Production process of efficient anti-dazzle glass

By adjusting the composition and temperature of the frosting liquid and polishing liquid in the anti-glare glass production process, the rate and uniformity of the glass frosting are improved, the anti-glare effect and polishing effect are improved, and the low etching rate in the existing process is solved. , poor uniformity and poor anti-glare effect have achieved efficient and economical glass production.

CN119461867APending Publication Date: 2025-02-18FUJIAN CHENGDA GLASS CO LTD
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Patent Information

Application Number
CN202411625071.0
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-11-14
Publication Date
2025-02-18

AI Technical Summary

Technical Problem

The existing anti-glare glass process has problems such as low etching rate of glass frosting liquid, poor etching uniformity, uneven surface concave and convexity, poor anti-glare effect, and difficult to remove impurities on the glass surface.

Method used

A production process of high-efficiency anti-glare glass is adopted, including original sheet cutting, one-time cleaning, film patching, frosting, polishing, secondary cleaning, film tearing, three-time cleaning, inspection and finished product packaging. By adding hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, and ammonium chloride to the frosting liquid, and controlling the liquid temperature between 45℃-60℃, and adding hydrofluoric acid, ammonium hydrogen fluoride, and organic acid to the polishing liquid, the temperature is controlled. At 30℃-50℃, the polishing rate is controlled at 2000r/min-5000r/min to improve the frosting effect and polishing effect.

Benefits of technology

The rate and uniformity of glass frosting are improved, the anti-glare effect of glass is improved, the surface of glass tends to be flattened, and the bending resistance of glass after etching is improved. The composition of frosting liquid and polishing liquid is easier to obtain. Lower cost and better economic benefits.

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Abstract

The invention provides a production process of efficient anti-dazzle glass, and belongs to the technical field of anti-dazzle glass production. Comprising the following steps of raw sheet cutting, primary cleaning, film pasting, frosting, polishing, secondary cleaning, film tearing, third cleaning, inspection and flattening and packaging. The raw sheet cutting specifically comprises the following steps: cutting a glass raw sheet into required specifications and sizes by using a cutting machine; the specific process of primary cleaning is as follows: cleaning the cut glass with clear water to remove dust, impurities and dirt on the surface of the glass. According to the invention, the frosting rate and uniformity of the glass are improved, the anti-dazzle effect of the glass is improved, and the surface of the glass tends to be flat, so that the purpose of polishing the glass is achieved, the bending resistance of the etched glass is higher, the components of the frosting liquid and the polishing liquid are easier to obtain, the cost is lower, and the economic benefit is better.
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Description

Technical Field

[0001] The invention relates to the technical field of anti-glare glass production, and in particular to a production process of high-efficiency anti-glare glass. Background Art

[0002] Among the light entering the human eye, blue light and ultraviolet light are more harmful and are one of the main causes of glare. Therefore, anti-glare glass came into being. Anti-glare glass, referred to as AG glass, is a glass with a special surface treatment. The principle is to process one or both sides of the glass to make it have a lower reflectivity than ordinary glass, thereby reducing the interference of ambient light and reducing the occurrence of glare.

[0003] In the prior art, the production of anti-glare glass is mostly carried out by spraying, etching, sandblasting, coating and laminating. Spraying anti-glare glass is to form a layer of uniformly dispersed nano-scale silica particle suspension on the glass surface by spraying, and then adhere to the glass surface after heat treatment to accumulate into an uneven film layer. Etching anti-glare glass is to dissolve the silicon and oxygen on the surface of the glass with hydrofluoric acid, and obtain a glossy surface or a matte surface according to the solubility of the residual salts.

[0004] The present application aims to improve the problems of low etching rate of glass frosting liquid, poor etching uniformity, uneven surface, poor anti-glare effect, and difficulty in removing impurities on the glass surface during the actual production process of etched anti-glare glass, and provides a production process for efficient anti-glare glass to meet the needs. Summary of the invention

[0005] The technical problem to be solved by the present invention is to provide a production process for efficient anti-glare glass to solve the problems of low etching rate of glass frosting liquid, poor etching uniformity, uneven surface, poor anti-glare effect and difficulty in removing impurities on the glass surface in the actual production process of the existing etched anti-glare glass.

[0006] In order to solve the above technical problems, the present invention provides the following technical solutions:

[0007] A production process of high-efficiency anti-glare glass, comprising the following steps: original sheet cutting → primary cleaning → film application → frosting → polishing → secondary cleaning → film tearing → tertiary cleaning → inspection → flat packing;

[0008] The specific process of the original sheet cutting is: using a cutting machine to cut the glass original sheet into required specifications and sizes;

[0009] The specific process of the first cleaning is: using clean water to clean the cut glass to remove dust, impurities and dirt on the surface of the glass;

[0010] The specific process of film laminating is: using a film to laminating the non-frosted surface of the glass to protect the non-frosted surface from being affected by the frosting liquid and the frosting operation;

[0011] The specific frosting process is as follows: immersing the glass in the frosting liquid for etching, so that the glass and the frosting liquid are fully immersed and reacted, and finally the desired frosting effect is obtained;

[0012] The specific polishing process is as follows: putting the frosted glass into the polishing liquid for liquid polishing, and adjusting the concentration and rate of the polishing liquid to achieve the purpose of polishing the glass surface;

[0013] The specific process of the secondary cleaning is: washing the frosted surface of the glass with 3% to 8% hydrochloric acid to remove the frosting liquid residue on the glass surface, and then washing the glass with clean water to remove dust, impurities and dirt on the glass surface;

[0014] The specific process of film peeling is as follows: using an automatic film peeling machine to remove the film on the non-frosted surface of the glass;

[0015] The specific process of the three cleanings is: using clean water to clean the frosted and film-removed glass to remove stains and impurities on the glass surface;

[0016] The specific inspection process is as follows: inspect the frosted glass to determine whether the product quality is qualified;

[0017] The specific process of finished product packaging is as follows: the glass that has been frosted and inspected and passed the test is the finished product and can be packaged.

[0018] In some examples, the film used for the film is made of PVC material.

[0019] In some examples, the frosting liquid is a mixture of hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, ammonium chloride and water, and the specific ratio of the frosting liquid is: by mass percentage, hydrofluoric acid 10% to 20%, sulfuric acid 10% to 15%, nitric acid 10% to 15%, oxalic acid 8% to 15%, ammonium chloride 10% to 25%, and water 40% to 60%.

[0020] In some examples, the polishing liquid is a mixture of hydrofluoric acid, ammonium bifluoride, an organic acid and water, and the specific ratio of the polishing liquid is: 8% to 15% hydrofluoric acid, 5% to 15% ammonium bifluoride, 5% to 20% organic acid, and 50% to 80% water by mass.

[0021] In some examples, the organic acid is one of carboxylic acid, sulfonic acid and sulfinic acid.

[0022] In some examples, the liquid temperature of the frosting liquid is controlled at 45° C.-60° C., the liquid temperature of the polishing liquid is controlled at 30° C.-50° C., and the polishing rate is controlled at 2000 r / min-5000 r / min.

[0023] Compared with the prior art, the present invention has at least the following beneficial effects:

[0024] 1. The production process of this high-efficiency anti-glare glass uses frosting liquid to etch the glass during the glass frosting process, and uses polishing liquid to liquid-polish the surface of the glass. By adjusting and using the composition, specific gravity and temperature of the frosting liquid and polishing liquid, the glass surface can achieve the desired frosting effect and the anti-glare purpose.

[0025] 2. The production process of this high-efficiency anti-glare glass aims to solve the problems of low etching rate, poor etching uniformity, uneven surface, poor anti-glare effect, etc. in traditional glass frosting liquid. In this glass frosting process, hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, and ammonium chloride are added to the frosting liquid, and the liquid temperature of the frosting liquid is controlled at 45°C-60°C, thereby increasing the rate and uniformity of glass frosting and improving the anti-glare effect of the glass. In addition, the frosting liquid components are easier to obtain, the cost is lower, and the economic benefits are better.

[0026] 3. The production process of this high-efficiency anti-glare glass adds hydrofluoric acid, ammonium bifluoride, and organic acid to the polishing liquid, and the temperature is controlled at 30℃-50℃. It can effectively remove impurities on the glass surface, reduce the unevenness of the glass surface, and make the glass surface smooth, thereby achieving the purpose of glass polishing. It also makes the etched glass more resistant to bending, and the polishing liquid is easier to obtain, the cost is lower, and the economic benefits are better. BRIEF DESCRIPTION OF THE DRAWINGS

[0027] The accompanying drawings, which are incorporated herein and constitute a part of the specification, illustrate embodiments of the present disclosure and, together with the description, further serve to explain the principles of the present disclosure and to enable those skilled in the relevant art to make and use the present disclosure.

[0028] Figure 1 The figure is a flowchart of a production process of a highly efficient anti-glare glass. DETAILED DESCRIPTION

[0029] In order to enable those skilled in the art to better understand the scheme of the present invention, the technical scheme in the embodiments of the present invention will be clearly and completely described below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work should fall within the scope of protection of the present invention.

[0030] As described in the background art, in the actual production process of etched anti-glare glass, there are problems such as low etching rate of glass frosting liquid, poor etching uniformity, uneven surface, poor anti-glare effect, and difficulty in removing impurities on the glass surface.

[0031] In order to solve this technical problem, the present invention provides a production process of high-efficiency anti-glare glass, which is applied to the production of high-efficiency anti-glare glass.

[0032] Example 1

[0033] The embodiment of the present invention provides a production process of high-efficiency anti-glare glass, including the following steps: original sheet cutting → primary cleaning → film lamination → frosting → polishing → secondary cleaning → film tearing → tertiary cleaning → inspection → flat packing;

[0034] The specific process of the original sheet cutting is: using a cutting machine to cut the glass original sheet into required specifications and sizes;

[0035] The specific process of the first cleaning is: using clean water to clean the cut glass to remove dust, impurities and dirt on the surface of the glass;

[0036] The specific process of film laminating is: using a film to laminating the non-frosted surface of the glass to protect the non-frosted surface from being affected by the frosting liquid and the frosting operation;

[0037] The specific frosting process is as follows: immersing the glass in the frosting liquid for etching, so that the glass and the frosting liquid are fully immersed and reacted, and finally the desired frosting effect is obtained;

[0038] The specific polishing process is as follows: putting the frosted glass into the polishing liquid for liquid polishing, and adjusting the concentration and rate of the polishing liquid to achieve the purpose of polishing the glass surface;

[0039] The specific process of the secondary cleaning is: washing the frosted surface of the glass with 4% hydrochloric acid to remove the frosting liquid residue on the glass surface, and then washing the glass with clean water to remove dust, impurities and dirt on the glass surface;

[0040] The specific process of film peeling is as follows: using an automatic film peeling machine to remove the film on the non-frosted surface of the glass;

[0041] The specific process of the three cleanings is: using clean water to clean the frosted and film-removed glass to remove stains and impurities on the glass surface;

[0042] The specific inspection process is as follows: inspect the frosted glass to determine whether the product quality is qualified;

[0043] The specific process of finished product packaging is as follows: the glass that has been frosted and inspected and passed the test is the finished product and can be packaged.

[0044] It should be further explained in this embodiment that the film used for the film is made of PVC material.

[0045] In some examples, the frosting liquid is a mixture of hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, ammonium chloride and water, and the specific ratio of the frosting liquid is: 15% hydrofluoric acid, 12% sulfuric acid, 10% nitric acid, 8% oxalic acid, 10% ammonium chloride and 45% water by mass percentage.

[0046] It should be further explained in this embodiment that the polishing liquid is a mixture of hydrofluoric acid, ammonium bifluoride, organic acid and water, and the specific ratio of the polishing liquid is: 10% hydrofluoric acid, 10% ammonium bifluoride, 15% organic acid and 65% water by mass.

[0047] It should be further explained in this embodiment that the organic acid is one of carboxylic acid, sulfonic acid and sulfinic acid.

[0048] It should be further explained in this embodiment that the liquid temperature of the frosting liquid is controlled at 50° C., the liquid temperature of the polishing liquid is controlled at 35° C., and the polishing rate is controlled at 2500 r / min.

[0049] Example 2

[0050] The embodiment of the present invention provides a production process of high-efficiency anti-glare glass, including the following steps: original sheet cutting → primary cleaning → film lamination → frosting → polishing → secondary cleaning → film tearing → tertiary cleaning → inspection → flat packing;

[0051] The specific process of the original sheet cutting is: using a cutting machine to cut the glass original sheet into required specifications and sizes;

[0052] The specific process of the first cleaning is: using clean water to clean the cut glass to remove dust, impurities and dirt on the surface of the glass;

[0053] The specific process of film laminating is: using a film to laminating the non-frosted surface of the glass to protect the non-frosted surface from being affected by the frosting liquid and the frosting operation;

[0054] The specific frosting process is as follows: immersing the glass in the frosting liquid for etching, so that the glass and the frosting liquid are fully immersed and reacted, and finally the desired frosting effect is obtained;

[0055] The specific polishing process is as follows: putting the frosted glass into the polishing liquid for liquid polishing, and adjusting the concentration and rate of the polishing liquid to achieve the purpose of polishing the glass surface;

[0056] The specific process of the secondary cleaning is: washing the frosted surface of the glass with 6% hydrochloric acid to remove the frosting liquid residue on the glass surface, and then washing the glass with clean water to remove dust, impurities and dirt on the glass surface;

[0057] The specific process of film peeling is as follows: using an automatic film peeling machine to remove the film on the non-frosted surface of the glass;

[0058] The specific process of the three cleanings is: using clean water to clean the frosted and film-removed glass to remove stains and impurities on the glass surface;

[0059] The specific inspection process is as follows: inspect the frosted glass to determine whether the product quality is qualified;

[0060] The specific process of finished product packaging is as follows: the glass that has been frosted and inspected and passed the test is the finished product and can be packaged.

[0061] It should be further explained in this embodiment that the film used for the film is made of PVC material.

[0062] In some examples, the frosting liquid is a mixture of hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, ammonium chloride and water, and the specific ratio of the frosting liquid is: 10% hydrofluoric acid, 10% sulfuric acid, 10% nitric acid, 10% oxalic acid, 10% ammonium chloride and 50% water by mass percentage.

[0063] It should be further explained in this embodiment that the polishing liquid is a mixture of hydrofluoric acid, ammonium bifluoride, organic acid and water, and the specific ratio of the polishing liquid is: 8% hydrofluoric acid, 12% ammonium bifluoride, 20% organic acid and 55% water by mass.

[0064] It should be further explained in this embodiment that the organic acid is one of carboxylic acid, sulfonic acid and sulfinic acid.

[0065] It should be further explained in this embodiment that the liquid temperature of the frosting liquid is controlled at 55° C., the liquid temperature of the polishing liquid is controlled at 40° C., and the polishing rate is controlled at 3500 r / min.

[0066] Example 3

[0067] The embodiment of the present invention provides a production process of high-efficiency anti-glare glass, including the following steps: original sheet cutting → primary cleaning → film lamination → frosting → polishing → secondary cleaning → film tearing → tertiary cleaning → inspection → flat packing;

[0068] The specific process of the original sheet cutting is: using a cutting machine to cut the glass original sheet into required specifications and sizes;

[0069] The specific process of the first cleaning is: using clean water to clean the cut glass to remove dust, impurities and dirt on the surface of the glass;

[0070] The specific process of film laminating is: using a film to laminating the non-frosted surface of the glass to protect the non-frosted surface from being affected by the frosting liquid and the frosting operation;

[0071] The specific frosting process is as follows: immersing the glass in the frosting liquid for etching, so that the glass and the frosting liquid are fully immersed and reacted, and finally the desired frosting effect is obtained;

[0072] The specific polishing process is as follows: putting the frosted glass into the polishing liquid for liquid polishing, and adjusting the concentration and rate of the polishing liquid to achieve the purpose of polishing the glass surface;

[0073] The specific process of the secondary cleaning is: washing the frosted surface of the glass with 8% hydrochloric acid to remove the frosting liquid residue on the glass surface, and then washing the glass with clean water to remove dust, impurities and dirt on the glass surface;

[0074] The specific process of film peeling is as follows: using an automatic film peeling machine to remove the film on the non-frosted surface of the glass;

[0075] The specific process of the three cleanings is: using clean water to clean the frosted and film-removed glass to remove stains and impurities on the glass surface;

[0076] The specific inspection process is as follows: inspect the frosted glass to determine whether the product quality is qualified;

[0077] The specific process of finished product packaging is as follows: the glass that has been frosted and inspected and passed the test is the finished product and can be packaged.

[0078] It should be further explained in this embodiment that the film used for the film is made of PVC material.

[0079] In some examples, the frosting liquid is a mixture of hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, ammonium chloride and water, and the specific ratio of the frosting liquid is: 10% hydrofluoric acid, 10% sulfuric acid, 10% nitric acid, 10% oxalic acid, 20% ammonium chloride and 40% water by mass percentage.

[0080] It should be further explained in this embodiment that the polishing liquid is a mixture of hydrofluoric acid, ammonium bifluoride, organic acid and water, and the specific ratio of the polishing liquid is: 12% hydrofluoric acid, 12% ammonium bifluoride, 16% organic acid and 60% water by mass.

[0081] It should be further explained in this embodiment that the organic acid is one of carboxylic acid, sulfonic acid and sulfinic acid.

[0082] It should be further explained in this embodiment that the liquid temperature of the frosting liquid is controlled at 55° C., the liquid temperature of the polishing liquid is controlled at 45° C., and the polishing rate is controlled at 4000 r / min.

[0083] The product performance test table in the above embodiment is as follows:

[0084]

[0085]

[0086] The technical solution provided by the present invention increases the rate and uniformity of glass frosting, improves the anti-glare effect of the glass, and can make the glass surface smooth, thereby achieving the purpose of glass polishing, and also makes the bending resistance of the etched glass higher, and the components of the frosting liquid and the polishing liquid are easier to obtain, the cost is lower, and the economic benefit is better.

[0087] The present invention covers any substitution, modification, equivalent method and scheme made on the essence and scope of the present invention. In order to make the public have a thorough understanding of the present invention, specific details are described in detail in the following preferred embodiments of the present invention, but those skilled in the art can fully understand the present invention without the description of these details. In addition, in order to avoid unnecessary confusion about the essence of the present invention, well-known methods, processes, procedures, components and circuits are not described in detail.

[0088] A person skilled in the art will appreciate that all or part of the steps in the above-mentioned embodiment method can be completed by instructing related hardware through a program, and the program can be stored in a computer-readable storage medium, such as ROM / RAM, a disk, an optical disk, etc.

[0089] The above is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the principle of the present invention. These improvements and modifications should also be regarded as the scope of protection of the present invention.

Claims

1. A production process for high-efficiency anti-glare glass, characterized in that: The following steps are involved: Original film cutting → primary cleaning → film pasting → frosting → polishing → secondary cleaning → film tearing → tertiary cleaning → inspection → flat packing; The specific process of the original sheet cutting is: using a cutting machine to cut the glass original sheet into required specifications and sizes; The specific process of the first cleaning is: using clean water to clean the cut glass to remove dust, impurities and dirt on the surface of the glass; The specific process of film laminating is: using a film to laminating the non-frosted surface of the glass to protect the non-frosted surface from being affected by the frosting liquid and the frosting operation; The specific frosting process is as follows: immersing the glass in the frosting liquid for etching, so that the glass and the frosting liquid are fully immersed and reacted, and finally the desired frosting effect is obtained; The specific polishing process is as follows: putting the frosted glass into the polishing liquid for liquid polishing, and adjusting the concentration and rate of the polishing liquid to achieve the purpose of polishing the glass surface; The specific process of the secondary cleaning is: washing the frosted surface of the glass with 3% to 8% hydrochloric acid to remove the frosting liquid residue on the glass surface, and then washing the glass with clean water to remove dust, impurities and dirt on the glass surface; The specific process of film peeling is as follows: using an automatic film peeling machine to remove the film on the non-frosted surface of the glass; The specific process of the three cleanings is: using clean water to clean the frosted and film-removed glass to remove stains and impurities on the glass surface; The specific inspection process is as follows: inspect the frosted glass to determine whether the product quality is qualified; The specific process of finished product packaging is as follows: the glass that has been frosted and inspected and passed the test is the finished product and can be packaged.

2. The production process of a high-efficiency anti-glare glass according to claim 1, characterized in that: The film used for the film is made of PVC material.

3. The production process of a high-efficiency anti-glare glass according to claim 1, characterized in that: The frosting liquid is mixed with hydrofluoric acid, sulfuric acid, nitric acid, oxalic acid, ammonium chloride and water, and the specific proportions of the frosting liquid are: by mass percentage, 10% to 20% of hydrofluoric acid, 10% to 15% of sulfuric acid, 10% to 15% of nitric acid, 8% to 15% of oxalic acid, 10% to 25% of ammonium chloride and 40% to 60% of water.

4. The production process of a high-efficiency anti-glare glass according to claim 1, characterized in that The polishing liquid is a mixture of hydrofluoric acid, ammonium bifluoride, organic acid and water, and the specific proportions of the polishing liquid are: 8% to 15% hydrofluoric acid, 5% to 15% ammonium bifluoride, 5% to 20% organic acid, and 50% to 80% water by mass percentage.

5. The production process of a high-efficiency anti-glare glass according to claim 4, characterized in that: The organic acid is one of carboxylic acid, sulfonic acid and sulfinic acid.

6. The production process of a high-efficiency anti-glare glass according to claim 1, characterized in that: The liquid temperature of the frosting liquid is controlled at 45° C.-60° C., the liquid temperature of the polishing liquid is controlled at 30° C.-50° C., and the polishing rate is controlled at 2000 r / min-5000 r / min.

Citation Information

Patent Citations

  • Process for producing anti-glare glass by using high-boron silicon and high-aluminium silicon glasses

    CN102887647A

  • Etching process of glass for refrigerator

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  • Laminated and film-coated anti-reflection glass and preparation method thereof

    CN107129159A

  • Anti-glare glass and a preparation method thereof

    CN110903035A

  • Gradient anti-dazzle glass, and preparation method and application thereof

    CN113860752A