Preparation method, device and application of basic ionic liquid for animals

Abstract

The invention relates to the technical field of biological agriculture, in particular to a preparation method, device and application of basic ionic liquid for animals, and the basic ionic liquid comprises potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromic oxide, chitosan oligosaccharide and purified water. The preparation method and device of the basic ionic liquid for animals and the application have the beneficial effects that through scientific proportioning and careful preparation, the basic ionic liquid can remarkably improve the growth performance, the immunity and the intestinal health level of animals, improve the villus height and the crypt depth of jejunum and ileum, and improve the animal immunity. And a ratio of fluff length to recess depth; and by optimizing the equipment structure and the operation process, the preparation efficiency and quality are improved, and the labor cost and the error rate are reduced.

Description

Technical Field

[0001] The invention relates to the technical field of biological agriculture, and in particular to a method, a device and an application of an alkaline ionic liquid for animals. Background Art

[0002] In modern animal husbandry, the use of animal feed additives is of great significance for improving animal production performance, enhancing immunity, improving intestinal health, etc. Traditional feed additives often have problems such as single effect and obvious side effects, which are difficult to meet the needs of modern animal husbandry for high efficiency, environmental protection and safety. Therefore, it is particularly important to develop an animal feed additive with multiple functions, safety and reliability.

[0003] As a new type of feed additive, alkaline ionic liquid has gradually attracted attention in animal husbandry due to its unique chemical properties and biological activity. However, most alkaline ionic liquids on the market currently have a single component, limited functions, and a complex preparation process with high costs. Therefore, it is of great significance to develop an alkaline ionic liquid for animals that has diverse components, simple preparation, and significant effects. Summary of the invention

[0004] The purpose of the present invention is to provide a method, device and application of preparing alkaline ionic liquid for animals to solve the problems raised in the above background technology.

[0005] To achieve the above object, the present invention provides the following technical scheme: a method for preparing an alkaline ionic liquid for animals, wherein the alkaline ionic liquid comprises: potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, chitosan oligosaccharide and purified water, and the specific composition content thereof is: 30-50 parts of potassium bicarbonate, 500-1200 parts of potassium carbonate, 200-800 parts of sodium bicarbonate, 40-80 parts of sodium carbonate, 0.5-12 parts of germanium dioxide, 0.4-3 parts of sodium selenite, 0.2-2 parts of chromium oxide, 300-800 parts of chitosan oligosaccharide and 600-1500 parts of purified water; the parts are parts by weight;

[0006] The preparation method comprises the following steps:

[0007] Each component is gradually dissolved in 600-1450 parts of purified water at 55°C or above, stirred in a reaction kettle for 1-2 hours to fully mix, and placed at 32-38°C for 30-35 hours to fully react with the complex, and then used;

[0008] The material is fully homogenized through the homogenization process, and the material is homogenized by the homogenizer. The plunger pump sucks the original material at a low speed of 0.25 to 0.5 m / s, and the pressure of the homogenization system is adjusted through the pressure regulating device connected to the homogenization valve;

[0009] The dry powder core material is obtained by spray drying, and then compounded to include the following components by weight: 2-8 parts of sodium citrate, 0.5-2 parts of yeast selenium, 0.5-1 parts of methionine chromium, and 0.5-1 parts of nicotinate chromium.

[0010] A device for preparing alkaline ionic liquid for animals is applied to a method for preparing alkaline ionic liquid for animals. The device comprises a reactor, a homogenizer, a spray dryer and a mixer. Materials are mixed evenly by the reactor and then put into the homogenizer for homogenization. The homogenized materials are spray dried by the spray dryer and then compounded by the mixer. The reactor comprises a storage tank. A cover is installed on the top of the storage tank. The top of the cover is rotatably connected to a liquid storage cylinder. A stirring shaft is fixed to the bottom end of the liquid storage cylinder. A through hole is provided on the bottom surface of the liquid storage cylinder. A pressing block is slidably connected to the inside of the liquid storage cylinder. When the pressing block falls on the bottom plate of the liquid storage cylinder, the pressing block covers the through hole. A turntable is rotatably connected to the inside of the cover. A plurality of storage slots are provided on the surface of the turntable. A discharge port is provided on the bottom surface of the storage slot. A feeding hopper is plugged and fixed on the top plate of the cover. A servo motor 2 is fixed on the top plate of the cover. The rotating shaft of the servo motor 2 passes through the top plate of the cover and is fixed to the top surface of a gear. The gear meshes with teeth, and the teeth are fixed on the surface of the turntable.

[0011] Preferably, the top end of the storage tank and the bottom end of the cover are both integrally formed with connecting plates, the two connecting plates are connected by multiple sets of bolts, a gasket is inserted into the bottom end of the cover, the gasket is a circular ring plate with an "L"-shaped cross-section, the outer ring diameter of the gasket is equal to the inner ring diameter of the cover, the inner ring surface of the gasket is threaded with multiple screws, the screws penetrate the gasket and are threaded to the inner wall of the cover, the outer ring surface of the gasket is sleeved and fixed with a sealing gasket, the sealing gasket is a circular ring plate with an "L"-shaped cross-section, the top plate of the sealing gasket is clamped between the storage tank and the cover, the top surface of the gasket is embedded with multiple ball bearings, and the surface of the storage tank is plugged and fixed with a liquid injection valve tube.

[0012] Preferably, a bearing 1 is plugged and fixed on the top plate of the cover, the inner ring of the bearing 1 is fixed in the opening of the top plate of the cover, the inner ring of the bearing 1 is sleeved on the top of the liquid storage cylinder, the liquid storage cylinder is a "convex" shaped cylindrical structure, the top of the liquid storage cylinder is fixed to the bottom end of the rotating shaft of servo motor 1, the servo motor 1 is fixed to the top surface of the support plate, the support plate is a circular ring plate structure, a plurality of pillars are fixed on the bottom surface of the support plate, the bottom ends of the pillars are fixed to the top surface of the cover, an injection tube and a one-way air intake valve are plugged and fixed on the top of the liquid storage cylinder, the injection tube and the one-way air intake valve are symmetrically distributed about the top of the liquid storage cylinder, and a sealing cap is threadedly sleeved on the pipe mouth of the injection tube.

[0013] Preferably, the through holes are provided in plurality, and the plurality of through holes are distributed in a circle with the center of the bottom plate of the liquid storage cylinder in a circle. The pressing block is in a hemispherical structure. A mounting groove is provided on the bottom surface of the pressing block, and an electric telescopic rod 1 is plugged into the inside of the mounting groove. The bottom end of the electric telescopic rod 1 is fixed to the top surface of the bottom plate of the liquid storage cylinder, and the piston rod of the electric telescopic rod 1 is fixed to the top surface of the mounting groove. Two embedding grooves 1 are provided inside the mounting groove, and a battery is fixed inside the embedding groove 1. The battery and the electric telescopic rod 1 are electrically connected through a wire. A rubber pad is fixed to the bottom surface of the pressing block, and the rubber pad is in an annular plate structure. A mounting groove 2 is provided on the bottom surface of the pressing block, and the mounting groove 2 is in an annular groove. A rubber cover is fixed to the top surface of the embedding groove 2, and the bottom end of the rubber cover is fixed to the top surface of the bottom plate of the liquid storage cylinder.

[0014] Preferably, the turntable is in the form of a "convex" shaped circular ring plate, the inner ring surface of the turntable is provided with an inner ring groove, the inner ring groove is in the form of a "convex" shaped circular groove, a retaining ring is fixed to the bottom surface of the top plate of the cover, the retaining ring is in the form of an inverted "convex" shaped circular plate, the inner ring diameter of the retaining ring is larger than the outer diameter of the liquid storage cylinder, a bearing 2 is fixed on the bottom end of the retaining ring, the outer ring of the bearing 2 is inserted into the top notch of the inner ring groove, a plurality of teeth are fixed on the outer ring surface of the inner ring groove, a plurality of servo motors 2 are provided, and the plurality of servo motors 2 are arranged equidistantly along the edge of the top surface of the cover.

[0015] Preferably, a material guide cover is inserted at the top of the material storage trough, and the material guide cover is an inverted table-shaped ring plate. The top plate of the material guide cover is fixed to the top surface of the turntable by screws, and a sealing block is inserted into the inside of the discharge port, and the sealing block is fixed to the top surface of the traction plate. A plurality of electric telescopic rods 2 are fixed inside the inner ring groove, and the electric telescopic rods 2 correspond to the traction plates one by one. The piston rod of the electric telescopic rod 2 passes through the bottom plate of the turntable and is fixed to the top surface of the traction plate.

[0016] The invention discloses an application of alkaline ionic liquid for animals in improving the villus height and crypt depth of the jejunum and ileum and the ratio of the villus length to the crypt depth. 200-500 g / ton of alkaline ionic liquid for animals is added to animal feed.

[0017] An application of an alkaline ionic liquid for animals in relieving stress, increasing feed intake or reducing feed-to-meat ratio, wherein 200-500 g / ton of the alkaline ionic liquid for animals is added to animal feed.

[0018] An alkaline ionic liquid for animals is used to increase the lean meat rate of carcasses, resist oxidation, reduce drip loss, improve meat color, and increase the slaughter rate of livestock and poultry. 200-500 grams / ton of the alkaline ionic liquid for animals is added to animal feed.

[0019] Compared with the prior art, the present invention has the following beneficial effects:

[0020] The alkaline ionic liquid preparation method, device and application for animals proposed in the present invention can significantly improve the growth performance, immune ability and intestinal health level of animals through scientific proportioning and careful preparation, and improve the villus height and crypt depth of the jejunum and ileum, as well as the ratio of villus length to crypt depth; by optimizing the equipment structure and operation process, the preparation efficiency and quality are improved, and the labor cost and error rate are reduced. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] Figure 1 It is a schematic diagram of the structure of the present invention;

[0022] Figure 2 It is a top view of the structure of the present invention;

[0023] Figure 3 for Figure 2 Structural cross-section view at AA in the middle;

[0024] Figure 4 for Figure 3 A schematic diagram of the structure enlargement in the middle;

[0025] Figure 5 for Figure 3 A magnified schematic diagram of the structure at B in the middle;

[0026] Figure 6 for Figure 3 A magnified schematic diagram of the structure at C in the middle;

[0027] Figure 7 for Figure 3 A magnified schematic diagram of the structure at D in the middle;

[0028] Figure 8 It is a schematic diagram of the structure of the turntable of the present invention;

[0029] Fig. 9 This is a schematic diagram of the structure of the material guide cover of the present invention;

[0030] Fig.10 It is a schematic diagram of the connection structure between the sealing block and the traction plate of the present invention;

[0031] Fig.11 This is a schematic diagram of the connection structure between the liquid storage cylinder and the stirring shaft of the present invention;

[0032] Fig.12 The figure is a flow chart of the method of the present invention.

[0033] In the figure: storage tank 1, sealing cover 2, liquid storage cylinder 3, stirring shaft 4, servo motor 1 5, support plate 6, pillar 7, bearing 1 8, injection pipe 9, one-way air inlet valve 10, through hole 11, pressure block 12, installation groove 13, embedded groove 1 14, battery 15, electric telescopic rod 1 16, rubber pad 17, embedded groove 2 18, rubber cover 19, turntable 20, inner ring groove 21, retaining ring 22, bearing 2 23, storage trough 24, discharge port 25, sealing block 26, traction plate 27, electric telescopic rod 2 28, material guide cover 29, feeding hopper 30, pad 31, ball 32, sealing pad 33, servo motor 2 34, gear 35, teeth 36, injection valve pipe 37, observation port 38, transparent window plate 39, label 40. DETAILED DESCRIPTION

[0034] In order to make the purpose and technical solution of the present invention clearly and completely described, and the advantages more clearly understood, the embodiments of the present invention are further described in detail with reference to the accompanying drawings. It should be understood that the specific embodiments described herein are part of the embodiments of the present invention, not all of them, and are only used to explain the embodiments of the present invention, and are not used to limit the embodiments of the present invention. All other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0035] For example, see Fig.12 The present invention provides a technical solution: a method for preparing an alkaline ionic liquid for animals, wherein the alkaline ionic liquid comprises: potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, chitosan oligosaccharide and purified water, and the specific composition content thereof is: 30-50 parts of potassium bicarbonate, 500-1200 parts of potassium carbonate, 200-800 parts of sodium bicarbonate, 40-80 parts of sodium carbonate, 0.5-12 parts of germanium dioxide, 0.4-3 parts of sodium selenite, 0.2-2 parts of chromium oxide, 300-800 parts of chitosan oligosaccharide and 600-1500 parts of purified water; the parts are parts by weight;

[0036] The preparation method comprises the following steps:

[0037] Each component is gradually dissolved in 600-1450 parts of purified water at 55°C or above, stirred in a reaction kettle for 1-2 hours to fully mix, and placed at 32-38°C for 30-35 hours to fully react with the complex, and then used;

[0038] The material is fully homogenized through the homogenization process, and the material is homogenized by the homogenizer. The plunger pump sucks the original material at a low speed of 0.25 to 0.5 m / s, and the pressure of the homogenization system is adjusted through the pressure regulating device connected to the homogenization valve;

[0039] The dry powder core material is obtained by spray drying, and then compounded to include the following components by weight: 2-8 parts of sodium citrate, 0.5-2 parts of yeast selenium, 0.5-1 parts of methionine chromium, and 0.5-1 parts of nicotinate chromium.

[0040] Example 2. On the basis of Example 1, a composite ion activator for animals is proposed. 40 parts of potassium bicarbonate, 800 parts of potassium carbonate, 400 parts of sodium bicarbonate, 60 parts of sodium carbonate, 6 parts of germanium dioxide, 2 parts of sodium selenite, 1 part of chromium oxide, and 550 parts of chitosan oligosaccharides are gradually (all components are added to water together and gradually dissolved) dissolved in 1000 parts of purified water at 55°C and stirred for 2 hours to fully mix them, placed at 35°C for 35 hours to fully react with the complex, and then homogenized by a homogenizer (0.3 m / s), and then spray-dried to make a composite ion activator product for animals, and packaged.

[0041] Example 3. On the basis of Example 1, a composite ion activator for animals is proposed. 35 parts of potassium bicarbonate, 700 parts of potassium carbonate, 450 parts of sodium bicarbonate, 50 parts of sodium carbonate, 5 parts of germanium dioxide, 1 part of sodium selenite, 1 part of chromium oxide, and 600 parts of chitosan oligosaccharides are gradually (all components are added to water together and gradually dissolved) dissolved in 1000 parts of purified water at 58°C and stirred for 1.5 hours to fully mix them, placed at 35°C for 35 hours to fully react with the complex, and then homogenized by a homogenizer (0.3 m / s), and then spray-dried to make a composite ion activator product for animals, and packaged.

[0042] Example 4. On the basis of Example 1, a composite ion activator for animals is proposed. 40 parts of potassium bicarbonate, 700 parts of potassium carbonate, 500 parts of sodium bicarbonate, 60 parts of sodium carbonate, 6 parts of germanium dioxide, 2 parts of sodium selenite, 1 part of chromium oxide, and 500 parts of chitosan oligosaccharides are gradually dissolved in 1000 parts of purified water at 55°C and stirred for 2 hours to fully mix them. They are placed at 38°C for 35 hours to fully react with the complex, and then homogenized by a homogenizer (0.3 m / s), and then spray-dried to make a composite ion activator product for animals, and packaged.

[0043] Example 5: Based on Example 2, the composite ion activator product for animals prepared in Example 2 is mixed with 5 parts of sodium citrate, 1 part of yeast selenium, 1 part of methionine chromium and 1 part of nicotinate chromium, and stirred to obtain a new ion activator product. Among them, sodium citrate, yeast selenium, methionine chromium and nicotinate chromium are all 80-120 mesh.

[0044] Comparative Example

[0045] Chitosan oligosaccharide is used as a complex ion activator for animals.

[0046] Application Examples

[0047] 120 weaned piglets (Durrito-Changda Sanyuan pigs with an initial weight of about 7.90 kg) with similar health status, breed and weight were selected, and control group 1, control group 2, experimental group 1, experimental group 2, experimental group 3, and experimental group 4 included 20 piglets respectively.

[0048] The control group 1 was fed with a diet (i.e., a complete feed). The control group 2 was fed with a diet (i.e., a complete feed) + chitosan oligosaccharide (the amount of chitosan oligosaccharide added to the complete feed was 300 g / ton).

[0049] Test group 1 was fed with complete feed + the composite ion activator of Example 1 (300 g of animal anti-stress feed additive was added per ton of complete feed), test group 2 was fed with complete feed + the composite ion activator of Example 3 (300 g of animal anti-stress feed additive was added per ton of complete feed), test group 3 was fed with complete feed + the composite ion activator of Example 4 (300 g of animal anti-stress feed additive was added per ton of complete feed), and test group 4 was fed with complete feed + the composite ion activator of Example 5 (300 g of animal anti-stress feed additive was added per ton of complete feed).

[0050] The above feed was fed for 28 days, and the piglet weight, diarrhea rate, feed intake, ileal villus length and crypt depth, serum IgG, and serum IgM were measured. Feed intake, piglet weight, and diarrhea rate were recorded daily. The villus length, crypt depth, serum IgG, and serum IgM in Table 1 are the measurement results at the end of 28 days of feeding, where the villus length and crypt depth are the average values ​​of the measurement results obtained by slaughtering 4 pigs in each group, and serum IgG and serum IgM are the average values ​​of the measurement results of all 20 pigs in each group. During this period, the piglets were managed according to the daily habits of the breeding base.

[0051] Then continue to feed the pigs with the above feed until they are ready for slaughter (marketing), and calculate the lean meat rate after slaughter. Maintain daily lighting time, carry out epidemic prevention and disinfection according to the prescribed procedures, and if sick pigs appear, count the number of pigs and keep them in isolation.

[0052] Table 1 Comparison of technical effects

[0053]

[0054]

[0055] Although one pig in the experimental group 2 had diarrhea, the diarrhea was mild and lasted for a short time (only 1 day). As shown in Table 1, the composite ion activator for animals of the present invention significantly increased the lean meat rate of carcasses, improved the growth performance and immune ability of piglets, improved the intestinal tract, increased the length of villi, and reduced the depth of crypts.

[0056] Embodiment 6, refer to the attached Figures 1 to 11On the basis of Example 1, a device for preparing alkaline ionic liquid for animals is proposed, which is applied to the method for preparing alkaline ionic liquid for animals, including a reactor, a homogenizer, a spray dryer and a mixer. The materials are mixed evenly by the reactor and then put into the homogenizer for homogenization treatment. The homogenized materials are spray-dried by the spray dryer and then compounded by the mixer. The reactor includes a storage tank 1, a cover 2 is installed on the top of the storage tank 1, and the top of the storage tank 1 and the bottom of the cover 2 are both integrally formed with a connecting plate. The two connecting plates are connected by multiple groups of bolts. A gasket 31 is inserted at the bottom end of the cover 2. The gasket 31 is a circular plate with an "L"-shaped cross section. The outer ring diameter of the gasket 31 is equal to the inner ring diameter of the cover 2. A plurality of screws are screwed on the inner ring surface of the gasket 31. The screws penetrate the gasket 31 and are screwed on the inner wall of the cover 2. A sealing gasket 33 is fixed on the outer ring surface of the gasket 31. The sealing gasket 33 is a circular plate with an "L"-shaped cross section. The top plate of the sealing gasket 33 is clamped between the storage tank 1 and the cover 2, a plurality of balls 32 are embedded on the top surface of the gasket 31, a liquid injection valve tube 37 is plugged and fixed on the surface of the storage tank 1, the top of the cover 2 is rotatably connected to the liquid storage cylinder 3, the bottom end of the liquid storage cylinder 3 is fixed with a stirring shaft 4, a bearing 8 is plugged and fixed on the top plate of the cover 2, the inner ring of the bearing 8 is fixed in the opening of the top plate of the cover 2, the inner ring of the bearing 8 is sleeved on the top of the liquid storage cylinder 3, and the liquid storage cylinder 3 is "convex". The top of the liquid storage cylinder 3 is fixed to the bottom of the rotating shaft of the servo motor 5, and the servo motor 5 is fixed to the top surface of the support plate 6. The support plate 6 is a circular plate structure. A plurality of pillars 7 are fixed to the bottom surface of the support plate 6. The bottom ends of the pillars 7 are fixed to the top surface of the cover 2. The top of the liquid storage cylinder 3 is plugged and fixed with a liquid injection pipe 9 and a one-way air intake valve 10. The liquid injection pipe 9 and the one-way air intake valve 10 are symmetrically distributed about the top of the liquid storage cylinder 3. A sealing cap is screwed on the pipe mouth of the liquid injection pipe 9.

[0057] After the turntable 20 is inserted into the bottom end of the cover 2, the pad 31 is inserted into the bottom end of the cover 2, and then the pad 31 is fixed to the bottom end of the cover 2 with the help of screws. At this time, the turntable 20 is limited by the pad 31, and the turntable 20 will not fall off. The cover 2 is overlapped on the storage tank 1, and the connecting plates of the storage tank 1 and the cover 2 are fixed together by bolts. At this time, the top plate of the sealing gasket 33 is clamped between the storage tank 1 and the cover 2 to produce elastic deformation, thereby improving the sealing performance of the storage tank 1 and the cover 2 after the connection; after triggering the switch of the servo motor 5, the servo motor 5 drives the liquid storage cylinder 3 and the stirring shaft 4 to rotate. When purified water needs to be stored in the liquid storage cylinder 3, the sealing cap at the end of the injection tube 9 is unscrewed and removed, and the purified water is injected into the liquid storage cylinder 3, and then the sealing cap is screwed back to seal the end of the injection tube 9.

[0058] The bottom surface of the liquid storage cylinder 3 is provided with a through hole 11, and a pressing block 12 is slidably connected inside the liquid storage cylinder 3. When the pressing block 12 falls on the bottom plate of the liquid storage cylinder 3, the pressing block 12 covers the through hole 11. There are multiple through holes 11, and the multiple through holes 11 are distributed in a circle with the center of the bottom plate of the liquid storage cylinder 3. The pressing block 12 has a hemispherical structure. The bottom surface of the pressing block 12 is provided with a mounting groove 13, and an electric telescopic rod 16 is inserted into the mounting groove 13. The bottom end of the electric telescopic rod 16 is fixed on the top surface of the bottom plate of the liquid storage cylinder 3. The activity of the electric telescopic rod 16 The plug rod is fixed to the top surface of the mounting groove 13, and two embedding grooves 14 are provided inside the mounting groove 13. A battery 15 is fixed inside the embedding groove 14. The battery 15 and the electric telescopic rod 16 are electrically connected through a wire. A rubber pad 17 is fixed to the bottom surface of the pressing block 12. The rubber pad 17 is an annular plate structure. An embedding groove 2 18 is provided on the bottom surface of the pressing block 12. The embedding groove 2 18 is an annular groove. A rubber cover 19 is fixed to the top surface of the embedding groove 2 18. The bottom end of the rubber cover 19 is fixed to the top surface of the bottom plate of the liquid storage cylinder 3.

[0059] When a small amount of purified water inside the storage tank 1 needs to be replenished, the switch of the electric telescopic rod 16 is triggered, and the piston rod of the electric telescopic rod 16 is lifted, lifting the pressure block 12, and the rubber pad 17 at the bottom of the pressure block 12 no longer covers the through hole 11, and the purified water inside the liquid storage cylinder 3 leaks downward from the through hole 11 into the storage tank 1, and at this time the rubber cover 19 is stretched and deformed, and the deformed rubber cover 19 surrounds the outside of the electric telescopic rod 16. After the purified water is replenished, the piston rod of the electric telescopic rod 16 is triggered to retract until the pressure block 12 presses the rubber pad 17 on the bottom plate of the liquid storage cylinder 3. At this time, the through hole 11 is covered by the rubber pad 17, and the one-way air inlet valve 10 is used to replenish the air pressure when the liquid storage cylinder 3 is discharged.

[0060] The cover 2 is internally rotatably connected with a turntable 20, a plurality of material storage troughs 24 are provided on the surface of the turntable 20, a discharge port 25 is provided on the bottom surface of the material storage trough 24, a feeding hopper 30 is plugged and fixed on the top plate of the cover 2, a servo motor 2 34 is fixed on the top plate of the cover 2, a rotating shaft of the servo motor 2 34 passes through the top plate of the cover 2 and is fixed on the top surface of a gear 35, the gear 35 meshes with teeth 36, and the teeth 36 are fixed on the surface of the turntable 20, the turntable 20 is a "convex" shaped circular ring plate, an inner ring surface of the turntable 20 is provided with an inner ring groove 21, and the inner ring groove 21 is a "convex" shaped circular groove, a retaining ring 22 is fixed on the bottom surface of the top plate of the cover 2, the retaining ring 22 is an inverted "convex" shaped circular plate, the inner ring diameter of the retaining ring 22 is larger than the outer diameter of the liquid storage cylinder 3, and the bottom end of the retaining ring 22 is sleeved with a fixed There is a bearing 23, the outer ring of the bearing 23 is inserted into the top notch of the inner ring groove 21, and a plurality of teeth 36 are fixed on the outer ring surface of the inner ring groove 21. A plurality of servo motors 34 are provided, and the plurality of servo motors 34 are arranged and distributed at equal distances along the top edge of the cover 2; a material guide cover 29 is inserted at the top of the storage trough 24, and the material guide cover 29 is an inverted table-shaped ring plate, and the top plate of the material guide cover 29 is fixed to the top surface of the turntable 20 by screws, and a sealing block 26 is inserted into the inside of the discharge port 25, and the sealing block 26 is fixed to the top surface of the traction plate 27, and a plurality of electric telescopic rods 28 are fixed inside the inner ring groove 21, and the electric telescopic rods 28 correspond to the traction plates 27 one by one, and the piston rod of the electric telescopic rod 28 passes through the bottom plate of the turntable 20 and is fixed to the top surface of the traction plate 27.

[0061] Potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, and chitosan oligosaccharides are stored in eight storage troughs 24 respectively. When the cover 2 is installed on the top of the storage tank 1, when it is necessary to feed materials into the storage trough 24, the cover plate on the top of the feeding hopper 30 is opened, and the materials are fed into the guide cover 29 through the feeding hopper 30. The guide cover 29 guides the materials into the corresponding storage troughs 24. After one group of materials is fed, the switch of the servo motor 2 34 is triggered, and the servo motor 2 34 drives the turntable 20 to rotate until the next group of storage troughs 24 is under the feeding hopper 30, and then another group of materials is fed into the corresponding storage troughs 24, and potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, and chitosan oligosaccharides are stored in the eight storage troughs 24 respectively.

[0062] When it is necessary to put multiple materials into the purified water inside the storage tank 1 in sequence for mixing, the corresponding electric telescopic rod 28 is triggered. After the piston rod of the electric telescopic rod 28 is extended, the traction plate 27 is pushed downward, and the traction plate 27 drives the sealing block 26 to be withdrawn from the discharge port 25, and the materials inside the storage tank 24 are scattered downward. In order to avoid concentrated feeding, the switch of the servo motor 234 can be triggered during the feeding process at the discharge port 25 to drive the gear 35 to engage the turntable 20 to rotate, so as to achieve the material spreading in a circular trajectory; in order to facilitate the identification of the materials stored in the storage tank 24, a label 40 is fixed on the top surface of the turntable 20, and the label 40 records the material information loaded in the corresponding storage tank 24, and an observation port 38 is opened on the top surface of the cover 2, and a transparent window plate 39 is fixed inside the observation port 38, and the information recorded on the surface of the label 40 can be viewed through the transparent window plate 39.

[0063] The use process of the alkaline ionic liquid preparation device for animals is as follows:

[0064] Insert the turntable 20 into the bottom end of the cover 2. Insert the pad 31 into the bottom end of the cover 2, and use screws to fix the pad 31 on the cover 2 to ensure that the turntable 20 is limited. Overlap the cover 2 onto the storage tank 1, and fix the connecting plates of the two together with bolts. Ensure that the sealing gasket 33 is clamped between the storage tank 1 and the cover 2, and elastic deformation is generated to improve the sealing. The top of the liquid storage cylinder 3 is fixed on the rotating shaft of the servo motor 5, and ensure that the liquid storage cylinder 3 is firmly fixed on the cover 2 through the bearing 8. Connect the injection tube 9 and the one-way air inlet valve 10 to the liquid storage cylinder 3, and install the sealing cap at the mouth of the injection tube 9. Screw and remove the sealing cap at the end of the injection tube 9. Inject purified water into the liquid storage cylinder 3. Screw the sealing cap back to seal the end of the injection tube 9. Open the cover of the hopper 30. Potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, and chitosan oligosaccharide are placed in the corresponding material guide cover 29 through the feeding hopper 30 in order, and then introduced into the storage tank 24. After each group of materials is put in, the turntable 20 is driven to rotate by the servo motor 2 34, so that the next group of storage tanks 24 are aligned with the feeding hopper 30, and the next group of materials is continued to be put in. Trigger the servo motor 1 5 to drive the liquid storage cylinder 3 and the stirring shaft 4 to rotate so that the purified water is evenly distributed in the storage tank 1. When a small amount of purified water is needed, the pressing block 12 is lifted by the electric telescopic rod 16, so that the purified water leaks from the through hole 11 into the storage tank 1. After completion, the electric telescopic rod 16 retracts and the pressing block 12 covers the through hole 11. It should be noted that the pre-installed purified water inside the storage tank 1 is injected into the storage tank 1 through the injection valve tube 37. The corresponding electric telescopic rod 28 is triggered in sequence to pull the traction plate 27 and the sealing block 26 away from the discharge port 25, so that the material in the storage tank 24 falls into the purified water. In order to spread the material evenly, the servo motor 234 can be triggered during the unloading process to rotate the turntable 20 in a circular trajectory. The evenly mixed material is taken out of the reactor and put into the homogenizer for homogenization. The homogenized material is spray-dried by a spray dryer. Finally, the formula is compounded by a mixer to complete the preparation of the alkaline ionic liquid. Through the transparent window plate 39 on the top surface of the cover 2, the material information recorded on the label 40 is observed to ensure that the material is correctly put.

[0065] Example 7, based on Example 1, proposes an application of an alkaline ionic liquid for animals in increasing the villus height and crypt depth of the jejunum and ileum and the ratio of villus length to crypt depth, and 200-500 g / ton of alkaline ionic liquid for animals is added to animal feed.

[0066] Example 8, based on Example 1, proposes an application of alkaline ionic liquid for animals in relieving stress, increasing feed intake or reducing feed-to-meat ratio, and 200-500 g / ton of alkaline ionic liquid for animals is added to animal feed.

[0067] Example 9, based on Example 1, proposes an application of alkaline ionic liquid for animals to increase carcass lean meat rate, anti-oxidation, reduce drip loss, improve meat color, and increase livestock and poultry slaughter rate. 200-500 g / ton of alkaline ionic liquid for animals is added to animal feed.

[0068] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A method for preparing an alkaline ionic liquid for animals, characterized in that: The alkaline ionic liquid comprises: potassium bicarbonate, potassium carbonate, sodium bicarbonate, sodium carbonate, germanium dioxide, sodium selenite, chromium oxide, chitosan oligosaccharide and purified water, and its specific composition content is: 30-50 parts of potassium bicarbonate, 500-1200 parts of potassium carbonate, 200-800 parts of sodium bicarbonate, 40-80 parts of sodium carbonate, 0.5-12 parts of germanium dioxide, 0.4-3 parts of sodium selenite, 0.2-2 parts of chromium oxide, 300-800 parts of chitosan oligosaccharide and 600-1500 parts of purified water; the parts are parts by weight; The preparation method comprises the following steps: Each component is gradually dissolved in 600-1450 parts of purified water at 55°C or above, stirred in a reaction kettle for 1-2 hours to fully mix, and placed at 32-38°C for 30-35 hours to fully react with the complex, and then used; The material is fully homogenized through the homogenization process, and the material is homogenized by the homogenizer. The plunger pump sucks the original material at a low speed of 0.25 to 0.5 m / s, and the pressure of the homogenization system is adjusted through the pressure regulating device connected to the homogenization valve; The dry powder core material is obtained by spray drying, and then compounded to include the following components by weight: 2-8 parts of sodium citrate, 0.5-2 parts of yeast selenium, 0.5-1 parts of methionine chromium, and 0.5-1 parts of nicotinate chromium.

2. An alkaline ionic liquid preparation device for animals, applied to the alkaline ionic liquid preparation method for animals described in claim (1), comprising a reactor, a homogenizer, a spray dryer and a mixer, wherein the materials are mixed evenly in the reactor and then put into the homogenizer for homogenization treatment, the homogenized materials are spray dried by the spray dryer, and then compounded by the mixer, characterized in that: The reactor comprises a material storage tank (1), a sealing cover (2) is installed on the top of the material storage tank (1), the top of the sealing cover (2) is rotatably connected to a liquid storage cylinder (3), the bottom end of the liquid storage cylinder (3) is fixed with a stirring shaft (4), a through hole (11) is opened on the bottom surface of the liquid storage cylinder (3), a pressing block (12) is slidably connected inside the liquid storage cylinder (3), when the pressing block (12) falls on the bottom plate of the liquid storage cylinder (3), the pressing block (12) covers the through hole (11), and the inside of the sealing cover (2) is rotatably connected to a turntable ( 20), a plurality of material storage troughs (24) are provided on the surface of the turntable (20), a discharge port (25) is provided on the bottom surface of the material storage trough (24), a feeding hopper (30) is plugged and fixed on the top plate of the cover (2), a servo motor 2 (34) is fixed on the top plate of the cover (2), a rotating shaft of the servo motor 2 (34) passes through the top plate of the cover (2) and is fixed on the top surface of a gear (35), the gear (35) meshes with teeth (36), and the teeth (36) are fixed on the surface of the turntable (20).

3. The alkaline ionic liquid preparation device for animals according to claim 2, characterized in that: The top end of the storage tank (1) and the bottom end of the cover (2) are both integrally formed with a connecting plate, and the two connecting plates are connected by a plurality of sets of bolts. A pad (31) is inserted into the bottom end of the cover (2), and the pad (31) is a circular ring plate with an "L"-shaped cross section. The outer ring diameter of the pad (31) is equal to the inner ring diameter of the cover (2). The inner ring surface of the pad (31) is screwed with a plurality of screws, and the screws penetrate the pad (31) and are screwed to the inner wall of the cover (2). A sealing gasket (33) is sleeved and fixed on the outer ring surface of the pad (31), and the sealing gasket (33) is a circular ring plate with an "L"-shaped cross section. The top plate of the sealing gasket (33) is clamped between the storage tank (1) and the cover (2), and a plurality of balls (32) are embedded on the top surface of the pad (31). A liquid injection valve tube (37) is inserted and fixed to the surface of the storage tank (1).

4. The alkaline ionic liquid preparation device for animals according to claim 2, characterized in that: A bearing (8) is inserted and fixed on the top plate of the cover (2); the inner ring of the bearing (8) is fixed in the opening of the top plate of the cover (2); the inner ring of the bearing (8) is sleeved on the top of the liquid storage cylinder (3); the liquid storage cylinder (3) is a "convex"-shaped cylindrical structure; the top of the liquid storage cylinder (3) is fixed to the bottom end of the rotating shaft of the servo motor (5); the servo motor (5) is fixed to the top surface of the support plate (6); the support plate (6) is a circular ring plate structure; a plurality of pillars (7) are fixed on the bottom surface of the support plate (6); the bottom ends of the pillars (7) are fixed to the top surface of the cover (2); a liquid injection pipe (9) and a one-way air intake valve (10) are inserted and fixed on the top of the liquid storage cylinder (3); the liquid injection pipe (9) and the one-way air intake valve (10) are symmetrically distributed about the top of the liquid storage cylinder (3); a sealing cap is sleeved and screwed at the pipe mouth of the liquid injection pipe (9).

5. The alkaline ionic liquid preparation device for animals according to claim 2, characterized in that: The through holes (11) are provided in plurality, and the plurality of through holes (11) are distributed in a circle with the bottom plate of the liquid storage cylinder (3) as the center. The pressing block (12) is in a hemispherical structure. The bottom surface of the pressing block (12) is provided with a mounting groove (13). An electric telescopic rod (16) is inserted into the inside of the mounting groove (13). The bottom end of the electric telescopic rod (16) is fixed to the top surface of the bottom plate of the liquid storage cylinder (3). The piston rod of the electric telescopic rod (16) is fixed to the top surface of the mounting groove (13). The inside of the mounting groove (13) is provided with two embedded grooves. A storage battery (15) is fixed inside the embedding groove (14), and the storage battery (15) and the electric telescopic rod (16) are electrically connected through a wire. A rubber pad (17) is fixed on the bottom surface of the pressing block (12), and the rubber pad (17) is in an annular plate structure. A embedding groove (18) is opened on the bottom surface of the pressing block (12), and the embedding groove (18) is in an annular groove. A rubber cover (19) is fixed on the top surface of the embedding groove (18), and the bottom end of the rubber cover (19) is fixed on the top surface of the bottom plate of the liquid storage cylinder (3).

6. The device for preparing alkaline ionic liquid for animals according to claim 2, characterized in that: The rotating disk (20) is in the form of a convex circular plate. An inner ring surface of the rotating disk (20) is provided with an inner ring groove (21). The inner ring groove (21) is in the form of a convex circular groove. A retaining ring (22) is fixed to the bottom surface of the top plate of the cover (2). The retaining ring (22) is in the form of an inverted convex circular plate. The inner ring diameter of the retaining ring (22) is larger than the outer diameter of the liquid storage cylinder (3). A second bearing (23) is sleeved and fixed to the bottom end of the retaining ring (22). The outer ring of the second bearing (23) is inserted into the top notch of the inner ring groove (21). A plurality of teeth (36) are fixed to the outer ring surface of the inner ring groove (21). A plurality of servo motors (34) are provided. The plurality of servo motors (34) are arranged and distributed at equal distances along the edge of the top surface of the cover (2).

7. The device for preparing alkaline ionic liquid for animals according to claim 6, characterized in that: A material guide cover (29) is inserted at the top of the material storage trough (24), and the material guide cover (29) is an inverted platform-shaped ring plate. The top plate of the material guide cover (29) is fixed to the top surface of the turntable (20) by screws. A sealing block (26) is inserted inside the discharge port (25), and the sealing block (26) is fixed to the top surface of the traction plate (27). A plurality of electric telescopic rods (28) are fixed inside the inner ring groove (21), and the electric telescopic rods (28) and the traction plates (27) correspond to each other one by one. The piston rods of the electric telescopic rods (28) penetrate the bottom plate of the turntable (20) and are fixed to the top surface of the traction plate (27).

8. Use of the alkaline ionic liquid for animals as claimed in claim 1 for increasing the villus height and crypt depth and the ratio of villus length to crypt depth in the jejunum and ileum, characterized in that: Add 200-500 g / ton of alkaline ionic liquid for animals to animal feed.

9. A use of the alkaline ionic liquid for animals as claimed in claim 1 for relieving stress, increasing feed intake or reducing feed-to-meat ratio, characterized in that: Add 200-500 g / ton of alkaline ionic liquid for animals to animal feed.

10. An application of the alkaline ionic liquid for animals as claimed in claim 1 to increase carcass lean meat rate, resist oxidation, reduce drip loss, improve meat color, and increase livestock and poultry slaughter rate, characterized in that: Add 200-500 g / ton of alkaline ionic liquid for animals to animal feed.

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