A bio-calcium far-infrared material and its preparation method

Abstract

This invention discloses a bio-calcium far-infrared material and its preparation method, belonging to the field of functional materials technology. It is mainly composed of calcium carbonate powder, the raw material source of which includes the shells of aquatic organisms. The calcium carbonate powder is prepared into a porous honeycomb structure, within which far-infrared radiation waves are concentrated. In a first state, the far-infrared radiation waves concentrated within the honeycomb structure remain within the structure. In a second state, the far-infrared radiation waves concentrated within the honeycomb structure resonate with a target, thereby activating cells and promoting metabolism. This invention achieves the effects of improving human microcirculation and enhancing bodily functions while reducing environmental damage during production and conserving resources.

Description

Technical Field

[0001] This invention relates to the field of functional materials technology, and in particular to a far-infrared material, especially a bio-calcium far-infrared material and its preparation method. Background Technology

[0002] Sunlight can be broadly divided into visible light and invisible light. Visible light, when refracted through a prism, produces rays of violet, blue, cyan, green, yellow, orange, and red (the spectrum). Light beyond the red zone, with wavelengths ranging from 0.76 to 1000 micrometers in the spectrum, is called infrared light, also known as infrared radiation. Infrared radiation belongs to the electromagnetic spectrum and is a type of radiation with strong thermal effects. The wavelength range of infrared radiation is very wide; it is divided into near-infrared, mid-infrared, and far-infrared regions, with corresponding electromagnetic waves called near-infrared, mid-infrared, and far-infrared radiation. Infrared radiation is a type of light wave; its wavelength is shorter than radio waves but longer than visible light. Infrared radiation is invisible to the naked eye, but all objects emit infrared radiation. Hot objects emit stronger infrared radiation than cold objects. In the medical field, infrared radiation with wavelengths greater than 2.5 μm is generally referred to as far-infrared radiation. Among these, the wavelength band of 4-16 μm is called "life-giving light" because it can be effectively absorbed by living organisms.

[0003] Far-infrared rays offer numerous health benefits. By emitting far-infrared rays, their frequencies resonate with the body's surface, promoting microcirculation and overall health. Many infrared-emitting products are currently available. For example:

[0004] Existing technology (CN106726628B) discloses a negative ion far-infrared nano-multifunctional material, comprising, by weight: 1-86 parts of ore powder; 1-115 parts of rare earth powder; and 1-200 parts of silica gel. The functional material provided by this invention, based on existing technology, offers a method to significantly enhance the ability of ores and rare earth salts to ionize air and generate negative ions, while also significantly enhancing the ability of ores and rare earth salts to release infrared rays.

[0005] Existing technology (CN107523158A) discloses a method for preparing an interior wall coating that sustainably releases negative ions and far-infrared rays. The weight percentage of the raw materials in the coating is as follows: acrylic emulsion and modified acrylic emulsion 20-30%, ethylene glycol 1-2%, defoamer 0.2-0.5%, wetting and dispersing agent 0.2-0.3%, film-forming aid 0.8-1.2%, heavy calcium carbonate 10-20%, titanium dioxide 10-15%, tourmaline 10-15%, negative ion initiator 0.8-1.2%, kaolin 8-12%, thickener 0.2-0.8%, bactericide 0.1-0.2%, and grade III water 20-40%. This invention selects tourmaline as the far-infrared emitting material, ionizes it through an initiator, and adds it to the interior wall coating to form a negative ion source indoors. The product meets the requirements of GB6566-2010 "Limits of Radionuclides in Building Materials" for building materials standards.

[0006] However, in the process of implementing the technical solution in the prior art, the applicant discovered the following technical problems in the prior art:

[0007] Current technologies inevitably use tourmaline, rare earth elements, and ores as raw materials for far-infrared materials. However, the complex chemical composition of these materials results in varying radiation peaks in the emitted far-infrared radiation. The more peaks, the more complex the resonance, which can negatively impact the body's microcirculation. Furthermore, the large-scale mining of tourmaline, rare earth elements, and ores for far-infrared functional materials easily damages the ecological environment. If we could rely on the continuous supply of marine biological resources and the reuse of their waste, we could not only achieve innovative waste-to-treasure transformation but also create broader economic and social benefits. Summary of the Invention

[0008] The technical problem to be solved by this invention is to provide a biological calcium far-infrared material, which solves the problems of poor effect of infrared materials on promoting human microcirculation, damage to the ecological environment and waste of resources during production, as well as the safety hazards of excessive radioactive nuclides that may exist when functional materials act on the human body. It achieves one of the technical effects of improving human microcirculation and promoting metabolism, reducing environmental damage during production and saving resources, and eliminating the safety hazards of functional materials.

[0009] To solve the above-mentioned technical problems, the technical solution of the present invention is as follows:

[0010] A bio-calcium far-infrared material, mainly composed of calcium carbonate, the raw material source of which includes the shells of aquatic organisms; the calcium carbonate material is prepared into a porous honeycomb structure, and far-infrared radiation waves are concentrated within the honeycomb structure.

[0011] In the first state, the far-infrared radiation waves gathered within the honeycomb structure of the bio-calcium far-infrared material remain within the honeycomb structure.

[0012] In the second state, the far-infrared radiation waves gathered within the honeycomb structure of the bio-calcium far-infrared material resonate with the target location; the resonance between the bio-calcium far-infrared material and the target location can prevent the far-infrared radiation waves gathered within the honeycomb structure from being released and depleted.

[0013] Preferably, the calcium carbonate content is above 95%; the wavelength range of the far-infrared radiation wave is 2.5-25 μm; the effective far-infrared radiation wavelength range is 4-16 μm; the radiation energy in the effective far-infrared radiation wavelength range is greater than 50% of its total radiation energy; and the normal emissivity of the far-infrared radiation wave reaches 0.85.

[0014] Preferably, the first state is a storage state, and the second state is the state when acting on the target; the target includes a human body part.

[0015] More preferably, the calcium carbonate content is 98% or more; the wavelength range of the far-infrared radiation wave is 2.5-25 μm; the effective far-infrared radiation wavelength range is 4-16 μm, and more preferably, the radiation energy in the effective far-infrared radiation wavelength range is greater than 70% of its total radiation energy.

[0016] More preferably, the calcium carbonate material is mainly composed of a biological shell.

[0017] More preferably, the far-infrared radiation wave exists within the honeycomb structure in the form of an electromagnetic wave.

[0018] More preferably, the normal total emissivity of the far-infrared radiation wave reaches 0.9, and the energy spectrum of the far-infrared radiation wave detected during nuclear magnetic resonance detection exhibits a relatively single peak.

[0019] More preferably, the inner cavity of the honeycomb structure is larger than the outlet. After an energy imparting process, far-infrared radiation waves generate a cyclone in the inner cavity of the honeycomb structure, wherein the cyclone does not leave the outlet of the honeycomb structure when it is in a static state.

[0020] Another problem to be solved by the present invention is to provide a method for preparing a bio-calcium far-infrared material, comprising the following steps:

[0021] (S1) Raw material preparation: Use the shells of aquatic organisms containing biological calcium as raw materials;

[0022] (S2) Cleaning raw materials: Clean the raw materials and remove impurities;

[0023] (S3) Raw material crushing: The cleaned and impurity-removed raw materials are crushed into blocks for further processing;

[0024] (S4) Raw material grinding: Grind the crushed raw material into powder to obtain calcium carbonate powder material;

[0025] (S5) Energizing: The finished product is obtained by applying energy to the calcium carbonate powder material with a preset power and a preset time through an energy application device.

[0026] Preferably, in step (S2), when removing impurities, an infrared wave with a spiral waveform is emitted and applied to the raw material; in step (S5), the applied energy includes one or more energy-generating processes and a detection process.

[0027] More preferably, the calcium carbonate content of the raw material is greater than 98%. In step (S2), during impurity removal, a spiral-shaped infrared wave is used to emit a vibration frequency and apply it to the raw material; in step (S5), the applied energy undergoes multiple energizing and detection processes; the finished product is in the form of at least powder or granules.

[0028] The enabling process includes at least one of the following processes:

[0029] The first enabling process includes the following steps:

[0030] Place the raw material into the powder material storage device of the powder material empowerment resonator, start the resonator and resonate for 30-60 minutes at a power of 2-10KW and a frequency of 100-200KHz, and then store the powder.

[0031] The resonator includes an energy generating device, wherein the radiation wave emitted by the power generator of the energy generating device is in the shape of an Archimedean spiral; wherein the resonator emits a frequency of 12000K-100000K MHz according to the wavelength range of far-infrared light emitted by the power generator.

[0032] The storage device has a Ferris wheel structure and includes multiple powder storage boxes, a polygonal transmission mechanism, and a transmission motor. The transmission motor shaft is connected to the polygonal rotation mechanism, which consists of multiple symmetrical polygonal plates fixedly connected by a connecting shaft. Each corner of the inner side of the polygonal plates is provided with a hook, and the powder storage boxes are movably suspended on the hooks. A vertical stirring device is provided inside the powder storage box. The powder is stirred up and down inside the storage box by the vertical stirring device to improve the contact between the powder and far-infrared radiation.

[0033] The second energizing process involves placing powder in a shielded irradiation chamber or dynamically passing it through the shielded irradiation chamber; the shielded irradiation chamber consists of one or more irradiation chambers; the shielded irradiation chamber is equipped with multiple electron guns (the electron guns emit at a frequency of 10000K-100000KMHz), the upper end of the accelerating tube is connected to the electron gun, the lower end of the accelerating tube is connected to the scanning box through a vacuum tube, and a focusing coil and waveguide system are provided on the outside of the accelerating tube;

[0034] When the powder passes through the shielded irradiation chamber, which consists of an irradiation chamber, it first falls from the top of the shielded irradiation chamber in an hourglass manner, receiving energy from the electron gun during the falling process; and then falls onto the conveyor belt located below the shielded irradiation chamber, and is carried away from the shielded irradiation chamber by the conveyor belt when it is started.

[0035] When the powder dynamically passes through the shielded irradiation chamber composed of multiple irradiation chambers, the powder first falls from the top irradiation chamber in an hourglass manner and falls to the bottom of the irradiation chamber. During this process, it is stirred for several minutes by a vertical stirring device located inside the irradiation chamber. Then, it falls to the next layer of irradiation chamber in an hourglass manner, and the stirring action is repeated to the next layer of irradiation chamber until the bottom layer of irradiation chamber. Finally, it is carried away from the bottom layer of irradiation chamber by a conveyor belt. The powder undergoes three hourglass-like falls, during which it can fully contact the infrared irradiation sensor.

[0036] The powder can undergo a first empowerment process followed by a second empowerment process, or vice versa.

[0037] The third energizing process involves placing powder in an irradiation chamber filled with an inert gas (such as nitrogen or argon). The irradiation chamber has multiple horizontally rotating supports, on which powder containers are placed. The powder containers rotate with the supports. Each support has multiple exhaust pipes with vent holes, connected to an infrared radiation gas source (the infrared radiation gas is an inert gas, such as argon or nitrogen, preferably nitrogen, which is applied to the powder after infrared irradiation). The irradiation chamber also has multiple irradiation source assemblies, applying infrared irradiation through multiple sources simultaneously.

[0038] The powder can undergo the first, second, and third empowerment processes in any order;

[0039] In the cleaning process described in (S2), the raw material is placed in a water tank and water that has undergone resonance treatment is poured in. Then, resonance energy is applied to decompose the unfavorable impurities to ensure the uniformity of the material composition.

[0040] The inner walls of the powder material-energized resonator, the inner walls of the shielded irradiation chamber, and the inner walls of the nitrogen-purified irradiation chamber are all coated with a paint that radiates infrared rays.

[0041] The main component of the infrared-emitting coating is seashells, which are mainly derived from oyster shells. The seashells are crushed into powder and mixed with other powders to prepare the infrared-emitting coating. The radiation material has a single component to reduce interference from other radiation.

[0042] One or more technical solutions provided in this application have at least the following technical effects or advantages:

[0043] The above technical solution utilizes calcium carbonate as its raw material, with the calcium carbonate powder sourced from the shells of aquatic organisms. The calcium carbonate material is prepared using a series of techniques to create a porous honeycomb structure, within which far-infrared radiation waves are concentrated. This ensures that in its first state, the far-infrared radiation waves concentrated within the honeycomb structure remain within the structure; in its second state, the far-infrared radiation emitted by the material itself at the target location resonates with the far-infrared radiation waves concentrated within the honeycomb structure. By fully utilizing aquatic organism shells as raw materials, the composition is relatively simple, eliminating the need for materials such as tourmaline and rare earth elements, thus avoiding the environmental damage caused by mining. This effectively solves the technical problems of existing technologies, such as poor promotion of human microcirculation and environmental damage and resource waste during production, thereby achieving the technical effects of improving human microcirculation, reducing environmental damage during production, and conserving resources. Attached Figure Description

[0044] Figure 1 This is a schematic diagram of the present invention in a powder-stacking state;

[0045] Figure 2 XRD patterns of tourmaline from different regions are presented in the existing technology (Journal of Geology of Chinese Universities, September 2008, Vol. 14, No. 3, pp. 426-432).

[0046] Figure 3 This is an image showing the infrared emission NMR results of the present invention in a liquid state;

[0047] Figure 4 This is an infrared thermal image of the powder of the present invention.

[0048] Figure 5 This is a perspective view of one type of device used in the empowerment process of the present invention;

[0049] Figure 6 This is a schematic diagram of the structure of one of the devices used in the empowerment process of the present invention;

[0050] Figure 7 This is a schematic diagram of the energy waveform used in the energy-enabling process of the present invention;

[0051] Figure 8 This is a schematic diagram of the irradiation gun used in the energizing process of this invention;

[0052] Figure 9 For use in invention-enabling processes;

[0053] Figure 10 For use in inventing energizing processes;

[0054] Figure 11 An hourglass structure installed in an irradiation chamber.

[0055] In the diagram, 1-computer control system color display screen, 2-alarm flashing light, 3-emergency stop button, 4-power generator, 5-energy control module, 6-power control module, 7-lighting device, 8-octagonal plate, 9-powder storage box, 10-drive motor, 11a-first exhaust port, 11b-second exhaust port, 12-powder resonant processing chamber, 13-front panel, 14-powder resonant processing chamber door, 15-transparent window, 16-side panel, 17-casters, 18-frame. Detailed Implementation

[0056] The specific embodiments of the present invention will be further described below with reference to the accompanying drawings. It should be noted that these descriptions are for the purpose of aiding understanding the present invention, but do not constitute a limitation thereof. Furthermore, the technical features involved in the various embodiments of the present invention described below can be combined with each other as long as they do not conflict with each other.

[0057] Existing technologies use tourmaline as a raw material to release far-infrared radiation into the human body. However, due to the complex composition of tourmaline, the released far-infrared radiation waves produce different characteristic peaks. The more characteristic peaks there are, the more the resonance effect is affected, thus significantly reducing the promotion of microcirculation in the human body.

[0058] Furthermore, since tourmaline is a type of mineral, its mining process inevitably causes environmental damage, which is detrimental to environmental protection.

[0059] On the other hand, seashells, a significant part of marine biological resources, exist globally as substantial solid waste. The total amount of discarded seashells in my country and worldwide exceeds 95.9574 million tons and 294.7164 million tons respectively, occupying land resources and causing environmental pollution. The total amount of various types of seashells farmed nationwide is approximately 6-8 million tons, with an annual output of no less than 1.5 million tons of discarded seashells. Therefore, if discarded seashells can be comprehensively utilized and developed, it will not only solve the problem of marine ecological environment pollution but also benefit the sustainable development of various shellfish farming industries.

[0060] The technical solution of this application provides a bio-calcium far-infrared material, which solves the problems of poor effect of infrared materials on promoting human microcirculation and environmental damage and resource waste during production in the prior art. The bio-calcium far-infrared material is mainly composed of calcium carbonate shell material derived from aquatic organisms. Moreover, the calcium carbonate material is prepared as a calcium carbonate powder material with a porous honeycomb structure. Combined with the far-infrared radiation waves gathered in the honeycomb structure, it achieves a comprehensive effect of improving human microcirculation, reducing environmental damage during production, and saving resources.

[0061] The overall concept of the implementation scheme of the present invention to solve the above-mentioned technical problems is as follows:

[0062] A bio-calcium far-infrared material is disclosed, composed of calcium carbonate, the raw material for which includes the shells of aquatic organisms. Specifically, the calcium carbonate material is primarily composed of seashells.

[0063] The calcium carbonate material is a calcium carbonate powder material prepared with a porous honeycomb structure, in which far-infrared radiation waves are concentrated.

[0064] When the bio-calcium far-infrared material is in its first state, the far-infrared radiation waves gathered within the honeycomb structure remain within the honeycomb structure. When the bio-calcium far-infrared material is in its second state, the far-infrared radiation emitted by the material itself at the target location resonates with the far-infrared radiation waves gathered within the honeycomb structure.

[0065] It makes full use of aquatic organism shells as raw materials, with a relatively simple composition, eliminating the need for materials such as tourmaline and avoiding the environmental damage caused by mining.

[0066] To better understand the above technical solutions, the following will provide a detailed explanation of the technical solutions in conjunction with the accompanying drawings and specific implementation methods.

[0067] A bio-based far-infrared calcium material is disclosed, primarily composed of calcium carbonate, with a calcium carbonate content of 95%. The calcium carbonate is derived from biological shells. The calcium carbonate material is prepared as a porous honeycomb structure, within which far-infrared radiation waves are concentrated. These far-infrared radiation waves exist within the honeycomb structure in the form of electromagnetic waves. The wavelength range of the far-infrared radiation waves is 2.5-25 μm, preferably 3-21 μm (refer to...). Figure 4 (Based on the infrared thermal imager detection results), the wavelength of the far-infrared radiation wave is more preferably 4-16µm.

[0068] Because the inner cavity of the honeycomb structure is larger than the outlet, after the energy imparting process, the far-infrared radiation wave generates a cyclone in the inner cavity of the honeycomb structure. When the bio-calcium far-infrared material is in a static state (inactive state), the cyclone does not leave the outlet of the honeycomb structure, and the far-infrared radiation wave is stored in the inner cavity of the honeycomb structure and rotates inside.

[0069] Among them, when the bio-calcium far-infrared material is in storage, the far-infrared radiation waves gathered in the honeycomb structure are kept within the honeycomb structure.

[0070] Specifically, when the bio-calcium far-infrared material acts on a target location, it resonates with the far-infrared radiation emitted by the human body. The human body serves as the target location for the far-infrared radiation waves.

[0071] Specifically, the total normal emissivity of far-infrared radiation waves reaches 0.9, and the energy spectrum of far-infrared radiation waves detected during nuclear magnetic resonance imaging exhibits a relatively single peak.

[0072] This invention also provides a method for preparing a bio-calcium far-infrared material, comprising the following steps:

[0073] (S1) Raw material preparation: Use the shells of aquatic organisms containing biological calcium as raw materials;

[0074] (S2) Cleaning raw materials: Clean the raw materials and remove impurities;

[0075] (S3) Raw material crushing: The cleaned and impurity-removed raw materials are crushed into blocks for further processing;

[0076] (S4) Raw material grinding: Grind the crushed raw material into powder to obtain calcium carbonate powder material;

[0077] (S5) Energizing: The finished product is obtained by applying energy to the calcium carbonate powder material with a preset power and a preset time through an energy application device.

[0078] Specifically, in (S2) when removing impurities, an infrared wave with a spiral waveform is used to emit a vibration frequency and apply it to the raw material; (S5) applying energy includes at least one energizing process and a detection process. In the energizing process, an infrared wave with a spiral waveform is also used to apply to the calcium carbonate powder material in different directions.

[0079] During the cleaning process, the raw materials are placed in a water tank and water that has undergone resonance treatment is poured in. Then, resonance energy is applied to decompose any undesirable impurities, thus ensuring the uniformity of the material composition.

[0080] More specifically, the preset power and preset time are 3.5KW-6.5KW and 30-60 minutes, respectively.

[0081] like Figure 5 and Figure 6 As shown, the energy-generating process is carried out through a powder material energy-generating resonator, including a frame 18, a powder material resonant processing cavity 12, and an energy generating device. The powder material resonant processing cavity 12 and the energy generating device are both installed inside the frame 18. The energy generating device is located above the powder material resonant processing cavity 12. The energy generating device includes a power generator 4, which is electrically connected to a power control module 6 and an energy control module 5. The energy wave emitted by the power generator 4 is in the shape of an Archimedean spiral. The powder material resonant processing cavity 12 is equipped with a powder material storage device, which includes eight powder storage boxes 9, a polygonal transmission mechanism, and a transmission motor 10. The transmission motor 10 is shaft-connected to the polygonal rotation mechanism. The polygonal rotation mechanism consists of two symmetrical octagonal plates 8 fixedly connected by a connecting shaft. Each corner of the inner side of the octagonal plate 8 is provided with a hook, and the powder storage boxes 9 are movably suspended on the hooks.

[0082] like Figure 7 As shown, because the energy wave is in the shape of an Archimedean spiral, this geometry can generate the densest energy wave in a finite space. The wavelength of the energy wave is in the far-infrared range.

[0083] The powder material storage device is shaped like a Ferris wheel. The powder storage box 9 is suspended on a hook and hangs down naturally. When the powder material storage device rotates, the powder storage box 9 also rotates with it, and its weight causes it to hang down naturally while rotating.

[0084] Among them, the power generator 4 is cylindrical in shape.

[0085] The powder material resonant processing cavity 12 is provided with a first exhaust hole 11a, a second exhaust hole 11b and a lighting device 7. The first exhaust hole 11a and the second exhaust hole 11b are located on the outer walls of the left and right sides of the powder material resonant processing cavity 12 near the bottom, respectively. The lighting device 7 is fixedly installed on the inner wall of the powder material resonant processing cavity 12.

[0086] The waste gas generated during the powder resonance process can be discharged in time from the first exhaust port 11a or the second exhaust port 11b.

[0087] The enabling equipment also includes a computer control system color display screen 1, a front panel 13, an alarm flashing light 2, an emergency stop button 3, a side panel 16, a powder material resonant processing chamber door 14, a transparent window 15, and casters 17. The front panel 13 and the side panel 16 are fixedly installed on the outside of the frame 18; the computer control system color display screen 1 is fixedly installed on the front panel 13; the alarm flashing light 2 and the emergency stop button 3 are fixedly installed on the side panel 16; the transparent window 15 is located on the powder material resonant processing chamber door 14; and the casters 17 are installed at the four corners below the frame 18.

[0088] In case of equipment failure, press the emergency stop button 3 to stop the equipment from running.

[0089] When taking out or putting out powder, the powder material storage device rotates slowly, and the powder storage box 9 also rotates accordingly, making it easy to take out or put out powder.

[0090] During testing, 100g of powder can be randomly selected from powder storage box 9 for infrared energy parameter testing. Infrared energy parameter testing can include XRD testing or Fourier transform infrared spectroscopy testing to obtain XRD diffraction patterns and infrared emissivity.

[0091] The preferred particle size of the bio-calcium far-infrared material is below 20 μm. Within this range, both high surface activity and good composite compatibility can be obtained, as well as good infrared radiation effect.

[0092] Reference Figure 2 and Figure 3 Compared with the far-infrared radiation waves of tourmaline in the prior art, the bio-calcium far-infrared material of this invention has a relatively single characteristic peak, resulting in strong penetration and resonance capabilities into the human body. In contrast, the infrared materials in the prior art, due to their complex composition, exhibit multiple characteristic peaks, thus weakening their resonance capability with the target.

[0093] To further enhance the empowerment effect, in the empowerment process, multiple cylindrical power generators 4 can be arranged into a circular power generator 4 assembly. The powder is placed in a container and conveyed through the assembly of multiple power generators 4 via a conveyor belt. Then it enters... Figure 5 and Figure 6 The powder material-energized resonator shown is used for further energization.

[0094] Furthermore, a circular rotary conveyor belt is established, and multiple power generator assemblies arranged in a circle are placed on the conveyor belt. The powder circulates within the conveyor belt, receiving 2-3 kW of power. After 10-20 cycles, the powder is then placed... Figure 5 and Figure 6 The powder material is further energized using an energizing resonator. The circumference of the annular rotary conveyor belt is 100-200 meters.

[0095] The enabling process may also include at least one of the following processes:

[0096] The first enabling process includes the following steps:

[0097] Place the raw material into the powder material storage device of the powder material empowerment resonator, start the resonator and resonate for 30-60 minutes at a power of 2-10KW and a frequency of 100-200KHz, and then store the powder.

[0098] The resonator includes an energy generating device, wherein the power generator of the energy generating device emits radiation waves in an Archimedean spiral shape; wherein the resonator emits far-infrared wavelengths, and the power generator emits frequencies of 12000K-100000K MHz.

[0099] The storage device has a Ferris wheel structure and includes multiple powder storage boxes, a polygonal transmission mechanism, and a transmission motor. The transmission motor shaft is connected to the polygonal rotation mechanism, which consists of multiple symmetrical polygonal plates fixedly connected by a connecting shaft. Each corner of the inner side of the polygonal plate is provided with a hook, and the powder storage boxes are movably suspended on the hooks. In step (S2), during cleaning, the raw materials are placed in a water tank and water that has undergone resonance treatment is poured in. Then, resonance energy is applied to decompose unfavorable impurities to ensure the uniformity of the material composition.

[0100] The second energizing process involves placing the powder in a shielded irradiation chamber, which contains multiple electron guns. The upper end of an accelerating tube is connected to the electron guns, and the lower end of the accelerating tube is connected to a scanning box via a vacuum tube. A focusing coil and a waveguide system are located on the outside of the accelerating tube. The powder can undergo the first energizing process first and then the second energizing process, or the second energizing process first and then the first energizing process, or the second energizing process can be performed directly.

[0101] The third energizing process involves placing the powder in a nitrogen-filled irradiation chamber. The irradiation chamber is equipped with multiple horizontally rotating supports, on which powder containers are placed. The powder containers rotate with the horizontally rotating supports. The supports are equipped with multiple exhaust pipes with exhaust holes, which are connected to infrared radiation gas sources. The irradiation chamber is also equipped with multiple irradiation source assemblies. Infrared irradiation is applied through multiple channels, allowing the powder to absorb irradiation more evenly and thoroughly.

[0102] The powder can undergo the first, second, and third empowerment processes in any order.

[0103] To further enhance the application of infrared irradiation, the inner walls of the powder-enhanced resonator, the shielded irradiation chamber, and the nitrogen-purified irradiation chamber are all coated with infrared-radiating paint to reduce energy loss.

[0104] The main component of the infrared-emitting coating is seashells, which are mainly derived from oyster shells. The seashells are crushed into powder and mixed with other powders to prepare the infrared-emitting coating. The radiation source material is relatively simple to reduce interference from other radiation sources.

[0105] The raw materials for the bio-calcium far-infrared material of this invention can be recycled by manufacturers that generate seashell solid waste and a certain solid waste recycling service fee can be charged. Thus, without spending money to purchase raw materials, a fee can be charged in the process of obtaining raw materials.

[0106] Shell powder is made from crushed seashells. Its main component is calcium carbonate (95%), with small amounts of amino acids, polysaccharides, and chitin. The antibacterial properties of chitin and the antiviral properties of amino acids in shell powder are beneficial to the human body.

[0107] The surface temperature of the human body is approximately 30-33℃. When the radiation wavelength of the radiation source matches the absorption wavelength of the radiated object, the human skin has a good absorption effect on the 4-16µm infrared radiation of the bio-calcium far-infrared material of this invention. The far-infrared radiation wave exists in the form of electromagnetic waves within the honeycomb structure of the bio-calcium far-infrared material. When it interacts with the human body, the infrared energy released by the human body resonates with it at the same frequency, which can improve blood circulation, promote metabolism, and enhance cell vitality, thereby benefiting human health.

[0108] Depending on actual needs, the finished product of bio-calcium far-infrared material can be processed into the required form, which includes at least one of powder or granules.

[0109] In practical applications, bio-calcium far-infrared materials can also be slightly soluble in water. The radiation effect of bio-calcium far-infrared materials can be used to change the structure of water molecules, turning the large molecular structure of ordinary water into a small molecular structure, thus creating energy water with a small molecular structure.

[0110] The embodiments of the present invention use nuclear magnetic resonance results when the liquid state is as follows: Figure 3 As shown.

[0111] The testing unit was Shanghai Fuda Testing Technology Group Co., Ltd., located at Fudan University in Shanghai. The half-peak width (WHM) test result using a JEOL 600MHz instrument was 44.5015Hz. Its representative spectrum showed only one peak, while the test results for tourmaline far-infrared radiation waves in existing technologies showed multiple peaks. This demonstrates that the component in this invention is singular, ensuring the stability of the far-infrared radiation wavelength, making it easier to resonate with the human body, thereby improving microcirculation and allowing for better penetration into the body to activate cells and enhance bodily functions.

[0112] Different production processes have a certain impact on far-infrared materials made from bio-calcium.

[0113] The enabling process includes at least one of the following processes:

[0114] First enabling process: The first enabling process includes the following steps:

[0115] Place the raw material into the powder material storage device of the powder material empowerment resonator, start the resonator and resonate for 30-60 minutes at a power of 2-10KW and a frequency of 100-200KHz, and then store the powder.

[0116] The resonator includes an energy generating device, wherein the power generator of the energy generating device emits radiation waves in an Archimedean spiral shape; wherein the resonator emits far-infrared wavelengths, and the power generator emits frequencies of 12000K-100000K MHz.

[0117] The storage device has a Ferris wheel structure and includes multiple powder storage boxes, a polygonal transmission mechanism, and a transmission motor. The transmission motor shaft is connected to the polygonal rotation mechanism, which consists of multiple symmetrical polygonal plates fixedly connected by a connecting shaft. Each corner of the inner side of the polygonal plate is equipped with a hook, and the powder storage boxes are movably suspended on the hooks. A vertical stirring device is installed inside the powder storage box, and the powder is lifted and fell under the action of the vertical stirring device inside the storage box.

[0118] The second energizing process involves placing the powder in a shielded irradiation chamber or dynamically passing it through the shielded irradiation chamber. The shielded irradiation chamber consists of one or more irradiation chambers. Multiple electron guns are installed inside the shielded irradiation chamber. The upper end of the accelerating tube is connected to the electron gun, and the lower end of the accelerating tube is connected to the scanning box through a vacuum tube. A focusing coil and a waveguide system are installed on the outside of the accelerating tube.

[0119] When the powder passes through the shielded irradiation chamber, which consists of an irradiation chamber, it first falls from the top of the shielded irradiation chamber in an hourglass manner, receiving energy from the electron gun during the falling process; and then falls onto the conveyor belt located below the shielded irradiation chamber, and is carried away from the shielded irradiation chamber by the conveyor belt when it is started.

[0120] When the powder passes through the shielded irradiation chamber, which consists of multiple irradiation chambers, it first falls from the top irradiation chamber in an hourglass manner and falls to the bottom of the irradiation chamber. During this process, it is stirred for several minutes by a vertical stirring device installed in the irradiation chamber. Then, it falls to the next layer of irradiation chamber in an hourglass manner. The stirring action is repeated to the next layer of irradiation chamber until the bottom layer of irradiation chamber. Finally, it is carried away from the bottom layer of irradiation chamber by a conveyor belt.

[0121] The powder can undergo a first empowerment process followed by a second empowerment process, or a second empowerment process followed by a first empowerment process, or the second empowerment process can be performed directly.

[0122] The third energizing process involves placing the powder in a nitrogen-filled irradiation chamber. The irradiation chamber is equipped with multiple horizontally rotating supports, on which powder containers are placed. The powder containers rotate with the horizontally rotating supports and are equipped with a vertical stirring device inside. The supports are equipped with multiple exhaust pipes with vent holes, which are connected to an infrared radiation gas source. The irradiation chamber is also equipped with multiple irradiation source assemblies. Infrared irradiation is applied through multiple channels simultaneously.

[0123] The powder can undergo the first, second, and third empowerment processes in any order;

[0124] In step (S2), during the cleaning process, the raw material is placed in a water tank and water that has undergone resonance treatment is poured in. Then, resonance energy is applied to decompose the unfavorable impurities, thus ensuring the uniformity of the material composition.

[0125] Among them, the inner wall of the powder material-energized resonator, the inner wall of the shielded irradiation chamber, and the inner wall of the nitrogen-purified irradiation chamber are all coated with a coating that radiates infrared rays.

[0126] The main component of the infrared-emitting coating is seashells, which are mainly derived from oyster shells. The seashells are crushed into powder and mixed with other powders to prepare the infrared-emitting coating. The seashell component is singular in order to reduce interference from other radiation.

[0127] Examples of the production process are as follows:

[0128] Example 1

[0129] The first power-enabling process involves the resonator resonating for 60 minutes at a power of 10KW and a frequency of 200KHz; wherein the resonator emits far-infrared wavelengths, and the power generator emits frequencies of 32000KMHz.

[0130] Example 2

[0131] Second enabling process.

[0132] Example 3

[0133] The third enabling process.

[0134] Example 4

[0135] The first enabling process is combined with the second enabling process.

[0136] Example 5

[0137] The first enabling process combines the second and third enabling processes.

[0138] The first, second, and third empowerment processes do not have a vertical stirring device as comparative examples.

[0139] Compare with Example 1

[0140] In Example 4, a vertical stirring device is not used.

[0141] Compare with Example 2

[0142] In Example 5, a vertical stirring device is not used.

[0143] Compare with Example 3

[0144] In Example 2, the method of combining hourglass spillage with a vertical stirring device is not used.

[0145] Compare with Example 4

[0146] In Example 2, a vertical stirring device was not used.

[0147] Compare with Example 5

[0148] In Example 2, the hourglass method is not used.

[0149] The method for testing the examples and control examples is to randomly sample from the top, bottom and middle of a packaged powder and perform infrared radiation detection using an infrared radiation detector.

[0150] The basic principle of infrared radiation is:

[0151] All objects with a temperature above absolute zero radiate infrared radiation. An object's infrared emissivity is represented by its emissivity ε, which is calculated using the formula:

[0152] ε=M / M b

[0153] In the formula: M represents the radiance of the object, W / m2; Mb represents the radiance of the blackbody, W / m2.

[0154] Radiance represents the radiant power emitted per unit surface area of ​​a source into a hemispherical space; it is also called emissivity. ε reflects the magnitude of an object's emissivity relative to a blackbody. A blackbody is an ideal object with an emissivity (or absorptivity) ε of 1. Other infrared radiating objects with a certain temperature have emissivity less than 1.

[0155] The preferred wavelength for far-infrared radiation is determined by the following formula: λmT = b, where b = 2898 ± 0.4 μm·K, and temperature T is room temperature (25℃, 298.15K). The principle is as follows: According to Wien's displacement law, as the temperature of a blackbody increases, the wavelength λm corresponding to its maximum monochromatic radiant output shifts towards shorter wavelengths according to the law of T. The relationship between the wavelength of the maximum monochromatic radiant output of an absolute blackbody and temperature is: λmT = b, where b = 2898 ± 0.4 μm·K. Therefore, at room temperature (25℃, 298.15K), the wavelength corresponding to the maximum monochromatic radiant output of a blackbody is 9.72 μm.

[0156] When the radiation wavelength of the radiation source matches the absorption wavelength of the irradiated object, human skin exhibits a good absorption effect on the 9-10 μm infrared radiation from tourmaline. Specifically, the surface temperature of the human body is approximately 31-33℃ (304.15-306.15K), and the peak wavelength calculated according to Wien's displacement law is 9.53-9.47 μm.

[0157] Table 1 shows the results of the examples and control examples using a far-infrared emissivity tester at a temperature of 22°C.

[0158] Table 1 Infrared emissivity of different embodiments / control examples

[0159]

[0160]

[0161] The effective infrared radiation wavelength range is 4-16 μm.

[0162] As shown in Table 1, the more thorough the empowerment process, the higher the total infrared emissivity and the higher the effective radiation ratio of the bio-calcium far-infrared material (powder). The comparative examples show a difference in total infrared emissivity between the use of a vertical stirring device and its absence.

[0163] By using a vertical stirring device, the powder is stirred up, increasing the effective contact between the powder and infrared radiation.

[0164] Furthermore, as can be seen from Comparative Examples 4 and 5, hourglass sprinkling provides more adequate infrared radiation contact to the powder than a vertical stirring device. The reason for this finding is:

[0165] When the powder is at rest, the powder on the surface can fully contact the infrared radiation, but the powder in the powder pile cannot fully contact the powder. Therefore, the infrared emissivity of the powder that cannot fully contact the powder is lower.

[0166] When the powder is in a vertically rotating state, the powder that was in a static state within the powder pile is lifted up, coming into contact with infrared radiation, thereby increasing its total infrared emissivity. However, if the powder is lifted at too high a speed, turbulence may occur, which affects the uniformity of the powder's absorption of infrared radiation.

[0167] When the powder is in the hourglass state, it floats in the air and has enough time to come into contact with infrared radiation, thus gaining better energy and exhibiting better infrared emissivity.

[0168] The far-infrared radiation of bio-calcium far-infrared materials can excite water molecules to vibrate, causing some hydrogen bonds to break. This breaks large water molecule clusters into smaller clusters containing only 5-6 water molecules, thus reactivating the water and improving its permeability, solubility, and metabolism. Consequently, it can improve human microcirculation and enhance immunity.

[0169] The composition of far-infrared materials also affects their infrared emissivity. Referring to Table 2, the more complex the composition, the more unfavorable the effect.

[0170] Table 2 Infrared emissivity of control examples with different components

[0171]

[0172] In Table 2:

[0173] The sample composition of Comparative Examples 6 and 7 is as follows:

[0174] SiO2, 36.64; Al2O3, 22.70; B2O3, 8.59; Fe2O3, 19.70; FeO, 0.25; MgO, 4.11; CaO, 1.73; Na2O, 0.92; MnO, 0.055; Cr2O3, 0.025.

[0175] The sample composition of Comparative Examples 8 and 9 is as follows:

[0176] SiO2, 45.00; Al2O3, 20.86; B2O3, 8.36; Fe2O3, 1.78; FeO, 1.71; MgO, 4.74; CaO, 6.35; Na2O, 0.61; K2O, 0.98; TiO2, 0.49.

[0177] Comparative Examples 6-9 are tourmaline samples, which are rich in components, each with its own radiation release, resulting in a lower infrared emissivity than the examples. Factors affecting the emissivity of an object include material type, temperature, sample morphology, chemical characteristics, and physical structure.

[0178] It is evident that the simpler the composition, the more beneficial the radiation to the human body.

[0179] Comparative Example 10, unlike Example 1, does not employ the cleaning step of placing the raw material in a water tank, adding water that has undergone resonance treatment, and then applying resonance energy. In this case, its infrared emissivity is lower than that of Example 1. Because Comparative Example 10 omits the cleaning step of placing the raw material in a water tank, adding water that has undergone resonance treatment, and then applying resonance energy, it cannot decompose undesirable impurities, potentially compromising the uniformity of the material composition, thereby possibly resulting in an infrared emissivity lower than that of Example 1.

[0180] The embodiments of the present invention contain natural and simple ingredients, which are conducive to resonance with the human body, thereby improving metabolic capacity and thus improving human microcirculation and enhancing immunity.

[0181] The embodiments of the present invention have been described in detail above with reference to the accompanying drawings, but the present invention is not limited to the described embodiments. For those skilled in the art, various changes, modifications, substitutions, and variations can be made to these embodiments without departing from the principles and spirit of the present invention, and these variations still fall within the protection scope of the present invention.

Claims

1. A biological calcium far infrared material, characterized in that: The calcium carbonate material mainly consists of calcium carbonate material, the raw material source of which includes the shell of aquatic organisms; the calcium carbonate material is prepared into a calcium carbonate material with a porous honeycomb structure, and far infrared radiation waves are gathered in the honeycomb structure; In the first state, the far infrared radiation waves gathered in the honeycomb structure are kept in the honeycomb structure; In the second state, the far infrared radiation waves gathered in the honeycomb structure resonate with the infrared rays of the target itself; The calcium carbonate content of the calcium carbonate material is more than 95%, so as to improve the relative simplicity of the raw material composition and the stability of the far infrared wavelength; the wavelength range of the far infrared radiation waves is 2.5-25um; wherein, the effective far infrared radiation wavelength range is 4-16um, and the radiation energy in the effective far infrared radiation wavelength range of the far infrared wavelength is more than 50% of the total radiation energy; The first state is a storage state, and the second state is a state when it acts on a target; the target includes a human body part; The inner cavity of the honeycomb structure is larger than the outlet, and after an energy imparting process, far infrared radiation waves generate a cyclone in the inner cavity of the honeycomb structure, wherein, in a stationary state, the cyclone does not leave the outlet of the honeycomb structure.

2. The bio-calcium far infrared material according to claim 1, characterized in that: The calcium carbonate material mainly consists of the shell of aquatic organisms.

3. The bio-calcium far infrared material according to claim 1, characterized in that: The far infrared radiation waves exist in the honeycomb structure in the form of electromagnetic waves.

4. The bio-calcium far infrared material according to claim 1, characterized in that: The normal total emissivity of the far infrared radiation waves is more than 0.85, and the energy spectrum detected in the nuclear magnetic resonance detection of the far infrared radiation waves presents a relatively single wave peak, which shows the simplicity of the material composition.

5. A method for preparing the biological calcium far infrared material according to any one of claims 1-4, characterized in that: The method comprises the following steps: (S1) Raw material preparation: using the shell of aquatic organisms containing biological calcium as raw material; (S2) Cleaning the raw material: cleaning the raw material and removing impurities; (S3) Raw material crushing: crushing the cleaned and impurity-removed raw material into blocks for further processing; (S4) Raw material grinding: grinding the crushed raw material into powder to obtain a calcium carbonate material; (S5) Energy imparting: imparting energy to the calcium carbonate material by an energy imparting device at a preset power and for a preset time to obtain a finished product.

6. The method of claim 5, wherein the method further comprises the step of: In (S2), the infrared wave with a spiral waveform is used to vibrate the raw material; ​ (S5) The energy imparting includes one or more energy imparting processes and a detection process; the form of the finished product includes at least one of powder or particles; The energy imparting process includes at least one of the following processes: The first energy imparting process includes the following steps: Put the raw material into the powder material storage device of the powder material energy imparting resonator, start the resonator, and resonate at a power of 2-10KW and a frequency of 100-200KHz for 30-60 minutes, and then store the powder; wherein, the resonator includes an energy generating device, and the radiation wave emitted by the power generator of the energy generating device is in the form of an Archimedes spiral; the frequency of the power generator is 12000K-100000K MHz; The storage device is in a Ferris wheel structure, and comprises a plurality of powder storage boxes, a polygonal transmission mechanism and a transmission motor. The second energizing process is to place the powder in a shielding irradiation chamber or to dynamically pass through the shielding irradiation chamber. When the powder dynamically passes through the shielding irradiation chamber composed of one irradiation chamber, the powder is first sprinkled from the top of the shielding irradiation chamber in the form of an hourglass, and falls into the bottom of the irradiation chamber during which the powder is stirred by the vertical stirring device arranged in the irradiation chamber for several minutes, and then is sprinkled to the irradiation chamber of the next layer in the form of an hourglass, and the stirring action is repeated to the irradiation chamber of the next layer until the irradiation chamber of the bottom layer, and finally is taken away from the irradiation chamber of the bottom layer by the conveying belt. The third energizing process is to place the powder in a nitrogen-containing irradiation chamber, and the irradiation chamber is provided with a plurality of horizontally rotating supports, and the powder container is placed on the horizontally rotating supports, and the powder container rotates with the horizontally rotating supports, and the supports are provided with a plurality of exhaust pipes with exhaust holes, and the exhaust pipes are connected with the infrared radiation gas source. The powder can be subjected to the first energizing process, the second energizing process and the third energizing process in any order. The main component of the radiation infrared coating is shell, and the shell mainly comes from oyster shells. The shell is crushed into powder and mixed with other powders to prepare the radiation infrared coating, and the radiation material composition is single to reduce other radiation interference. ​

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