating material delivery module is recorded and stored, and the delivery time of the coating material delivery module is controlled according to the process preset data;Record and store the temperature, pressure, and slurry pH values ​​within the reactor, compare these values ​​with the preset process data, adjust the heating temperature of the heating module, the weight and pH value of the alkaline substance added by the alkaline substance addition module, and the weight and pH value of the pure water added by the pure water addition module, and iterate each data to generate the optimal process data.

[0007] Furthermore, a cleaning module is included to clean the reactor.

[0008] Furthermore, the alkaline substance addition module includes a pH sensor, a flow meter and an alarm, wherein the pH sensor is used to monitor the pH value of the slurry in the reactor in real time; the flow meter monitors the weight of the alkaline substance added into the reactor in real time; and the alarm sends an alarm signal when it detects a sudden change in the pH value of the slurry in the reactor.

[0009] Furthermore, the pure water delivery module includes a pH sensor, a flow meter and an alarm, wherein the pH sensor is used to monitor the pH value of the pure water delivered into the reactor in real time; the flow meter is used to monitor the weight of the pure water delivered into the reactor in real time; and the alarm sends an alarm signal when the pH sensor detects a sudden change in the pH value of the pure water delivered into the reactor.

[0010] Furthermore, the iron removal module includes an iron remover, which is arranged before the slurry enters the reactor and at the discharge port.

[0011] Furthermore, the cleaning module adopts a multi-layer spray head.

[0012] Furthermore, the coating material delivery module includes a flow meter for monitoring the weight of the coating material delivered into the reactor in real time.

[0013] Furthermore, the slurry delivery module includes a flow meter for real-time monitoring of the weight of the premixed slurry delivered into the reactor.

[0014] Another aspect of the present invention discloses a control method for an automated water-washing reactor, comprising the following steps:

[0015] The slurry premixing module completes the ratio of high nickel ternary powder and pure water according to process requirements and formula ratio;

[0016] The slurry feeding module adds the premixed slurry mixed by the slurry premixing module into the reactor, monitors the weight of the slurry fed into the reactor in real time, and transmits the monitored weight of the slurry fed into the reactor to the control module;

[0017] The control module receives, records and stores the real-time monitored weight of the slurry added to the reactor, and compares the received value with the process preset data. If the weight of the slurry added is less than the process preset data, the slurry addition module controls the flow rate or addition time of the slurry;

[0018] The pure water delivery module adds the required pure water into the reactor. The pH sensor in the pure water delivery module monitors the pH value of the delivered pure water in real time. The flow meter in the pure water delivery module monitors the flow rate of the delivered pure water in real time. The pure water delivery module transmits the real-time monitored pH value of the delivered pure water and the flow rate of the delivered pure water to the control module.

[0019] The control module receives, records, and stores the pH value and flow rate of the pure water being added, which are monitored in real time. It compares the received values ​​with the process preset data. If the weight of the pure water added is less than the process preset data, the pure water addition module is controlled to increase the flow rate or add time of the pure water. If a sudden change in the pH value of the pure water is detected, the pure water addition module is controlled to stop adding the pure water immediately.

[0020] The alkaline substance delivery module adds the required alkaline substance into the reactor. The pH sensor in the alkaline substance delivery module monitors the pH value of the delivered alkaline substance in real time. The alkaline substance delivery module monitors the flow rate of the delivered alkaline substance in real time. The alkaline substance delivery module transmits the pH value and flow rate of the alkaline substance monitored in real time to the control module.

[0021] The control module receives, records, and stores the pH value of the alkaline substance and the flow rate of the alkaline substance that are monitored in real time, and compares the received values ​​with the process preset data. If the weight value of the alkaline substance is less than the process preset data, the alkaline substance delivery module is controlled to deliver the alkaline substance at a certain flow rate or at a certain time. If a sudden change in the pH value of the alkaline substance is detected, the alkaline substance delivery module is controlled to immediately stop delivery.

[0022] The coating material feeding module adds the coating material into the reactor, monitors the flow rate of the coating material into the reactor in real time, and transmits the monitored flow rate of the coating material into the reactor to the control module;

[0023] The control module receives, records, and stores the flow rate of the coating material delivered by the coating material module monitored in real time, and compares the received value with the process preset data. If the weight value of the delivered coating material is less than the process preset data, the coating material delivery module is controlled to deliver the coating material at a flow rate or delivery time.

[0024] The heating module heats the slurry in the reactor, and the temperature sensor and pressure sensor in the reactor monitor the temperature and pressure values ​​in the reactor in real time, and transmit the monitored real-time temperature and pressure values ​​to the control module;

[0025] The control module receives, records and stores the temperature and pressure values ​​monitored in real time, compares the received temperature and pressure values ​​with the process preset temperature and pressure values, and controls the heating power and heating time of the heating module according to the process preset temperature and pressure values;

[0026] The iron removal module removes ferromagnetic substances from the slurry. The control module uses the parameters obtained by the above modules and the data of the iron content in the slurry to generate influencing factors for comparison and optimize the process parameters.

[0027] The control module controls the unloading speed of the unloading module. When an emergency occurs, the control module can realize emergency unloading.

[0028] The coating quality of each batch of products is tested, and the parameters obtained from each module are compared with the database generated by the coating quality test data and the influencing factors. The data in the database is iterated to obtain the optimal process data.

[0029] Furthermore, when controlling the unloading speed of the unloading module, the control module controls the cleaning module to clean the inside of the reactor according to the unloading speed of the unloading module.

[0030] Beneficial technical effects:

[0031] 1. The present invention discloses an automated water washing reactor system, comprising a reactor, a slurry premixing module, a slurry feeding module, an alkaline substance feeding module, a pure water feeding module, a coating material feeding module, a stirring module, an iron removal module, a heating module, a discharging module and a control module. The control module controls the other modules, realizes the automation and intelligence of the water washing reaction process, realizes the monitoring and control of the entire process of water washing and coating of high-nickel ternary cathode materials, and effectively improves the water washing and coating effect of high-nickel ternary cathode materials.

[0032] 2. The automated water-washing reactor system disclosed in the present invention includes a slurry premixing module, which completes the ratio of high-nickel ternary powder and pure water according to process requirements and formula ratio. That is, before putting the high-nickel ternary powder and pure water into the reactor, the high-nickel ternary powder and pure water are mixed first, which effectively avoids the dust effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0033] In order to more clearly illustrate the technical solution of the present invention, the following briefly introduces the drawings required for describing the embodiments.

[0034] Figure 1This is a structural schematic diagram of an automatic water washing reactor system described in the present invention. DETAILED DESCRIPTION

[0035] The following describes embodiments of the present invention in detail. Examples of the embodiments are shown in the accompanying drawings, wherein the same or similar reference numerals throughout represent the same or similar elements or elements having the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary and are intended only to explain the present invention and are not to be construed as limiting the present invention.

[0036] It should be noted that the terms used herein are only for describing specific embodiments and are not intended to limit the exemplary embodiments according to the present application. As used herein, unless the context clearly indicates otherwise, the singular form is also intended to include the plural form. In addition, it should be understood that when the terms "comprise" and / or "include" are used in this specification, they indicate the presence of features, steps, operations, devices, components and / or combinations thereof.

[0037] Unless otherwise specifically stated, the relative arrangement of the parts and steps, the numerical expressions and the numerical values ​​set forth in these embodiments do not limit the scope of the present invention. At the same time, it should be understood that, for ease of description, the sizes of the various parts shown in the drawings are not drawn according to the actual proportional relationship. The techniques, methods and equipment known to those of ordinary skill in the relevant art may not be discussed in detail, but where appropriate, the techniques, methods and equipment should be considered as part of the authorization specification. In all examples shown and discussed here, any specific values ​​should be interpreted as being merely exemplary and not as limiting. Therefore, other examples of the exemplary embodiments may have different values. It should be noted that similar numbers and letters represent similar items in the following figures, and therefore, once an item is defined in one figure, it does not need to be further discussed in subsequent figures.

[0038] The embodiments of the present invention will be described in detail below with reference to the accompanying drawings.

[0039] The present invention discloses an automatic water washing reactor system. Figure 1 (It should be noted that the attached Figure 1The solid line in the figure indicates the flow direction of the slurry, and the dotted line indicates the transmission direction of the signal), including a reactor, a slurry premixing module, a slurry feeding module, an alkaline substance feeding module, a pure water feeding module, a coating material feeding module, a stirring module, an iron removal module, a heating module, an unloading module and a control module, wherein a temperature sensor, a pressure sensor and a pH sensor are arranged in the reactor, wherein the temperature sensor is used to monitor the temperature value in the reactor in real time and transmit the temperature value to the control module; the pressure sensor is used to monitor the pressure value in the reactor in real time and transmit the pressure value to the control module; the pH sensor is used to monitor the pH value in the reactor in real time and transmit the pH value to the control module; the slurry premixing module is used to complete the ratio of high nickel ternary powder and pure water according to the process requirements and formula ratio, that is, to complete the premixing of high nickel ternary powder and pure water in advance, thereby effectively avoiding dust flying; the slurry feeding module It is used to add the premixed slurry mixed by the slurry premixing module into the reactor, and monitor the weight of the slurry added into the reactor in real time, and transmit the monitored weight of the slurry added into the reactor to the control module. Preferably, the slurry adding module includes a flow meter for monitoring the weight of the premixed slurry added into the reactor in real time; the alkaline substance adding module is used to add the required alkaline substance into the reactor, and monitor the weight of the alkaline substance added and the pH value of the alkaline substance in real time, and transmit the real-time monitored weight of the alkaline substance added and the pH value of the alkaline substance to the control module. Preferably, the alkaline substance adding module includes a pH sensor, a flow meter and an alarm, wherein the pH sensor is used to monitor the pH value of the slurry in the reactor in real time; the flow meter monitors the weight of the alkaline substance added into the reactor in real time; and the alarm sends an alarm signal when it monitors that the pH value of the slurry in the reactor changes suddenly.

[0040] As an embodiment of the present invention, the pure water delivery module is used to add the required pure water into the reactor, and monitor the weight of the delivered pure water and the pH value of the pure water in real time, and transmit the real-time monitored weight of the delivered pure water and the pH value of the pure water to the control module. Preferably, the pure water delivery module includes a pH sensor, a flow meter and an alarm, wherein the pH sensor is used to monitor the pH value of the pure water delivered into the reactor in real time; the flow meter is used to monitor the weight of the pure water delivered into the reactor in real time; and the alarm sends an alarm signal when the pH sensor detects that the pH value of the pure water delivered into the reactor has changed suddenly.

[0041] As an embodiment of the present invention, the coating material delivery module is used to add the coating material into the reactor, and monitor the weight of the coating material delivered into the reactor in real time, and transmit the monitored weight of the coating material delivered into the reactor to the control module. Preferably, the coating material delivery module includes a flow meter for monitoring the weight of the coating material delivered into the reactor in real time.

[0042] As an embodiment of the present invention, the stirring module achieves better mixing and coating of the slurry in the reactor through a certain stirring speed. Specifically, a motor with sufficient power to drive the reactor is selected to provide sufficient torque. At the same time, the accuracy requirements of the control module for the motor need to be considered. For example, a DC motor with an encoder is selected to meet the requirements of the control system. At the same time, factors such as transmission coefficient, transmission efficiency and durability are considered. Bearings and couplings are used in the transmission system to ensure that they can withstand the load of the motor and provide sufficient axial and radial support. An emergency stop button and circuit breaker are set or an emergency stop is performed when the control system issues an emergency stop signal to ensure the reactor and The equipment can operate normally. The impeller uses an improved inclined-blade open turbine impeller. Through rapid and uniform stirring, the reaction system can obtain better mixing and coating effects. The impeller speed is programmed through the control system to achieve the optimal speed under different working conditions. That is, the speed of the impeller under different working conditions is controlled by the control system to control the speed of the stirring motor. It can achieve the fastest uniform stirring without dead zones that meets the process requirements, and at the same time reduce the stirring power to achieve energy-saving production. The pressure sensor installed in the kettle uploads the pressure value to the control module in real time. If the pressure value exceeds the preset safety value, the control module controls the motor to stop to ensure safe production.

[0043] As an embodiment of the present invention, the iron removal module is used to remove ferromagnetic substances in the slurry. Specifically, when the slurry is added and unloaded, a pipeline iron remover is set to remove ferromagnetic substances in the ternary positive electrode material to achieve the effect of iron removal. The pipeline iron remover is located before the slurry enters the reactor and at the discharge port. It removes iron through the principle of magnetic separation and ensures that there is no iron pollution in the reactor. It should be understood that after water washing and coating, the iron content of the product can be further tested. If it is unqualified, the product will be further iron-removed by a special iron removal system independent of the reactor. The selection and control of all the above parameters and the iron removal effect are compared to generate a database and influencing factors, and through data iteration, the process engineering and parameter selection control can be secondary optimized.

[0044] As an embodiment of the present invention, the heating module is used to heat the slurry in the reactor; the unloading module is used to complete the unloading. Specifically, the heating module adopts jacket heat transfer technology, is arranged on the inner wall outside the reactor, and introduces a high-temperature medium (such as steam or heat transfer oil) for heat transfer. At the same time, a jacket temperature measuring port is provided in the jacket, and the jacket temperature measuring port is provided to monitor the temperature changes in the jacket, and to adjust the temperature in the reactor in conjunction with the temperature data detected by the temperature sensor in the reactor and the optimal reaction temperature.

[0045] As an embodiment of the present invention, the control module is used to record and store the weight of the alkaline substance and the pH value of the alkaline substance sent by the alkaline substance feeding module, and control the feeding time of the alkaline substance feeding module according to the process preset data; record and store the weight of the pure water and the pH value of the pure water fed by the pure water feeding module, and compare the obtained weight of the pure water and the pH value of the pure water with the process preset data to control the feeding time of the pure water feeding module; record and store the weight of the slurry fed into the reactor sent by the slurry feeding module, and control the feeding time of the slurry feeding module according to the process preset data. The method comprises the following steps: recording and storing the weight of the coating material put into the reactor by the coating material putting module, and controlling the putting time of the coating material putting module according to the process preset data; recording and storing the temperature value, pressure value and slurry pH value in the reactor, and comparing the obtained temperature value, pressure value and slurry pH value in the reactor with the process preset data, adjusting the heating temperature of the heating module, the weight and pH value of the alkaline substance put into the alkaline substance putting module, and the weight and pH value of the pure water put into the pure water putting module, iterating various data, and generating the optimal process data.

[0046] As a preferred embodiment of the present invention, the automated water-washing reactor system also includes a cleaning module for cleaning the reactor. Specifically, the cleaning module adopts a multi-layer spray nozzle, and the number, size, position and spray direction of the cleaning nozzles and other parameters match the structure of the reactor, which can ensure dead-angle flushing. The cleaning force is sufficient to flush away the materials remaining on the inner wall and the agitator, so as to ensure the best cleaning effect and the lowest water consumption.

[0047] It should be noted that the automated water washing reactor disclosed in the present invention is not only used for water washing and coating of high-nickel ternary positive electrode materials, but can also be applied to other industries with slight modifications according to specific application scenarios.

[0048] Another aspect of the present invention discloses a control method for an automated water-washing reactor, which specifically comprises the following steps:

[0049] The slurry premixing module completes the ratio of high nickel ternary powder and pure water according to process requirements and formula ratio;

[0050] The slurry feeding module adds the premixed slurry mixed by the slurry premixing module into the reactor, monitors the weight of the slurry fed into the reactor in real time, and transmits the monitored weight of the slurry fed into the reactor to the control module;

[0051] The control module receives, records and stores the real-time monitored weight of the slurry added to the reactor, and compares the received value with the process preset data. If the weight of the slurry added is less than the process preset data, the slurry addition module controls the flow rate or addition time of the slurry;

[0052] The pure water delivery module adds the required pure water into the reactor. The pH sensor in the pure water delivery module monitors the pH value of the delivered pure water in real time. The flow meter in the pure water delivery module monitors the flow rate of the delivered pure water in real time. The pure water delivery module transmits the real-time monitored pH value of the delivered pure water and the flow rate of the delivered pure water to the control module.

[0053] The control module receives, records, and stores the pH value and flow rate of the pure water being added, which are monitored in real time. It compares the received values ​​with the process preset data. If the weight of the pure water added is less than the process preset data, the pure water addition module is controlled to increase the flow rate or add time of the pure water. If a sudden change in the pH value of the pure water is detected, the pure water addition module is controlled to stop adding the pure water immediately.

[0054] The alkaline substance delivery module adds the required alkaline substance into the reactor. The pH sensor in the alkaline substance delivery module monitors the pH value of the delivered alkaline substance in real time. The alkaline substance delivery module monitors the flow rate of the delivered alkaline substance in real time. The alkaline substance delivery module transmits the pH value and flow rate of the alkaline substance monitored in real time to the control module.

[0055] The control module receives, records, and stores the pH value of the alkaline substance and the flow rate of the alkaline substance that are monitored in real time, and compares the received values ​​with the process preset data. If the weight value of the alkaline substance is less than the process preset data, the alkaline substance delivery module is controlled to deliver the alkaline substance at a certain flow rate or at a certain time. If a sudden change in the pH value of the alkaline substance is detected, the alkaline substance delivery module is controlled to immediately stop delivery.

[0056] The coating material feeding module adds the coating material into the reactor, monitors the flow rate of the coating material into the reactor in real time, and transmits the monitored flow rate of the coating material into the reactor to the control module;

[0057] The control module receives, records, and stores the flow rate of the coating material delivered by the coating material module monitored in real time, and compares the received value with the process preset data. If the weight value of the delivered coating material is less than the process preset data, the coating material delivery module is controlled to deliver the coating material at a flow rate or delivery time.

[0058] The heating module heats the slurry in the reactor, and the temperature sensor and pressure sensor in the reactor monitor the temperature and pressure values ​​in the reactor in real time, and transmit the monitored real-time temperature and pressure values ​​to the control module;

[0059] The control module receives, records and stores the temperature and pressure values ​​monitored in real time, compares the received temperature and pressure values ​​with the process preset temperature and pressure values, and controls the heating power and heating time of the heating module according to the process preset temperature and pressure values;

[0060] The iron removal module removes ferromagnetic substances from the slurry. The control module uses the parameters obtained by the above modules and the data of the iron content in the slurry to generate influencing factors for comparison and optimize the process parameters.

[0061] The control module controls the unloading speed of the unloading module. When an emergency occurs, the control module controls the unloading module to realize emergency unloading. Preferably, when controlling the unloading speed of the unloading module, the control module controls the cleaning module to clean the inside of the reactor according to the unloading speed of the unloading module.

[0062] The coating quality of each batch of products is tested, and the parameters obtained from each module are compared with the database generated by the coating quality test data and the influencing factors. The data in the database is iterated to obtain the optimal process data.

[0063] The automated water washing reactor disclosed in the present invention is provided with a control module to monitor and control the reaction process, record and store real-time data of the reaction, compare the real-time monitored data with the process preset values, control each other module through the control module, and obtain the control parameter data of the optimal batch by comparing the quality of products of different batches. Through data iteration, the optimal control parameters are obtained, and the optimal process data are obtained.

[0064] Throughout this specification, reference to terms such as "one embodiment," "some embodiments," "examples," "specific examples," or "some examples" means that a specific feature, structure, material, or characteristic described in conjunction with that embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

[0065] The above embodiments are merely descriptions of preferred implementations of the present invention and are not intended to limit the scope of the present invention. Without departing from the spirit of the present invention, various modifications and improvements made to the technical solutions of the present invention by ordinary engineers and technicians in this field should fall within the scope of protection determined by the claims of the present invention.

Claims

1. An automatic water washing reactor system, characterized in that: include: A reactor is provided with: The temperature sensor is used to monitor the temperature in the reactor in real time and transmit the temperature value to the control module; The pressure sensor is used to monitor the pressure value in the reactor in real time and transmit the pressure value to the control module; pH sensor, used to monitor the pH value in the reactor in real time and transmit the pH value to the control module; Slurry premixing module, used to complete the ratio of high nickel ternary powder and pure water according to process requirements and formula ratio; The slurry feeding module is used to add the premixed slurry mixed by the slurry premixing module into the reactor, monitor the weight of the slurry fed into the reactor in real time, and transmit the monitored weight of the slurry fed into the reactor to the control module; An alkaline substance feeding module is used to add the required alkaline substance into the reactor, monitor the weight of the alkaline substance and the pH value of the alkaline substance in real time, and transmit the real-time monitored weight of the alkaline substance and the pH value of the alkaline substance to the control module; The pure water feeding module is used to add the required pure water into the reactor, monitor the weight of the pure water added and the pH value of the pure water in real time, and transmit the real-time monitored weight of the pure water added and the pH value of the pure water to the control module; A coating material delivery module is used to add the coating material into the reactor, monitor the weight of the coating material delivered into the reactor in real time, and transmit the monitored weight of the coating material delivered into the reactor to the control module; The stirring module achieves better mixing and coating of the slurry in the reactor through a certain stirring speed; Iron removal module, used to remove ferromagnetic substances from the slurry; A heating module is used to heat the slurry in the reactor; Unloading module, used to complete unloading; The control module is used to record and store the weight of the alkaline substance and the pH value of the alkaline substance sent by the alkaline substance delivery module, and control the delivery time of the alkaline substance delivery module according to the process preset data; record and store the weight of the pure water delivered by the pure water delivery module and the pH value of the pure water, and compare the obtained weight and pH value of the delivered pure water with the process preset data to control the delivery time of the pure water delivery module; record and store the weight of the slurry delivered to the reactor sent by the slurry delivery module, and control the delivery time of the slurry delivery module according to the process preset data; record and store the weight of the coating material delivered to the reactor by the coating material delivery module, and control the delivery time of the coating material delivery module according to the process preset data; record and store the temperature value, pressure value and pH value of the slurry in the reactor, and compare the obtained temperature value, pressure value and pH value of the slurry in the reactor with the process preset data, adjust the heating temperature of the heating module, the weight and pH value of the alkaline substance delivered by the alkaline substance delivery module, and the weight and pH value of the pure water delivered by the pure water delivery module, iterate various data, and generate optimal process data.

2. The automatic water washing reactor system according to claim 1, characterized in that: It also includes a cleaning module for cleaning the reactor.

3. The automatic water washing reactor system according to claim 1, characterized in that: The alkaline substance delivery module includes: pH sensor, used to monitor the pH value of the slurry in the reactor in real time; A flow meter monitors the weight of the alkaline substance added to the reactor in real time; The alarm will send out an alarm signal when it detects a sudden change in the pH value of the slurry in the reactor.

4. The automatic water washing reactor system according to claim 1, characterized in that: The pure water delivery module includes: pH sensor, used to monitor the pH value of pure water added to the reactor in real time; Flow meter, used to monitor the weight of pure water added to the reactor in real time; The alarm device sends out an alarm signal when the pH sensor detects that the pH value of the pure water put into the reactor changes suddenly.

5. The automatic water washing reactor system according to claim 1, characterized in that: The iron removal module includes an iron remover, which is arranged before the slurry enters the reactor and at the discharge port.

6. The automatic water washing reactor system according to claim 2, characterized in that: The cleaning module adopts a multi-layer spray head.

7. The automatic water washing reactor system according to claim 1, characterized in that: The coating material delivery module includes a flow meter for real-time monitoring of the weight of the coating material delivered into the reactor.

8. The automatic water washing reactor system according to claim 1, characterized in that: The slurry delivery module includes a flow meter for real-time monitoring of the weight of the premixed slurry delivered into the reactor.

9. A control method for an automated water-washing reactor, characterized in that: The following steps are involved: The slurry premixing module completes the ratio of high nickel ternary powder and pure water according to process requirements and formula ratio; The slurry feeding module adds the premixed slurry mixed by the slurry premixing module into the reactor, monitors the weight of the slurry fed into the reactor in real time, and transmits the monitored weight of the slurry fed into the reactor to the control module; The control module receives, records and stores the real-time monitored weight of the slurry added to the reactor, and compares the received value with the process preset data. If the weight of the slurry added is less than the process preset data, the slurry addition module controls the flow rate or addition time of the slurry; The pure water delivery module adds the required pure water into the reactor. The pH sensor in the pure water delivery module monitors the pH value of the delivered pure water in real time. The flow meter in the pure water delivery module monitors the flow rate of the delivered pure water in real time. The pure water delivery module transmits the real-time monitored pH value of the delivered pure water and the flow rate of the delivered pure water to the control module. The control module receives, records, and stores the real-time monitored pH value of the pure water and the flow rate of the pure water, and compares the received values ​​with the process preset data. If the weight value of the pure water added is less than the process preset data, the pure water addition module is controlled to increase the flow rate or time of pure water addition. If a sudden change in the pH value of the pure water is detected, the pure water addition module is controlled to stop the addition immediately. The alkaline substance delivery module adds the required alkaline substance into the reactor. The pH sensor in the alkaline substance delivery module monitors the pH value of the delivered alkaline substance in real time. The flow meter in the alkaline substance delivery module monitors the flow rate of the delivered alkaline substance in real time. The alkaline substance delivery module transmits the pH value and flow rate of the alkaline substance monitored in real time to the control module. The control module receives, records, and stores the pH value of the alkaline substance and the flow rate of the alkaline substance that are monitored in real time, and compares the received values ​​with the process preset data. If the weight value of the alkaline substance that is added is less than the process preset data, the alkaline substance addition module controls the flow rate or addition time of the alkaline substance. If the pH value of the alkaline substance is monitored to change suddenly, the alkaline substance addition module is controlled to stop the addition immediately. The coating material feeding module adds the coating material into the reactor, monitors the flow rate of the coating material into the reactor in real time, and transmits the monitored flow rate of the coating material into the reactor to the control module; The control module receives, records, and stores the flow rate of the coating material delivered by the coating material module monitored in real time, and compares the received value with the process preset data. If the weight value of the delivered coating material is less than the process preset data, the coating material delivery module is controlled to deliver the coating material at a flow rate or delivery time. The heating module heats the slurry in the reactor, and the temperature sensor and pressure sensor in the reactor monitor the temperature and pressure values ​​in the reactor in real time, and transmit the monitored real-time temperature and pressure values ​​to the control module; The control module receives, records and stores the temperature and pressure values ​​monitored in real time, compares the received temperature and pressure values ​​with the process preset temperature and pressure values, and controls the heating power and heating time of the heating module according to the process preset temperature and pressure values; The iron removal module removes ferromagnetic substances from the slurry. The control module uses the parameters obtained by the above modules and the data of the iron content in the slurry to generate influencing factors for comparison and optimize the process parameters. The control module controls the unloading speed of the unloading module; The coating quality of each batch of products is tested, and the parameters obtained from each module are compared with the database generated by the coating quality test data and the influencing factors. The data in the database is iterated to obtain the optimal process data.

10. The control method of an automatic water washing reactor according to claim 9, characterized in that: When the control module controls the unloading speed of the unloading module, the control module controls the cleaning module to clean the inside of the reactor according to the unloading speed of the unloading module.

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