一种低成本黑磷晶体的制备方法

By utilizing high-entropy carbide ceramic material baffles and tracks in a vertical reactor, the directional growth of black phosphorus crystals and the reuse of by-products are achieved, solving the problem of high cost in black phosphorus crystal preparation and improving production efficiency and raw material utilization.

CN119776982BActive Publication Date: 2026-07-17HUBEI XINGFA CHEM GRP CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
HUBEI XINGFA CHEM GRP CO LTD
Filing Date
2024-12-09
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

The preparation cost of black phosphorus crystals in the existing technology is high, making it difficult to achieve low-cost, large-scale, and efficient preparation. In addition, the recycling and treatment of by-products is inconvenient, which affects production efficiency and cost.

Method used

A vertical reactor is used to fix high-entropy carbide ceramic materials on the track and partition plate, and the by-products are used as catalysts to achieve directional growth and efficient separation of black phosphorus crystals. The by-products are processed and reused to reduce the cost of catalysts.

Benefits of technology

This method enables low-cost and high-efficiency preparation of black phosphorus crystals, simplifies byproduct treatment, allows for catalyst reuse, and improves raw material utilization and production efficiency.

✦ Generated by Eureka AI based on patent content.

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Abstract

本发明公开了一种低成本黑磷晶体的制备方法。其中黑磷晶体制备装置是反应器,具体表现是在反应器内壁原料端管壁上安装可上下移动的轨道。方法首先是在惰性氛围下在反应器原料端投入一定量的磷原料、催化剂及输运剂,待投料全部完成后,将隔板放入到反应器中,隔板在反应器原料端可上下移动,待到合适位置后将其固定在轨道上,然后密封反应器成核端,设置升温程序进行加热,程序结束后打开反应器可得到高质量的黑磷晶体。副产物全部附着在隔板上,在将隔板取下来后进行收集方便下次使用(代替催化剂)。本发明操作简单、工艺简单、质量稳定、效率高、副产物回收利用方便,生产产品成本将大大降低。
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