Energy spectrometer for automatic analysis and detection of biological material samples
By designing the injection mechanism in the energy spectrometer, evacuating oxygen with nitrogen and automatically opening the sealed tube, the problem of oxidation of biomaterial samples is solved and the detection accuracy and adaptability are improved.
Patent Information
- Application Number
- CN202411849856.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-16
- Publication Date
- 2025-08-12
- Estimated Expiration
- 2044-12-16
AI Technical Summary
Biomaterial samples cannot effectively isolate oxygen in the air before entering the energy spectrometer analysis chamber, resulting in an oxidation reaction affecting the accuracy of detection.
An energy spectrometer for automatic analysis and detection of biological material samples was designed, including a sample injection mechanism, which uses telescopic components, sealed tubes, drive modules and rotary frames to evacuate oxygen by venting nitrogen between the sealed tubes and the arc-shaped shell, and automatically open the sealed tube after the sample enters the analysis chamber to prevent oxidation reactions.
Effectively prevent oxidation of biomaterial samples, improve the accuracy of detection results, and can adapt to uneven surfaces or irregular shapes of samples, adjust the detection distance to ensure comprehensive inspection.
Smart Images

Figure CN119757439B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of energy spectrometers, and in particular to an energy spectrometer for automatic analysis and detection of biological material samples. Background Art
[0002] Photoelectron spectroscopy (PES) is an analytical tool widely used in materials science, surface science, and chemistry to study the electronic structure, chemical state, and surface properties of sample materials.
[0003] Patent No. CN118425212A discloses a sample protection device, including a sample base, a first groove is provided on the top of the sample base, and the first groove is sealed when the sealing cover is buckled on the sample base. A clamping rod is arranged on the sample base, and the clamping rod abuts against the upper side of the sealing cover. A negative pressure driving mechanism is arranged on the sample base to drive the clamping rod to move away from the upper side of the sealing cover. A torsion spring is connected between the hinged end of the sealing cover and the sample base, so that the sample can be isolated from the external air during the transfer to the sampling chamber of the X-ray photoelectron spectrometer, thereby preventing the sample from being oxidized during the transfer process and affecting the accuracy of the detection and analysis. The negative pressure driving mechanism is then used to drive the clamping rod to move away from the sealing cover, and the torsion spring drives the sealing cover to flip open, so that the sample is exposed to the sampling chamber for convenient detection and analysis, thereby ensuring the accuracy of the X-ray photoelectron spectrometer in detecting and analyzing the material.
[0004] When the detection object of the above technical solution is a biological material sample, there are still the following defects: biological material samples include cell samples, tissue samples, blood samples, body fluid samples and microbial samples. Since the biological sample cannot be effectively isolated from the oxygen in the air before entering the analysis chamber, the biological sample is very likely to undergo oxidation reaction, thereby affecting the accuracy of the spectrometer's detection and analysis of the material. Summary of the Invention
[0005] The purpose of the present invention is to provide an energy spectrometer for automatic analysis and detection of biological material samples, aiming to solve the problems existing in the use of existing photoelectron spectrometers.
[0006] To achieve the above objectives, the present invention provides the following technical solution: an energy spectrometer for automatic analysis and detection of biological material samples, comprising a metal shielding shell, an analysis chamber, an energy analyzer, an ion pump, an ion gauge, a molecular pump, a control display, and an injection port, wherein the analysis chamber is provided within the metal shielding shell, the energy analyzer, ion pump, ion gauge, and molecular pump are all fixedly connected within the metal shielding shell, the injection port and the control display are provided on the surface of the metal shielding shell, the analysis chamber is connected to the injection port, and further comprising:
[0007] The sampling mechanism includes a telescopic assembly, a sealing tube, a drive module, a rotating frame and a sample placement portion. The telescopic assembly includes an arc-shaped shell, a first helical gear, a fixed cover and a first electric telescopic rod. The first electric telescopic rod is fixedly connected between the metal shielding shell and the arc-shaped shell. The fixed cover is fixedly connected to one end of the arc-shaped shell. The first helical gear is connected to the fixed cover. The arc-shaped shell is in sliding contact with the inner wall of the injection port. The sealing tube is movably sleeved in the arc-shaped shell. A take-and-place port is provided on the surface of the sealing tube. A second helical gear is provided at the end of the sealing tube. One side of the first helical gear is transmission-connected to the second helical gear.
[0008] The driving module includes a driving part, a second central tube, a third bevel gear, a first key bar, a second key bar, a second electric telescopic rod, a sleeve plate, a nitrogen tank, a micro air pump and a flexible tube, the third bevel gear is fixedly connected to the second central tube, the other side of the first bevel gear is transmission-connected to the third bevel gear, a second key bar is provided on the surface of the second central tube, the second central tube passes through the driving part, the second electric telescopic rod is fixedly connected between the fixed cover and the sleeve plate, the sleeve plate is movably sleeved on the surface of the second central tube, one end of the micro air pump is connected to the nitrogen tank, the other end of the micro air pump is connected to the flexible tube, the end of the flexible tube is movably connected to the second central tube, and the driving part, the nitrogen tank and the micro air pump are all installed in the fixed cover;
[0009] The two ends of the rotating frame are respectively fixedly connected to the third center tube and the fourth center tube, the third center tube is movably sleeved on the surface of the second center tube, the third center tube is provided with a first key groove and an accommodating cavity, the second key bar is slidably connected to the first key groove, a one-way valve is provided in the fourth center tube, and the lofting part is connected to the rotating frame.
[0010] As a further solution of the present invention, the sample placement part includes a sample placement dish, a bracket, a clamping piece and a tooth groove. The sample placement dish is fixedly connected to the bracket, the surface of the bracket is provided with a tooth groove, the inner wall of the rotating frame is in sliding contact with the bracket, the end of the second center tube is fixedly connected to the second transmission gear, the tooth groove is in transmission connection with the second transmission gear, and the clamping piece is connected to the bracket.
[0011] As a further solution of the present invention, the telescopic assembly also includes a fixed tube, both ends of the arc shell are fixedly connected to the fixed tube, both ends of the sealing tube are fixedly connected to the first center tube, the second bevel gear is fixedly connected to the first center tube, the first center tube is movably sleeved on the outside of the fixed tube, and the third center tube and the fourth center tube are movably sleeved on the inside of the fixed tube.
[0012] As a further solution of the present invention, the driving part includes a driving motor, a transmission tube and a first transmission gear. The transmission tube is rotatably connected to the inner wall of the fixed cover, the driving motor is fixedly connected to the inner wall of the fixed cover, the first transmission gear is fixedly connected to the transmission tube, the driving motor is connected to the driving gear, the first transmission gear is transmission-connected to the driving gear, and the second center tube passes through the transmission tube.
[0013] As a further solution of the present invention, a first key strip is further provided on the surface of the second central tube, a second key groove is provided on the inner wall of the transmission tube, and the first key strip is slidably connected to the second key groove.
[0014] As a further solution of the present invention, when the second electric telescopic rod drives the second key bar to be located in the first key groove, the third bevel gear is disengaged from the first bevel gear; when the second electric telescopic rod drives the second key bar to be located in the accommodating cavity, the tooth groove is transmission-connected with the second transmission gear; when the second electric telescopic rod drives the third bevel gear to be transmission-connected with the first bevel gear, the second key bar is located in the accommodating cavity, and the tooth groove is disengaged from the second transmission gear.
[0015] As a further solution of the present invention, a limit frame is provided on the inner wall of the rotating frame, and both sides and the bottom of the bracket are in contact with the limit frame. A gas detection probe is fixedly connected to the position of the inner wall of the rotating frame corresponding to the fourth central tube.
[0016] As a further solution of the present invention, the two ends of the arc-shaped shell are fixedly connected with a first sealing plate and a second sealing plate, the first sealing plate and the second sealing plate are used to seal the injection port from the inside and outside respectively, and the fixed tube passes through the second sealing plate.
[0017] The beneficial effects of the present invention are that, on the one hand, the sealing tube can be automatically controlled to seal the biomaterial sample to be tested after the sample is set out, and the purpose of exhausting oxygen is achieved by discharging nitrogen between the sealing tube and the arc-shaped shell, thereby preventing the biomaterial sample to be tested from undergoing an oxidation reaction before entering the analysis chamber; on the other hand, the nitrogen can be extracted and the sealing tube can be automatically opened after the biomaterial sample to be tested enters the analysis chamber, thereby facilitating the use of an energy analyzer to detect the biomaterial sample to be tested, and having the characteristics of facilitating adjustment and improving the accuracy of the test results. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] Figure 1 This is the first stereogram of the present invention.
[0019] Figure 2 This is an exploded view of the sample injection mechanism according to an embodiment of the present invention.
[0020] Figure 3 This is a three-dimensional diagram of a telescopic assembly according to an embodiment of the present invention.
[0021] Figure 4 This is a three-dimensional diagram of a sealing tube according to an embodiment of the present invention.
[0022] Figure 5 2. It is a cross-sectional view of the telescopic assembly and the sealing tube according to an embodiment of the present invention.
[0023] Figure 6 This is an exploded view of a driving module according to an embodiment of the present invention.
[0024] Figure 7 This is a three-dimensional diagram of a rotating frame according to an embodiment of the present invention.
[0025] Figure 8 It is a planar cross-sectional view of a rotating rack according to an embodiment of the present invention.
[0026] Figure 9 It is a three-dimensional diagram of the lofting part of an embodiment of the present invention.
[0027] Figure 10 This is the first cross-sectional view of the sample injection mechanism of the embodiment of the invention.
[0028] Figure 11 This is a second cross-sectional view of the sample injection mechanism according to an embodiment of the present invention.
[0029] Figure 12 This is the third cross-sectional view of the sample injection mechanism according to an embodiment of the present invention.
[0030] Figure 13 This is the fourth cross-sectional view of the sample injection mechanism according to an embodiment of the present invention.
[0031] Figure 14 This is a planar cross-sectional view of the sample injection mechanism according to an embodiment of the present invention.
[0032] Figure 15 This is a second perspective view of the present invention.
[0033] Figure 16 It is a planar cross-sectional view of the present invention.
[0034] Figure 17 It is a partial planar sectional view of the present invention.
[0035] Figure numerals: 1-metal shielding shell, 2-analysis chamber, 3-injection mechanism, 31-telescopic assembly, 311-arc shell, 312-first sealing plate, 313-second sealing plate, 314-fixed cover, 315-first electric telescopic rod, 316-fixed tube, 317-first bevel gear, 32-sealing tube, 321-take-and-release port, 322-first center tube, 323-second bevel gear, 33-drive module, 331-drive part, 3311-drive motor, 3312-transmission tube, 3313-first transmission gear, 332-second center tube, 3321-third bevel gear, 3322-second transmission gear , 3323-first key bar, 3324-second key bar, 333-second electric telescopic rod, 3331-sleeve plate, 334-nitrogen tank, 3341-micro air pump, 3342-flexible tube, 34-rotating frame, 341-third central tube, 342-first key slot, 343-gas detection probe, 344-fourth central tube, 345-limiting frame, 346-one-way valve, 347-accommodating chamber, 35-sampling part, 351-sampling dish, 352-bracket, 353-tooth groove, 354-clamping part, 4-energy analyzer, 5-ion pump, 6-ion gauge, 7-molecular pump, 8-control display, 9-injection port. DETAILED DESCRIPTION
[0036] In order to make the purpose, technical solutions and advantages of the present invention clearer, the present invention is further described in detail below with reference to the accompanying drawings and specific embodiments. It should be understood that the specific embodiments described herein are only used to explain the present invention and are not intended to limit the present invention.
[0037] The specific implementation of the present invention is described in detail below with reference to specific embodiments.
[0038] See also Figures 1 to 17 In one embodiment of the present invention, a spectrometer for automatic analysis and detection of biological material samples includes a metal shielding shell 1, an analysis chamber 2, an energy analyzer 4, an ion pump 5, an ion gauge 6, a molecular pump 7, a control display 8, and an injection port 9. The analysis chamber 2 is provided inside the metal shielding shell 1, and the energy analyzer 4, ion pump 5, ion gauge 6, and molecular pump 7 are all fixedly connected to the metal shielding shell 1. The injection port 9 and the control display 8 are provided on the surface of the metal shielding shell 1. The analysis chamber 2 is connected to the injection port 9, and further includes:
[0039] The sampling mechanism 3 includes a telescopic assembly 31, a sealing tube 32, a driving module 33, a rotating frame 34 and a sample placement portion 35. The telescopic assembly 31 includes an arcuate shell 311, a first bevel gear 317, a fixed cover 314 and a first electric telescopic rod 315. The first electric telescopic rod 315 is fixedly connected between the metal shielding shell 1 and the arcuate shell 311. The fixed cover 314 is fixedly connected to one end of the arcuate shell 311. The first bevel gear 317 is connected to the fixed cover 314. The arcuate shell 311 is in sliding contact with the inner wall of the sampling port 9. The sealing tube 32 is movably sleeved in the arcuate shell 311. A take-and-put port 321 is provided on the surface of the sealing tube 32. A second bevel gear 323 is provided at the end of the sealing tube 32. One side of the first bevel gear 317 is transmission-connected to the second bevel gear 323.
[0040] The driving module 33 includes a driving part 331, a second central tube 332, a third bevel gear 3321, a first key bar 3323, a second key bar 3324, a second electric telescopic rod 333, a sleeve 3331, a nitrogen tank 334, a micro air pump 41 and a flexible tube 3342. The third bevel gear 3321 is fixedly connected to the second central tube 332. The other side of the first bevel gear 317 is transmission-connected to the third bevel gear 3321. The surface of the second central tube 332 is provided with a second key bar 3324. The second central tube 332 passes through the driving unit 331. The second electric telescopic rod 333 is fixedly connected between the fixed cover 314 and the sleeve 3331. The sleeve 3331 is movably sleeved on the surface of the second central tube 332. One end of the micro air pump 41 is connected to the nitrogen tank 334, and the other end of the micro air pump 41 is connected to the flexible tube 3342. The end of the flexible tube 3342 is movably connected to the second central tube 332. The driving unit 331, the nitrogen tank 334, and the micro air pump 41 are all installed in the fixed cover 314.
[0041] The two ends of the rotating frame 34 are respectively fixedly connected to the third center tube 341 and the fourth center tube 344. The third center tube 341 is movably sleeved on the surface of the second center tube 332. The third center tube 341 is provided with a first key groove 342 and a accommodating cavity 347. The second key bar 3324 is slidably connected to the first key groove 342. A one-way valve 346 is provided in the fourth center tube 344. The lofting part 35 is connected to the rotating frame 34.
[0042] See also Figure 3 、 Figure 5 and Figure 13Furthermore, the telescopic assembly 31 also includes a fixed tube 316, both ends of the arc shell 311 are fixedly connected to the fixed tube 316, both ends of the sealing tube 32 are fixedly connected to the first center tube 322, the second bevel gear 323 is fixedly connected to the first center tube 322, the first center tube 322 is movably sleeved on the outside of the fixed tube 316, and the third center tube 341 and the fourth center tube 344 are movably sleeved on the inside of the fixed tube 316.
[0043] See also Figure 6 and Figure 13 Furthermore, the driving part 331 includes a driving motor 3311, a transmission tube 3312 and a first transmission gear 3313. The transmission tube 3312 is rotatably connected to the inner wall of the fixed cover 314. The driving motor 3311 is fixedly connected to the inner wall of the fixed cover 314. The first transmission gear 3313 is fixedly connected to the transmission tube 3312. The driving motor 3311 is connected to the driving gear. The first transmission gear 3313 is in transmission connection with the driving gear. The second center tube 332 passes through the transmission tube 3312.
[0044] See also Figure 6 、 Figure 10-14 Furthermore, a first key strip 3323 is provided on the surface of the second central tube 332, a second key groove is provided on the inner wall of the transmission tube 3312, and the first key strip 3323 is slidably connected to the second key groove.
[0045] See also Figure 3 and Figure 15 Furthermore, the two ends of the arc-shaped shell 311 are fixedly connected with a first sealing plate 312 and a second sealing plate 313 respectively, and the fixed tube 316 passes through the second sealing plate 313.
[0046] In the embodiment of the present invention, the specific working principles of the energy analyzer 4, the ion pump 5, the ion gauge 6, and the molecular pump 7 are referred to patent CN218956453U3 and will not be described in detail. The first sealing plate 312 and the second sealing plate 313 are used to seal the sample inlet 9 from the inner and outer sides respectively to prevent external air from entering the analysis chamber 2. When the second electric telescopic rod 333 drives the second key bar 3324 to be located in the first key groove 342, the third bevel gear 3321 is disengaged from the first bevel gear 317. When the second electric telescopic rod 333 drives the second key bar 3324 to be located in the accommodating chamber 347, the tooth groove 353 is transmission-connected with the second transmission gear 3322. When the second electric telescopic rod 333 drives the third bevel gear 3321 to be transmission-connected with the first bevel gear 317, the second key bar 3324 is located in the accommodating chamber 347, and the tooth groove 353 is disengaged from the second transmission gear 3322.
[0047] See also Figure 9 、 Figure 10-14In one embodiment of the present invention, the sample placement portion 35 includes a sample placement dish 351, a bracket 352, a clamping member 354 and a tooth groove 353. The sample placement dish 351 is fixedly connected to the bracket 352. The tooth groove 353 is provided on the surface of the bracket 352. The inner wall of the rotating frame 34 is in sliding contact with the bracket 352. The end of the second center tube 332 is fixedly connected to the second transmission gear 3322. The tooth groove 353 is in transmission connection with the second transmission gear 3322. The clamping member 354 is connected to the bracket 352.
[0048] See also Figure 7 and Figure 10 Furthermore, a limit frame 345 is provided on the inner wall of the rotating frame 34, and both sides and the bottom of the bracket 352 are in contact with the limit frame 345. A gas detection probe 343 is fixedly connected to the position corresponding to the inner wall of the rotating frame 34 and the fourth central tube 344.
[0049] In an embodiment of the present invention, when the tooth groove 353 is disengaged from the second transmission gear 33, the limit frame 345 serves to support the bracket 35 and the sample dish 351, and the gas detection probe 343 is communicated with the control display to monitor the gas composition passing through the fourth center tube 344, thereby being used to determine whether the oxygen in the sealed cavity between the arc shell 311 and the sealing tube 32 is emptied. The specific model of the gas detection probe 34 is not limited. Since the gas detection probe 34 is widely used in the prior art, the specific structure will not be repeated. The specific structure of the clamping member 354 is not limited. The clamping member 354 can be an elastic clamp or a limit clamp controlled by a screw.
[0050] Working principle: First, the control display 8 is used to control the first electric telescopic rod 315 to move the arc shell 311 out of the sample inlet 9. At this time, the first sealing plate 312 seals the sample inlet 9 from the inside to prevent outside air from entering the analysis chamber 2. The biological material sample to be tested is placed in the sample dish 351 and fixed by the clamping member 354. The control display 8 is used to control the second electric telescopic rod 333 to move the third bevel gear 3321 to a position where it is transmission-connected with the first bevel gear 317. Since the second key bar 3324 is located in the accommodating cavity 347 at this time, the second transmission tooth is disengaged from the tooth groove 353. Therefore, when the driving motor 3311 controls the second central tube 332 to rotate through the transmission tube 3312, the second limiting groove, and the first key bar 3323, the rotating second central tube 332 will only control the sealing tube 32 to rotate 180 degrees through the third bevel gear 3321 and the first bevel gear 317, so that the taking and placing port 321 is located in the arc shell 311.
[0051] The micro air pump 41 is turned on by controlling the control display 8. The micro air pump 41 discharges the nitrogen in the nitrogen tank 334 into the sealed cavity between the arc shell 311 and the sealing tube 32 through the flexible tube 3342 and the second central tube 332, and is used to discharge the air in the sealed cavity to the outside through the one-way valve 346. The gas detection probe 343 is used to monitor the gas composition passing through the fourth central tube 344. When the control display 8 shows that the gas composition monitored by the gas detection probe 343 does not contain oxygen or only nitrogen, the micro air pump 41 is controlled to be turned off. The control display 8 is used to control The first electric telescopic rod 315 is used to move the arc-shaped housing 311 into the sample inlet 9. The second sealing plate 313 is used to seal the sample inlet 9 from the outside. The control display 8 is again used to control the micro air pump 41 to start. The suction function of the micro air pump 41 is used to re-draw the nitrogen in the sealed chamber into the nitrogen tank 334. Finally, the driving motor 3311 is used to control the sealing tube 32 to rotate 180 degrees again, so that the access port 321 is located outside the arc-shaped housing 311. At this time, the biological material sample to be tested is completely exposed to the analysis chamber 2, thereby facilitating detection by the energy analyzer 4.
[0052] When the surface of the biomaterial sample to be tested is uneven or irregular in shape, the control display 8 is used to control the second electric telescopic rod 333 to move the second key bar 3324 to the position of the first key groove 342. At this time, the second transmission gear 3322 is located in a position in transmission connection with the tooth groove 353. When the second central tube 332 is controlled to rotate by the drive motor 3311, the rotating second central tube 332 drives the rotating frame 34, the sample placement part 35 and the biomaterial sample to be tested to rotate between -20 degrees and 20 degrees around the third central tube 341 as the axis through the second key bar 3324 and the first key groove 342, thereby facilitating the energy analyzer 4 to detect different positions on the surface of the biomaterial sample.
[0053] When the control display 8 is used to control the second electric telescopic rod 333 to move the second key bar 3324 into the accommodating cavity 347, and the second transmission gear 3322 is located in a position for transmission connection with the tooth groove 353, when the drive motor 3311 is used to control the rotation of the second central tube 332, the rotating second central tube 332 drives the bracket 352 and the sample dish 351 to move in the limit frame 345 through the second transmission gear 3322 and the tooth groove 353, so that the detection distance between it and the energy analyzer 4 can be adjusted according to the volume of the biological material sample.
[0054] In summary, the present application utilizes the structural design of the mutual cooperation among the telescopic component 31, the sealing tube 32, the driving module 33, the rotating frame 34 and the sample placement part 35 in the sample introduction mechanism 3. (1) On the one hand, it can automatically control the sealing tube 32 to seal the biological material sample to be tested after the sample is placed, and achieve the purpose of exhausting oxygen by discharging nitrogen between the sealing tube 32 and the arc shell 311, thereby preventing the biological material sample to be tested from undergoing an oxidation reaction before entering the analysis chamber 2. On the other hand, it can also extract the nitrogen and automatically open the sealing tube 32 after the biological material sample to be tested enters the analysis chamber 2, thereby facilitating the detection of the biological material sample to be tested by using the energy analyzer 4. (2) When the surface of the biomaterial sample to be tested is uneven or irregular in shape, the driving module 33 is used to control the biomaterial sample to be tested to rotate between -20 degrees and 20 degrees with the third central tube 341 as the axis, so that the energy analyzer 4 can detect different positions on the surface of the biomaterial sample; the driving module 33 is used to control the movement of the biomaterial sample to be tested and the sample dish 351 in the rotating frame 34, so that the detection distance between the biomaterial sample and the energy analyzer 4 can be automatically adjusted according to the volume of the biomaterial sample, which has the characteristics of facilitating adjustment and improving the accuracy of the detection results.
[0055] For those skilled in the art, although several embodiments and examples of the present invention have been described, these embodiments and examples are provided as examples and are not intended to limit the scope of the invention. These new embodiments can be implemented in various other ways, and various omissions, substitutions, and changes can be made without departing from the scope of the invention.
[0056] In addition, it should be understood that although this specification is described in terms of implementation methods, not every implementation method contains only one independent technical solution. This narrative method of the specification is only for the sake of clarity. Those skilled in the art should regard the specification as a whole. The technical solutions in each embodiment can also be appropriately combined to form other implementation methods that can be understood by those skilled in the art.
Claims
1. A spectrometer for automatic analysis and detection of biological material samples, comprising a metal shielding shell (1), an analysis chamber (2), an energy analyzer (4), an ion pump (5), an ion gauge (6), a molecular pump (7), a control display (8) and an injection port (9), wherein the metal shielding shell (1) is provided with an analysis chamber (2), the energy analyzer (4), the ion pump (5), the ion gauge (6) and the molecular pump (7) are all fixedly connected in the metal shielding shell (1), the surface of the metal shielding shell (1) is provided with an injection port (9) and a control display (8), the analysis chamber (2) is communicated with the injection port (9), and the invention is characterized in that: Also includes: The sample feeding mechanism (3) comprises a telescopic assembly (31), a sealing tube (32), a driving module (33), a rotating frame (34) and a sample setting portion (35); the telescopic assembly (31) comprises an arcuate shell (311), a first bevel gear (317), a fixed cover (314) and a first electric telescopic rod (315); the first electric telescopic rod (315) is fixedly connected between the metal shielding shell (1) and the arcuate shell (311); the fixed cover (314) is fixedly connected to the metal shielding shell (1) and the arcuate shell (311); One end of the arc-shaped shell (311) is fixedly connected, the first bevel gear (317) is connected to the fixed cover (314), the arc-shaped shell (311) is in sliding contact with the inner wall of the injection port (9), the sealing tube (32) is movably sleeved in the arc-shaped shell (311), the surface of the sealing tube (32) is provided with a take-in and put-out port (321), the end of the sealing tube (32) is provided with a second bevel gear (323), and one side of the first bevel gear (317) is transmission-connected to the second bevel gear (323); The driving module (33) comprises a driving portion (331), a second central tube (332), a third bevel gear (3321), a first key bar (3323), a second key bar (3324), a second electric telescopic rod (333), a sleeve (3331), a nitrogen tank (334), a micro air pump (41) and a flexible tube (3342); the third bevel gear (3321) is fixedly connected to the second central tube (332); the other side of the first bevel gear (317) is transmission-connected to the third bevel gear (3321); a second key bar (3324) is provided on the surface of the second central tube (332); The second central tube (332) passes through the driving part (331), the second electric telescopic rod (333) is fixedly connected between the fixed cover (314) and the sleeve (3331), the sleeve (3331) is movably sleeved on the surface of the second central tube (332), one end of the micro air pump (41) is connected to the nitrogen tank (334), and the other end of the micro air pump (41) is connected to the flexible tube (3342), the end of the flexible tube (3342) is movably connected to the second central tube (332), and the driving part (331), the nitrogen tank (334) and the micro air pump (41) are all installed in the fixed cover (314); The two ends of the rotating frame (34) are respectively fixedly connected with a third central tube (341) and a fourth central tube (344); the third central tube (341) is movably sleeved on the surface of the second central tube (332); a first key groove (342) and a receiving cavity (347) are provided in the third central tube (341); the second key bar (3324) is slidably connected to the first key groove (342); a one-way valve (346) is provided in the fourth central tube (344); and the lofting portion (35) is connected to the rotating frame (34).
2. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 1, characterized in that: The sample placement portion (35) comprises a sample placement dish (351), a bracket (352), a clamping piece (354) and a tooth groove (353); the sample placement dish (351) is fixedly connected to the bracket (352); the surface of the bracket (352) is provided with a tooth groove (353); the inner wall of the rotating frame (34) is in sliding contact with the bracket (352); the end of the second central tube (332) is fixedly connected to a second transmission gear (3322); the tooth groove (353) is transmission-connected to the second transmission gear (3322); and the clamping piece (354) is connected to the bracket (352).
3. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 2, characterized in that: The telescopic assembly (31) further includes a fixed tube (316), both ends of the arc-shaped shell (311) are fixedly connected to the fixed tube (316), both ends of the sealing tube (32) are fixedly connected to the first central tube (322), the second bevel gear (323) is fixedly connected to the first central tube (322), the first central tube (322) is movably sleeved on the outside of the fixed tube (316), and the third central tube (341) and the fourth central tube (344) are movably sleeved on the inside of the fixed tube (316).
4. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 3, characterized in that: The driving portion (331) includes a driving motor (3311), a transmission tube (3312) and a first transmission gear (3313); the transmission tube (3312) is rotatably connected to the inner wall of the fixed cover (314); the driving motor (3311) is fixedly connected to the inner wall of the fixed cover (314); the first transmission gear (3313) is fixedly connected to the transmission tube (3312); the driving motor (3311) is connected to the driving gear; the first transmission gear (3313) is transmission-connected to the driving gear; and the second center tube (332) passes through the transmission tube (3312).
5. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 4, characterized in that: The surface of the second central tube (332) is further provided with a first key strip (3323), the inner wall of the transmission tube (3312) is provided with a second key groove, and the first key strip (3323) is slidably connected to the second key groove.
6. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 2, characterized in that: When the second electric telescopic rod (333) drives the second key bar (3324) to be located in the first key groove (342), the third bevel gear (3321) is disengaged from the first bevel gear (317); when the second electric telescopic rod (333) drives the second key bar (3324) to be located in the accommodating cavity (347), the tooth groove (353) is transmission-connected to the second transmission gear (3322); when the second electric telescopic rod (333) drives the third bevel gear (3321) to be transmission-connected to the first bevel gear (317), the second key bar (3324) is located in the accommodating cavity (347), and the tooth groove (353) is disengaged from the second transmission gear (3322).
7. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 6, characterized in that: A limiting frame (345) is provided on the inner wall of the rotating frame (34), and both sides and the bottom of the bracket (352) are in contact with the limiting frame (345). A gas detection probe (343) is fixedly connected to a position on the inner wall of the rotating frame (34) corresponding to the fourth central tube (344).
8. The energy spectrometer for automatic analysis and detection of biological material samples according to claim 3, characterized in that: The two ends of the arc-shaped shell (311) are respectively fixedly connected with a first sealing plate (312) and a second sealing plate (313), the first sealing plate (312) and the second sealing plate (313) are used to seal the injection port (9) from the inside and outside, respectively, and the fixed tube (316) passes through the second sealing plate (313).
Citation Information
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