A homogenizing reactor for mixing red phosphorus and porous nanocarbon

Abstract

The invention discloses a homogenizing reactor for mixing red phosphorus and porous nano-carbon. The invention relates to the technical field of reactors. When red phosphorus is heated to become liquid, the red phosphorus in contact with the inner wall of the reactor body begins to become liquid first. During the stirring process, a scraper is usually used to scrape the inner wall of the reactor body. However, after the scraping is completed, the inner material squeezes the outer material, so that the scraped material is pushed toward the inner wall of the reactor tank by the inner material again, causing the liquefied red phosphorus to contact the inner wall of the reactor tank again, reducing the scraping effect and easily causing uneven heating. Therefore, the spiral plate drives the liquefied red phosphorus to move inwards and upwards through the spiral shape, so that the liquefied red phosphorus and the porous carbon are fully contacted and mixed, and can cooperate with a scraper to prevent the material scraped by the scraper from being pushed toward the inner wall of the reactor tank again by the inner material, causing the liquefied red phosphorus to contact the inner wall of the reactor tank again, reducing the scraping effect and easily causing uneven heating.

Description

Technical Field

[0001] The invention relates to the technical field of reactors, in particular to a homogenizing reactor for mixing red phosphorus and porous nano-carbon. Background Art

[0002] At present, red phosphorus is a purple or slightly brown amorphous powder, shiny, stable in the air, sublimated when heated to 416°C, and its ignition point is about 240°C. Red phosphorus is often used to make matches, pesticides, fireworks, etc. It is also often used in chemical experiments, such as determining the oxygen content in the air. The mixing steps of red phosphorus and porous nanocarbon are as follows: add red phosphorus and porous nanocarbon in proportion and mix them together, put them into an autoclave, open the pressure, and heat them to melt the red phosphorus. Under high pressure, the red phosphorus fills the pores of the porous carbon, releases the pressure after condensation, and then crushes it into a ball mill;

[0003] When red phosphorus is heated and becomes liquid, the red phosphorus in contact with the inner wall of the kettle body begins to become liquid first. During the stirring process, a scraper is usually used to scrape the inner wall of the kettle body. However, after the scraping is completed, the inner material squeezes the outer material, causing the scraped material to be pushed toward the inner wall of the kettle again by the inner material, causing the liquefied red phosphorus to contact the inner wall of the kettle again, reducing the scraping effect and easily causing uneven heating. Summary of the invention

[0004] To achieve the above objectives, the present invention is implemented by the following technical scheme: a homogenizing reactor for mixing red phosphorus and porous nanocarbon, comprising:

[0005] A frame having a frame supporting the structural components, a pressure pump being fixedly mounted on the top of the frame, and a lifting platform extending from one side of the top of the frame, and a motor being fixedly mounted on the top of the lifting platform of the frame;

[0006] A kettle tank, which provides a place for homogenous reaction, and the kettle tank is installed inside the frame, a connecting pipe is fixedly installed on the top of the outer side of the kettle tank, and the kettle tank is connected to the pressure pump through the connecting pipe, and a material port is opened at the bottom of the kettle tank, and a blocking block is threadedly connected at the material port;

[0007] A feeding mechanism, which is used for the entry of materials and is installed on the top of the outside of the kettle;

[0008] A homogenizing mechanism, which is used for stirring and mixing materials, and is installed inside the kettle;

[0009] In which, the homogenizing mechanism includes a rotating shaft, the top of the rotating shaft is connected to the output end of the motor, and the bottom of the rotating shaft is fixedly connected to a rotating frame, the outer side of the rotating shaft is fixedly connected to a fixing ring, the bottom of the fixing ring is rotatably connected to a chassis, the bottom of the chassis is fixedly connected to the top of the kettle, and the bottom of the rotating frame is fixedly connected to a connecting ring. The number of the connecting rings is two and they are symmetrically arranged along the center position of the axis of the kettle, and scrapers are fixedly connected between the connecting rings, the scrapers are evenly installed along the center position of the connecting ring, and the outer side of the scraper is in contact with the inner wall of the kettle, and the inner wall of the connecting ring is fixedly connected to a spiral plate, which cooperates with the scraper through the spiral shape of the spiral plate, and when the scraper rotates After scraping up the red phosphorus that is first liquefied in contact with the inner wall of the kettle and pushing it inward for a certain distance, the spiral plate drives the liquefied red phosphorus to move inward and upward at the same time through the spiral shape, so that the liquefied red phosphorus and the porous carbon are fully contacted and mixed. At the same time, it can cooperate with the scraper to prevent the material scraped by the scraper from being pushed toward the inner wall of the kettle again by the internal material, causing the liquefied red phosphorus to contact the inner wall of the kettle again, reducing the scraping effect and easily causing uneven heating. The spiral plate is located between the connecting rings and is evenly installed along the center position of the connecting ring. An arc scraper is fixedly installed on the bottom of the connecting ring below. The arc scraper is evenly installed along the center position of the connecting ring, and the inner wall of the connecting ring below is fixedly connected with an internal stirring component.

[0010] Preferably, the internal stirring assembly comprises a fixed disk and a connecting rod, the connecting rod is evenly installed on the outer side of the fixed disk along the center position of the fixed disk, the fixed disk is fixedly connected to the inner wall of the connecting ring through the connecting rod, the top of the fixed disk is fixedly installed with a base, the center position of the top of the base is fixedly installed with a fixed shaft, the outer side of the fixed shaft is fixedly installed with a shaft sleeve, the outer side of the shaft sleeve is fixedly installed with a support plate, the support plates are evenly installed along the center position of the fixed shaft, and the outer side of the support plates is fixedly connected with the connecting shaft, the outer side of the connecting shaft is evenly provided with strip-shaped protrusions, the outer side of the connecting shaft is sleeved with an inner stirring wheel, the inner wall of the inner stirring wheel is evenly provided with strip-shaped grooves, and the grooves of the inner wall of the inner stirring wheel are fixedly connected with spring plates, and through the elastic deformation characteristics of the spring plates, The spring plate cooperates with the groove on the inner wall of the inner stirring wheel and the strip protrusion on the outer side of the connecting shaft, so that the reaction force of the material on the inner stirring wheel presses the spring plate to deform into the groove and releases the contact with the strip protrusion, so that the inner stirring wheel can rotate along the center of the fixed axis while rotating along the center of the connecting axis, so that the inner stirring wheel turns the material at the center position, so that the material is fully driven to contact, the spring plate is located between the strip protrusions of the connecting shaft, and the outer side of the inner stirring wheel is evenly provided with spiral blades. Through the spiral blades on the outer side of the inner stirring wheel, in the process of the inner stirring wheel rotating along the center of the fixed axis, the porous carbon and red phosphorus at the center position are transmitted to the outside through its own spiral blades, close to the inner wall of the kettle, and cooperate with the scraper bar and the spiral plate to make the material fully contact with the inner wall of the kettle, so that the material is evenly heated and the homogeneous mixing effect is improved at the same time.

[0011] Preferably, the kettle tank includes an outer cover tube, the center position of the outer side of the outer cover tube is fixedly connected to the inner wall of the frame, and the inner wall of the outer cover tube is fixedly connected to the kettle tube, there is a space between the kettle tube and the outer cover tube, and the inner wall of the kettle tube fits with the outer side of the connecting ring, the top of the kettle tube is fixedly connected to the bottom of the chassis, the outer cover tube is made of heat insulating material, a material port is installed at the center position of the bottom of the kettle tube, and the material port of the kettle tube is closed by a block, a liquid inlet pipe is fixedly installed at the top of the outer side of the outer cover tube, and a liquid outlet pipe is fixedly installed at the bottom of the outer side of the outer cover tube, the feeding mechanism includes a fixed tube, the outer side of the fixed tube is fixedly connected to the inner wall of the kettle tube, and the end of the fixed tube away from the kettle tube is fixedly connected to a cavity tube, and the outer side of the cavity tube is fixedly connected to a rotating The buckle, the cavity tube is rotatably installed with a tube cover by a turning buckle, the inner wall of the tube cover is fixedly connected with a ring cover, the inner wall of the fixed tube is slidably installed with a slide cylinder, the top of the outer side of the slide cylinder is an inwardly concave inclined surface, and the outer side of the slide cylinder is clamped with the inner wall of the cavity tube, the ring cover is made of elastic deformation material, and is pushed by the pressure under the high pressure in the kettle cylinder through the slide cylinder, slides upward along the inner wall of the fixed tube, and contacts with the elastic inner wall of the ring cover through the inclined surface of its own outer top, and squeezes the ring cover to the inner wall of the cavity tube to deform, when the tube cover and the cavity tube are fixed, the air outlet gap is reduced, the sealing is improved, and air leakage is prevented during the homogenous reaction, resulting in a decrease in air pressure and affecting the reaction, and the inner wall of the ring cover is in contact with the inclined surface of the outer side of the slide cylinder, and the bottom end of the slide cylinder is a closed concave arc surface.

[0012] The present invention provides a homogenizing reactor for mixing red phosphorus and porous nanocarbon. It has the following beneficial effects:

[0013] 1. The homogenizing reactor for mixing red phosphorus and porous nano-carbon cooperates with the scraper through the spiral shape of the spiral plate. After the scraper rotates to scrape up the red phosphorus that is first liquefied in contact with the inner wall of the reactor and pushes it inward for a certain distance, the spiral plate drives the liquefied red phosphorus to move inward and upward at the same time through the spiral shape, so that the liquefied red phosphorus and the porous carbon are fully contacted and mixed. At the same time, the scraper can be cooperated with to prevent the material scraped by the scraper from being pushed to the inner wall of the reactor again by the internal material, causing the liquefied red phosphorus to contact the inner wall of the reactor again, reducing the scraping effect and easily causing uneven heating.

[0014] Second, the homogenizing reactor for mixing red phosphorus and porous nano-carbon uses the elastic deformation characteristics of the spring plate to make the spring plate cooperate with the groove on the inner wall of the inner stirring wheel and the strip protrusion on the outer side of the connecting shaft, so that the reaction force of the material on the inner stirring wheel presses the spring plate to deform into the groove, releasing the contact with the strip protrusion, so that the inner stirring wheel can rotate along the center of the fixed axis while rotating along the center of the connecting axis, so that the inner stirring wheel turns the material at the center position, so that the material is fully driven to contact.

[0015] 3. The homogenizing reactor for mixing red phosphorus and porous nano-carbon uses the spiral blades on the outer side of the inner stirring wheel. During the rotation of the inner stirring wheel along the center of the fixed axis, the spiral blades transmit the porous carbon and red phosphorus at the center to the outside and close to the inner wall of the reactor. The scraper and the spiral plate are used to make the materials fully contact with the inner wall of the reactor, so that the materials are evenly heated and the homogenizing mixing effect is improved.

[0016] Fourth, the homogenizing reactor in which red phosphorus and porous nano-carbon are mixed is pushed by the pressure under high pressure in the reactor cylinder through the slide cylinder, slides upward along the inner wall of the fixed tube, and contacts the inner wall of the elastic ring cover through the inclined surface of its outer top, squeezes the ring cover toward the inner wall of the cavity tube, and when the tube cover and the cavity tube are fixed, the air outlet gap is reduced, the sealing is improved, and air leakage is prevented during the homogenizing reaction, which causes the air pressure to drop and affects the reaction. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 This is a schematic diagram of the external structure of a homogenizing reactor for mixing red phosphorus and porous nano-carbon according to the present invention;

[0018] Figure 2 This is a partial structural schematic diagram of a homogenizing reactor for mixing red phosphorus and porous nano-carbon according to the present invention;

[0019] Figure 3 This is a partial structural dissection diagram of a homogenizing reactor for mixing red phosphorus and porous nano-carbon according to the present invention;

[0020] Figure 4 It is a schematic diagram of the homogenizing mechanism structure of the present invention;

[0021] Figure 5 It is a partial structural schematic diagram of the homogenizing mechanism of the present invention;

[0022] Figure 6 This is a schematic diagram of the structure of the internal stirring component of the present invention;

[0023] Figure 7 It is a partial structural anatomical diagram of the internal stirring component of the present invention;

[0024] Figure 8 This is a schematic diagram of the kettle structure of the present invention;

[0025] Fig. 9 It is a schematic diagram of the structure of the feeding mechanism of the present invention;

[0026] Fig.10 It is a structural dissection diagram of the feeding mechanism of the present invention.

[0027] In the figure: 1. frame; 2. homogenizing mechanism; 3. kettle; 4. feeding mechanism; 5. pressure pump; 6. connecting pipe; 7. motor; 8. block; 21. rotating shaft; 22. chassis; 23. rotating frame; 24. connecting ring; 25. fixing ring; 26. internal stirring assembly; 27. arc scraper; 28. spiral plate; 29. ​​scraper bar; 261. connecting rod; 262. fixing plate; 263. base; 264. fixing shaft; 265. bushing; 266. connecting shaft; 267. spring plate; 268. internal stirring wheel; 269. supporting plate; 31. outer cover tube; 32. liquid outlet pipe; 33. liquid inlet pipe; 34. kettle tube; 41. fixing tube; 42. cavity tube; 43. turn buckle; 44. tube cover; 46. slide tube; 45. ring cover. DETAILED DESCRIPTION

[0028] The present invention is further described in detail below in conjunction with the accompanying drawings and specific embodiments. The embodiments of the present invention are provided for the purpose of illustration and description, and are not intended to be exhaustive or to limit the present invention to the disclosed forms. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiments are selected and described in order to better illustrate the principles and practical applications of the present invention, and to enable those of ordinary skill in the art to understand the present invention and thereby design various embodiments with various modifications suitable for specific uses.

[0029] The first embodiment, as Figures 1 to 5 As shown, the present invention provides a technical solution: a homogenizing reactor for mixing red phosphorus and porous nanocarbon, comprising:

[0030] A frame 1 having a frame supporting the structural components, a pressure pump 5 is fixedly installed on the top of the frame 1, and a lifting platform extends from one side of the top of the frame 1, and a motor 7 is fixedly installed on the top of the lifting platform of the frame 1;

[0031] The kettle 3 provides a place for homogenization reaction, and the kettle 3 is installed inside the frame 1. A connecting pipe 6 is fixedly installed on the top of the outer side of the kettle 3, and the kettle 3 is connected to the pressure pump 5 through the connecting pipe 6. A material port is opened at the bottom of the kettle 3, and a blocking block 8 is threadedly connected to the material port;

[0032] A feeding mechanism 4, which is used for feeding materials, and is installed on the top of the outer side of the kettle 3;

[0033] A homogenizing mechanism 2, which is used for stirring and mixing materials, and is installed inside the kettle 3;

[0034] Among them, the homogenizing mechanism 2 includes a rotating shaft 21, the top of the rotating shaft 21 is connected to the output end of the motor 7, and the bottom of the rotating shaft 21 is fixedly connected to a rotating frame 23, the outer side of the rotating shaft 21 is fixedly connected to a fixing ring 25, the bottom of the fixing ring 25 is rotatably connected to a chassis 22, the bottom of the chassis 22 is fixedly connected to the top of the kettle 3, and the bottom of the rotating frame 23 is fixedly connected to a connecting ring 24. There are two connecting rings 24 and they are symmetrically arranged along the center position of the axis of the kettle 3, and scrapers 29 are fixedly connected between the connecting rings 24. The scrapers 29 are evenly installed along the center position of the connecting rings 24, and the outer side of the scrapers 29 fits the inner wall of the kettle 3. When the motor 7 drives the homogenizing mechanism 2 to rotate, the motor 7 drives the rotating shaft 21 to rotate, so that the rotating shaft 21 drives the rotating frame 23 to rotate under the restriction of the fixing ring 25 and the chassis 22, so that the rotating frame 23 drives the connecting ring 24 and the scraper 29 to rotate along the inner wall of the kettle cylinder 34. During the rotation, the scraper bar 29 scrapes the heated liquefied red phosphorus material on the inner wall of the kettle cylinder 34 and scrapes it inward for a certain distance. The inner wall of the connecting ring 24 is fixedly connected with a spiral plate 28. The spiral plate 28 is located between the connecting rings 24 and is evenly installed along the center position of the connecting ring 24. The bottom of the connecting ring 24 located below is fixedly installed with an arc scraper plate 27. During the rotation, the spiral plate 28 cooperates with the scraper bar 29 to drive the liquefied red phosphorus material that has been scraped inward for a certain distance. Through its own spiral shape, the material inside moves inward while being driven upward, so that the material can move in the vertical direction. At the same time, it cooperates with the stirring of the internal stirring component 26 at the center position to make the liquefied red phosphorus fully contact with the porous carbon and fill the holes of the porous carbon. The arc scraper plate 27 is evenly installed along the center position of the connecting ring 24, and the inner wall of the connecting ring 24 located below is fixedly connected with the internal stirring component 26.

[0035] The second embodiment is based on the first embodiment. Figure 6 to Figure 7 As shown, the internal stirring assembly 26 includes a fixed disk 262 and a connecting rod 261. The connecting rod 261 is evenly installed on the outer side of the fixed disk 262 along the center position of the fixed disk 262. The fixed disk 262 is fixedly connected to the inner wall of the connecting ring 24 through the connecting rod 261. A base 263 is fixedly installed on the top of the fixed disk 262. The fixed disk 262 is connected to the connecting ring 24 through the connecting rod 261, so that when the connecting ring 24 rotates, the fixed disk 262 drives the fixed shaft 264 to rotate through the base 263. When the fixed shaft 264 rotates, the inner stirring wheel 268 is driven to rotate through the contact between the strip protrusion on the outer side of the connecting shaft 266 and the spring plate 267. The fixed shaft 264 is fixedly installed at the center position of the top of the base 263.

[0036] A shaft sleeve 265 is fixedly installed on the outer side of the fixed shaft 264, and a support plate 269 is fixedly installed on the outer side of the shaft sleeve 265. The support plates 269 are evenly installed along the center position of the fixed shaft 264, and the outer side of the support plates 269 are fixedly connected to the connecting shaft 266. The outer side of the connecting shaft 266 is evenly provided with strip-shaped protrusions. The outer side of the connecting shaft 266 is sleeved with an inner stirring wheel 268. During the rotation of the inner stirring wheel 268, the material at the center position is driven to move through the outer spiral blades, and at the same time The reaction force of the material on the inner stirring wheel 268 presses the spring plate 267, causing the spring plate 267 to deform under pressure and break away from the restriction of the strip-shaped protrusion of the connecting shaft 266, so that the inner stirring wheel 268 rotates along the axis center of the connecting shaft 266. The inner wall of the inner stirring wheel 268 is evenly provided with strip-shaped grooves, and the grooves on the inner wall of the inner stirring wheel 268 are fixedly connected with spring plates 267. The spring plate 267 is located between the strip-shaped protrusions of the connecting shaft 266, and the outer side of the inner stirring wheel 268 is evenly provided with spiral blades.

[0037] The third embodiment is based on the first and second embodiments. Figures 8 to 10 As shown, the kettle 3 includes an outer cover tube 31, the center position of the outer side of the outer cover tube 31 is fixedly connected to the inner wall of the frame 1, and the inner wall of the outer cover tube 31 is fixedly connected to the kettle tube 34, there is a space between the kettle tube 34 and the outer cover tube 31, and the inner wall of the kettle tube 34 fits the outer side of the connecting ring 24, the top of the kettle tube 34 is fixedly connected to the bottom of the chassis 22, the outer cover tube 31 is made of heat-insulating material, and a material port is installed at the center of the bottom of the kettle tube 34, and the material port of the kettle tube 34 is closed by a blocking block 8. When hot water is introduced, the pipeline is respectively connected to the liquid inlet pipe 33 and the liquid outlet pipe 32. The outer cover tube 31 and the kettle tube 34 are connected so that hot water can enter the gap between the outer cover tube 31 and the kettle tube 34 through the liquid inlet pipe 33, and the heat of the hot water can be transferred to the material inside the kettle tube 34 through the kettle tube 34, so that the red phosphorus is melted by the heat. The liquid inlet pipe 33 is fixedly installed on the top of the outer side of the outer cover tube 31. The red phosphorus fills the pores of the porous carbon under high pressure. At the same time, the red phosphorus and the porous carbon are fully mixed with the rotation of the homogenizing mechanism 2. After the homogenizing reaction is completed, the block 8 is removed, and the material inside the kettle tube 34 is discharged from the material port at the bottom. The outer cover tube 31 has a liquid outlet pipe 32 fixedly installed on the bottom of the outer side of the outer cover tube 31.

[0038] The feeding mechanism 4 includes a fixed tube 41, the outer side of the fixed tube 41 is fixedly connected to the inner wall of the kettle cylinder 34, and the end of the fixed tube 41 away from the kettle cylinder 34 is fixedly connected to a cavity tube 42, the outer side of the cavity tube 42 is fixedly connected to a turn buckle 43, the cavity tube 42 is rotatably mounted with a tube cover 44 through the turn buckle 43, the inner wall of the tube cover 44 is fixedly connected to a ring cover 45, and the inner wall of the fixed tube 41 is slidably mounted with a slide tube 46, the top of the outer side of the slide tube 46 is an inwardly concave inclined surface, the tube cover 44 and the cavity tube 42 are opened, and the slide tube 46 is taken out to make the pipeline between the cavity tube 42 and the fixed tube 41 conductive, and the red phosphorus and porous carbon are introduced into the interior of the kettle cylinder 34 through the pipeline, and the material is charged into the fixed tube 41. After all the materials are put in, the slide 46 is put into the fixed tube 41, and the position of the slide 46 is limited by the cavity 42. Finally, the tube cover 44 is clamped and closed with the cavity 42, so that the inner wall of the ring cover 45 fits with the inclined surface of the outer side of the slide 46, and the outer side of the slide 46 is clamped with the inner wall of the cavity 42. The ring cover 45 is made of elastic deformation material, and the inner wall of the ring cover 45 fits with the inclined surface of the outer side of the slide 46. Under the condition of internal high pressure, the air pressure pushes the slide 46 inside the fixed tube 41 to move upward. During the upward movement, the inclined surface of the slide 46 presses the ring cover 45 outward to deform, thereby increasing the sealing degree, and the bottom end of the slide 46 is a closed concave arc surface.

[0039] When in use, workers put red phosphorus and porous nanocarbon into the kettle 3 through the feeding mechanism 4 in proportion, and connect hot water to the kettle 3 through a pipe to heat the materials in the kettle 3, and introduce gas into the kettle 3 through the connecting pipe 6 through the pressure pump 5 to create a high temperature and high pressure environment in the kettle 3. Then the workers start the motor 7 to drive the homogenizing mechanism 2 to stir the internal materials for mixing.

[0040] When hot water is introduced, the pipeline is connected with the liquid inlet pipe 33 and the liquid outlet pipe 32 respectively, so that the hot water enters the gap between the outer cover tube 31 and the kettle tube 34 through the pipeline from the liquid inlet pipe 33, and the heat of the hot water is transferred to the material inside the kettle tube 34 through the kettle tube 34, so that the red phosphorus is melted by the heat. Under high pressure, the red phosphorus fills the pores of the porous carbon. At the same time, with the rotation of the homogenizing mechanism 2, the red phosphorus and the porous carbon are fully mixed. After the homogenizing reaction is completed, the blockage 8 is removed, and the material inside the kettle tube 34 is discharged from the material outlet at the bottom.

[0041] When the material is introduced through the feeding mechanism 4, the tube cover 44 and the cavity tube 42 are opened, and the slide 46 is taken out to make the pipeline between the cavity tube 42 and the fixed tube 41 conductive, and the red phosphorus and porous carbon are introduced into the interior of the kettle tube 34 through the pipeline. After all the materials are put in, the slide 46 is put into the interior of the fixed tube 41, and the position of the slide 46 is limited by the cavity tube 42. Finally, the tube cover 44 and the cavity tube 42 are snap-fitted and closed, so that the inner wall of the ring cover 45 fits with the inclined surface of the outer side of the slide 46. Under the condition of internal high pressure, the air pressure pushes the slide 46 inside the fixed tube 41 to move upward. During the upward movement, the inclined surface of the slide 46 presses the ring cover 45 outward to deform, thereby increasing the sealing degree.

[0042] When the motor 7 drives the homogenizing mechanism 2 to rotate, the motor 7 drives the rotating shaft 21 to rotate, so that the rotating shaft 21 drives the rotating frame 23 to rotate under the restriction of the fixed ring 25 and the chassis 22, so that the rotating frame 23 drives the connecting ring 24 and the scraper bar 29 to rotate along the inner wall of the kettle cylinder 34. During the rotation, the red phosphorus material on the inner wall of the kettle cylinder 34 that is heated and liquefied is scraped by the scraper bar 29 and is scraped inward for a certain distance. During the rotation, the spiral plate 28 cooperates with the scraper bar 29 to drive the liquefied red phosphorus material that has been scraped inward for a certain distance. Through its own spiral shape, while the internal material moves inward, it is driven upward, so that the material can move in the vertical direction. At the same time, the stirring of the internal stirring component 26 at the center position is cooperated to make the liquefied red phosphorus fully contact with the porous carbon and fill the pores of the porous carbon.

[0043] In the internal stirring assembly 26, the fixed disk 262 is connected to the connecting ring 24 through the connecting rod 261, so that when the connecting ring 24 rotates, the fixed disk 262 is driven to rotate, and the fixed disk 262 drives the fixed shaft 264 to rotate through the base 263. When the fixed shaft 264 rotates, the contact between the strip protrusion on the outside of the connecting shaft 266 and the spring plate 267 drives the internal stirring wheel 268 to rotate. During the rotation of the internal stirring wheel 268, the material at the center position is driven to move through the spiral blades on the outside. At the same time, the reaction force of the material on the internal stirring wheel 268 presses the spring plate 267, so that the spring plate 267 is deformed under pressure, breaking away from the restriction of the strip protrusion of the connecting shaft 266, and causing the internal stirring wheel 268 to rotate along the axis center of the connecting shaft 266.

[0044] Obviously, the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field and related fields without creative work should fall within the scope of protection of the present invention. The structures, devices and operating methods not specifically described and explained in the present invention are implemented according to the conventional means in the field unless otherwise specified and limited.

Claims

1. A homogenizing reactor for mixing red phosphorus and porous nanocarbon, characterized in that: include: A frame (1), the frame (1) having a frame supporting a structural component, a pressure pump (5) being fixedly mounted on the top of the frame (1), and a lifting platform extending from one side of the top of the frame (1), and a motor (7) being fixedly mounted on the top of the lifting platform of the frame (1); A kettle (3), the kettle (3) providing a place for homogenizing reaction, and the kettle (3) being installed inside the frame (1), a connecting pipe (6) being fixedly installed on the top of the outer side of the kettle (3), and the kettle (3) being connected to a pressure pump (5) via the connecting pipe (6), a material port being opened at the bottom of the kettle (3), and a blocking block (8) being threadedly connected at the material port; A feeding mechanism (4), the feeding mechanism (4) is used for feeding materials, and the feeding mechanism (4) is installed on the top of the outer side of the kettle (3); A homogenizing mechanism (2), the homogenizing mechanism (2) is used for stirring and mixing materials, and the homogenizing mechanism (2) is installed inside the kettle (3); The homogenizing mechanism (2) comprises a rotating shaft (21), the top of the rotating shaft (21) is connected to the output end of the motor (7), and the bottom of the rotating shaft (21) is fixedly connected to a rotating frame (23), the outer side of the rotating shaft (21) is fixedly connected to a fixing ring (25), the bottom of the fixing ring (25) is rotatably connected to a chassis (22), the bottom of the chassis (22) is fixedly connected to the top of the kettle (3), the bottom of the rotating frame (23) is fixedly connected to a connecting ring (24), and the connecting ring (25) is fixedly connected to the bottom of the rotating frame (23). The number of the connecting rings (24) is two and they are symmetrically arranged along the central position of the axis of the kettle (3), and a scraper strip (29) is fixedly connected between the connecting rings (24), the scraper strip (29) is evenly installed along the center position of the circle of the connecting ring (24), and the outer side of the scraper strip (29) is in contact with the inner wall of the kettle (3), and the inner wall of the connecting ring (24) is fixedly connected with a spiral plate (28), the spiral plate (28) is located between the connecting rings (24) and evenly installed along the center position of the circle of the connecting ring (24); An arc scraper (27) is fixedly mounted on the bottom of the lower connecting ring (24), the arc scraper (27) being evenly mounted along the center of the connecting ring (24), and an internal stirring assembly (26) is fixedly connected to the inner wall of the lower connecting ring (24); The internal stirring assembly (26) comprises a fixed disk (262) and a connecting rod (261); the connecting rod (261) is evenly mounted on the outer side of the fixed disk (262) along the center position of the fixed disk (262); the fixed disk (262) is fixedly connected to the inner wall of the connecting ring (24) via the connecting rod (261); a base (263) is fixedly mounted on the top of the fixed disk (262); and a fixed shaft (264) is fixedly mounted at the center position of the top of the base (263); A shaft sleeve (265) is fixedly mounted on the outer side of the fixed shaft (264), a support plate (269) is fixedly mounted on the outer side of the shaft sleeve (265), the support plates (269) are evenly mounted along the center of the fixed shaft (264), and the outer sides of the support plates (269) are fixedly connected to connecting shafts (266), and the outer sides of the connecting shafts (266) are evenly provided with strip-shaped protrusions; An inner stirring wheel (268) is sleeved on the outer side of the connecting shaft (266), and strip-shaped grooves are evenly formed on the inner wall of the inner stirring wheel (268). Spring plates (267) are fixedly connected to the grooves on the inner wall of the inner stirring wheel (268), and the spring plates (267) are located between the strip-shaped protrusions of the connecting shaft (266). Spiral blades are evenly formed on the outer side of the inner stirring wheel (268); The kettle (3) comprises an outer cover tube (31), the center position of the outer side of the outer cover tube (31) is fixedly connected to the inner wall of the frame (1), and the inner wall of the outer cover tube (31) is fixedly connected to a kettle tube (34), there is a space between the kettle tube (34) and the outer cover tube (31), and the inner wall of the kettle tube (34) is in contact with the outer side of the connecting ring (24), and the top of the kettle tube (34) is fixedly connected to the bottom of the chassis (22); The outer cover tube (31) is made of a heat-insulating material, a material opening is installed at the center of the bottom of the kettle tube (34), and the material opening of the kettle tube (34) is closed by a block (8), a liquid inlet pipe (33) is fixedly installed at the top of the outer side of the outer cover tube (31), and a liquid outlet pipe (32) is fixedly installed at the bottom of the outer side of the outer cover tube (31); The feeding mechanism (4) comprises a fixed tube (41), the outer side of the fixed tube (41) is fixedly connected to the inner wall of the kettle cylinder (34), and the end of the fixed tube (41) away from the kettle cylinder (34) is fixedly connected to a cavity tube (42), the outer side of the cavity tube (42) is fixedly connected to a turn buckle (43), and the cavity tube (42) is rotatably mounted with a tube cover (44) via the turn buckle (43).

2. The homogenizing reactor for mixing red phosphorus and porous nanocarbon according to claim 1, characterized in that: The inner wall of the tube cover (44) is fixedly connected with a ring cover (45), and the inner wall of the fixed tube (41) is slidably mounted with a slide tube (46), the top of the outer side of the slide tube (46) is an inwardly concave inclined surface, and the outer side of the slide tube (46) is clamped with the inner wall of the cavity tube (42).

3. The homogenizing reactor for mixing red phosphorus and porous nanocarbon according to claim 2, characterized in that: The ring cover (45) is made of an elastic deformable material, and the inner wall of the ring cover (45) fits the inclined surface of the outer side of the slide cylinder (46), and the bottom end of the slide cylinder (46) is a closed concave arc surface.

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