Tooth-strengthening mouthwash and preparation method thereof

Abstract

The invention provides a tooth-strengthening mouthwash and a preparation method thereof, and belongs to the technical field of oral care products, the mode of combining traditional Chinese medicine extracts and Chinese herbal medicines is adopted, the principle of monarch, minister, assistant and guide is fully applied, and the characteristics of good permeability and quick effect of modern essential oil are combined, so that the prepared mouthwash has the effects of effectively relieving gomphiasis and strengthening teeth. The teeth are stabilized; and inflammation and pain of the teeth and gingiva are relieved.

Description

Technical Field

[0001] The invention relates to the technical field of oral care products, and in particular to a teeth-strengthening mouthwash and a preparation method thereof. Background Art

[0002] With the continuous improvement of living standards in today's society, people's eating habits are gradually changing. Coupled with bad living habits, many oral problems have emerged, such as periodontitis, caries, bad breath, oral ulcers, etc. As an oral hygiene product, mouthwash has the effect of inhibiting bacteria and sterilizing and preventing caries, gingivitis and bad breath caused by microorganisms. It helps to clear mucus and food residues in the throat, keep the mouth and teeth clean, promote fresh breath, care for gums, maintain a good oral microenvironment, etc. Although mouthwash is easy to use, most of the ingredients of mouthwash sold on the market are made of industrial chemicals. Long-term use is prone to oral problems, easy to stain the surface of teeth and oral mucosa, reduce the taste of taste buds, and inhibit the secretion of saliva, causing dry mouth, burning pain and other discomfort symptoms.

[0003] At the same time, among the traditional Chinese medicine mouthwashes on the market, some have a relatively single type of traditional Chinese medicine and a relatively single function, and fail to bring into play the synergistic effect of the mutual compatibility of traditional Chinese medicinal materials; another part is that the antibacterial active ingredients used in these mouthwashes are not highly targeted and have broad-spectrum antibacterial properties, which further leads to a decrease in oral immunity and a reduction in the self-healing ability of various tissues to damage.

[0004] Moreover, since plant essential oils are of natural origin, have good permeability, have a certain impact on plaque biofilms, and have good antibacterial properties, the use of plant essential oils is a new direction in the research of mouthwashes. However, the plant essential oil mouthwashes currently studied mostly use a high alcohol system, which will aggravate the destructiveness to the oral mucosa and is not conducive to wound healing in patients with oral ulcers.

[0005] In summary, how to improve gums and stabilize teeth by combining Chinese herbal extracts and essential oil extracts has become a research hotspot and a technical problem that needs to be solved urgently. Summary of the invention

[0006] In view of this, in order to overcome the above-mentioned shortcomings and deficiencies in the prior art, the present invention provides a tooth-strengthening mouthwash and a preparation method thereof, which combines Chinese herbal medicine extracts and Chinese herbal medicines, fully applies the principle of monarch, minister, assistant and envoy, and combines the characteristics of good penetration and fast effect of modern essential oils, so that the prepared mouthwash has the effects of effectively alleviating loose teeth, stabilizing teeth and alleviating teeth and gingival inflammation and pain.

[0007] In order to achieve the above object, the present invention provides the following technical solutions:

[0008] The invention provides a tooth-strengthening mouthwash, comprising the following components: 4%-6% of sorbitol, 75.50%-76.05% of water, 0.30%-0.35% of preservative, 0.01%-0.02% of menthol, 0.3%-0.5% of citric acid, 0.004%-0.006% of hydrogenated castor oil, 8%-12% of active component A, 1.4%-2.2% of active component B, 0.4%-0.6% of cyperus rotundus root extract, and 6%-8% of isocyanate;

[0009] The active component A comprises xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water;

[0010] The active component B comprises bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil.

[0011] Preferably, the weight ratio of xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water is 0.5:3:0.6:4.4:0.2:5.

[0012] Preferably, the weight ratio of bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil is 0.1:0.5:0.5:0.5.

[0013] Preferably, the teeth-strengthening mouthwash of the present invention comprises the following components, by weight: 5% sorbitol, 76.03% water, 0.35% preservative, 0.02% menthol, 0.5% citric acid, 0.006% hydrogenated castor oil, 10% active ingredient A, 1.6% active ingredient B, 0.5% Cyperus rotundus root extract, and 5% isocyanate.

[0014] Preferably, the preservatives include sodium benzoate and potassium sorbate.

[0015] Preferably, the mass ratio of bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil is 1:5:5:5.

[0016] The present invention also provides a method for preparing the above-mentioned teeth-strengthening mouthwash, comprising the following preparation steps:

[0017] 1) firstly mixing sorbitol, citric acid and water, and heating to 90-95° C. to obtain a mixed phase A; then mixing the active component A, cyperus rotundus root extract, isocyanate, menthol and a preservative to obtain a mixed phase B; and finally mixing the active component B and hydrogenated castor oil to obtain a mixed phase C;

[0018] 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

[0019] Compared with the prior art, the teeth-strengthening mouthwash provided by the present invention has the following beneficial effects:

[0020] The present invention combines Chinese herbal extracts and Chinese herbal medicines, fully applies the principle of monarch, minister, assistant and envoy, and combines the characteristics of good penetration and rapid effect of modern essential oils, so that the prepared mouthwash has the effects of effectively alleviating loose teeth, stabilizing teeth and alleviating teeth and gingival inflammation and pain.

[0021] The teeth-strengthening and gum-protecting mouthwash provided by the present invention achieves the effects of anti-inflammation and swelling reduction, blood circulation and blood stasis removal, analgesia and anti-inflammation, and inhibition of dry and itchy throat by combining the Centella asiatica extract and the Tremella fuciformis extract and the combination of the two with the Myrrh essential oil extract. By combining the added Cyperus rotundus root extract, Isatis salt and eucalyptus essential oil, the prepared mouthwash has the effects of sterilization and anti-inflammation, qi-promoting and analgesia, and prevention and treatment of gingival bleeding.

[0022] The mouthwash provided by the present invention has ideal bactericidal and anti-inflammatory effects, has a significant improvement effect on oral inflammation, can make breath fresh, and effectively cover up bad breath, and has good development prospects. DETAILED DESCRIPTION

[0023] The invention provides a tooth-strengthening mouthwash, which comprises the following components by weight: 4%-6% of sorbitol, 75.50%-76.05% of water, 0.30%-0.35% of preservative, 0.01%-0.02% of menthol, 0.3%-0.5% of citric acid, 0.004%-0.006% of hydrogenated castor oil, 8%-12% of active component A, 1.4%-2.2% of active component B, 0.4%-0.6% of cyperus rotundus root extract, and 6%-8% of isocyanate.

[0024] The active component A comprises xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water; the active component B comprises bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil.

[0025] In the present invention, the weight ratio of xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water is preferably 0.5:3:0.6:4.4:0.2:5; the weight ratio of bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil is preferably 0.1:0.5:0.5:0.5.

[0026] In the present invention, the dosage of each component in the mouthwash, by weight, is preferably 5%-sorbitol, 76.03% water, 0.35% preservative, 0.02% menthol, 0.5% citric acid, 0.006% hydrogenated castor oil, 10% active component A, 1.6% active component B, 0.5% Cyperus rotundus root extract, and 5% isocyanate.

[0027] The teeth-strengthening and gum-protecting mouthwash provided by the present invention achieves the effects of anti-inflammation and swelling reduction, blood circulation and blood stasis removal, analgesia and anti-inflammation, and inhibition of dry and itchy throat by combining the Centella asiatica extract and the Tremella fuciformis extract and the combination of the two with the Myrrh essential oil extract. By combining the added Cyperus rotundus root extract, Isatis salt and eucalyptus essential oil, the prepared mouthwash has the effects of sterilization and anti-inflammation, qi-promoting and analgesia, and prevention and treatment of gingival bleeding.

[0028] In the present invention, the preservatives are preferably sodium benzoate and potassium sorbate; the mass ratio of the bisabolol, eucalyptus oil, clove leaf oil and orange fruit oil is preferably 1:5:5:5.

[0029] The mouthwash provided by the present invention has ideal bactericidal and anti-inflammatory effects, has a significant improvement effect on oral inflammation, can make breath fresh, and effectively cover up bad breath, and has good development prospects.

[0030] The preparation method of the tooth-strengthening mouthwash of the present invention comprises the following preparation steps:

[0031] 1) First, sorbitol, citric acid and water are mixed and heated to 90-95° C. to obtain a mixed phase A; then, active component A, cyperus rotundus root extract, isocyanate, menthol and preservative are mixed to obtain a mixed phase B; finally, active component B and hydrogenated castor oil are mixed to obtain a mixed phase C

[0032] 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

[0033] In the present invention, the sterilization step of phase A is preferably: heating phase A to 90-95°C and stirring to mix, keeping warm for 30 minutes, and then cooling to 45°C; the mass ratio of phase A, phase B and phase C is preferably 41:53:1.3.

[0034] The present invention combines Chinese herbal extracts and Chinese herbal medicines, fully applies the principle of monarch, minister, assistant and envoy, and combines the characteristics of good penetration and rapid effect of modern essential oils, so that the prepared mouthwash has the effects of effectively alleviating loose teeth, stabilizing teeth and alleviating teeth and gingival inflammation and pain.

[0035] In order to better understand the present invention, the content of the present invention is further explained below in conjunction with the embodiments, but the content of the present invention is not limited to the following embodiments.

[0036] Example 1

[0037] The tooth-strengthening mouthwash in this embodiment includes the following components by weight: 5%-sorbitol, 76.03% water, 0.35% preservative, 0.02% menthol, 0.5% citric acid, 0.006% hydrogenated castor oil, 10% active component A, 1.6% active component B, 0.5% Cyperus rotundus root extract, and 5% cerium salt;

[0038] The active component A comprises 0.5% xylitol, 3% dehydrated xylitol, 0.6% Centella asiatica extract, 4.4% Tremella fuciformis extract, 0.2% 1,2-hexanediol and 1.3% water;

[0039] The active component B comprises 0.1% of bisabolol, 0.5% of eucalyptus globulus oil, 0.5% of clove leaf oil and 0.5% of orange fruit oil.

[0040] The preparation method of the teeth strengthening mouthwash in this embodiment comprises the following preparation steps:

[0041] 1) firstly mixing sorbitol, citric acid and water, and heating to 90-95° C. to obtain a mixed phase A; then mixing the active component A, cyperus rotundus root extract, isocyanate, menthol and a preservative to obtain a mixed phase B; and finally mixing the active component B and hydrogenated castor oil to obtain a mixed phase C;

[0042] 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

[0043] Example 2

[0044] The tooth-strengthening mouthwash in this embodiment includes the following components by weight: 5% sorbitol, 75.55% water, 0.32% preservative, 0.01% menthol, 0.4% citric acid, 0.005% hydrogenated castor oil, 12% active component A, 2.1% active component B, 0.5% cyperus root extract, and 5% daqing salt;

[0045] The active component A comprises xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water;

[0046] The active component B comprises bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil.

[0047] The preparation method of the teeth strengthening mouthwash in this embodiment comprises the following preparation steps:

[0048] 1) firstly mixing sorbitol, citric acid and water, and heating to 90-95° C. to obtain a mixed phase A; then mixing the active component A, cyperus rotundus root extract, isocyanate, menthol and a preservative to obtain a mixed phase B; and finally mixing the active component B and hydrogenated castor oil to obtain a mixed phase C;

[0049] 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

[0050] Example 3

[0051] The tooth-strengthening mouthwash in this embodiment includes the following components by weight: 5% sorbitol, 75.85% water, 0.34% preservative, 0.02% menthol, 0.3% citric acid, 0.006% hydrogenated castor oil, 11% active component A, 1.5% active component B, 0.4% Cyperus rotundus root extract, and 8% ceramide salt;

[0052] The active component A comprises xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water;

[0053] The active component B comprises bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil.

[0054] The preparation method of the teeth strengthening mouthwash in this embodiment comprises the following preparation steps:

[0055] 1) firstly mixing sorbitol, citric acid and water, and heating to 90-95° C. to obtain a mixed phase A; then mixing the active component A, cyperus rotundus root extract, isocyanate, menthol and a preservative to obtain a mixed phase B; and finally mixing the active component B and hydrogenated castor oil to obtain a mixed phase C;

[0056] 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

[0057] Performance Testing

[0058] The present invention tested the tooth strengthening effect of the mouthwash prepared in Example 1 by 100 volunteer subjects suffering from symptoms such as bleeding gums, gingivitis, loose teeth, etc. The test time was 3 months, the mouthwash was used 6 times a day, each time for two minutes, and one month was a course of treatment. The progress of the disease in the volunteer subjects was observed and recorded every day. The specific statistical data are shown in Table 1.

[0059] Table 1

[0060] category Case Significant effect efficient invalid Total effective rate / % Bleeding gums 61 40 16 5 91.8 Gingivitis 55 38 13 4 92.7 Loose teeth 90 60 25 5 94.4

[0061] It can be seen from the data in Table 1 that the mouthwash prepared by Examples 1-3 of the present invention has an improving effect on symptoms such as bleeding gums and loose teeth, especially on loose teeth. In other words, the mouthwash prepared by the present invention significantly achieves the effect of alleviating loose teeth, stabilizing teeth and alleviating teeth and gingival inflammation pain.

[0062] In summary, the gum-protecting and tooth-solidifying mouthwash provided by the present invention combines Chinese medicine extracts and Chinese herbal medicines, fully applies the principle of monarch, minister, assistant and envoy, and combines the characteristics of good penetration and fast effect of modern essential oils, so that the prepared mouthwash has the effect of effectively alleviating loose teeth, stabilizing teeth and alleviating teeth and gingival inflammation and pain. At the same time, the mouthwash prepared by the present invention has an ideal bactericidal and anti-inflammatory effect, has a significant improvement effect on oral inflammation, can make the breath fresh, and effectively cover up bad breath, and has a good development prospect.

[0063] The above is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the principle of the present invention. These improvements and modifications should also be regarded as the scope of protection of the present invention.

Claims

1. A tooth-strengthening mouthwash, characterized in that: The invention comprises the following components by weight: sorbitol 4%-6%, water 75.50%-76.05%, preservative 0.30%-0.35%, menthol 0.01%-0.02%, citric acid 0.3%-0.5%, hydrogenated castor oil 0.004%-0.006%, active component A 8%-12%, active component B 1.4%-2.2%, cyperus rotundus root extract 0.4%-0.6%, and isocyanate 6%-8%; The active component A comprises xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water; The active component B comprises bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil.

2. The teeth strengthening mouthwash according to claim 1, characterized in that: The weight ratio of the xylitol, dehydrated xylitol, Centella asiatica extract, Tremella fuciformis extract, 1,2-hexanediol and water is 0.5:3:0.6:4.4:0.2:

5.

3. The teeth strengthening mouthwash according to claim 1, characterized in that: The weight ratio of the bisabolol, eucalyptus globulus oil, clove leaf oil and orange fruit oil is 0.1:0.5:0.5:0.

5.

4. The teeth strengthening mouthwash according to claim 1, characterized in that: The invention comprises the following components by weight: 5% sorbitol, 76.03% water, 0.35% preservative, 0.02% menthol, 0.5% citric acid, 0.006% hydrogenated castor oil, 10% active component A, 1.6% active component B, 0.5% cyperus rotundus root extract and 5% isocyanate.

5. The teeth strengthening mouthwash according to claim 1, characterized in that: Such preservatives include sodium benzoate and potassium sorbate.

6. The teeth strengthening mouthwash according to claim 5, characterized in that: The mass ratio of the sodium benzoate to potassium sorbate is 1:

1.

7. The method for preparing the teeth strengthening mouthwash according to claim 1, characterized in that: The method comprises the following preparation steps: 1) firstly mixing sorbitol, citric acid and water, and heating to 90-95° C. to obtain a mixed phase A; then mixing the active component A, cyperus rotundus root extract, isocyanate, menthol and a preservative to obtain a mixed phase B; and finally mixing the active component B and hydrogenated castor oil to obtain a mixed phase C; 2) After sterilizing phase A, the phase A is mixed with phase B and phase C in sequence, and then filtered to obtain the tooth-strengthening mouthwash.

8. The preparation method according to claim 7, characterized in that: The sterilization step of phase A is as follows: heating phase A to 90-95° C. and stirring to mix well, keeping the temperature for 30 minutes, and then cooling to 45° C.