A methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid and a method of using the same

By designing a methoxyacetic acid methyl ester removal device including a driving part, a lifting part and a swing mechanism, the problems of insufficient heating uniformity and fractionation efficiency in the prior art are solved, and more efficient material heating and fractionation effects are achieved.

CN119455423BActive Publication Date: 2025-05-02SHANXI RUISEKE ENVIRONMENTAL PROTECTION TECH CO LTD
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Patent Information

Application Number
CN202510029460.5
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-01-08
Publication Date
2025-05-02
Estimated Expiration
2045-01-08

AI Technical Summary

Technical Problem

In the prior art, the methyl methoxyacetate removal device has insufficient heating uniformity and fractionation efficiency, resulting in low product purity and fractionation efficiency.

Method used

A device including a base, a driving part, a lifting part and a swing mechanism is designed. By driving the drive shaft to rotate, the mounting frame swings relative to the drive shaft, so that the material in the tank flows from one end to the other, and the material is fully and evenly heated by disturbing power in multiple directions.

Benefits of technology

Through multi-directional disturbance, the material is fully heated, which improves fractionation efficiency and product purity, and enhances the product fractionation rate.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a methyl methoxyacetate removal device for preparing methoxyacetic acid and a method for using the device, and belongs to the technical field of methoxyacetic acid preparation. A methyl methoxyacetate removal device for preparing methoxyacetic acid comprises a base, and also comprises: a driving part, the driving part comprises a driving motor fixed in the base and a driving shaft connected to the output shaft of the driving motor, and a mounting frame is connected to the outer side of the driving shaft; a lifting part, the lifting part is provided with two groups and arranged on both sides of the mounting frame, each group of lifting parts is connected with a transverse movement assembly, a tank body is provided between the two transverse movement assemblies, and a heating chamber with an electric heating element installed inside is opened on the tank body; and a swing mechanism, the swing mechanism is arranged on the mounting frame, and is used to drive the mounting frame to swing back and forth relative to the driving shaft; the invention makes the material in the tank body be subjected to disturbance forces in multiple directions, so that the material in the tank body is fully mixed and heated evenly, thereby ensuring the fractionation efficiency and fractionation quality.
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Description

Technical Field

[0001] The invention relates to the technical field of methoxyacetic acid preparation, and in particular to a methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid and a use method thereof. Background Art

[0002] Methoxyacetic acid is a chemical substance with the chemical formula C3H6O3 and a molecular weight of 90.08. A methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid is a device for removing methoxyacetic acid methyl ester to obtain methoxyacetic acid. The overall removal device includes a distillation device and the like.

[0003] In the prior art, such as the "A device for removing methyl methoxyacetate for preparing methoxyacetic acid" disclosed in the patent with patent application number CN202222065962.8 and the "A device for removing methyl methoxyacetate for preparing methoxyacetic acid" disclosed in the patent with patent application number CN202021534192.1, both control the axial movement of the stirring blade during the stirring process to fully mix the materials to improve the processing efficiency; however, in the specific operation process, the stirring blade is only controlled to move axially along the drive shaft during rotation, so that the material in the tank body only flows and mixes circumferentially around the inside of the tank body, and the efficiency of uniform heating of the material is still low, thereby reducing the purity and efficiency of the distillation product. Summary of the invention

[0004] The purpose of the present invention is to solve the problems existing in the prior art and to propose a methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid and a use method thereof.

[0005] In order to achieve the above object, the present invention adopts the following technical solutions:

[0006] A methyl methoxyacetate removal device for preparing methoxyacetic acid comprises a base and also comprises:

[0007] A driving unit, the driving unit comprising a driving motor fixed in the base and a driving shaft connected to an output shaft of the driving motor, and a mounting frame is connected to the outer side of the driving shaft;

[0008] A lifting part, wherein the lifting part is provided in two groups and is arranged on both sides of the mounting frame, each group of the lifting parts is connected to a transverse movement assembly, a tank body is provided between the two transverse movement assemblies, and a heating cavity with an electric heating element installed inside is opened on the tank body;

[0009] A swing mechanism, the swing mechanism is arranged on the mounting frame and is used to drive the mounting frame to swing back and forth relative to the driving shaft;

[0010] Wherein, the tank body is provided with a feeding pipe, a discharging pipe, an exhaust pipe and a conduit, and the conduit is provided with a vacuum pump.

[0011] Preferably, the outer side of the driving shaft is connected to a driving gear that rotates on the mounting frame, the inner side wall of the mounting frame is fixedly provided with a fixed gear ring, a movable gear is meshedly connected between the fixed gear ring and the driving gear, a rotating ring is rotatably connected to the mounting frame, and the lifting part is arranged on the rotating ring and connected to the movable gear.

[0012] Preferably, the lifting part includes a lifting rod rotatably connected to a rotating ring and connected to a movable gear, a sleeve threadedly connected to the outside of the lifting rod, and a connecting piece connected to the sleeve, wherein the connecting piece is connected to the transverse movement assembly, and the lifting rod includes a reciprocating screw fixedly connected to the movable gear and a first elastic telescopic rod fixedly connected to the reciprocating screw.

[0013] Preferably, the transverse movement assembly includes a first bevel gear fixedly mounted on the end of the first elastic telescopic rod, a fixed rod fixedly mounted on the first bevel gear, and a transverse movement rod movably mounted between the fixed rod and the tank body.

[0014] Preferably, the connecting member includes a connecting rod fixedly connected to the sleeve and a connecting plate connected to an end of the connecting rod away from the sleeve, and the connecting plate is rotationally connected to the first bevel gear.

[0015] Preferably, a stirring rod is rotatably connected in the tank body, a stirring blade is arranged on the stirring rod, an L-shaped plate is movably connected between the end of the stirring rod and the first bevel gear, and a second bevel gear meshing with the first bevel gear is arranged at the end of the stirring rod.

[0016] Preferably, the stirring rod includes a main rod body connected to the second bevel gear and a sleeve sleeved on the outside of the main rod body and connected to the tank body, a guide bar is fixedly provided on the outside of the main rod body, a guide groove for the sliding of the guide bar is provided on the inner wall of the sleeve, a connecting shaft connected to the stirring blade is provided on the main rod body, a concave hole for the movement of the connecting shaft is provided on the sleeve, a driven gear is provided on the connecting shaft, and a rack plate meshing with the driven gear is provided on the inner wall of the concave hole.

[0017] Preferably, the swing mechanism includes a force block fixed on the inner wall of the mounting frame, the driving shaft is provided with an abutment rod which movably abuts against the force block, the driving shaft is fixed with a sphere, the mounting frame is provided with a ball sleeve which matches with the sphere, a second elastic telescopic rod is movably arranged between the bottom of the mounting frame and the top of the base, a plurality of third elastic telescopic rods are evenly arranged in a circle on the outer side of the driving shaft, and the end of the third elastic telescopic rod away from the driving shaft is connected to the driving gear.

[0018] Preferably, a ball is provided at the bottom of the abutment rod, and an extrusion slope that abuts against the ball is provided at the top of the force-bearing block.

[0019] The present invention also discloses a method for using a methyl methoxyacetate removal device for preparing methoxyacetic acid, comprising the following steps:

[0020] S1: First, the electric heating element in the heating chamber is operated to heat the material in the tank through the heating chamber, and then the vacuum pump is controlled to operate, and the vacuum pump draws the tank into a vacuum state through the conduit;

[0021] S2: Then the driving motor is controlled to run, and the output shaft of the driving motor drives the driving shaft to rotate. When the driving gear rotates, the outer abutment rod presses against the inclined surface of the force block through the ball bearing, so that the mounting frame swings relative to the driving shaft, so that each end of the tank body arranged on the upper side of the mounting frame is intermittently raised and lowered, so that the material in the tank body flows from one end to the other end;

[0022] S3: When the driving shaft rotates, the driving gear can be driven to rotate in the mounting frame through the third elastic telescopic rod. The driving gear cooperates with the fixed gear ring to drive the movable gear to move in the mounting frame, so that the tank body rotates around the central axis of the driving shaft. When the movable gear moves, the reciprocating screw on the rotating ring is driven to rotate, and the sleeve moves along the axial direction of the reciprocating screw.

[0023] S4: When the sleeve moves upward along the reciprocating screw rod, the sleeve drives the tank body upward through the connecting piece and the transverse moving assembly. When the sleeve moves downward along the reciprocating screw rod, the sleeve drives the tank body downward through the connecting piece and the transverse moving assembly, so that the material in the tank body can be subjected to disturbance forces in multiple directions;

[0024] S5: When the reciprocating screw rotates, the first bevel gear is driven to rotate through the first elastic telescopic rod. When the first bevel gear rotates, the tank body is pushed to swing back and forth between the two transverse moving components through the fixed rod and the transverse moving rod. When the first bevel gear rotates, it meshes with the second bevel gear, so that the stirring rod drives the stirring blade to rotate in the tank body. With the reciprocating shaking of the tank body, the stirring blade can stir and mix the materials at different positions in the tank body, accelerate the uniform heating of the materials in the tank body, and then quickly fractionate the products.

[0025] Compared with the prior art, the present invention has the following beneficial effects:

[0026] 1. The methyl methoxyacetate removal device for preparing methoxyacetic acid and the use method thereof, by subjecting the material in the tank to disturbance forces in multiple directions, makes the material in the tank fully and evenly heated, thereby ensuring the fractionation efficiency and improving the purity of the product obtained by fractionation;

[0027] 2. The methyl methoxyacetate removal device for preparing methoxyacetic acid and its use method, when the tank body moves horizontally relative to the stirring rod, the sleeve and the main rod body move relatively, the rack plate on the sleeve and the driven gear on the connecting shaft are meshed and driven, so that the stirring blade can rotate around the connecting shaft when rotating around the axial direction of the stirring rod, so as to achieve disturbance of materials in different directions in the tank body, accelerate the heating of the product, and improve the product fractionation rate;

[0028] 3. The methoxyacetic acid methyl ester removal device and the use method thereof make the stirring blade rotate from bottom to top, so that the stirring blade can stir the material deposited on the lower side of the tank body, so that the material deposited on the lower side of the tank body can continuously participate in the mixing work, so that the material in the tank body is evenly heated, and the fractionation quality of the product is guaranteed. BRIEF DESCRIPTION OF THE DRAWINGS

[0029] Figure 1 The structure of the present invention is schematically shown Figure 1 ;

[0030] Figure 2 For the present invention Figure 1 A partial enlarged structural diagram of the middle part;

[0031] Figure 3 The structure of the present invention is schematically shown Figure 2 ;

[0032] Figure 4 It is a partial cross-sectional structural schematic diagram of the present invention;

[0033] Figure 5 For the present invention Figure 4 A schematic diagram of the partially enlarged structure of the middle B part;

[0034] Figure 6 It is a partial cross-sectional structural schematic diagram of the mounting frame of the present invention;

[0035] Figure 7 It is a schematic diagram of the external structure of the lifting rod of the present invention;

[0036] Figure 8 It is a schematic diagram of the overall structure of the tank body of the present invention;

[0037] Fig. 9 It is a schematic diagram of the cross-sectional structure of the tank body of the present invention;

[0038] Fig.10 It is a schematic diagram of the cross-sectional structure of the sleeve of the present invention;

[0039] Fig.11 It is a partial structural schematic diagram of the stirring rod of the present invention.

[0040] In the figure: 1, base; 2, driving motor; 201, driving shaft; 2011, sphere; 202, driving gear; 3, mounting frame; 301, fixed gear ring; 302, movable gear; 303, rotating ring; 4, tank body; 401, heating chamber; 402, feeding pipe; 403, discharging pipe; 404, exhaust pipe; 405, conduit; 4051, vacuum pump; 5, lifting rod; 501, sleeve; 502, connecting piece; 5021, connecting rod; 5022, connecting plate; 503, reciprocating screw rod; 504, the first An elastic telescopic rod; 6, a first bevel gear; 601, a fixed rod; 602, a transverse rod; 7, a stirring rod; 701, a main rod body; 7011, a guide strip; 702, a sleeve; 7021, a guide groove; 703, a connecting shaft; 7031, a driven gear; 704, a stirring blade; 705, a concave hole; 7051, a rack plate; 8, an L-shaped plate; 801, a second bevel gear; 9, a force block; 10, abutting rod; 1001, a ball; 11, a ball sleeve; 12, a second elastic telescopic rod; 13, a third elastic telescopic rod. DETAILED DESCRIPTION

[0041] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0042] In the description of the present invention, it is necessary to understand that the terms "upper", "lower", "front", "back", "left", "right", "top", "bottom", "inside", "outside", etc., indicating the orientation or position relationship are based on the orientation or position relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0043] Example 1: Reference Figure 1 , Figure 3 , Figure 4 , Figure 6 , Figure 7 , Figure 8 and Fig. 9 , a methyl methoxyacetate removal device for preparing methoxyacetic acid, comprising a base 1, and also comprising:

[0044] The driving part includes a driving motor 2 fixed in the base 1 and a driving shaft 201 connected to the output shaft of the driving motor 2, and a mounting frame 3 is connected to the outer side of the driving shaft 201;

[0045] Lifting parts, two groups of lifting parts are arranged on both sides of the mounting frame 3, each group of lifting parts is connected to a transverse moving assembly, a tank body 4 is arranged between the two transverse moving assemblies, and a heating chamber 401 with an electric heating element installed inside is opened on the tank body 4;

[0046] A swing mechanism, which is disposed on the mounting frame 3 and is used to drive the mounting frame 3 to swing back and forth relative to the driving shaft 201;

[0047] The tank body 4 is provided with a feeding pipe 402 , a discharging pipe 403 , an exhaust pipe 404 and a conduit 405 , and the conduit 405 is provided with a vacuum pump 4051 .

[0048] Specifically, first, the electric heating element in the heating chamber 401 is operated to heat the material in the tank body 4 through the heating chamber 401, and then the vacuum pump 4051 is controlled to operate. The vacuum pump 4051 draws the tank body 4 into a vacuum state through the conduit 405, and then the driving motor 2 of the driving unit is controlled to operate. The output shaft of the driving motor 2 drives the mounting frame 3 to rotate through the driving shaft 201, so that the lifting part, the swing mechanism and the transverse movement component are moved, so that the material in the tank body 4 is subjected to disturbance forces in multiple directions, so that the material in the tank body 4 is fully and evenly heated, thereby ensuring the distillation efficiency and improving the purity of the product obtained by distillation.

[0049] Example 2: Reference Figure 1 , Figure 2 , Figure 3 , Figure 4 , Figure 5 , Figure 6 , Figure 7 and Figure 8 , a methyl methoxyacetate removal device for preparing methoxyacetic acid, based on Example 1, further, the outer side of the driving shaft 201 is connected to a driving gear 202 rotating on a mounting frame 3, the inner side wall of the mounting frame 3 is fixedly provided with a fixed gear ring 301, a movable gear 302 is meshedly connected between the fixed gear ring 301 and the driving gear 202, a rotating ring 303 is rotatably connected to the mounting frame 3, and the lifting part is arranged on the rotating ring 303 and connected to the movable gear 302.

[0050] The lifting part includes a lifting rod 5 rotatably connected to the rotating ring 303 and connected to the movable gear 302, a sleeve 501 threadedly connected to the outside of the lifting rod 5, and a connecting piece 502 connected to the sleeve 501, the connecting piece 502 is connected to the transverse movement assembly, and the lifting rod 5 includes a reciprocating screw rod 503 fixedly connected to the movable gear 302 and a first elastic telescopic rod 504 fixedly connected to the reciprocating screw rod 503.

[0051] The transverse movement assembly includes a first bevel gear 6 fixedly mounted at the end of the first elastic telescopic rod 504 , a fixed rod 601 fixedly mounted on the first bevel gear 6 , and a transverse movement rod 602 movably mounted between the fixed rod 601 and the tank body 4 .

[0052] The connecting member 502 includes a connecting rod 5021 fixedly connected to the sleeve 501 and a connecting plate 5022 connected to one end of the connecting rod 5021 away from the sleeve 501 . The connecting plate 5022 is rotationally connected to the first bevel gear 6 .

[0053] Specifically, when the driving shaft 201 rotates, it drives the driving gear 202 to rotate in the mounting frame 3. The driving gear 202 cooperates with the fixed gear ring 301 to drive the movable gear 302 to move in the mounting frame 3, so that the tank body 4 rotates around the central axis of the driving shaft 201. When the movable gear 302 moves, it drives the reciprocating screw rod 503 on the rotating ring 303 to rotate, and the sleeve 501 moves axially along the reciprocating screw rod 503. When the sleeve 501 moves up along the reciprocating screw rod 503, the sleeve 501 drives the tank body 4 to move up through the connecting piece 502 and the transverse movement assembly, and the sleeve 501 moves upward along the reciprocating screw rod 503. When the reciprocating screw rod 503 moves downward, the sleeve 501 drives the tank body 4 to move downward through the connecting piece 502 and the transverse movement assembly, and the first elastic telescopic rod 504 is compressed. When the reciprocating screw rod 503 rotates, it also drives the first bevel gear 6 to rotate through the first elastic telescopic rod 504. When the first bevel gear 6 rotates, it pushes the tank body 4 to swing back and forth between the two transverse movement assemblies through the fixed rod 601 and the transverse movement rod 602, so that the material in the tank body 4 can be subjected to disturbance forces in multiple directions, which accelerates the uniform heating of the material in the tank body 4, thereby allowing the product to be quickly fractionated and improving the product fractionation rate.

[0054] Example 3: Reference Figure 1 , Figure 2 , Figure 3 , Figure 4 , Figure 8 and Fig. 9 , a methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid, based on Example 2, further, a stirring rod 7 is rotatably connected in the tank body 4, and a stirring blade 704 is provided on the stirring rod 7. An L-shaped plate 8 is movably connected between the end of the stirring rod 7 and the first bevel gear 6, and a second bevel gear 801 meshing with the first bevel gear 6 is provided at the end of the stirring rod 7.

[0055] Specifically, when the reciprocating screw rod 503 rotates, the first bevel gear 6 is driven to rotate through the first elastic telescopic rod 504. When the first bevel gear 6 rotates, it pushes the tank body 4 to swing back and forth between the two transverse moving components through the fixed rod 601 and the transverse moving rod 602. When the first bevel gear 6 rotates, it meshes with the second bevel gear 801, so that the stirring rod 7 drives the stirring blade 704 to rotate in the tank body 4. In conjunction with the reciprocating shaking of the tank body 4, the stirring blade 704 can stir and mix the materials at different positions in the tank body 4, thereby increasing its stirring working range, accelerating the uniform heating of the materials in the tank body 4, and then quickly fractionating the products. The tank body 4 is placed horizontally, and by rotating the stirring blade 704 from bottom to top, it is convenient for the stirring blade 704 to push the materials deposited on the lower side of the tank body 4 upward, so that the materials deposited on the lower side of the tank body 4 can continuously participate in the mixing work, so that the materials in the tank body 4 are heated evenly, and the fractionation quality of the products is guaranteed.

[0056] Example 4: Reference Fig. 9 , Fig.10 and Fig.11 , a methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid, based on Example 3, further, the stirring rod 7 includes a main rod body 701 connected to the second bevel gear 801 and a sleeve 702 sleeved on the outside of the main rod body 701 and connected to the tank body 4, a guide bar 7011 is fixedly provided on the outside of the main rod body 701, and a guide groove 7021 for sliding of the guide bar 7011 is provided on the inner wall of the sleeve 702, a connecting shaft 703 connected to a stirring blade 704 is provided on the main rod body 701, a concave hole 705 for the movement of the connecting shaft 703 is provided on the sleeve 702, a driven gear 7031 is provided on the connecting shaft 703, and a rack plate 7051 meshing with the driven gear 7031 is provided on the inner wall of the concave hole 705.

[0057] Specifically, when the transverse movement assembly is working, the main rod body 701 will slide relative to the sleeve 702, and the rack plate 7051 on the sleeve 702 will mesh with the driven gear 7031 on the connecting shaft 703 for transmission, so that the stirring blade 704 can rotate around the connecting shaft 703 when it rotates axially around the stirring rod 7, thereby realizing the disturbance of the material in different directions in the tank body 4, accelerating the mixing of the product, making it evenly heated, and improving the product fractionation rate.

[0058] Example 5: Reference Figure 1 , Figure 3 , Figure 4 and Figure 5, a methoxyacetic acid methyl ester removal device for preparing methoxyacetic acid, based on Example 4, further, the swing mechanism includes a force block 9 fixedly mounted on the inner wall of the mounting frame 3, a driving shaft 201 is provided with a contact rod 10 that movably abuts against the force block 9, a sphere 2011 is fixedly mounted on the driving shaft 201, a ball sleeve 11 that matches the sphere 2011 is provided on the mounting frame 3, a second elastic telescopic rod 12 is movably arranged between the bottom of the mounting frame 3 and the top of the base 1, a plurality of third elastic telescopic rods 13 are evenly arranged on the outer side of the driving shaft 201 in a circumferential manner, and the end of the third elastic telescopic rod 13 away from the driving shaft 201 is connected to the driving gear 202.

[0059] Furthermore, a ball 1001 is provided at the bottom of the abutting rod 10 , and an extrusion slope that movably abuts against the ball 1001 is provided at the top of the force-bearing block 9 .

[0060] Specifically, by controlling the operation of the driving motor 2, the output shaft of the driving motor 2 drives the driving shaft 201 to rotate. When the driving gear 202 rotates, the outer abutment rod 10 presses against the inclined surface of the force block 9 through the ball 1001, and the mounting frame 3 moves on the outside of the ball 2011 through the ball sleeve 11, so that the mounting frame 3 swings relative to the driving shaft 201, so that each end of the tank body 4 arranged on the upper side of the mounting frame 3 is intermittently raised and lowered, so that the material in the tank body 4 flows from one end to the other end, and further makes the material in the tank body 4 fully and evenly heated, thereby ensuring the distillation efficiency and improving the purity of the product obtained by distillation.

[0061] The present invention also discloses a method for using a methyl methoxyacetate removal device for preparing methoxyacetic acid, comprising the following steps:

[0062] S1: First, the electric heating element in the heating chamber 401 is operated to heat the material in the tank body 4 through the heating chamber 401, and then the vacuum pump 4051 is controlled to operate, and the vacuum pump 4051 draws the tank body 4 into a vacuum state through the conduit 405;

[0063] S2: Then the driving motor 2 is controlled to run, and the output shaft of the driving motor 2 drives the driving shaft 201 to rotate. When the driving gear 202 rotates, the outer abutting rod 10 presses against the inclined surface of the force block 9 through the ball 1001, so that the mounting frame 3 swings relative to the driving shaft 201, so that each end of the tank body 4 arranged on the upper side of the mounting frame 3 is intermittently raised and lowered, so that the material in the tank body 4 flows from one end to the other end;

[0064] S3: When the driving shaft 201 rotates, it can drive the driving gear 202 to rotate in the mounting frame 3 through the third elastic telescopic rod 13. The driving gear 202 cooperates with the fixed gear ring 301 to drive the movable gear 302 to move in the mounting frame 3, so that the tank body 4 rotates around the central axis of the driving shaft 201. When the movable gear 302 moves, it drives the reciprocating screw 503 on the rotating ring 303 to rotate, and the sleeve 501 moves axially along the reciprocating screw 503;

[0065] S4: When the sleeve 501 moves upward along the reciprocating screw rod 503, the sleeve 501 drives the tank body 4 to move upward through the connecting piece 502 and the transverse moving assembly. When the sleeve 501 moves downward along the reciprocating screw rod 503, the sleeve 501 drives the tank body 4 to move downward through the connecting piece 502 and the transverse moving assembly, so that the material in the tank body 4 can be subjected to disturbance forces in multiple directions.

[0066] S5: When the reciprocating screw 503 rotates, it drives the first bevel gear 6 to rotate through the first elastic telescopic rod 504. When the first bevel gear 6 rotates, it pushes the tank body 4 to swing back and forth between the two transverse components through the fixed rod 601 and the transverse rod 602. When the first bevel gear 6 rotates, it meshes with the second bevel gear 801, so that the stirring rod 7 drives the stirring blade 704 to rotate in the tank body 4. With the reciprocating shaking of the tank body 4, the stirring blade 704 can stir and mix the materials at different positions in the tank body 4, accelerate the uniform heating of the materials in the tank body 4, and then quickly fractionate the products.

[0067] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A methyl methoxyacetate removal device for preparing methoxyacetic acid, comprising a base (1), characterized in that: Also includes: A driving unit, the driving unit comprising a driving motor (2) fixedly mounted in the base (1) and a driving shaft (201) connected to an output shaft of the driving motor (2), wherein the outer side of the driving shaft (201) is connected to a mounting frame (3); Lifting parts, the lifting parts are provided in two groups and are arranged on both sides of the mounting frame (3), each group of the lifting parts is connected to a transverse movement assembly, a tank body (4) is provided between the two transverse movement assemblies, and a heating chamber (401) with an electric heating element installed inside is provided on the tank body (4); A swing mechanism, the swing mechanism being arranged on the mounting frame (3) and being used to drive the mounting frame (3) to swing back and forth relative to the drive shaft (201); The tank body (4) is provided with a feeding pipe (402), a discharging pipe (403), an exhaust pipe (404) and a conduit (405), and the conduit (405) is provided with a vacuum pump (4051); The outer side of the driving shaft (201) is connected to a driving gear (202) that rotates on the mounting frame (3); a fixed gear ring (301) is fixedly provided on the inner side wall of the mounting frame (3); a movable gear (302) is meshedly connected between the fixed gear ring (301) and the driving gear (202); a rotating ring (303) is rotatably connected to the mounting frame (3); and the lifting portion is arranged on the rotating ring (303) and is connected to the movable gear (302); The lifting part comprises a lifting rod (5) rotatably connected to a rotating ring (303) and connected to a movable gear (302), a sleeve (501) threadedly connected to the outside of the lifting rod (5), and a connecting piece (502) connected to the sleeve (501), wherein the connecting piece (502) is connected to a transverse movement assembly, and the lifting rod (5) comprises a reciprocating screw rod (503) fixedly connected to the movable gear (302) and a first elastic telescopic rod (504) fixedly connected to the reciprocating screw rod (503); The transverse movement assembly comprises a first bevel gear (6) fixedly mounted on the end of a first elastic telescopic rod (504), a fixed rod (601) fixedly mounted on the first bevel gear (6), and a transverse movement rod (602) movably mounted between the fixed rod (601) and the tank body (4); The swing mechanism comprises a force-bearing block (9) fixedly mounted on the inner wall of the mounting frame (3); an abutting rod (10) movably abutting against the force-bearing block (9) is arranged on the driving shaft (201); a sphere (2011) is fixedly mounted on the driving shaft (201); a ball sleeve (11) matched with the sphere (2011) is arranged on the mounting frame (3); a second elastic telescopic rod (12) is movably arranged between the bottom of the mounting frame (3) and the top of the base (1); a plurality of third elastic telescopic rods (13) are evenly arranged in a circumferential manner on the outer side of the driving shaft (201); one end of the third elastic telescopic rod (13) away from the driving shaft (201) is connected to the driving gear (202); a ball (1001) is arranged at the bottom of the abutting rod (10); and an extrusion inclined surface movably abutting against the ball (1001) is provided on the top of the force-bearing block (9).

2. A methyl methoxyacetate removal device for preparing methoxyacetic acid according to claim 1, characterized in that: The connecting member (502) comprises a connecting rod (5021) fixedly connected to the sleeve (501) and a connecting plate (5022) connected to an end of the connecting rod (5021) away from the sleeve (501), and the connecting plate (5022) is rotationally connected to the first bevel gear (6).

3. A methyl methoxyacetate removal device for preparing methoxyacetic acid according to claim 2, characterized in that: A stirring rod (7) is rotatably connected inside the tank body (4), and a stirring blade (704) is provided on the stirring rod (7). An L-shaped plate (8) is movably connected between the end of the stirring rod (7) and the first bevel gear (6), and a second bevel gear (801) meshing with the first bevel gear (6) is provided at the end of the stirring rod (7).

4. A methyl methoxyacetate removal device for preparing methoxyacetic acid according to claim 3, characterized in that: The stirring rod (7) comprises a main rod body (701) connected to the second bevel gear (801) and a sleeve (702) sleeved on the outside of the main rod body (701) and connected to the tank body (4); a guide bar (7011) is fixedly provided on the outside of the main rod body (701); a guide groove (7021) for the guide bar (7011) to slide is provided on the inner wall of the sleeve (702); a connecting shaft (703) connected to the stirring blade (704) is provided on the main rod body (701); a concave hole (705) for the connecting shaft (703) to move is provided on the sleeve (702); a driven gear (7031) is provided on the connecting shaft (703); and a rack plate (7051) meshing with the driven gear (7031) is provided on the inner wall of the concave hole (705).

5. A method for using the device for removing methyl methoxyacetate for preparing methoxyacetic acid according to claim 4, characterized in that: The following steps are involved: S1: firstly, the electric heating element in the heating chamber (401) is operated to heat the material in the tank body (4) through the heating chamber (401), and then the vacuum pump (4051) is controlled to operate, and the vacuum pump (4051) draws the tank body (4) into a vacuum state through the conduit (405); S2: Then, the driving motor (2) is controlled to operate, and the output shaft of the driving motor (2) drives the driving shaft (201) to rotate. When the driving gear (202) rotates, the outer abutting rod (10) presses against the inclined surface of the force bearing block (9) through the ball (1001), so that the mounting frame (3) swings relative to the driving shaft (201), thereby causing each end of the tank body (4) arranged on the upper side of the mounting frame (3) to be intermittently raised and lowered, so that the material in the tank body (4) flows from one end to the other end; S3: When the driving shaft (201) rotates, the driving gear (202) can be driven to rotate in the mounting frame (3) through the third elastic telescopic rod (13); the driving gear (202) cooperates with the fixed gear ring (301) to drive the movable gear (302) to move in the mounting frame (3), so that the tank body (4) rotates around the central axis of the driving shaft (201); when the movable gear (302) moves, the reciprocating screw (503) on the rotating ring (303) is driven to rotate, and the sleeve (501) moves along the axial direction of the reciprocating screw (503); S4: When the sleeve (501) moves upward along the reciprocating screw rod (503), the sleeve (501) drives the tank body (4) to move upward through the connecting piece (502) and the transverse movement assembly. When the sleeve (501) moves downward along the reciprocating screw rod (503), the sleeve (501) drives the tank body (4) to move downward through the connecting piece (502) and the transverse movement assembly, so that the material in the tank body (4) can be subjected to disturbance forces in multiple directions. S5: When the reciprocating screw (503) rotates, the first bevel gear (6) is driven to rotate via the first elastic telescopic rod (504). When the first bevel gear (6) rotates, the tank body (4) is pushed to swing back and forth between the two transverse moving components via the fixed rod (601) and the transverse moving rod (602). When the first bevel gear (6) rotates, it meshes with the second bevel gear (801), so that the stirring rod (7) drives the stirring blade (704) to rotate in the tank body (4). In conjunction with the reciprocating shaking of the tank body (4), the stirring blade (704) can stir and mix materials at different positions in the tank body (4), thereby accelerating the uniform heating of the materials in the tank body (4), thereby allowing the products to be fractionated out quickly.

Citation Information

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