A method for treating Trichosanthes kirilowii Maxim. waste and its application in the preparation of Trichosanthes kirilowii Maxim. wine

Through the liquid-electric effect treatment in the hydraulic and electrical reaction tank, the crushing, disinfection, pickling and alkali washing processes of Trichosanthes waste are simplified, production efficiency is improved, and efficient utilization materials suitable for the brewing of Trichosanthes wine are obtained.

CN119680990BActive Publication Date: 2025-06-20ANHUI HUIYUEJI FOOD CO LTD
View PDF 2 Cites 0 Cited by

Patent Information

Application Number
CN202510033759.8
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-01-09
Publication Date
2025-06-20
Estimated Expiration
2045-01-09

AI Technical Summary

Technical Problem

In the prior art, the treatment process of Trichosanthes waste is complicated and the equipment is different, which seriously restricts the improvement of production efficiency.

Method used

The hydroelectric reaction tank is used for hydroelectric effect treatment, and the hydroelectric effect is generated through the pulse power supply. The Trichosanthes waste is crushed, disinfected, pickled and alkaline washing, and the treatment process is simplified.

Benefits of technology

The efficient treatment of Trichosanthes waste is achieved, and the production efficiency is significantly improved. The secondary utilization material of Trichosanthes waste obtained does not exceed 3mm, has a high porosity and a large specific surface area, which is suitable for the brewing of Trichosanthes wine.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN119680990B_ABST
    Figure CN119680990B_ABST
Patent Text Reader

Abstract

The present invention belongs to the field of solid waste treatment. Specifically, it relates to a method for treating Trichosanthes kirilowii Maxim. waste and its application in the preparation of Trichosanthes kirilowii Maxim. wine. In the present invention, Trichosanthes kirilowii Maxim. waste materials, ellipsoidal conductive stirrers and a first solvent are placed in a liquid-electric reaction tank. Under sealed conditions, through the liquid-electric effect, the Trichosanthes kirilowii Maxim. waste materials are broken into Trichosanthes kirilowii Maxim. waste secondary utilization materials with high porosity and large specific surface area, which can be used for the brewing of Trichosanthes kirilowii Maxim. wine / industrial alcohol, and the by-products will not affect wine brewing. The present invention can perform operations similar to "crushing", "disinfection", "pickling" and "alkaline washing" on Trichosanthes kirilowii Maxim. waste. The operation method is simple, greatly simplifies the production process, and has high production efficiency.
Need to check novelty before this filing date? Find Prior Art

Description

Technical Field

[0001] The present invention belongs to the technical field of solid waste treatment, and particularly relates to a method for treating Trichosanthes kirilowii Maxim waste and its application in the preparation of Trichosanthes kirilowii Maxim wine. Background Art

[0002] Trichosanthes kirilowii Maxim is also called medicinal melon, and its scientific name is Trichosanthes kirilowii Maxim. It is a treasure all over. The melon shell can be used as medicine. After the mature Trichosanthes kirilowii Maxim seeds are dried, they can be used as health care and leisure foods, and the roots of Trichosanthes kirilowii Maxim can be made into trichosanthin, with great utilization value and high economic benefits.

[0003] In the treatment of Trichosanthes kirilowii Maxim, whether for medicinal use or food use, a large amount of solid waste will be generated, such as waste materials and by-products such as Trichosanthes kirilowii Maxim roots, pulp, peel, and Trichosanthes kirilowii Maxim kernel meal, which are usually treated as waste. If these Trichosanthes kirilowii Maxim wastes are not comprehensively utilized, it will cause great waste.

[0004] In the secondary processing of Trichosanthes kirilowii Maxim waste, it can be fermented to produce industrial alcohol or Trichosanthes kirilowii Maxim wine. When studying the fermentation using Trichosanthes kirilowii Maxim waste as raw material, it is necessary to preliminarily process the Trichosanthes kirilowii Maxim waste, such as processes like crushing, disinfection, pickling, and alkali washing (reference can be made to the "A Process for Recycling and Treating Traditional Chinese Medicine Waste" disclosed in publication number CN115090646A). Especially for Trichosanthes kirilowii Maxim roots, although their starch content is relatively high, they also carry more pathogens. Pickling or alkali washing can ensure more thorough sterilization, and in addition, it can also loosen the root fibers, which is beneficial for subsequent fermentation.

[0005] However, the above processes such as crushing, disinfection, pickling, and alkali washing are complicated in steps, and the equipment used is also different, which severely restricts the improvement of production efficiency.

[0006] Therefore, it is necessary to invent a new method or equipment that can simultaneously perform processes such as crushing, disinfection, pickling, and alkali washing on Trichosanthes kirilowii Maxim waste, which is beneficial to improving production efficiency. Summary of the Invention

[0007] The purpose of the present invention is to provide a method for treating Trichosanthes kirilowii Maxim waste and its application in the preparation of Trichosanthes kirilowii Maxim wine to solve the above problems.

[0008] On the one hand, a method for treating Trichosanthes kirilowii Maxim waste includes the following steps:

[0009] Step 1: Remove impurities and wash the Trichosanthes kirilowii Maxim waste to obtain Trichosanthes kirilowii Maxim waste material;

[0010] Step 2: Pour the Trichosanthes kirilowii Maxim waste material, ellipsoidal conductive stirrers, and a first solvent into a liquid-electric reaction tank, and seal the liquid-electric reaction tank;

[0011] When the first electrode and the second electrode arranged in the liquid-electricity reaction tank are connected to the pulsed electricity, a liquid-electricity effect is generated, and the discarded trichosanthes kirilowii materials are broken into granular materials in the first solvent;

[0012] Step 3: Use a submersible sewage pump to discharge the granular materials and water in the liquid-electricity reaction tank from the liquid-electricity reaction tank, and drain them to obtain the secondary utilization materials of the discarded trichosanthes kirilowii.

[0013] For a further improvement, the liquid-electricity reaction tank includes an insulating tank body, a high-voltage pulse power supply, and an air pump. Inside the insulating tank body, a spherical segment-shaped first reaction area and a cylindrical second reaction area are sequentially arranged from top to bottom, and the first reaction area and the second reaction area are communicated; the high-voltage pulse power supply is respectively connected with a first electrode and a second electrode. The first electrode includes a first conductor embedded in the side wall of the second reaction area and a second conductor embedded in the bottom of the second reaction area. The second electrode includes a third conductor embedded in the side wall of the first reaction area; the volume of the first reaction area is smaller than the volume of the second reaction area.

[0014] For a further improvement, the liquid-electricity reaction tank further includes an air pump. A gate valve is installed below the insulating tank body. A discharge port is arranged at the bottom of the second reaction area. The discharge port includes an inverted cone-shaped upper hole section and a cylindrical lower hole section, and the upper hole section is communicated with the lower hole section. The lower hole section is communicated with the input end of the gate valve; a filter plate that completely covers the upper hole section is further arranged at the bottom of the second reaction area; an annular air injection pipe is further arranged inside the upper hole section. The air injection pipe is located below the filter plate and is connected with the air pump.

[0015] For a further improvement, the second conductor is sheet-shaped and multiple pieces are arranged. The first conductor is in the shape of a cylindrical spiral spring; the third conductor is in the shape of a circular ring and multiple pieces are arranged. The third conductors are arranged at equal intervals in the first reaction area.

[0016] For a further improvement, a cover for closing the first reaction area is arranged at the top of the insulating tank body. One end of the cover is hinged to the top of the insulating tank body, and a fastener connection is arranged between the other end of the cover and the top of the insulating tank body.

[0017] For a further improvement, the ratio of the volume of the second reaction area to the volume of the first reaction area is x, and 2.7 ≤ x ≤ 3.1.

[0018] For a further improvement, the mass of the discarded trichosanthes kirilowii materials in the insulating tank body is m2, and the mass of the conductive stirring bar is m1, and y = m1 / m2; 1.5 ≤ y ≤ 2;

[0019] The high-voltage pulse power supply outputs a voltage of 10 - 15 kV, the duration of each group of current is 5 s, and the pulse duty cycle is 33.3%.

[0020] For further improvement, the conductive stirrer is composed of a cast iron ellipsoid, a lead ellipsoid, and a chromium-plated iron ellipsoid with micropores on the surface, with a mass ratio of 2:2:1. The specific surface area of the cast iron ellipsoid with micropores on the surface is greater than 10 m 2 / g; the ratio of the major axis to the minor axis of the conductive stirrer is 3.2:1.

[0021] For further improvement, the first solvent is one or more of water and organic solvents.

[0022] On the other hand, the application of the Trichosanthes kirilowii waste treatment method in the preparation of Trichosanthes kirilowii wine. For example, the secondary utilization material of Trichosanthes kirilowii waste prepared by adopting the Trichosanthes kirilowii waste treatment method has a particle size not exceeding 3 mm (about the size of mung beans), and the secondary utilization material of Trichosanthes kirilowii waste can be classified according to needs, so as to be used as raw materials such as Daqu and Xiaoqu for brewing wine, and can also be used to replace part of the auxiliary materials or fillers for brewing wine (such as bran, grain husks, bagasse, etc.).

[0023] Compared with the prior art, the beneficial effects of the present invention are as follows:

[0024] 1. Through the liquid-electric effect carried out in the liquid-electric reaction tank of the present invention, operations such as "crushing", "disinfection", "acid washing" and "alkali washing" can be carried out on the Trichosanthes kirilowii waste. The operation method is simple, greatly simplifying the production process and having high production efficiency.

[0025] 2. The secondary utilization material of Trichosanthes kirilowii waste obtained through the liquid-electric effect has a particle size not exceeding 3 mm, a porosity of up to 89.3%, and a specific surface area of up to 705 m 2 / g; there is no carbonization phenomenon in the Trichosanthes kirilowii waste, there will be no large amount of foam during the reaction process, there is no oily substance in the product, the content of aldehyde substances in the solution of the product is less than 90 mg / 100 ml, the solution of the product does not contain ethanol and methanol, and is neutral; the secondary utilization material of Trichosanthes kirilowii waste has a high porosity and a large specific surface area, and the by-products will not affect the subsequent wine brewing. Whether the secondary utilization material of Trichosanthes kirilowii waste is used for making koji or directly replacing part of the brewing raw materials, it can be applied to the brewing of Trichosanthes kirilowii wine. Description of the Drawings

[0026] Figure 1 It is a schematic structural diagram of the liquid-electric reaction tank of the present invention;

[0027] Figure 2 It is a schematic diagram of the bottom of the insulating tank body;

[0028] In the drawings, the list of components represented by each reference numeral is as follows:

[0029] 10. Insulated tank body; 11. Second reaction zone; 12. First reaction zone; 13. Discharge port; 131. Upper hole section; 132. Lower hole section; 14. Gate valve; 15. Sealing cover; 16. Fastener; 17. Filter plate;

[0030] 21. Third conductor; 22. First conductor; 23. Second conductor;

[0031] 30. Jet pipe. Detailed implementation manner

[0032] The present invention will be further described in detail below through specific embodiments in conjunction with the drawings.

[0033] In the description of the present invention, it should be noted that unless otherwise specified, the meaning of "a plurality of" is two or more; the orientation or positional relationships indicated by the terms "upper", "lower", "left", "right", "inner", "outer", "front end", "rear end", "head", "tail", etc. are based on the orientation or positional relationships shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be construed as a limitation to the present invention. In addition, the terms "first", "second", "third", etc. are only used for descriptive purposes and cannot be construed as indicating or implying relative importance.

[0034] In the description of the present invention, it should be noted that unless otherwise clearly specified and defined, the terms "installation", "connection", and "connection" should be understood in a broad sense. For example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be directly connected or indirectly connected through an intermediate medium, and it can be the communication inside two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood according to specific situations.

[0035] Embodiment 1

[0036] A method for treating Trichosanthes kirilowii waste, comprising the following steps:

[0037] Step 1: Remove impurities and wash the Trichosanthes kirilowii waste to obtain Trichosanthes kirilowii waste material;

[0038] Step 2: Pour the Trichosanthes kirilowii waste material, ellipsoidal conductive stirrers, and a first solvent into a liquid-electric reaction tank, and seal the liquid-electric reaction tank;

[0039] When a first electrode and a second electrode arranged in the liquid-electric reaction tank are connected to a pulsed electric current, a liquid-electric effect is generated, and the Trichosanthes kirilowii waste material is broken into particulate materials in the first solvent;

[0040] Step 3: Use a submersible sewage pump to discharge the granular material and water in the liquid-electric reaction tank from the liquid-electric reaction tank, and drain it to obtain the secondary utilization material of Trichosanthes kirilowii Maxim waste.

[0041] In the present invention, the liquid-electric effect refers to:

[0042] When a pulsed high voltage is applied to a pair of electrodes placed in a liquid, the electrode gap is instantaneously broken down, generating a strong arc spark discharge, and a series of remarkable physical, chemical, biological, and mechanical effects occur. This process is called the liquid-electric effect.

[0043] Liquid-phase discharge is an instantaneous energy conversion process. High-density electrical energy is converted into high-intensity light energy, sound energy, electromagnetic energy, mechanical energy, and chemical energy in a very short time by means of the formation of a high-temperature and high-intensity plasma in the discharge channel in the liquid, causing drastic changes in the sound, light, electromagnetic, mechanical, and chemical states in the environment, and generating mechanical effects, chemical effects, electromagnetic radiation effects, supercritical liquid effects, biological effects, etc.

[0044] The mechanical effect, also known as the mechanical effect, generates a shock wave that propagates rapidly (supersonically) through the liquid phase and will exhibit an ultra-high-power mechanical action on the outside world, that is, a mechanical effect capable of cutting and crushing solid materials is generated.

[0045] Chemical effect. During liquid-phase discharge, due to the combined action of factors such as sound, light, heat, and shock waves, the chemical components in the liquid phase will undergo significant changes, changing the original chemical properties of the liquid phase and making the liquid have extremely high chemical activity.

[0046] Supercritical liquid effect. The high temperature and high pressure generated by liquid-phase discharge make the local liquid in the liquid phase in a supercritical state, resulting in a huge change in the properties of the liquid.

[0047] Biological effect generally refers to sterilization, microbial inactivation, etc.

[0048] Therefore, in the present invention, through the liquid-electric effect carried out in the liquid-electric reaction tank, operations similar to "crushing", "disinfection", "acid washing", and "alkali washing" can be performed on the Trichosanthes kirilowii Maxim waste. The operation method is particularly simple, greatly simplifying the production process and significantly improving the production efficiency.

[0049] Example 2

[0050] As Figures 1-2As shown in the figure, the liquid-electric reaction tank includes an insulating tank body 10, a high-voltage pulse power supply, and an air pump. The insulating tank body 10 is preferably made of cast concrete. Inside the insulating tank body 10, a spherical segment-shaped first reaction zone 12 and a cylindrical second reaction zone 11 are sequentially arranged from top to bottom. The first reaction zone 12 and the second reaction zone 11 are connected; the high-voltage pulse power supply is respectively connected to a first electrode and a second electrode. The first electrode includes a first conductor 22 embedded in the side wall of the second reaction zone 11 and a second conductor 23 embedded in the bottom of the second reaction zone 11. The second electrode includes a third conductor 21 embedded in the side wall of the first reaction zone 12; the volume of the first reaction zone 12 is smaller than the volume of the second reaction zone 11.

[0051] Among them, the second conductor 23 is sheet-shaped and multiple pieces are provided. The first conductor 22 is in the shape of a cylindrical spiral spring; the third conductor 21 is in the shape of a circular ring and multiple roots are provided. The third conductors 21 are arranged at equal intervals in the first reaction zone 12.

[0052] The ratio of the volume of the second reaction zone 11 to the volume of the first reaction zone 12 is x, and 2.7 ≤ x ≤ 3.1.

[0053] The mass of the Trichosanthes kirilowii Maxim waste in the insulating tank body 10 is m2, and the mass of the conductive stirring bar is m1. y = m1 / m2; 1.5 ≤ y ≤ 2;

[0054] The high-voltage pulse power supply has an output voltage of 10 - 15 kV, the duration of each group of current is 5 s, and the pulse duty cycle is 33.3%.

[0055] The conductive stirring bar is composed of a cast iron ellipsoid with micropores on the surface, a lead ellipsoid, and a chromium-plated iron ellipsoid in a mass ratio of 2:2:1. The specific surface area of the cast iron ellipsoid with micropores on the surface is greater than 10 m 2 / g; the ratio of the major axis to the minor axis of the conductive stirring bar is 3.2:1. Among them, the cast iron ellipsoid with micropores on the surface can be made by acid corrosion.

[0056] In this embodiment, the first solvent is preferably water.

[0057] In the present invention, the role of the conductive stirring bar is to form a series of conductive channels between the first electrode and the second electrode, so as to better promote the occurrence of the liquid-electric effect, enabling the Trichosanthes kirilowii Maxim waste to be broken better and more evenly.

[0058] It is well-known in the art that in the field of brewing, raw materials must have a certain porosity. Especially for making starter cultures, such as the manual stepping process, it is beneficial to microbial fermentation. Manual stepping can better control the tightness of the starter culture blocks, thereby affecting the air permeability and fermentation effect. Manual stepping can produce starter culture blocks with a "turtle-back shape", that is, the four sides are tight and the middle is loose. This shape is beneficial to microbial fermentation, increases the fermentation space, and also helps to retain water in the starter culture blocks.

[0059] From this, it can be seen that if the brewing raw materials can have a large enough porosity / specific surface area, whether it is used for making starter cultures or directly replacing part of the brewing raw materials, it is beneficial to fermentation. Therefore, the core of the present invention, on the one hand, needs to ensure that the Trichosanthes kirilowii Maxim waste is broken to the specified particle size within a short time, and on the other hand, it also needs to ensure that the secondary utilization material of the Trichosanthes kirilowii Maxim waste obtained after crushing has a sufficient porosity / specific surface area.

[0060] In this embodiment, the fermentation process of Trichosanthes kirilowii Maxim wine follows the existing fermentation process of GB / T 19328-2007 Geographical Indication Products - Kouzijiao Liquor. The brewing raw materials mainly include sorghum, wheat, barley, peas, rice, and glutinous rice, etc. In the present invention, to ensure the taste, the secondary utilization material of Trichosanthes kirilowii Maxim waste is used to replace 20% of the brewing raw materials. If it is for fermenting industrial alcohol, all the brewing raw materials are the secondary utilization material of Trichosanthes kirilowii Maxim waste.

[0061] In this embodiment, the volume of the second reaction zone 11 is 18L, the volume of the first reaction zone 12 is 6L, and x = 3. The Trichosanthes kirilowii Maxim waste is 5kg, the conductive stirrer is 8kg, and y = 1.6; the first solvent fills the first reaction zone 12.

[0062] React in the liquid-electricity reaction tank for 6 minutes. The finally obtained secondary utilization material of Trichosanthes kirilowii Maxim waste has a particle size not exceeding 3mm, a porosity of up to 89.3%, and a specific surface area of up to 705m 2 / g; there is no carbonization phenomenon in the Trichosanthes kirilowii Maxim waste, there will be no large amount of foam during the reaction process, there is no oily substance in the product, the content of aldehyde substances in the solution of the product is less than 90mg / 100ml, the solution of the product does not contain ethanol and methanol, and is neutral.

[0063] Because the first conductor 22 is in the shape of a cylindrical spiral spring, the arc trend around it is spiral upward. Combining the shape of the second reaction zone 11 being cylindrical and the shape and position of the second conductor 23, the ultimate goal is to generate an upward shock wave in the second reaction zone 11, so as to better break the Trichosanthes kirilowii Maxim waste.

[0064] If the volume of the first reaction zone 12 is larger than the volume of the second reaction zone 11, it will lead to uneven crushing. After reacting in the liquid-electricity reaction tank for 10 minutes, there will still be a part of the residual material with a particle size larger than 5mm, and the mass of the residual material accounts for about 12% of the Trichosanthes kirilowii Maxim waste.

[0065] If the first reaction zone 12 and the second reaction zone 11 are both cylindrical structures with the same diameter, or the first reaction zone 12 is a single-leaf hyperbolic structure, these are not conducive to increasing the residence time in the first reaction zone 12; moreover, if the first reaction zone 12 is a single-leaf hyperbolic structure, it will also cause the local arc to be too strong, thereby causing the content of miscellaneous alcohols in the product in the liquid-electric reactor to be too high, exceeding 1770 mg / 100 ml.

[0066] The conductive stirrer must be a combination of three conductive materials of different materials, and the difference in conductivity between the three materials cannot be too large. This is conducive to forming a certain potential difference between the three conductive stirrers of different materials, which is beneficial to the crushing and decomposition of Trichosanthes waste.

[0067] If the conductive stirring bar is a polyhedral structure (such as a cylinder, a cube, an octahedron, etc.), it will cause a portion of the Trichosanthes waste to be carbonized. These carbonized Trichosanthes wastes are difficult to separate and are not conducive to subsequent winemaking.

[0068] If the conductive stirring bar is spherical, its stirring efficiency is not as good as that of the ellipsoidal conductive stirring bar, and it needs to react in the liquid-electric reaction tank for at least 17 minutes, and the particle size of the obtained Trichosanthes waste secondary utilization material does not exceed 3 mm.

[0069] The effects of different compositions of conductive stirrers on the products in the liquid-electric reactor were tested and the results are shown in Table 1:

[0070] Table 1

[0071]

[0072] As shown in Table 1, the conductive stirrer is made of different materials and has different conductive properties, which will eventually affect the porosity, specific surface area and whether other impurities will appear in the product. The presence of oily substances and a large amount of aldehydes in the product will pollute the recycled material of Trichosanthes waste and affect the subsequent brewing of Trichosanthes wine.

[0073] In addition, the study found that the ratio of the major axis to the minor axis of the conductive stirrer also significantly affects the product. The specific results are shown in Table 2:

[0074] Table 2

[0075]

[0076] Therefore, for brewing Trichosanthes wine, the ratio of the major axis to the minor axis of the conductive stirring bar is preferably 3.2:1.

[0077] Example 3

[0078] In Example 2, for the convenience of discharging materials, the liquid-electric reaction tank further includes an air pump. A gate valve 14 is installed below the insulating tank body 10. A discharge port 13 is provided at the bottom of the second reaction zone 11. The discharge port 13 includes an inverted conical upper hole section 131 and a cylindrical lower hole section 132. The upper hole section 131 is communicated with the lower hole section 132, and the lower hole section 132 is communicated with the input end of the gate valve 14. A filter plate 17 that completely covers the upper hole section 131 is further provided at the bottom of the second reaction zone 11. An annular air injection pipe 30 is further provided inside the upper hole section 131. The air injection pipe 30 is located below the filter plate 17, and the air injection pipe 30 is connected to the air pump.

[0079] Compressed air is intermittently introduced into the air injection pipe 30 through the air pump, so as to apply a pulsed impact force to the area near the discharge port 13 to assist in discharging materials. The filter plate 17 is used to block the conductive stirrers, and water and granular materials can pass through the filter holes on the surface of the filter plate 17 and then be discharged through the discharge port 13. Among them, the structure of the upper hole section 131, in cooperation with the compressed air ejected by the air injection pipe 30, can discharge materials more effectively and effectively prevent material blockage.

[0080] Example 4

[0081] In Example 2, for the convenience of sealing the insulating tank body 10, a cover 15 for closing the first reaction zone 12 is provided at the top of the insulating tank body 10. One end of the cover 15 is hinged to the top of the insulating tank body 10, and a fastener 16 is provided between the other end of the cover 15 and the top of the insulating tank body 10 for connection.

[0082] Among them, there are many types of fasteners 16, as long as the effect of fastening the cover 15 is satisfied. Its structure can be as follows:

[0083] The fastener 16 includes a convex plate and an L-shaped plug inserted in the top of the insulating tank body 10. A through hole for the convex plate to enter and exit is provided at the end of the cover 15, and a jack matching the L-shaped plug is provided on the convex plate.

[0084] After the cover 15 is covered, the convex plate protrudes from the through hole, and then the L-shaped plug is inserted into the jack. As for sealing, it can be considered to use a sealing ring for sealing.

[0085] The above are only the preferred embodiments of the present invention and are not used to limit the present invention. For those skilled in the art, the present invention can have various changes and modifications. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

Claims

1. A method for treating Trichosanthes waste, characterized in that: The following steps are involved: Step 1, removing impurities and cleaning the Trichosanthes waste to obtain Trichosanthes waste material; Step 2, pouring the Trichosanthes waste material, the ellipsoidal conductive stirring bar and the first solvent into the liquid-electric reaction tank, and sealing the liquid-electric reaction tank; When the first electrode and the second electrode arranged in the liquid-electric reaction tank are connected to pulse electricity, a liquid-electric effect is generated, and the waste material of Trichosanthes kirilowii is broken into granular material in the first solvent; Step 3: using a submersible sewage pump to discharge the granular material and water in the liquid-electric reaction tank from the liquid-electric reaction tank, draining, and obtaining the secondary utilization material of the Trichosanthes waste; The liquid-electric reaction tank includes an insulating tank body, a high-voltage pulse power supply, and an air pump. A spherical first reaction zone and a cylindrical second reaction zone are arranged in sequence from top to bottom inside the insulating tank body, and the first reaction zone and the second reaction zone are connected; the high-voltage pulse power supply is respectively connected to a first electrode and a second electrode, the first electrode includes a first conductor embedded in the side wall of the second reaction zone and a second conductor embedded in the bottom of the second reaction zone, and the second electrode includes a third conductor embedded in the side wall of the first reaction zone; the volume of the first reaction zone is smaller than that of the second reaction zone.

2. A method for treating Trichosanthes waste according to claim 1, characterized in that: The liquid-electric reaction tank also includes an air pump, a gate valve is installed below the insulating tank body, a discharge port is arranged at the bottom of the second reaction zone, the discharge port includes an inverted cone-shaped upper hole section and a cylindrical lower hole section, the upper hole section is connected with the lower hole section, and the lower hole section is connected with the input end of the gate valve; a filter plate that completely covers the upper hole section is also arranged at the bottom of the second reaction zone; a circular injection pipe is also arranged inside the upper hole section, the injection pipe is located below the filter plate, and the injection pipe is connected to the air pump.

3. A method for treating Trichosanthes waste according to claim 1, characterized in that: The second conductor is in sheet form and is provided in multiple pieces, the first conductor is in a cylindrical helical spring structure; the third conductor is in a circular ring structure and is provided in multiple pieces, and the third conductor is arranged at equal intervals in the first reaction zone.

4. A method for treating Trichosanthes waste according to claim 1, characterized in that: A cover for sealing the first reaction zone is arranged on the top of the insulating tank body, one end of the cover is hinged to the top of the insulating tank body, and a fastener is arranged between the other end of the cover and the top of the insulating tank body.

5. A method for treating Trichosanthes waste according to claim 3, characterized in that: The ratio of the volume of the second reaction zone to the volume of the first reaction zone is x, 2.7≤x≤3.

1.

6. A method for treating Trichosanthes waste according to claim 5, characterized in that: The mass of the waste Trichosanthes kirilowii in the insulating tank is m2, the mass of the conductive stirring bar is m1, y=m1 / m2; 1.5≤y≤2; The high-voltage pulse power supply has an output voltage of 10-15 kV, a duration of each current group of 5 seconds, and a pulse duty ratio of 33.3%.

7. A method for treating Trichosanthes waste according to claim 6, characterized in that: The conductive stirring bar is composed of a cast iron ellipsoid with micropores on the surface, a lead ellipsoid and a chrome-plated iron ellipsoid in a mass ratio of 2:2:

1. The specific surface area of ​​the cast iron ellipsoid with micropores on the surface is greater than 10m 2 / g; the ratio of the major axis to the minor axis of the conductive stirring bar is 3.2:

1.

8. A method for treating Trichosanthes waste according to claim 1, characterized in that: The first solvent is one or more of water and an organic solvent.

9. Use of a method for treating Trichosanthes waste according to any one of claims 1 to 8 in preparing Trichosanthes wine.

Citation Information

Patent Citations

  • Recycling treatment process for traditional Chinese medicine waste

    CN115090646A

  • Procyanidine auxiliary extracting device based on electrohydraulic pulse method

    CN108654537A