A preparation method for calligraphy and painting ink suitable for high-temperature calcined Dian tiles

Abstract

The present invention relates to the technical field of calligraphy and painting ink for Yunnan tiles, and specifically is a preparation method for calligraphy and painting ink suitable for high-temperature calcined Yunnan tiles, and the steps are as follows: S1, glaze preparation; S2, coloring oxide preparation; S3, blending agent preparation; S4, diluent preparation; S5, mixing and blending; S6, blending agent dilution; S7, calligraphy and painting ink corrosion prevention; S8, calligraphy and painting ink filtration; S9, calligraphy and painting ink bottling and packaging. The present invention improves the smoothness of calligraphy and painting ink by blending agent, the glue in the blending agent increases the adhesion of calligraphy and painting ink, uses tea water brewed twice as a diluent, reduces dust and impurities in the tea water, improves the fineness of calligraphy and painting ink after mixing, and antiseptics calligraphy and painting ink, performs filtering operation after preparation, and grinds the filtrate and mixes it into calligraphy and painting ink again to avoid changes in the content of elements in calligraphy and painting ink, ensure the purity of ink color after calcination, and improves the brightness of ink by adding alum red into brilliant black.

Description

Technical Field

[0001] The invention relates to the technical field of special calligraphy and painting ink for Yunnan tiles, and in particular to a preparation method of special calligraphy and painting ink suitable for high-temperature calcination of Yunnan tiles. Background Art

[0002] Dian tile purple clay is the source of pottery handed down from ancient China and is the oldest pottery. In terms of mineral composition, the raw materials are taken from the local siliceous powder rock in Luoshipu, Jiangchuan District, and the original ore mud is used. No harmful substances are added during the firing process, and no glaze is applied. In terms of trace metal elements, it contains a variety of trace mineral elements and does not contain harmful substances such as lead, cadmium and other heavy metals. It is made through multiple processes. In order to increase the beauty of Dian tile purple clay, it is generally given through calligraphy and painting. Dian tile special calligraphy and painting ink is used for writing calligraphy and painting. Dian tile special calligraphy and painting ink needs to be calcined at high temperature, and it is required that the Dian tile special calligraphy and painting ink will not fade under high temperature calcination. Therefore, a special calligraphy and painting ink suitable for high temperature calcination of Dian tiles has emerged.

[0003] However, the calligraphy and painting inks currently available on the market that are suitable for high-temperature calcined Dian tiles are all prepared by mixing conventional glazes, coloring oxides, and tea. The prepared calligraphy and painting inks have low smoothness, which is not conducive to smooth writing. The adhesion of the calligraphy and painting inks is low, and they are prone to falling off after calcination, which is not conducive to the production effect of Dian tiles. Therefore, those skilled in the art provide a method for preparing calligraphy and painting inks that are suitable for high-temperature calcined Dian tiles to solve the problems raised in the above background technology. Summary of the Invention

[0004] The purpose of the present invention is to provide a method for preparing calligraphy and painting ink suitable for high-temperature calcination of Dian tiles, so as to solve the problems raised in the above background technology.

[0005] To achieve the above-mentioned purpose, the present invention provides the following technical solution: a method for preparing calligraphy and painting ink suitable for high-temperature calcination of Dian tiles, comprising the following steps:

[0006] S1. Glaze preparation: The steps for glaze preparation are as follows:

[0007] S101, taking out 7-8 parts of glaze A and 4-5 parts of glaze B by weight;

[0008] S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use;

[0009] S2, coloring oxide production: take out 60-80 parts of brilliant black and 1-3 parts of alum red by weight, mix the brilliant black and alum red and grind them, and store the ground materials as coloring oxide for later use;

[0010] S3, preparation of formulation: take out 40-50 parts of glue, 23-31 parts of glycerin, and 7-12 parts of frankincense oil by weight, mix glycerin and frankincense oil, add glue after mixing and stir clockwise, after stirring, place the material in a negative pressure tank for negative pressure treatment to remove bubbles in the material, and the treated material is stored as a formulation for standby use;

[0011] S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment and age for 5 days. Filter out the tea leaves in the liquid and save the liquid as the diluent for later use.

[0012] S5, mixing and blending: taking out 8-10 parts of glaze, 1-2 parts of coloring oxide and 0.2-0.4 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution;

[0013] S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink;

[0014] S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative;

[0015] S8, calligraphy and painting ink filtration: the calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again;

[0016] S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it.

[0017] As a further solution of the present invention: the glaze A in S1 is composed of the following components in parts by weight: calcium oxide, zinc oxide, barium oxide, magnesium oxide, quartz, aluminum oxide, and boron oxide in a weight ratio of 6:2:1:2:25:3:45.

[0018] As a further solution of the present invention: the glaze B in S1 is composed of the following components in parts by weight: calcium oxide, zinc oxide, potassium oxide, quartz, aluminum oxide, and mineralized boric acid, in a weight ratio of 3:2:6:25:3:45.

[0019] As a further solution of the present invention: the calcination temperature in S1 is 280-340° C., and the grinding fineness is 15-50 nm.

[0020] As a further solution of the present invention: the stirring time in S3 is 25 to 30 minutes, and the negative pressure is -5 to -15 MPa.

[0021] As a further solution of the present invention: the soaking time in S4 is 5 to 10 seconds, and the constant temperature is 20 to 23°C.

[0022] As a further solution of the present invention: the filter fineness in S8 is 15-25nm, and the grinding fineness is 15-25nm.

[0023] Compared with the prior art, the present invention has the following beneficial effects:

[0024] The invention discloses a method for preparing calligraphy and painting ink suitable for high-temperature calcining of Dian tiles. The method adopts a mixed glaze prepared by mixing different glazes, glaze A and glaze B, as a main material, thereby improving the heat resistance of the calligraphy and painting ink for Dian tiles. The glaze does not contain lead, thereby improving the safety of the Dian tiles after firing and avoiding harm to the health of users.

[0025] The blending agent improves the smoothness of calligraphy and painting ink and the fluency of writing. The glue in the blending agent increases the adhesion of calligraphy and painting ink to prevent the calligraphy and painting ink from falling off during the calcination process of Dian tiles, which is beneficial to the production effect of Dian tiles.

[0026] Use the second brewed tea as a diluent to reduce dust and impurities in the tea, increase the fineness of the mixed calligraphy and painting ink, and further improve the writing effect;

[0027] Use preservatives to preserve calligraphy and painting ink to prevent it from deteriorating and forming mold during storage;

[0028] After production, the filter operation is carried out, and the filter material is ground and mixed into the calligraphy and painting ink again to avoid changes in the element content in the calligraphy and painting ink, ensure the purity of the ink color after calcination, and increase the brightness of the ink by adding alum red to the bright black. DETAILED DESCRIPTION Example

[0029] A method for preparing calligraphy and painting ink suitable for high-temperature calcined Dian tiles, comprising the following steps:

[0030] S1. Glaze preparation: The steps for glaze preparation are as follows:

[0031] S101, taking out 7 parts of glaze A and 4 parts of glaze B by weight;

[0032] S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use, the calcination temperature is 280-340° C., and the grinding fineness is 15-50 nm;

[0033] S2, coloring oxide production: take out 60 parts of brilliant black and 1 part of alum red by weight, mix the brilliant black and alum red and grind them, and the ground material is stored as a coloring oxide for later use;

[0034] S3, formulation making: take out 40 parts of glue, 23 parts of glycerine, 7 parts of frankincense oil by weight, mix glycerine and frankincense oil, add glue after mixing and stir clockwise, after stirring, material is placed in negative pressure tank and processed under negative pressure, remove the bubble in the material, the material after treatment is preserved as formulation for standby use, and the mixing time is 25~30min, negative pressure-5~-15MPa;

[0035] S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment to age for 5 days. Filter out the tea leaves in the liquid and save the liquid as a diluent for later use. Soak for 5 to 10 seconds at a constant temperature of 20 to 23°C.

[0036] S5, taking out 8 parts of glaze, 1 part of coloring oxide and 0.2 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution;

[0037] S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink;

[0038] S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative;

[0039] S8. Calligraphy and Painting Ink Filtration: The calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, and the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again. The filter fineness is 15-25nm, and the grinding fineness is 15-25nm;

[0040] S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it. Example

[0041] A method for preparing calligraphy and painting ink suitable for high-temperature calcined Dian tiles, comprising the following steps:

[0042] S1. Glaze preparation: The steps for glaze preparation are as follows:

[0043] S101, taking out 7 parts of glaze A and 4 parts of glaze B by weight;

[0044] S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use, the calcination temperature is 280-340° C., and the grinding fineness is 15-50 nm;

[0045] S2, coloring oxide production: take out 60 parts of brilliant black and 1 part of alum red by weight, mix the brilliant black and alum red and grind them, and the ground material is stored as a coloring oxide for later use;

[0046] S3, formulation making: take out 50 parts of glue, 31 parts of glycerine, 12 parts of frankincense oil by weight, mix glycerine and frankincense oil, add glue after mixing and stir clockwise, after stirring, material is placed in negative pressure tank and processed under negative pressure, remove the bubble in the material, the material after treatment is preserved as formulation for standby use, and the mixing time is 25~30min, negative pressure-5~-15MPa;

[0047] S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment to age for 5 days. Filter out the tea leaves in the liquid and save the liquid as a diluent for later use. Soak for 5 to 10 seconds at a constant temperature of 20 to 23°C.

[0048] S5. Mixing and blending: taking out 8 parts of glaze, 2 parts of coloring oxide and 0.4 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution;

[0049] S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink;

[0050] S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative;

[0051] S8. Calligraphy and Painting Ink Filtration: The calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, and the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again. The filter fineness is 15-25nm, and the grinding fineness is 15-25nm;

[0052] S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it. Example

[0053] A method for preparing calligraphy and painting ink suitable for high-temperature calcined Dian tiles, comprising the following steps:

[0054] S1. Glaze preparation: The steps for glaze preparation are as follows:

[0055] S101, taking out 8 parts of glaze A and 5 parts of glaze B by weight;

[0056] S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use, the calcination temperature is 280-340° C., and the grinding fineness is 15-50 nm;

[0057] S2, coloring oxide production: take out 80 parts of brilliant black and 3 parts of alum red by weight, mix the brilliant black and alum red and grind them, and the ground material is stored as a coloring oxide for later use;

[0058] S3, formulation making: take out 40 parts of glue, 23 parts of glycerine, 7 parts of frankincense oil by weight, mix glycerine and frankincense oil, add glue after mixing and stir clockwise, after stirring, material is placed in negative pressure tank and processed under negative pressure, remove the bubble in the material, the material after treatment is preserved as formulation for standby use, and the mixing time is 25~30min, negative pressure-5~-15MPa;

[0059] S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment to age for 5 days. Filter out the tea leaves in the liquid and save the liquid as a diluent for later use. Soak for 5 to 10 seconds at a constant temperature of 20 to 23°C.

[0060] S5, taking out 10 parts of glaze, 1 part of coloring oxide and 0.2 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution;

[0061] S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink;

[0062] S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative;

[0063] S8. Calligraphy and Painting Ink Filtration: The calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, and the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again. The filter fineness is 15-25nm, and the grinding fineness is 15-25nm;

[0064] S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it. Example

[0065] A method for preparing calligraphy and painting ink suitable for high-temperature calcined Dian tiles, comprising the following steps:

[0066] S1. Glaze preparation: The steps for glaze preparation are as follows:

[0067] S101, taking out 8 parts of glaze A and 5 parts of glaze B by weight;

[0068] S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use, the calcination temperature is 280-340° C., and the grinding fineness is 15-50 nm;

[0069] S2, coloring oxide production: take out 80 parts of brilliant black and 3 parts of alum red by weight, mix brilliant black and alum red and grind them, and the ground material is stored as a coloring oxide for later use;

[0070] S3, formulation making: take out 50 parts of glue, 31 parts of glycerine, 12 parts of frankincense oil by weight, mix glycerine and frankincense oil, add glue after mixing and stir clockwise, after stirring, material is placed in negative pressure tank and processed under negative pressure, remove the bubble in the material, the material after treatment is preserved as formulation for standby use, and the mixing time is 25~30min, negative pressure-5~-15MPa;

[0071] S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment to age for 5 days. Filter out the tea leaves in the liquid and save the liquid as a diluent for later use. Soak for 5 to 10 seconds at a constant temperature of 20 to 23°C.

[0072] S5, taking out 10 parts of glaze, 2 parts of coloring oxide and 0.4 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution;

[0073] S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink;

[0074] S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative;

[0075] S8. Calligraphy and Painting Ink Filtration: The calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, and the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again. The filter fineness is 15-25nm, and the grinding fineness is 15-25nm;

[0076] S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it.

[0077] The contents of Example 1, Example 2, Example 3 and Example 4 also include:

[0078] Glaze A is composed of the following parts by weight: calcium oxide, zinc oxide, barium oxide, magnesium oxide, quartz, aluminum oxide, and boron oxide in a weight ratio of 6:2:1:2:25:3:45. Glaze B is composed of the following parts by weight: calcium oxide, zinc oxide, potassium oxide, quartz, aluminum oxide, and mineralized boric acid in a weight ratio of 3:2:6:25:3:45.

[0079] The above is only a preferred specific embodiment of the present invention, but the scope of protection of the present invention is not limited thereto. Any technician familiar with this technical field, within the technical scope disclosed by the present invention, who makes equivalent replacements or changes based on the technical solutions and inventive concepts of the present invention, should be covered by the scope of protection of the present invention.

Claims

1. A method for preparing calligraphy and painting ink suitable for high-temperature calcination of Dian tiles, characterized in that: Here are the steps: S1. Glaze preparation: The steps for glaze preparation are as follows: S101, taking out 7-8 parts of glaze A and 4-5 parts of glaze B by weight; S102, calcining glaze A and glaze B at high temperature respectively, mixing the calcined glaze A and glaze B, grinding the mixed glaze, and storing the ground glaze for later use; S2, coloring oxide production: take out 60-80 parts of brilliant black and 1-3 parts of alum red by weight, mix the brilliant black and alum red and grind them, and store the ground materials as coloring oxide for later use; S3, preparation of formulation: take out 40-50 parts of glue, 23-31 parts of glycerin, and 7-12 parts of frankincense oil by weight, mix glycerin and frankincense oil, add glue after mixing and stir clockwise, after stirring, place the material in a negative pressure tank for negative pressure treatment to remove bubbles in the material, and the treated material is stored as a formulation for standby use; S4. Preparation of diluent: Select aged tea and brew it with boiling water. After soaking, pour out the liquid inside and pour in boiling water again. Place in a constant temperature environment and age for 5 days. Filter out the tea leaves in the liquid and save the liquid as the diluent for later use. S5, mixing and blending: taking out 8-10 parts of glaze, 1-2 parts of coloring oxide and 0.2-0.4 parts of blending agent by weight, stirring the above materials to obtain calligraphy and painting ink stock solution; S6, mixing and diluting ingredients: the required concentration of calligraphy and painting ink is 50%, take out 50% of calligraphy and painting ink stock solution and add 50% of diluent, mix the above materials to obtain calligraphy and painting ink; S7, calligraphy and painting ink antiseptic: add 0.2-0.5% of the weight of calligraphy and painting ink ink preservative, mix the above materials, and complete the addition of preservative; S8, calligraphy and painting ink filtration: the calligraphy and painting ink is filtered by filter pressing, the filtered solid is ground, the ground solid is mixed with the filtered calligraphy and painting ink again, and the mixed solid is filtered again; S9. Bottling and packaging of calligraphy and painting ink: Pour the prepared calligraphy and painting ink into a 500ml glass bottle, seal the glass bottle, fix the glass bottle with a wooden frame, put it in a paper box and label it.

2. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The glaze A in S1 is composed of the following components in parts by weight: calcium oxide, zinc oxide, barium oxide, magnesium oxide, quartz, aluminum oxide, and boron oxide in a weight ratio of 6:2:1:2:25:3:

45.

3. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The glaze B in S1 is composed of the following components in parts by weight: calcium oxide, zinc oxide, potassium oxide, quartz, aluminum oxide, and mineralized boric acid in a weight ratio of 3:2:6:25:3:

45.

4. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The calcination temperature in S1 is 280-340° C., and the grinding fineness is 15-50 nm.

5. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The stirring time in S3 is 25 to 30 minutes, and the negative pressure is -5 to -15 MPa.

6. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The soaking time in S4 is 5 to 10 seconds, and the constant temperature is 20 to 23°C.

7. The method for preparing a special calligraphy and painting ink suitable for high-temperature calcination of Dian tiles according to claim 1, characterized in that: The filter fineness in S8 is 15-25 nm, and the grinding fineness is 15-25 nm.