A device for separating and purifying microalgae oil

By introducing separation self-priming mechanism and laser measurement method into the microalgae oil separation and purification equipment, the problem of difficult oil layer thickness measurement caused by oil-water layer separation and purification is solved, efficient extraction of oil and fat and low moisture content is achieved, and subsequent distillation and purification processes are simplified.

CN119215488BActive Publication Date: 2025-06-10LINYI YOUKANG BIOLOGY CO LTD
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Patent Information

Application Number
CN202411396575.X
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-10-09
Publication Date
2025-06-10
Estimated Expiration
2044-10-09

AI Technical Summary

Technical Problem

The existing microalgae oil separation and purification equipment has oil-water stratification phenomenon during the oil-water separation stage, which makes it difficult to accurately measure the thickness of the oil layer, thereby increasing the oil and fat moisture content, increasing the distillation difficulty and purification time.

Method used

A microalgae oil separation and purification device is designed, using separation self-priming mechanism and laser measurement method to quickly measure the accurate distance of the liquid surface reflection point through photoelectric detection devices, obtain the actual height of the oil layer, and flexibly control the inlet end height of the oil suction pipe through mechanical transmission components to ensure that there is very little doping of external liquid in the oil.

Benefits of technology

Accurate measurement of the height of the oil layer is achieved, reducing the water content of the oil and grease, reducing the difficulty of subsequent distillation and purification time, and improving the efficiency of grease extraction.

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Abstract

The present invention discloses a device for separating and purifying microalgae oil, which relates to the technical field of microbial oil extraction. It includes a mixing bin, at the bottom of which a drying bin is fixedly installed. A mixing and flocculation mechanism is arranged inside the mixing bin, and a drying and turning mechanism is arranged on the rear wall of the drying bin. A separating and self-suction mechanism is arranged at the bottom of the drying bin. The separating and self-suction mechanism includes a bottom bracket, at the bottom of which a lower support plate is fixedly installed. A separating barrel is fixedly installed on the top of the lower support plate. A heating element is arranged at the bottom of the separating barrel. The mechanism accurately obtains the oil layer height through the laser measurement method, and under the cooperation of the mechanical transmission component, fully transfers the upper-layer oil out. During the process, it is an intermittent extraction, and the oil liquid will not shake, thereby avoiding the oil from diffusing into the lye again, greatly reducing the amount of oil incorporated into the inner and outer liquids, reducing the subsequent distillation difficulty, and shortening the time for the steps to proceed.
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Description

Technical Field

[0001] The invention relates to the technical field of microbial oil extraction, in particular to a microalgae oil separation and purification device. Background Art

[0002] Microbial oils, also known as single-cell oils, are oils and other commercially valuable lipids produced by microorganisms such as yeast, mold, bacteria and algae under certain conditions using carbohydrates, hydrocarbons and ordinary oils as carbon sources and nitrogen sources, supplemented by inorganic salts.

[0003] Algae plants have a relatively fast growth rate and strong environmental adaptability. Algae plants can carry out photosynthesis and convert solar energy into bioenergy. This growth environment can produce a large amount of oil in algae plants. Among many algae, Schizochytrium is a marine fungus rich in DHA. The extracted microbial oil contains polyunsaturated fatty acids needed by the human body. Therefore, it has high edible and medicinal properties and higher commercial value.

[0004] However, the existing microalgae oil separation and purification equipment has the following shortcomings:

[0005] The steps of extracting oil from Schizochytrium microorganisms can be divided into algae culture, algae fermentation, fermentation liquid agglomeration, algae powder preparation, alkali-heat wall breaking, oil-water separation and distillation purification. However, in the oil-water separation stage, the existing equipment gradually forms oil-water stratification as the standing time of the oil and water liquid increases and the density of oil and water is different. The existing method of extracting the oil layer cannot accurately measure the thickness of the oil layer, resulting in a higher water content in the extracted oil, which increases the difficulty of subsequent distillation and purification time.

[0006] Therefore, we propose a microalgae oil separation and purification device to solve the above-mentioned problems. Summary of the invention

[0007] The purpose of the present invention is to provide a microalgae oil separation and purification device, which collects two beams of reflected light at the same time through the separation self-priming mechanism, obtains two optical path offset values, and quickly obtains the accurate distance between the two liquid surface reflection points by the photoelectric detection device, corresponding to the actual height of the oil layer. After the obtained value is fed back to the equipment system, with the assistance of height data, the mechanical transmission component can be flexibly controlled to intermittently lower the liquid inlet end of the oil suction pipe to a specified height range, thereby ensuring that the extracted oil is rarely mixed with external liquid, so as to solve the problems raised by the above-mentioned background technology.

[0008] To achieve the above object, the present invention provides the following technical solution: a microalgae oil separation and purification device, comprising a mixing bin, a drying bin is fixedly installed at the bottom of the mixing bin;

[0009] The interior of the mixing bin is provided with a mixing and flocculation mechanism, the rear wall of the drying bin is provided with a drying and flipping mechanism, and the bottom of the drying bin is provided with a separation and self-priming mechanism;

[0010] The separation and self-priming mechanism includes a bottom bracket, a lower support plate is fixedly installed at the bottom of the bottom bracket, a separation barrel is fixedly installed at the top of the lower support plate, a heating element is arranged at the bottom of the separation barrel, a second bracket is fixedly installed at the top of the separation barrel, a first positioning sleeve is fixedly installed at the center of the second bracket, a first electric push rod is fixedly inserted into the inner wall of the first positioning sleeve, a first external connection plate and a second external connection plate are respectively fixedly installed on both sides of the outer wall of the second bracket, a wire collecting seat and a photoelectric detection device are respectively fixedly installed at the top of the first external connection plate, a laser emitting head is fixedly connected to the center of the bottom of the wire collecting seat, a light shielding cover is fixedly connected to the bottom of the wire collecting seat, a capture window is arranged inside the light shielding cover, a group of information lines are fixedly connected to the signal output end of the wire collecting seat, and the output ends of a group of information lines are all connected to the input end of the photoelectric detection device. A second positioning sleeve is fixedly installed inside the second external connection plate, a liquid extraction pump is fixedly inserted into the second positioning sleeve, a second locking frame is fixedly installed at the top of the second external connection plate, a second electric push rod is fixedly installed inside the second locking frame, an oil suction pipe is fixedly sleeved at the shaft end of the second electric push rod, a first hollow joint is fixedly communicated with the input end of the liquid extraction pump, a second hollow joint is fixedly communicated with the outer surface of the oil suction pipe, and the outer surface of the first hollow joint is fixedly communicated with a group of oil guiding hoses. The liquid inlet ends of a group of the oil guiding hoses all penetrate through the outer surface of the second hollow joint and are communicated with the inside of the second hollow joint.

[0011] Preferably, the mixing and flocculation mechanism includes a group of hollow covers, a group of the hollow covers are all fixedly installed on the rear surface of the mixing bin, a power supply connector is fixedly installed inside each hollow cover, a vibration rod is fixedly installed on the outer surface of each hollow cover, and a group of the vibration rods are all arranged inside the mixing bin. The wiring ends of each vibration rod are respectively connected to the output ends of the corresponding power supply connector.

[0012] Preferably, a wiring base and an independent power supply are respectively fixedly installed on the rear surface of the mixing bin. The output end of the independent power supply is fixedly connected to a first wire, the output end of the first wire is connected to the wiring end of the wiring base, a group of second wires are fixedly connected inside the wiring base, and the number of a group of the second wires is equal to the number of a group of the power supply connectors. The output ends of each second wire are respectively connected to the wiring ends of the corresponding power supply connector.

[0013] Preferably, a first square pipe is fixedly communicated with the bottom of the mixing bin, an extension elbow is fixedly communicated with the discharge end of the first square pipe, and a first electric valve is arranged inside the first square pipe.

[0014] Preferably, the drying and turning mechanism includes a first locking frame fixedly installed on the rear surface of the drying bin. A positive and negative servo motor is fixedly installed inside the first locking frame. A first rectangular frame is movably arranged inside the drying bin. A positioning frame is fixedly installed on the inner surface wall of the first rectangular frame, and a hollowed-out mesh plate is fixedly embedded inside the positioning frame.

[0015] Preferably, a first support is fixedly installed at the top of the first rectangular frame. A heat insulation sleeve is fixedly installed at the center of the first support. A driving motor is fixedly inserted inside the heat insulation sleeve. A first flange is fixedly sleeved at the shaft end of the driving motor. A U-shaped joint is installed at the bottom of the first flange. A horizontal rod is fixedly installed inside the U-shaped joint. A boosting bar is fixedly installed at the bottom of the horizontal rod.

[0016] Preferably, two load-bearing frames are welded on the front surface of the first rectangular frame. A second rectangular frame is fixedly installed between the outer surface walls of the two load-bearing frames. A group of inner lining plates are fixedly installed between the two inner walls of the second rectangular frame. High-resistance electric heating tubes are arranged inside the group of inner lining plates.

[0017] Preferably, a first outer plate and a second outer plate are respectively fixedly installed on the front and rear surfaces of the first rectangular frame. The shaft end of the positive and negative servo motor is fixedly inserted inside the first outer plate. A locking sleeve is fixedly installed on the outer surface wall of the second outer plate. A first solid rod is fixedly inserted inside the locking sleeve. An adapter socket is fixedly installed on the inner surface wall of the drying bin. One end of the outer wall of the first solid rod is movably inserted inside the adapter socket. A material collecting funnel is fixedly installed at the bottom of the drying bin. A second square tube is fixedly communicated with the bottom of the material collecting funnel.

[0018] Preferably, a roller bearing is fixedly sleeved at the shaft end of the first electric push rod, and a second flange is fixedly sleeved on the outer shaft surface wall of the roller bearing. A second solid rod is fixedly installed at the bottom of the second flange. A mechanical transformation component is fixedly installed at the bottom of the lower support plate. A transmission rod is movably inserted at the center of the separation barrel. The output end of the mechanical transformation component is connected to the bottom of the transmission rod. An adaptor slideway is opened at the bottom of the second solid rod. A docking head is fixedly installed at the top of the transmission rod. A group of stirring components are fixedly installed on the outer surface wall of the second solid rod.

[0019] Preferably, the top of the bottom bracket is connected to the bottom of the drying bin. A cover is arranged at the top of the mixing bin. A third square tube is fixedly communicated with the top of the cover. A second electric valve is arranged inside the third square tube. Grafting plates are fixedly installed on the four outer walls of the lower support plate. Adjustable support feet are fixedly installed on the outer surface wall of each grafting plate.

[0020] Compared with the prior art, the present invention has the following beneficial effects:

[0021] 1. The present invention sets a separation self-priming mechanism, which simultaneously performs alkali thermal wall breaking and oil separation. After the stirring component is pulled away from the alkali solution, the difference in density between the alkali solution and the oil is used to separate the two during the static time. The oil with a smaller density is distributed in the upper layer. The subsequent laser transmitter head can emit a vertical laser beam into the oil. By using the difference in light transmittance and density between the two, a single beam of light will generate two beams of reflected light on the two liquid surfaces, and generate two different optical path offsets. Since the optical path offset is proportional to the actual reflection distance of the optical path, when both offset values ​​are transmitted to the photoelectric detection device, the optical path offset can be quickly obtained. The exact distance of the reflection point corresponds to the actual height of the oil layer. After the obtained value is fed back to the equipment system, the mechanical transmission component can be flexibly controlled under the support of data to intermittently lower the liquid inlet end of the oil suction pipe to the specified height range to ensure that the extracted oil is rarely mixed with external liquid. The mechanism accurately obtains the oil layer height through laser measurement, and with the cooperation of the mechanical transmission component, fully transfers the upper layer of oil. The process is intermittent extraction and the oil will not shake, thereby preventing the oil from diffusing into the alkali solution again, greatly reducing the amount of internal and external liquid mixed with the oil, reducing the difficulty of subsequent distillation, and shortening the time of the steps.

[0022] 2. The present invention is provided with a drying and turning mechanism. During the algae powder preparation stage, the clumping algae cells can be placed on the hollow mesh plate at a fixed point. The mechanical transmission component contained in the mechanism can drive the booster bar to continuously push the clumping algae cells, and gradually fill the blank area on the hollow mesh plate with them. Because the booster bar is flush with the top of the first rectangular frame, it will have the effect of scraping and smoothing the clumping algae cells, and reasonably control the transfer amount of the clumping algae cells, so that the clumping algae cells can be evenly spread on the hollow mesh plate. Furthermore, the high temperature generated by the high-resistance electric heating tube can fully cover the bottom of the hollow mesh plate. Combined with the former, it can ensure that the drying rate of the clumping algae cells on the hollow mesh plate is consistent, thereby improving the subsequent algae powder generation quality. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 This is a main structural stereogram of a microalgae oil separation and purification device of the present invention;

[0024] Figure 2 This is a side structural stereogram of a microalgae oil separation and purification device of the present invention;

[0025] Figure 3 This is a bottom structure stereogram of a microalgae oil separation and purification device of the present invention;

[0026] Figure 4 This is a three-dimensional diagram of the split structure of a microalgae oil separation and purification device of the present invention;

[0027] Figure 5This is an enlarged three-dimensional view of the structure of the mixing and flocculation mechanism in a microalgae oil separation and purification device of the present invention;

[0028] Figure 6 This is an enlarged three-dimensional view of the structure connected to the outside of the mixing chamber in a microalgae oil separation and purification device of the present invention;

[0029] Figure 7 This is an enlarged three-dimensional view of the structure of the drying and turning mechanism in a microalgae oil separation and purification device of the present invention;

[0030] Figure 8 This is an enlarged three-dimensional view of the internal structure of the drying chamber in a microalgae oil separation and purification device of the present invention;

[0031] Figure 9 This is an enlarged three-dimensional view of the structure connected to the bottom of the first rectangular frame in a microalgae oil separation and purification device of the present invention;

[0032] Figure 10 This is a microalgae oil separation and purification device of the present invention Figure 9 An enlarged three-dimensional view of the structure at B;

[0033] Figure 11 This is an enlarged three-dimensional view of the structure of the separation and self-priming mechanism in a microalgae oil separation and purification device of the present invention;

[0034] Figure 12 This is a microalgae oil separation and purification device of the present invention Figure 11 An enlarged three-dimensional view of the structure at A;

[0035] Figure 13 This is an enlarged three-dimensional view of the structure connected to the second bracket in a microalgae oil separation and purification device of the present invention.

[0036] In the figure: 1, mixing bin; 2, drying bin; 3, mixing and flocculating mechanism; 301, hollow cover; 302, power supply connector; 303, vibrating rod; 304, wiring base; 305, independent power supply; 306, first wire; 307, second wire; 308, first square tube; 309, first electric valve; 310, extension elbow; 4, drying and flipping mechanism; 401, first locking frame; 402, positive and negative servo motor; 403, first rectangular frame; 404, positioning frame; 405, hollowed-out mesh plate; 406, first support; 407, heat insulation sleeve; 408, drive motor; 409, first flange; 410, U-shaped joint; 411, horizontal rod; 412, boosting strip; 413, bearing frame; 414, second rectangular frame; 415, lining plate; 416, high-resistance electric heating tube; 417, first outer plate; 418, second outer plate; 419, locking sleeve; 420, first solid rod; 421, connecting sleeve; 422, material collecting funnel; 423, second square tube; 5, separating and self-priming mechanism; 501, bottom bracket; 502, lower support plate; 503, separating barrel; 504, second support; 505, first positioning sleeve; 506, first electric push rod; 507, first external connecting plate; 508, second external connecting plate; 509, second flange; 510, second solid rod; 511, wire collecting base; 512, photoelectric detection device; 513, laser emitter; 514, light-shielding cover; 515, capture window; 516, information wire; 517, second positioning sleeve; 518, liquid pumping pump; 519, second locking frame; 520, second electric push rod; 521, oil suction pipe; 522, first hollow joint; 523, second hollow joint; 524, oil guiding hose; 525, machine transformation component; 526, adaptation slideway; 527, transmission rod; 528, docking head; 529, stirring component; 6, cover; 7, third square tube; 8, second electric valve; 9, grafting plate; 10, adjustable support feet. Specific implementation mode

[0037] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative work shall fall within the protection scope of the present invention.

[0038] Please refer to the attached Figure 1 - attached Figure 13 As shown in the figure, the present invention provides a technical solution: a microalgae oil separation and purification device, including a mixing bin 1, a drying bin 2 is fixedly installed at the bottom of the mixing bin 1, a mixing and flocculating mechanism 3 is arranged inside the mixing bin 1, a drying and flipping mechanism 4 is arranged on the rear wall of the drying bin 2, and a separating and self-priming mechanism 5 is arranged at the bottom of the drying bin 2.

[0039] According to Figure 1 、 Figure 11 、 Figure 12 and Figure 13 As shown, the separation self-priming mechanism 5 includes a bottom bracket 501. A lower support plate 502 is fixedly installed at the bottom of the bottom bracket 501. A separation barrel 503 is fixedly installed at the top of the lower support plate 502. A heating element is provided at the bottom of the separation barrel 503. A second bracket 504 is fixedly installed at the top of the separation barrel 503. A first positioning sleeve 505 is fixedly installed at the center of the second bracket 504. A first electric push rod 506 is fixedly inserted into the inner wall of the first positioning sleeve 505. A first external connection plate 507 and a second external connection plate 508 are respectively fixedly installed on both sides of the outer wall of the second bracket 504. A wire collecting base 511 and a photoelectric detection device 512 are respectively fixedly installed at the top of the first external connection plate 507. A laser emitting head 513 is fixedly connected to the center of the bottom of the wire collecting base 511. A light shielding cover 514 is fixedly connected to the bottom of the wire collecting base 511. A capture window 515 is provided inside the light shielding cover 514. A group of information lines 516 are fixedly connected to the signal output end of the wire collecting base 511. The output ends of the group of information lines 516 are all connected to the input end of the photoelectric detection device 512. A second positioning sleeve 517 is fixedly installed inside the second external connection plate 508. A liquid extraction pump 518 is fixedly inserted into the second positioning sleeve 517. A second locking frame 519 is fixedly installed at the top of the second external connection plate 508. A second electric push rod 520 is fixedly installed inside the second locking frame 519. An oil suction pipe 521 is fixedly sleeved on the shaft end of the second electric push rod 520. A first hollow joint 522 is fixedly communicated with the input end of the liquid extraction pump 518. A second hollow joint 523 is fixedly communicated with the outer wall of the oil suction pipe 521. A group of oil guiding hoses 524 are fixedly communicated with the outer wall of the first hollow joint 522. The liquid inlet ends of the group of oil guiding hoses 524 all penetrate through the outer wall of the second hollow joint 523 and are communicated with the inside of the second hollow joint 523.

[0040] According to Figure 1 、 Figure 5 and Figure 6 As shown, the mixing and flocculation mechanism 3 includes a group of hollow covers 301. The group of hollow covers 301 are all fixedly installed on the rear surface of the mixing chamber 1. A power supply connector 302 is fixedly installed inside each hollow cover 301. A vibrating rod 303 is fixedly installed on the outer wall of each hollow cover 301, and the group of vibrating rods 303 are all located inside the mixing chamber 1. The wiring ends of each vibrating rod 303 are respectively connected to the output end of a corresponding power supply connector 302. By presetting the above components, after the fermentation broth and an appropriate amount of flocculant are both injected into the mixing chamber 1, the vibrating rods 303 are fully wrapped. By utilizing the physical vibration generated on the surface of the vibrating rods 303, the mixing of the two can be accelerated, and the algal cells can be accelerated to aggregate into large lumps.

[0041] According to Figure 5 and Figure 6 As shown, a wiring base 304 and an independent power supply 305 are fixedly installed on the rear surface of the mixing bin 1 respectively. The output end of the independent power supply 305 is fixedly connected to a first wire 306. The output end of the first wire 306 is connected to the wiring end of the wiring base 304. A group of second wires 307 are fixedly connected inside the wiring base 304, and the number of the group of second wires 307 is equal to that of a group of power supply connectors 302. The output end of each second wire 307 is respectively connected to the wiring end of a corresponding power supply connector 302. By presetting the above components, the set independent power supply 305 can independently supply power to the vibrating rod 303 to ensure the stability of energy transmission and ensure the continuous oscillation mixing.

[0042] According to Figure 5 and Figure 6 As shown, a first square tube 308 is fixedly communicated with the bottom of the mixing bin 1. The discharging end of the first square tube 308 is fixedly communicated with an extension elbow 310. A first electric valve 309 is arranged inside the first square tube 308. By presetting the above components, by using the certain fluidity of the volvox cells, the volvox cells can be transferred to the hollow mesh plate 405 through the transportation of the first square tube 308 and the extension elbow 310.

[0043] According to Figure 1 、 Figure 7 、 Figure 8 and Figure 9 As shown, the drying and turning mechanism 4 includes a first locking frame 401. The first locking frame 401 is fixedly installed on the rear surface of the drying bin 2. A forward and reverse servo motor 402 is fixedly installed inside the first locking frame 401. A first rectangular frame 403 is movably arranged inside the drying bin 2. A positioning frame 404 is fixedly installed on the inner wall of the first rectangular frame 403. A hollow mesh plate 405 is fixedly embedded inside the positioning frame 404. By presetting the above components, there are a plurality of equally spaced small notches in the hollow mesh plate 405. Furthermore, the high temperature diffused at the bottom thereof will diverge into the volvox cells from each notch, accelerating the water loss rate and shortening the algal powder generation time.

[0044] According to Figure 8 、 Figure 9 and Figure 10As shown, a first support 406 is fixedly installed at the top of the first rectangular frame 403. A heat insulation sleeve 407 is fixedly installed at the center of the first support 406. A drive motor 408 is fixedly inserted inside the heat insulation sleeve 407. A first flange 409 is fixedly sleeved at the shaft end of the drive motor 408. A U-shaped joint 410 is installed at the bottom of the first flange 409. A horizontal rod 411 is fixedly installed inside the U-shaped joint 410. A booster bar 412 is fixedly installed at the bottom of the horizontal rod 411. By presetting the above components, the booster bar 412 is flush with the top of the first rectangular frame 403. After the colonial algae cells continuously fall onto the hollow mesh plate 405, the slowly rotating booster bar 412 can continuously push some of the colonial algae cells to fill the blank areas on the hollow mesh plate 405. And under the pressing of the height of the booster bar 412, the colonial algae cells will not overflow. The evenly spread colonial algae cells make the algal powder output consistent at each place.

[0045] According to Figure 8 and Figure 9 As shown, two load-bearing frames 413 are welded on the front surface of the first rectangular frame 403. A second rectangular frame 414 is fixedly installed between the outer surfaces of the two load-bearing frames 413. A group of inner lining plates 415 are fixedly installed between the two inner walls of the second rectangular frame 414. A high-resistance electric heating tube 416 is arranged inside the group of inner lining plates 415. By presetting the above components, after the high-resistance electric heating tube 416 is powered on, it can continuously dissipate heat to the bottom of the hollow mesh plate 405, providing necessary conditions for drying the colonial algae cells.

[0046] According to Figure 7 and Figure 8 As shown, a first outer plate 417 and a second outer plate 418 are respectively fixedly installed on the front and back surfaces of the first rectangular frame 403. The shaft end of the forward and reverse servo motor 402 is fixedly inserted inside the first outer plate 417. A locking sleeve 419 is fixedly installed on the outer surface of the second outer plate 418. A first solid rod 420 is fixedly inserted inside the locking sleeve 419. An adapter sleeve 421 is fixedly installed on the inner surface of the drying bin 2. One end of the outer wall of the first solid rod 420 is movably inserted inside the adapter sleeve 421. A material collecting funnel 422 is fixedly installed at the bottom of the drying bin 2. The bottom of the material collecting funnel 422 is fixedly communicated with a second square tube 423. By presetting the above components, through the mutual cooperation of each component, the first rectangular frame 403 and its connected components can rotate flexibly inside the drying bin 2 to realize the free pouring of the algal powder.

[0047] According to Figure 3 、 Figure 11 and Figure 13As shown, a roller bearing is fixedly sleeved on the shaft end of the first electric push rod 506, and a second flange 509 is fixedly sleeved on the outer wall of the outer shaft of the roller bearing. A second solid rod 510 is fixedly installed at the bottom of the second flange 509. A machine variable component 525 is fixedly installed at the bottom of the lower support plate 502. A transmission rod 527 is movably inserted at the center of the separation barrel 503. The output end of the machine variable component 525 is connected to the bottom of the transmission rod 527. An adaptation slideway 526 is opened at the bottom of the second solid rod 510. A docking head 528 is fixedly installed at the top of the transmission rod 527. A set of stirring components 529 is fixedly installed on the outer wall of the second solid rod 510.

[0048] According to Figure 1 , Figure 2 , Figure 3 , Figure 4 and Figure 11 shown, the top of the bottom bracket 501 is connected to the bottom of the drying bin 2. A cover 6 is provided at the top of the mixing bin 1. A third square pipe 7 is fixedly communicated at the top of the cover 6. A second electric valve 8 is provided inside the third square pipe 7. Grafting plates 9 are fixedly installed on the four outer walls of the lower support plate 502. Adjustable support feet 10 are fixedly installed on the outer wall of each grafting plate 9. By presetting the above components, the adjustable support feet 10 can be freely adjusted according to the ground conditions of the area, avoiding the inclination of the equipment body and affecting the normal operation of each mechanism, and reducing the use limitations of the equipment.

[0049] The effect achieved by the entire mechanism is as follows: In the equipment preparation stage, first move the equipment to the designated working area, reasonably adjust the height of each adjustable support foot 10 according to the ground conditions, straighten the equipment body, and then insert the external wires into the main power supply and the independent power supply 305 of the equipment respectively to provide energy for multiple electrical components included therein.

[0050] In the stage of the fermentation broth forming into a mass, open the second electric valve 8, open the inner channel of the third square pipe 7, and inject an appropriate amount of Schizochytrium fermentation broth into the mixing bin 1 through the transportation of the third square pipe 7, and then inject an appropriate amount of flocculant into the mixing bin 1 through the channel. After completion, both can fully wrap the vibrating rod 303. Open the independent power supply 305, and the energy is transmitted by the first wire 306 and the second wire 307, and power is supplied to each vibrating rod 303. The vibration generated on its surface can accelerate the mixing of the Schizochytrium fermentation broth and the flocculant, and promote the formation of agglomerated algal cells.

[0051] During the algal powder preparation stage, the first electric valve 309 is opened to open the internal passage of the first square tube 308. By taking advantage of the certain fluidity of the agglomerated algal cells, the agglomerated algal cells in the mixing bin 1 will continuously be transported through the first square tube 308 and the extended elbow 310, and transferred from one side of the first rectangular frame 403 to above the hollow mesh plate 405. At the same time, the drive motor 408 is started to drive the boosting strip 412 on the horizontal rod 411 to slowly rotate, continuously pushing some of the accumulated agglomerated algal cells into the blank area on the hollow mesh plate 405 until the area above the hollow mesh plate 405 is completely filled. Then, by means of the pressing and scraping of the boosting strip 412, the agglomerated algal cells are finally evenly spread on the hollow mesh plate 405. The first electric valve 309 timely closes the internal passage of the first square tube 308 to stop the transfer of the agglomerated algal cells. Further, the high-resistance electric heating tube 416 is powered on, and high temperature can be continuously diffused below the hollow mesh plate 405. On the one hand, it heats the hollow mesh plate 405 itself, and on the other hand, it can directly act on the evenly spread agglomerated algal cells through the divergence of each notch of the hollow mesh plate 405, gradually drying the water in the agglomerated algal cells and promoting the generation of algal powder. After the drying time is reached, the positive and negative servo motor 402 is started. By using the movable connection of the first solid rod 420 and the connecting sleeve 421, the first rectangular frame 403 and its connected components are driven to turn over, and the algal powder on the hollow mesh plate 405 is gradually poured down and gathered in the material collecting funnel 422, and then discharged through the second square tube 423.

[0052] During the stirring and separation stage, before the transfer of the algal powder, an appropriate amount of composite alkali solution is manually injected into the separation barrel 503, and the heating element at the bottom of the separation barrel 503 is powered on to quickly heat the composite alkali solution to within 80 °C. When the algal powder is completely transferred to the first rectangular frame 403 through the second square tube 423, it can be quickly mixed with the high-temperature alkali solution, and the wall-breaking reaction will follow. The first electric push rod 506 is started, and its inner shaft extends outwards, driving the second flange 509 and its connected components to slowly move downwards, gradually making the docking head 528 accurately inserted into the internal of the adapter slideway 526 to complete the combination of the second solid rod 510 and the mechanical transformation component 525. The mechanical transformation component 525 is started and acts on the transmission rod 527. By using the physical characteristics of the roller bearing, the stirring component 529 on the second solid rod 510 is driven to rotate uniformly in the high-temperature alkali solution, accelerating the progress of the wall-breaking reaction. The generated oil will be continuously separated from the alkali solution under the centrifugation of the rotating liquid flow. After the stirring duration is reached, each component is reset by the first electric push rod 506.

[0053] In the oil layer measurement stage, after the reaction liquid has been static for a period of time, the separated grease and lye are stratified, with the oil layer on top. The laser emission head 513 is turned on, and a laser beam is vertically emitted into the oil layer. Due to the different light transmittance and density of the oil body and the lye, when the beam contacts the two liquid surfaces, the capture window 515 receives the different beams reflected by the two liquid surfaces respectively, and two optical path offsets are obtained. The data obtained is transmitted in real time to the photoelectric detection device 512 through the information line 516. According to the characteristic that the optical path offset is proportional to the actual reflection distance of the optical path, the photoelectric detection device 512 calculates the distance between the reflection points of the two beams, accurately obtains the actual height of the oil layer, and the measured data can be shared with the equipment system. When the outer tube is connected to the output end of the liquid extraction pump 518, its end is inserted into the collection container. Further, the second electric push rod 520 is turned on to drive the oil suction pipe 521 to slowly descend until it contacts the oil layer. The liquid extraction pump 518 is started to make the liquid inlet end of the oil suction pipe 521 have a certain adsorption force. The system intermittently controls the extension length of the inner shaft of the second electric push rod 520 according to the numerical limit, and gradually extracts the oil body during the process until the liquid inlet end of the oil suction pipe 521 descends to the specified height range.

[0054] Although the present invention has been described in detail with reference to the foregoing embodiments, for those skilled in the art, they can still modify the technical solutions recorded in the foregoing embodiments, or perform equivalent replacements for some of the technical features. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims

1. A microalgae oil separation and purification device, characterized in that: It comprises a mixing bin (1), a drying bin (2) being fixedly mounted at the bottom of the mixing bin (1); The interior of the mixing bin (1) is provided with a mixing and flocculation mechanism (3), the rear surface wall of the drying bin (2) is provided with a drying and turning mechanism (4), and the bottom of the drying bin (2) is provided with a separation and self-priming mechanism (5); The mixing and flocculation mechanism (3) comprises a group of hollow covers (301), wherein the group of hollow covers (301) are fixedly mounted on the rear surface of the mixing chamber (1), a power supply connector (302) is fixedly mounted inside each of the hollow covers (301), a vibration rod (303) is fixedly mounted on the outer wall of each of the hollow covers (301), and a group of vibration rods (303) are placed inside the mixing chamber (1), and the wiring end of each of the vibration rods (303) is respectively connected to the output end of a corresponding power supply connector (302), and a wiring base (304) and an independent power supply (305) are respectively fixedly mounted on the rear surface of the mixing chamber (1), and the output end of the independent power supply (305) is fixedly mounted. A first wire (306) is fixedly connected to the mixing bin (1), the output end of the first wire (306) is connected to the wiring end of the wiring base (304), a group of second wires (307) is fixedly connected inside the wiring base (304), and the number of a group of second wires (307) is equal to a group of power supply connectors (302), and the output end of each second wire (307) is respectively connected to the wiring end of a corresponding power supply connector (302), the bottom of the mixing bin (1) is fixedly connected to a first square tube (308), the discharge end of the first square tube (308) is fixedly connected to an extended curved tube (310), and a first electric valve (309) is provided inside the first square tube (308); The drying and turning mechanism (4) comprises a first locking frame (401), the first locking frame (401) is fixedly mounted on the rear surface of the drying chamber (2), a forward and reverse servo motor (402) is fixedly mounted inside the first locking frame (401), a first rectangular frame (403) is movably mounted inside the drying chamber (2), a positioning frame (404) is fixedly mounted on the inner surface wall of the first rectangular frame (403), a hollow mesh plate (405) is fixedly embedded inside the positioning frame (404), and a top of the first rectangular frame (403) is fixedly mounted. A first bracket (406) is provided, a heat insulating sleeve (407) is fixedly installed at the center of the first bracket (406), a driving motor (408) is fixedly inserted inside the heat insulating sleeve (407), a first flange (409) is fixedly sleeved on the shaft end of the driving motor (408), a U-shaped joint (410) is installed at the bottom of the first flange (409), a transverse rod (411) is fixedly installed inside the U-shaped joint (410), a booster bar (412) is fixedly installed at the bottom of the transverse rod (411), and the first rectangular frame Two load-bearing frames (413) are welded on the front surface of (403), a second rectangular frame (414) is fixedly installed between the outer walls of the two load-bearing frames (413), a group of inner lining plates (415) are fixedly installed between the two sides of the inner wall of the second rectangular frame (414), and a high-resistance electric heating pipe (416) is arranged inside the group of inner lining plates (415), a first external plate (417) and a second external plate (418) are fixedly installed on the front and rear surfaces of the first rectangular frame (403), and the shaft ends of the forward and reverse servo motors (402) are fixedly inserted in the first Inside the external plate (417), a locking sleeve (419) is fixedly installed on the outer wall of the second external plate (418), a first solid rod (420) is fixedly inserted inside the locking sleeve (419), a connecting sleeve (421) is fixedly installed on the inner wall of the drying bin (2), one end of the outer wall of the first solid rod (420) is movably inserted inside the connecting sleeve (421), a material gathering funnel (422) is fixedly installed at the bottom of the drying bin (2), and a second square tube (423) is fixedly connected to the bottom of the material gathering funnel (422); The separation self-priming mechanism (5) comprises a bottom bracket (501), a lower support plate (502) is fixedly mounted on the bottom of the bottom bracket (501), a separation barrel (503) is fixedly mounted on the top of the lower support plate (502), a heating element is provided at the bottom of the separation barrel (503), a second bracket (504) is fixedly mounted on the top of the separation barrel (503), a first positioning sleeve (505) is fixedly mounted at the center of the second bracket (504), and a first electric push rod is fixedly inserted into the inner surface wall of the first positioning sleeve (505). (506), a first external board (507) and a second external board (508) are fixedly mounted on both sides of the outer wall of the second bracket (504), a line hub (511) and a photoelectric detection device (512) are fixedly mounted on the top of the first external board (507), a laser emitting head (513) is fixedly connected to the bottom center of the line hub (511), a light shield (514) is fixedly connected to the bottom of the line hub (511), a capture window (515) is provided inside the light shield (514), and the line hub (511) A group of information lines (516) are fixedly connected to the signal output end of the second external board (508), and the output ends of the group of information lines (516) are all connected to the input end of the photoelectric detection device (512). A second positioning sleeve (517) is fixedly installed inside the second external board (508), and a liquid pump (518) is fixedly inserted inside the second positioning sleeve (517). A second locking frame (519) is fixedly installed on the top of the second external board (508), and a second electric push rod (520) is fixedly installed inside the second locking frame (519). ), the shaft end fixed sleeve of the second electric push rod (520) is provided with an oil suction pipe (521), the input end of the liquid pump (518) is fixedly connected to a first hollow joint (522), the outer wall of the oil suction pipe (521) is fixedly connected to a second hollow joint (523), the outer wall of the first hollow joint (522) is fixedly connected to a group of oil guide hoses (524), and the liquid inlet ends of the group of oil guide hoses (524) all pass through the outer wall of the second hollow joint (523) and are connected to the interior of the second hollow joint (523).

2. The microalgae oil separation and purification device according to claim 1, characterized in that: The shaft end fixing sleeve of the first electric push rod (506) is provided with a roller bearing, and the outer shaft outer wall fixing sleeve of the roller bearing is provided with a second flange (509), the bottom of the second flange (509) is fixedly installed with a second solid rod (510), the bottom of the lower support plate (502) is fixedly installed with an organic variable component (525), the center of the separation barrel (503) is movably inserted with a transmission rod (527), the output end of the organic variable component (525) is connected to the bottom of the transmission rod (527), the bottom of the second solid rod (510) is provided with an adaptor slide (526), ​​the top of the transmission rod (527) is fixedly installed with a docking joint (528), and the outer wall of the second solid rod (510) is fixedly installed with a group of stirring components (529).

3. The microalgae oil separation and purification device according to claim 1, characterized in that: The top of the bottom bracket (501) is connected to the bottom of the drying bin (2), the top of the mixing bin (1) is provided with a cover (6), the top of the cover (6) is fixedly connected to a third-party oval tube (7), the interior of the third-party oval tube (7) is provided with a second electric valve (8), the four outer walls of the lower support plate (502) are fixedly installed with grafting plates (9), and the outer wall of each grafting plate (9) is fixedly installed with an adjustable foot (10).

Citation Information

Patent Citations

  • Technique for extracting and refining DHA enriched fatty acid from Crypthecodinium cohnii

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  • Sewage treatment flocculation tank

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  • Physical wall breaking process for sludge

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  • Settling device for preparing styrene-butadiene latex

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  • Continuous fluidized bed dryer for pesticide water dispersible granules

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