Metal sulfide nanometer material synthesis device

Abstract

The invention discloses a metal sulfide nano material synthesizing device which comprises a synthesizing cylinder, a driving mechanism is fixedly connected to the top of the synthesizing cylinder and extends into the synthesizing cylinder, a first supporting telescopic mechanism is fixedly connected to the synthesizing cylinder, and a swing mechanism is fixedly connected to the bottom of the first supporting telescopic mechanism; the second supporting telescopic mechanisms are arranged on the left and right sides of the synthesis cylinder and rotationally connected with the synthesis cylinder through first rotating shafts; the stirring mechanism is located in the synthesis cylinder and connected with the driving mechanism, and the stirring mechanism is used for promoting synthesis of the metal sulfide nano material in the synthesis cylinder; the device is driven by the motor, liquid can be continuously extruded, and the extrusion column can continuously slide in a reciprocating manner by virtue of hydraulic pressure, so that the extrusion column can continuously drive the synthesis barrel to rotate, the synthesis barrel is enabled to swing all the time, raw materials in the synthesis barrel can be continuously stirred in the swinging process due to the fact that the synthesis barrel swings and inclines at different angles, and the raw materials in the synthesis barrel can be continuously stirred in the swinging process. Therefore, the mixing effect is effectively achieved.

Description

Technical Field

[0001] The invention relates to the field of nano material synthesis, and in particular to a metal sulfide nano material synthesis device. Background Art

[0002] Metal sulfide nanomaterials are compounds composed of metal elements and sulfur elements, which have nanoscale size characteristics. This type of material has shown wide application potential in various fields, especially in energy storage, optoelectronic devices, catalysts, sensors and biomedicine. The following are some common metal sulfide nanomaterials and their applications:

[0003] Molybdenum disulfide (MoS2):

[0004] MoS2 is a typical metal sulfide nanomaterial with a layered structure.

[0005] In the energy field, MoS2 can be used as an electrode material for battery materials, such as lithium-ion batteries and sodium-ion batteries, as well as an electrode material for supercapacitors.

[0006] In the field of catalysis, MoS2 can be used as a catalyst, such as in hydrolysis reactions, hydrogenation reactions, and carbon dioxide reduction reactions.

[0007] Ferrous sulfide (FeS2, also known as pyrite):

[0008] Pyrite is a common metal sulfide nanomaterial with potential applications in optoelectronic devices, such as solar cells and photodetectors.

[0009] As a photoelectric material, pyrite has been widely studied and applied due to its excellent photoelectric properties, such as light absorption and carrier transport capabilities.

[0010] Molybdenum disulfide-tungsten disulfide (MoS2-WSe2) heterostructure:

[0011] This composite nanomaterial structure has a specific layered stacking and shows excellent optoelectronic properties.

[0012] In the field of optoelectronics, MoS2-WSe2 heterostructures are used as key materials for photodiodes and photodetectors, and their band structures and photoelectric conversion efficiencies have been intensively studied.

[0013] Copper Sulfide (CuS):

[0014] CuS is another important metal sulfide nanomaterial with good electrochemical performance and tunable magnetic properties.

[0015] In the field of energy storage, CuS can be used as capacitor material and cathode material for lithium-sulfur batteries, with the characteristics of high energy density and long cycle life.

[0016] Nickel Sulfide (NiS):

[0017] NiS is a metal sulfide nanomaterial with various crystalline phases, which has shown important applications in electrochemical sensors and catalysts.

[0018] As the working electrode of electrochemical sensors, NiS has high sensitivity and selectivity for detecting a variety of ions and molecules.

[0019] The existing public patent application number CN201811534964.9 records that the present invention discloses a metal sulfide nanomaterial synthesis device. The present invention uses the slider to move up and down, and under the action of the connecting rod, the sleeve moves back and forth horizontally along the turbine blade. The roller in the sleeve rotates and uses the rolling block to radially disturb the reaction raw materials on the turbine blade, so that the reaction raw materials can be better mixed and uniform. At the same time, under the action of the rotation of the roller, the second brush also rotates and intermittently sweeps up the reaction raw materials on the turbine blade, so that the reaction raw materials can be secondary disturbed and mixed, thereby improving the uniformity of the reaction mixture. Finally, the purpose of improving the stirring efficiency of the stirring device is achieved. In addition, when the slider moves downward, the connecting rod opens outward. The brush one on the connecting rod disturbs the reaction raw materials around the turbine disk, so that the reaction raw materials around the turbine disk will not be in a relatively static state, further improving the uniformity and stirring efficiency of the reaction raw material mixing.

[0020] The metal sulfide nanomaterial synthesis device recorded in the above-mentioned prior art adopts different stirring methods during the working process to promote better mixing of materials and improve the uniformity and stirring efficiency of raw material mixing. However, the mixing range of materials in the whole stirring process is not large, and can only be fully mixed at some positions in the barrel, and it is impossible to take into account the mixing of raw materials in various places in the whole barrel. Summary of the invention

[0021] The purpose of the present invention is to provide a metal sulfide nanomaterial synthesis device to solve the above technical problems.

[0022] In order to solve the above technical problems, the present invention adopts the following technical solutions:

[0023] A metal sulfide nanomaterial synthesis device comprises a synthesis cylinder, a driving mechanism is fixedly connected to the top of the synthesis cylinder, the driving mechanism extends into the interior of the synthesis cylinder, a first supporting telescopic mechanism is fixedly connected to the synthesis cylinder, and a swing mechanism is fixedly connected to the bottom of the first supporting telescopic mechanism;

[0024] The second supporting telescopic mechanism is located at the left and right sides of the synthetic cylinder and is rotatably connected to the synthetic cylinder through the first rotating shaft;

[0025] A stirring mechanism is located inside the synthesis cylinder and connected to the driving mechanism, and the stirring mechanism is used to promote the synthesis of the metal sulfide nanomaterial in the synthesis cylinder;

[0026] The driving mechanism is used to drive the synthesis drum to swing and the stirring mechanism to rotate.

[0027] Preferably, the second supporting telescopic mechanism comprises a first supporting column, a first sliding rod is slidably connected inside the first supporting column, a third supporting column is fixedly connected to the first sliding rod, a first rotating shaft is rotatably mounted on the third supporting column, and the first rotating shaft is fixedly connected to the synthesis cylinder;

[0028] The bottom of the first supporting column is fixedly connected with a base.

[0029] Preferably, the driving mechanism comprises a mounting frame, and the mounting frame is fixedly mounted on the top of the synthesis barrel;

[0030] The top of the mounting frame is fixedly connected to a motor, a third rotating shaft is fixedly connected to the power output shaft of the motor, two cams are fixedly connected to the third rotating shaft, grooves are provided on opposite sides of the two cams, an auxiliary rod is slidably connected inside the groove, a mounting plate is rotatably connected to the auxiliary rod, a fixed shaft is fixedly connected to the mounting plate, and an auxiliary wheel is fixedly connected to the fixed shaft;

[0031] The fixed shaft is fixedly connected with a piston cylinder, the piston cylinder is slidably connected with a storage cylinder, and the storage cylinder is fixedly connected with the synthesis cylinder.

[0032] Preferably, the driving mechanism further comprises a bent pipe, and the bent pipe is fixedly mounted on the third supporting column;

[0033] An extrusion column is slidably connected inside the bent pipe, and the extrusion column is connected to the bent pipe through a first spring;

[0034] The elbow is connected to the storage cylinder via a connecting hose;

[0035] A fixing plate is fixedly mounted on the first rotating shaft.

[0036] Preferably, the stirring mechanism comprises a second rotating shaft, which passes through the synthesis cylinder and is rotationally connected to the synthesis cylinder;

[0037] The second rotating shaft is fixedly connected with a connecting block, the connecting block is fixedly connected with a mounting frame, a fourth rotating shaft is rotatably mounted inside the mounting frame, a swing plate is fixedly connected with the fourth rotating shaft, a first gear is fixedly connected with the fourth rotating shaft, a rack is meshed with the first gear, the rack passes through the mounting frame and is slidably connected with the mounting frame, and a first magnetic block is fixedly connected with the rack;

[0038] A slide cylinder is fixedly connected to the installation frame, a connecting rod is fixedly and slidably connected inside the slide cylinder, one end of the connecting rod is fixedly connected to the first magnetic block, and the other end of the connecting rod is connected to the slide cylinder through a fourth spring.

[0039] Preferably, the stirring mechanism further comprises a rectangular column, and the rectangular column is fixedly mounted on the inner wall of the synthesis cylinder;

[0040] The rectangular column is fixedly connected with a first fixed block, the first fixed block is rotatably connected with a seventh rotating shaft, the seventh rotating shaft is rotatably connected with a second rotating plate, the second rotating plate is rotatably connected with a sixth rotating shaft, the sixth rotating shaft is rotatably connected with the first rotating plate, the first rotating plate is rotatably connected with a fifth rotating shaft, the fifth rotating shaft is rotatably connected with a second fixed block, the second fixed block is fixedly connected with a sliding sleeve, and the sliding sleeve is slidably connected with the rectangular column;

[0041] The sliding sleeve is fixedly connected with a second magnetic block, and the first magnetic block and the second magnetic block are magnetically attracted to each other;

[0042] A plurality of the second rotating plates are connected via a rubber soft sleeve.

[0043] Preferably, the swing mechanism comprises a plurality of arc-shaped plates, the arc-shaped plates are fixedly connected to the first support column, a sliding column is slidably connected between two of the arc-shaped plates, a sliding block is fixedly connected between the two sliding columns, and a groove is penetrated through the sliding block;

[0044] The top of the sliding block is fixedly connected with a rotating ring, the interior of the rotating ring is rotatably connected with a rotating disk, a tooth groove is provided in the middle of the rotating disk, a gear column is meshed inside the tooth groove, and the gear column is fixedly connected to the second rotating shaft.

[0045] Preferably, the rotating disk is provided with a plurality of thread grooves, and the second magnetic column is threadedly connected inside the thread grooves;

[0046] A plurality of thread grooves are formed at the bottom of the synthetic cylinder, and a first magnetic column is threadedly connected inside the thread groove, and the first magnetic column and the second magnetic column magnetically repel each other.

[0047] Preferably, the first supporting telescopic mechanism includes a second supporting column, the second supporting column is fixedly connected to the sliding block, the second supporting column is fixedly connected to a second sliding rod, the second sliding rod is slidably connected to a fourth supporting column, and the fourth supporting column is fixedly connected to the synthetic tube.

[0048] The beneficial effects of the present invention are:

[0049] 1. The present invention is driven by a motor and can continuously squeeze the liquid. The hydraulic energy can continuously make the squeezing column slide back and forth. In this way, the squeezing column will continuously drive the synthesis cylinder to rotate, so that the synthesis cylinder will swing all the time. As the synthesis cylinder swings, the synthesis cylinder will tilt at different angles, and the raw materials inside it can be continuously moved during the swinging process, thereby effectively achieving a mixing effect.

[0050] 2. When the present invention is driven by a motor, it will also drive the gear column to rotate. With the help of the gear column, the rotating disk can be effectively rotated, so that the second magnetic column can be effectively rotated continuously. The second magnetic column acts on the first magnetic column to effectively move the synthesis cylinder up and down continuously, and this process will occur when the synthesis cylinder swings. In this way, the synthesis cylinder can not only move while swinging, but also because the running trajectory of the synthesis cylinder is constantly changing, the raw materials inside it will also change accordingly, which can achieve a better mixing effect.

[0051] 3. When the motor of the present invention is started, the motor drives the second rotating shaft to rotate, and the second rotating shaft drives the swinging plate, the mounting frame, and the first magnetic block to move. When the first magnetic block rotates to a certain position, the first magnetic block and the second magnetic block approach each other, and the first magnetic block causes the swinging plate to swing. In this way, the swinging plate rotating around the second rotating shaft can rotate on itself, changing the flow path of the raw materials, thereby achieving a mixing effect, and the second magnetic block drives the sliding sleeve to move, which can effectively make the rubber soft sleeve continuously open and close, thereby effectively moving the raw materials, further achieving a mixing effect, and the entire working process is carried out simultaneously with the swinging and moving of the upper synthesis cylinder, so that the movement trajectory of the raw materials will vary greatly each time, thereby achieving a sufficient mixing effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0052] Figure 1 It is a structural schematic diagram of the present invention;

[0053] Figure 2 It is a rear view of the present invention;

[0054] Figure 3 It is a schematic diagram of the internal structure of the synthesis tube of the present invention;

[0055] Figure 4 for Figure 3 A magnified schematic diagram of part A;

[0056] Figure 5 It is a schematic diagram of the connection between the motor and the storage cylinder of the present invention;

[0057] Figure 6 It is a structural schematic diagram of the second supporting telescopic mechanism of the present invention;

[0058] Figure 7 It is a structural schematic diagram of the first supporting telescopic mechanism of the present invention;

[0059] Figure 8 It is a schematic diagram of the internal structure of the elbow of the present invention;

[0060] Fig. 9 It is a schematic diagram of the connection between the mounting frame and the rotating plate of the present invention;

[0061] Fig.10 for Fig. 9 An enlarged schematic diagram of part B;

[0062] Fig.11 for Fig. 9 Enlarged schematic diagram of part C of FIG.

[0063] Figure numerals: 1, base; 2, sliding block; 3, first support column; 4, arc plate; 5, synthesis cylinder; 6, fixed plate; 7, first rotating shaft; 8, storage cylinder; 9, motor; 10, mounting frame; 11, second support column; 12, connecting hose; 13, elbow; 14, second rotating shaft; 15, first magnetic block; 16, second magnetic block; 17, rotating ring; 18, gear column; 19, sliding column; 20, first magnetic column; 21, rotating disk; 22, second magnetic column; 23, auxiliary rod; 24, auxiliary wheel; 25, cam; 26, third rotating shaft; 27. Mounting plate; 28. Fixed shaft; 29. ​​Piston cylinder; 30. First slide rod; 31. Third support column; 32. Second slide rod; 33. Fourth support column; 34. Extrusion column; 35. First spring; 36. Mounting frame; 37. Swing plate; 38. Fourth rotating shaft; 39. First gear; 40. Rack; 41. Slide cylinder; 42. First fixed block; 43. Second fixed block; 44. Fifth rotating shaft; 45. Sliding sleeve; 46. Rectangular column; 47. First rotating plate; 48. Sixth rotating shaft; 49. Second rotating plate; 50. Rubber soft sleeve. DETAILED DESCRIPTION

[0064] In order to make the technical means, creative features, objectives and effects of the present invention easy to understand, the present invention is further described below in conjunction with specific embodiments and drawings, but the following embodiments are only preferred embodiments of the present invention, not all. Based on the embodiments in the implementation mode, other embodiments obtained by those skilled in the art without creative work are all within the scope of protection of the present invention.

[0065] The specific embodiments of the present invention are described below with reference to the accompanying drawings.

[0066] Embodiment 1:

[0067] like Figure 1-11 As shown, a metal sulfide nanomaterial synthesis device includes a synthesis tube 5, a driving mechanism is fixedly connected to the top of the synthesis tube 5, the driving mechanism extends into the synthesis tube 5, a first supporting telescopic mechanism is fixedly connected to the synthesis tube 5, and a swing mechanism is fixedly connected to the bottom of the first supporting telescopic mechanism;

[0068] The second supporting telescopic mechanism is located on the left and right sides of the synthesis tube 5 and is rotatably connected to the synthesis tube 5 through the first rotating shaft 7;

[0069] A stirring mechanism is located inside the synthesis cylinder 5 and connected to the driving mechanism, and the stirring mechanism is used to promote the synthesis of the metal sulfide nanomaterial in the synthesis cylinder 5;

[0070] The driving mechanism is used to drive the synthesis cylinder 5 to swing and the stirring mechanism to rotate.

[0071] The second supporting telescopic mechanism comprises a first supporting column 3, a first sliding rod 30 is slidably connected inside the first supporting column 3, a third supporting column 31 is fixedly connected to the first sliding rod 30, a first rotating shaft 7 is rotatably mounted on the third supporting column 31, and the first rotating shaft 7 is fixedly connected to the synthesis cylinder 5;

[0072] The bottom of the first support column 3 is fixedly connected to the base 1 .

[0073] The driving mechanism includes a mounting frame 10, which is fixedly mounted on the top of the synthesis tube 5;

[0074] The top of the mounting frame 10 is fixedly connected to a motor 9, a third rotating shaft 26 is fixedly connected to the power output shaft of the motor 9, two cams 25 are fixedly connected to the third rotating shaft 26, and grooves are provided on opposite sides of the two cams 25, an auxiliary rod 23 is slidably connected inside the groove, a mounting plate 27 is rotatably connected to the auxiliary rod 23, a fixed shaft 28 is fixedly connected to the mounting plate 27, and an auxiliary wheel 24 is fixedly connected to the fixed shaft 28;

[0075] The fixed shaft 28 is fixedly connected with a piston cylinder 29 , the piston cylinder 29 is slidably connected with a storage cylinder 8 , and the storage cylinder 8 is fixedly connected to the synthesis cylinder 5 .

[0076] The driving mechanism further includes a bent pipe 13, which is fixedly mounted on the third support column 31;

[0077] An extrusion column 34 is slidably connected inside the bent pipe 13, and the extrusion column 34 is connected to the bent pipe 13 through a first spring 35;

[0078] The elbow 13 is connected to the storage cylinder 8 via the connecting hose 12;

[0079] A fixing plate 6 is fixedly mounted on the first rotating shaft 7 .

[0080] The motor 9 is started, and the motor 9 drives the third rotating shaft 26 to rotate, and the third rotating shaft 26 drives the cam 25 to rotate. The cam 25 drives the piston cylinder 29 to move through the auxiliary rod 23, so that the piston cylinder 29 will continuously squeeze the water source in the storage cylinder 8, so that the water source in the storage cylinder 8 is pressurized and transported to the inside of the bent pipe 13, and the squeezing column 34 in the bent pipe 13 is squeezed out. In this way, the fixing plate 6 can be effectively squeezed by the squeezing column 34, so that the fixing plate 6 will rotate, and the rotation of the fixing plate 6 will drive the synthesis cylinder 5 to rotate;

[0081] As the synthesis barrel 5 rotates, the synthesis barrel 5 can be driven to swing continuously, so that the raw materials in the synthesis barrel 5 can be shaken greatly, thereby accelerating the mixing.

[0082] Embodiment 2:

[0083] like Figure 1-11 As shown, when other parts are the same as those of the embodiment 1, the difference between this embodiment and the embodiment 1 is that: the swing mechanism includes a plurality of arc plates 4, the arc plates 4 are fixedly connected to the first support column 3, a sliding column 19 is slidably connected between two arc plates 4, a sliding block 2 is fixedly connected between the two sliding columns 19, and a groove is formed through the sliding block 2;

[0084] A rotating ring 17 is fixedly connected to the top of the sliding block 2 , and a rotating disk 21 is rotatably connected inside the rotating ring 17 . A tooth groove is provided in the middle of the rotating disk 21 , and a gear column 18 is meshed inside the tooth groove. The gear column 18 is fixedly connected to the second rotating shaft 14 .

[0085] The rotating disk 21 is provided with a plurality of thread grooves, and the second magnetic column 22 is threadedly connected inside the thread grooves;

[0086] A plurality of thread grooves are formed at the bottom of the synthesis tube 5 , and a first magnetic column 20 is threadedly connected inside the thread groove. The first magnetic column 20 and the second magnetic column 22 repel each other magnetically.

[0087] The first supporting telescopic mechanism includes a second supporting column 11, which is fixedly connected to the sliding block 2, to which a second sliding rod 32 is fixedly connected, to which a fourth supporting column 33 is slidably connected, and to which the fourth supporting column 33 is fixedly connected to the synthesis tube 5.

[0088] When the third rotating shaft 26 rotates, it will also drive the second rotating shaft 14 to rotate, the second rotating shaft 14 will drive the gear column 18 to rotate, the gear column 18 will drive the rotating disk 21 to rotate, the rotating disk 21 will drive the second magnetic column 22 to rotate, when the second magnetic column 22 rotates to the specified position, the second magnetic column 22 will act on the first magnetic column 20, the first magnetic column 20 will move away from the second magnetic column 22, so that the synthesis cylinder 5 will move, and because the synthesis cylinder 5 is constantly swinging at this time, the synthesis cylinder 5 can continuously move up and down during the swinging process, thereby effectively achieving a mixing effect, and further achieving an effect of promoting mixing;

[0089] Furthermore, the first magnetic column 20 and the second magnetic column 22 can be installed according to the requirements, so as to achieve the effect of controlling the moving frequency of the synthesis cylinder 5.

[0090] Embodiment 3:

[0091] like Figure 1-11 As shown, when other parts are the same as those of the embodiment 1, the difference between this embodiment and the embodiment 1 is that: the stirring mechanism includes a second rotating shaft 14, the second rotating shaft 14 passes through the synthesis cylinder 5 and is rotatably connected to the synthesis cylinder 5;

[0092] The second rotating shaft 14 is fixedly connected with a connecting block, the connecting block is fixedly connected with a mounting frame 36, a fourth rotating shaft 38 is rotatably mounted inside the mounting frame 36, a swing plate 37 is fixedly connected with the fourth rotating shaft 38, a first gear 39 is fixedly connected with the fourth rotating shaft 38, a rack 40 is meshed with the first gear 39, the rack 40 passes through the mounting frame 36 and is slidably connected with the mounting frame 36, and a first magnetic block 15 is fixedly connected with the rack 40;

[0093] A slide cylinder 41 is fixedly connected to the mounting frame 36 , and a connecting rod is fixedly and slidably connected inside the slide cylinder 41 . One end of the connecting rod is fixedly connected to the first magnetic block 15 , and the other end of the connecting rod is connected to the slide cylinder 41 via a fourth spring.

[0094] The stirring mechanism further includes a rectangular column 46, which is fixedly mounted on the inner wall of the synthesis cylinder 5;

[0095] A first fixed block 42 is fixedly connected to the rectangular column 46, a seventh rotating shaft is rotatably connected to the first fixed block 42, a second rotating plate 49 is rotatably connected to the seventh rotating shaft, a sixth rotating shaft 48 is rotatably connected to the second rotating plate 49, a first rotating plate 47 is rotatably connected to the sixth rotating shaft 48, a fifth rotating shaft 44 is rotatably connected to the first rotating plate 47, a second fixed block 43 is rotatably connected to the fifth rotating shaft 44, a sliding sleeve 45 is fixedly connected to the second fixed block 43, and the sliding sleeve 45 is slidably connected to the rectangular column 46;

[0096] The sliding sleeve 45 is fixedly connected with the second magnetic block 16, and the first magnetic block 15 and the second magnetic block 16 are magnetically attracted to each other;

[0097] The plurality of second rotating plates 49 are connected by rubber sleeves 50 .

[0098] The rotation of the second rotating shaft 14 will also drive the swing plate 37, the mounting frame 36, and the first magnetic block 15 to move;

[0099] When the first magnetic block 15 rotates to a certain position, the first magnetic block 15 and the second magnetic block 16 approach each other, the first magnetic block 15 drives the rack 40 to move, the rack 40 moves to drive the first gear 39 to rotate, the first gear 39 drives the fourth rotating shaft 38 to rotate, the fourth rotating shaft 38 makes the swing plate 37 swing, so that the swing plate 37 rotating around the second rotating shaft 14 can rotate again, changing the flow path of the raw materials, thereby achieving a mixing effect;

[0100] The second magnetic block 16 will drive the sliding sleeve 45 to move, the sliding sleeve 45 will drive the second fixed block 43 to move, and the second fixed block 43 will drive the first rotating plate 47 and the second rotating plate 49 to rotate, so that the rubber soft sleeve 50 can be effectively opened and closed continuously, thereby effectively stirring the raw materials and further achieving a mixing effect. The entire working process is carried out simultaneously with the swinging and movement of the upper synthesis cylinder 5, so that the movement trajectory of the raw materials will change greatly each time, thereby achieving a sufficient mixing effect.

[0101] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments. The above embodiments and descriptions are only preferred examples of the present invention and are not intended to limit the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, which fall within the scope of the present invention. The scope of protection of the present invention is defined by the attached claims and their equivalents.

Claims

1. A metal sulfide nanomaterial synthesis device, comprising a synthesis tube, Features: The top of the synthesis cylinder (5) is fixedly connected to a driving mechanism, the driving mechanism extends into the interior of the synthesis cylinder (5), the synthesis cylinder (5) is fixedly connected to a first supporting telescopic mechanism, and the bottom of the first supporting telescopic mechanism is fixedly connected to a swinging mechanism; A second supporting telescopic mechanism is located on the left and right sides of the synthetic cylinder (5) and is rotatably connected to the synthetic cylinder (5) via a first rotating shaft (7); A stirring mechanism is located inside the synthesis cylinder (5) and is connected to the driving mechanism, and the stirring mechanism is used to promote the synthesis of the metal sulfide nanomaterial in the synthesis cylinder (5); The driving mechanism is used to drive the synthesis cylinder (5) to swing and to make the stirring mechanism rotate.

2. The metal sulfide nanomaterial synthesis device according to claim 1, Features: The second supporting telescopic mechanism comprises a first supporting column (3), a first sliding rod (30) is slidably connected inside the first supporting column (3), a third supporting column (31) is fixedly connected to the first sliding rod (30), a first rotating shaft (7) is rotatably mounted on the third supporting column (31), and the first rotating shaft (7) is fixedly connected to the synthesis cylinder (5); The bottom of the first support column (3) is fixedly connected to a base (1).

3. The metal sulfide nanomaterial synthesis device according to claim 2, Features: The driving mechanism comprises a mounting frame (10), and the mounting frame (10) is fixedly mounted on the top of the synthesis cylinder (5); The top of the mounting frame (10) is fixedly connected to a motor (9), a third rotating shaft (26) is fixedly connected to the power output shaft of the motor (9), two cams (25) are fixedly connected to the third rotating shaft (26), opposite sides of the two cams (25) are provided with grooves, an auxiliary rod (23) is slidably connected inside the groove, a mounting plate (27) is rotatably connected to the auxiliary rod (23), a fixed shaft (28) is fixedly connected to the mounting plate (27), an auxiliary wheel (24) is fixedly connected to the fixed shaft (28); The fixed shaft (28) is fixedly connected to a piston cylinder (29), the piston cylinder (29) is slidably connected to a storage cylinder (8), and the storage cylinder (8) is fixedly connected to the synthesis cylinder (5).

4. The metal sulfide nanomaterial synthesis device according to claim 3, Features: The driving mechanism further comprises a bent pipe (13), wherein the bent pipe (13) is fixedly mounted on the third supporting column (31); An extrusion column (34) is slidably connected inside the curved pipe (13), and the extrusion column (34) is connected to the curved pipe (13) via a first spring (35); The curved pipe (13) is connected to the storage cylinder (8) via a connecting hose (12); A fixing plate (6) is fixedly mounted on the first rotating shaft (7).

5. The metal sulfide nanomaterial synthesis device according to claim 1, Features: The stirring mechanism comprises a second rotating shaft (14), the second rotating shaft (14) passes through the synthesis cylinder (5) and is rotationally connected to the synthesis cylinder (5); The second rotating shaft (14) is fixedly connected with a connecting block, the connecting block is fixedly connected with a mounting frame (36), a fourth rotating shaft (38) is rotatably mounted inside the mounting frame (36), a swing plate (37) is fixedly connected with the fourth rotating shaft (38), a first gear (39) is fixedly connected with the fourth rotating shaft (38), a rack (40) is meshed with the first gear (39), the rack (40) passes through the mounting frame (36) and is slidably connected with the mounting frame (36), and a first magnetic block (15) is fixedly connected with the rack (40); A slide cylinder (41) is fixedly connected to the installation frame (36), a connecting rod is fixedly slidably connected inside the slide cylinder (41), one end of the connecting rod is fixedly connected to the first magnetic block (15), and the other end of the connecting rod is connected to the slide cylinder (41) via a fourth spring.

6. The metal sulfide nanomaterial synthesis device according to claim 5, Features: The stirring mechanism further comprises a rectangular column (46), wherein the rectangular column (46) is fixedly mounted on the inner wall of the synthesis cylinder (5); The rectangular column (46) is fixedly connected with a first fixed block (42), the first fixed block (42) is rotatably connected with a seventh rotating shaft, the seventh rotating shaft is rotatably connected with a second rotating plate (49), the second rotating plate (49) is rotatably connected with a sixth rotating shaft (48), the sixth rotating shaft (48) is rotatably connected with a first rotating plate (47), the first rotating plate (47) is rotatably connected with a fifth rotating shaft (44), the fifth rotating shaft (44) is rotatably connected with a second fixed block (43), the second fixed block (43) is fixedly connected with a sliding sleeve (45), and the sliding sleeve (45) is slidably connected to the rectangular column (46); The sliding sleeve (45) is fixedly connected to a second magnetic block (16), and the first magnetic block (15) and the second magnetic block (16) are magnetically attracted to each other; The plurality of second rotating plates (49) are connected via a rubber soft sleeve (50).

7. The metal sulfide nanomaterial synthesis device according to claim 6, Features: The swing mechanism comprises a plurality of arc-shaped plates (4), wherein the arc-shaped plates (4) are fixedly connected to the first support column (3), a sliding column (19) is slidably connected between two of the arc-shaped plates (4), a sliding block (2) is fixedly connected between the two sliding columns (19), and a groove is formed through the sliding block (2); The top of the sliding block (2) is fixedly connected to a rotating ring (17), the interior of the rotating ring (17) is rotatably connected to a rotating disk (21), a tooth groove is provided in the middle of the rotating disk (21), a gear column (18) is meshed inside the tooth groove, and the gear column (18) is fixedly connected to the second rotating shaft (14).

8. The metal sulfide nanomaterial synthesis device according to claim 7, Features: The rotating disk (21) is provided with a plurality of thread grooves, and the second magnetic column (22) is threadedly connected inside the thread grooves; The bottom of the synthetic cylinder (5) is provided with a plurality of thread grooves, the interior of the thread grooves is threadedly connected with a first magnetic column (20), and the first magnetic column (20) and the second magnetic column (22) are magnetically repelling each other.

9. The metal sulfide nanomaterial synthesis device according to claim 7, Features: The first supporting telescopic mechanism comprises a second supporting column (11), the second supporting column (11) is fixedly connected to the sliding block (2), the second supporting column (11) is fixedly connected to a second sliding rod (32), the second sliding rod (32) is slidably connected to a fourth supporting column (33), and the fourth supporting column (33) is fixedly connected to the synthesis tube (5).

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