Crystal growth data recording device, recording method thereof, storage medium and equipment

Abstract

The invention provides a recording device and recording method of crystal growth data, a storage medium and equipment. The recording device for the crystal growth data comprises crystal synthesis method experiment input and storage mechanisms, and each crystal synthesis method experiment input and storage mechanism comprises a crystal growth experiment process input and storage module and a crystal growth experiment result and characterization input and storage module. According to the recording device, the recording method thereof, the storage medium and the equipment, comprehensive standard experimental data of crystal material growth and performance characterization can be obtained, standard recording data can be unified, and scientific research efficiency is improved.

Description

Technical Field

[0001] The present invention belongs to the field of crystal material databases, and particularly relates to a recording device for crystal growth data, a recording method thereof, a storage medium, and a device. Background Art

[0002] Existing crystal material databases can provide some properties of materials, generally only including material structural formulas, space groups, and xrd data, and a small number provide preparation methods of materials. The preparation methods generally only include the ratio of raw materials, the containers used, and the preparation temperature. By adopting the preparation methods provided by the databases, some materials cannot be reproduced, and their authenticity needs to be questioned; the information recorded in each database is not comprehensive enough, and the data recording formats are all different. Often, multiple databases need to be used, which is not conducive to obtaining information.

[0003] How to obtain a standardized experimental data recording method for comprehensive crystal material growth and performance characterization has become a difficult problem to be solved urgently at present. Summary of the Invention

[0004] Therefore, the purpose of the present invention is to overcome the defects in the prior art and provide a recording device for crystal growth data, a recording method thereof, a storage medium, and a device. The recording device and recording method of the present invention can obtain standardized experimental data for comprehensive crystal material growth and performance characterization.

[0005] Before elaborating on the content of the present invention, the terms used herein are defined as follows:

[0006] The term "xrd" refers to: X-ray diffractometer, with the full English name X-ray diffractometer.

[0007] The term "eds" refers to: Energy Dispersive Spectrometer, which is used to analyze the types and contents of elemental components in the microregions of materials.

[0008] To achieve the above purpose, the first aspect of the present invention provides a recording device for crystal growth data, and the recording device includes: one or more crystal synthesis method experiment input and storage mechanisms, and each crystal synthesis method experiment input and storage mechanism includes:

[0009] A crystal growth experiment process input and storage module for inputting and storing data of the growth experiment process; and

[0010] A crystal growth experiment result and characterization input and storage module for inputting and storing growth experiment results and crystal characterization data;

[0011] Preferably, the crystal growth experiment result and characterization input and storage module includes: a crystal growth experiment result recording module and a characterization input and storage module.

[0012] According to the recording device of the first aspect of the present invention, wherein,

[0013] The experimental input and storage mechanism for the crystal synthesis method is selected from one or more of the following: a flux method crystal synthesis experimental input and storage mechanism, a Bridgman method crystal synthesis experimental input and storage mechanism, a solid-state reaction crystal synthesis experimental input and storage mechanism, a chemical vapor transport method experimental input and storage mechanism, a melting method crystal synthesis experimental input and storage mechanism, a high-temperature method crystal synthesis experimental input and storage mechanism, preferably selected from one or more of the following: a flux method crystal synthesis experimental input and storage mechanism, a solid-state reaction crystal synthesis experimental input and storage mechanism, a chemical vapor transport method experimental input and storage mechanism, a melting method crystal synthesis experimental input and storage mechanism, a high-temperature method crystal synthesis experimental input and storage mechanism; and / or

[0014] The crystal growth experimental process input and storage module includes data storage units selected from one or more of the following: an experimental scheme data storage unit, an experimental condition data storage unit, a starting material data storage unit, a heating and temperature reaction data storage unit, preferably including data storage units selected from one or more of the following: an experimental condition data storage unit, a starting material data storage unit, a heating and temperature reaction data storage unit.

[0015] According to the recording device of the first aspect of the present invention, wherein,

[0016] The experimental scheme data storage unit is used to store data including one or more of the following: the starting time of crystal growth, the ending time of crystal growth, the target product, the reaction method, the sample number, the flux, preferably including data selected from one or more of the following: the starting time of crystal growth, the ending time of crystal growth, the target product, the reaction method, the sample number, and more preferably including data selected from one or more of the following: the starting time of crystal growth, the target product, the reaction method, the sample number;

[0017] The experimental condition data storage unit is used to store data including one or more of the following: the crucible type, the inner diameter of the crucible, the depth of the crucible, the reaction atmosphere, whether to grind, whether to press tablets, whether to seal tantalum tubes, whether to seal quartz tubes, the cooling method, the furnace number, preferably including data selected from one or more of the following: the crucible type, the inner diameter of the crucible, the depth of the crucible, the reaction atmosphere, whether to seal tantalum tubes, whether to seal quartz tubes, the cooling method, the furnace number, and more preferably including data selected from one or more of the following: the crucible type, the inner diameter of the crucible, the reaction atmosphere, the cooling method, the furnace number;

[0018] The starting material data storage unit is used to store data including one or more selected from the following: material type, proportioning, actual mass, material form, preferably including data selected from one or more of the following: material type, proportioning, actual mass; and / or

[0019] The heating and temperature reaction data storage unit is used to store data including one or more selected from the following: furnace temperature, holding time in each temperature range, total reaction time, preferably including: furnace temperature and / or holding time in each temperature range.

[0020] The recording device according to the first aspect of the present invention, wherein the crystal growth experiment result recording module is used to record data including one or more selected from the following: product form, product photo, xrd test data, eds test data, eds test result, whether it is the target product, preferably including data selected from one or more of the following: product photo, xrd test data, eds test data, eds test result, whether it is the target product;

[0021] Preferably, the data recorded by the crystal growth experiment result recording module further includes standard external experiment data.

[0022] The recording device according to the first aspect of the present invention, wherein the characterization input storage module includes data storage units selected from one or more of the following: structure characterization data storage unit, component characterization data storage unit, magnetic characterization data storage unit, transport characterization data storage unit, specific heat characterization data storage unit, preferably including data storage units selected from one or more of the following: structure characterization data storage unit, component characterization data storage unit, transport characterization data storage unit, specific heat characterization data storage unit, more preferably including data storage units selected from one or more of the following: structure characterization data storage unit, component characterization data storage unit, magnetic characterization data storage unit, transport characterization data storage unit.

[0023] The recording device according to the first aspect of the present invention, wherein,

[0024] The structure characterization data storage unit is used to store data including one or more selected from the following: sample structure characterization photo, sample powder xrd data, sample single crystal xrd data, sample crystal information data; the data stored by the structure characterization data storage unit preferably includes structure characterization remarks;

[0025] The component characterization data storage unit is used to store: sample component characterization photo and / or sample component eds data; the data stored by the component characterization data storage unit preferably includes component characterization remarks;

[0026] The magnetic characterization data storage unit is used to store data including one or more selected from the following: sample magnetic characterization photos, sample magnetic characterization quality, sample magnetic characterization test data; the data stored by the magnetic characterization data storage unit preferably includes magnetic characterization remarks;

[0027] The transport characterization data storage unit is used to store: sample transport characterization photos and / or sample transport characterization test data; the data stored by the transport characterization data storage unit preferably includes transport characterization remarks; and / or

[0028] The specific heat characterization data storage unit is used to store data including one or more selected from the following: sample specific heat characterization photos, sample specific heat characterization quality, sample specific heat characterization test data; the data stored by the specific heat characterization data storage unit preferably includes specific heat characterization remarks.

[0029] The second aspect of the present invention provides a method for recording standardized crystal growth data, and the recording method includes using the recording device described in the first aspect;

[0030] Preferably, the recording method includes the following steps:

[0031] 1) According to the adopted crystal synthesis method, establish one or more experimental input and storage institutions for the crystal synthesis method. In each experimental input and storage institution for the crystal synthesis method, input and store crystal synthesis method data, and establish the input and storage module for the crystal growth experimental process and the input and storage module for the crystal growth experimental results and characterization;

[0032] 2) In the input and storage module for the crystal growth experimental process, input and store the data of the growth experimental process; and

[0033] 3) In the input and storage module for the crystal growth experimental results and characterization, input and store the data of the growth experimental results. When the data of the growth experimental results meets the data of the target product, characterize the target product and record the crystal characterization data; when the data of the growth experimental results does not meet the data of the target product, terminate the experiment.

[0034] According to the recording method of the second aspect of the present invention, wherein, after step 3) of the recording method, it further includes:

[0035] 4) Correlate the crystal synthesis method data input and stored in step 1) with the crystal characterization data input and stored in step 3).

[0036] The third aspect of the present invention provides a computer-readable storage medium, characterized in that the computer-readable storage medium includes: one or more computer programs;

[0037] When the computer program is executed by a processor, it constructs the recording device described in the first aspect and / or implements the recording method described in the second aspect.

[0038] A fourth aspect of the present invention provides an electronic device, which includes a memory and a processor, wherein:

[0039] The memory is used for storing a computer program; and

[0040] The processor includes the recording device described in the first aspect. When the processor is used to execute the computer program stored on the memory, it implements the recording method described in the second aspect.

[0041] According to a preferred embodiment of the present invention, the method for recording standardized crystal growth data includes:

[0042] Establish different categories of experimental record books according to the crystal synthesis method to realize the classified storage of experimental data, which is convenient for querying and managing experimental data.

[0043] By using different standard modules to electronically input and store crystal growth experimental data, the standardized input of experimental data is realized.

[0044] Experimental method: Record the start and end time of the experiment, the target product, the reaction method, and the sample number.

[0045] Experimental conditions: Record the crucible type, inner diameter, length, reaction atmosphere, whether it is ground, whether it is pressed into tablets, whether it is sealed with tantalum tubes, whether it is sealed with quartz tubes, the cooling method, and the furnace number.

[0046] Starting materials: Record the material type, ratio, actual mass, and material form.

[0047] Heating program: Record the change of reaction temperature.

[0048] Experimental results: Record the product form, product photos, xrd test data, eds test data, eds test results, whether it is the target product, and remarks can be added at the result to supplement experimental conditions outside the standard.

[0049] Structure characterization: Record sample photos, powder xrd data, single crystal xrd data, and crystal information data, and remarks can be made for explanation.

[0050] Component characterization: Record photos of the test samples and eds data.

[0051] Magnetic characterization: Record photos of the test samples, sample mass, and test data.

[0052] Transport characterization: Record photos of the test samples and test data.

[0053] Specific heat characterization: Record the photos, mass, and test data of the samples.

[0054] Then, classify and store the characterized experimental data according to the material category and associate it with the growth data.

[0055] The present invention is applicable to the material preparation and performance characterization processes of various scientific research institutions, enterprises, and institutions. Recording experimental data according to unified standards is beneficial for communication between units and helps to promote scientific research progress.

[0056] Compared with the prior art, the recording device, recording method, storage medium, and equipment for crystal growth data of the present invention may have, but are not limited to, the following beneficial effects:

[0057] 1. The recording device and recording method of the present invention can obtain comprehensive standardized experimental data on crystal material growth and performance characterization.

[0058] 2. The recording device and recording method of the present invention can record data according to unified standards, improving scientific research efficiency.

[0059] 3. The recording device and recording method of the present invention can make each set of characterization data correspond to a specific experiment, improving authenticity and reliability. BRIEF DESCRIPTION OF THE DRAWINGS

[0060] Hereinafter, the embodiments of the present invention will be described in detail with reference to the drawings, wherein:

[0061] Figure 1 Shows a schematic diagram of each crystal synthesis method experiment input and storage mechanism in the recording device for crystal growth data of the present invention.

[0062] Figure 2 Shows a flowchart of the standardized recording method for crystal growth data of the present invention.

[0063] Figure 3 Shows a schematic diagram of the recording device for crystal growth data of the present invention. DETAILED DESCRIPTION OF THE INVENTION

[0064] The present invention will be further described below through specific embodiments. However, it should be understood that these embodiments are only used for more detailed and specific descriptions and should not be construed as limiting the present invention in any form.

[0065] This part generally describes the materials and test methods used in the experiments of the present invention. Although many materials and operation methods used to achieve the purpose of the present invention are well known in the art, the present invention still describes them in as much detail as possible here. Those skilled in the art are aware that, in the context, if not otherwise specified, the materials and operation methods used in the present invention are well known in the art.

[0066] Example 1

[0067] This embodiment is an exemplary illustration of the recording device and method for the standardized crystal growth data of the present invention.

[0068] The recording device for the standardized crystal growth data of this embodiment includes the following crystal synthesis method experiment input and storage mechanisms. The crystal synthesis method experiment input and storage mechanisms are divided according to different crystal synthesis methods into: flux method crystal synthesis experiment input and storage mechanism, Bridgman method crystal synthesis experiment input and storage mechanism, solid-state reaction crystal synthesis experiment input and storage mechanism, chemical vapor transport method experiment input and storage mechanism, melting method crystal synthesis experiment input and storage mechanism, high-temperature method crystal synthesis experiment input and storage mechanism. Among them, each crystal synthesis method experiment input and storage mechanism includes:

[0069] A crystal growth experiment process input and storage module for inputting and storing the data of the growth experiment process; and

[0070] A crystal growth experiment result and characterization input and storage module for inputting and storing the growth experiment results and crystal characterization data;

[0071] Among them, the crystal growth experiment result and characterization input and storage module includes: a crystal growth experiment result recording module and a characterization input and storage module. The characterization input and storage module is only used when the target product is successfully prepared.

[0072] The crystal growth experiment process input and storage module includes: an experimental scheme data storage unit, an experimental condition data storage unit, a starting material data storage unit, a heating and temperature reaction data storage unit. The experimental scheme data storage unit is used to store the following data: crystal growth start time, crystal growth end time, target product, reaction method, sample number; the experimental condition data storage unit is used to store the following data: crucible type, crucible inner diameter, crucible depth, reaction atmosphere, whether to grind, whether to press tablets, whether to seal tantalum tubes, whether to seal quartz tubes, cooling method, furnace number; the starting material data storage unit is used to store the following data: material type, ratio, actual mass, material form; the heating and temperature reaction data storage unit is used to store the following data: furnace temperature, holding time in each temperature range, total reaction time.

[0073] The crystal growth experiment result and characterization input and storage module includes: a crystal growth experiment result recording module and a characterization input and storage module. The crystal growth experiment result recording module also includes standard external experiment data.

[0074] The crystal growth experiment result recording module is used to store the following data: product form, product photo, xrd test data, eds test data, eds test result, and whether it is the target product.

[0075] The characterization input and storage module includes the following data storage units: structure characterization data storage unit, component characterization data storage unit, magnetic characterization data storage unit, transport characterization data storage unit, and specific heat characterization data storage unit.

[0076] The structure characterization data storage unit is used to store the following data: sample structure characterization photo, sample powder xrd data, sample single crystal xrd data, sample crystal information data, and structure characterization remarks can also be added.

[0077] The component characterization data storage unit is used to store the following data: sample component characterization photo, sample characterization eds data, and component characterization remarks can also be added.

[0078] The magnetic characterization data storage unit is used to store the following data: sample magnetic characterization photo, sample magnetic characterization mass, sample magnetic characterization test data, and magnetic characterization remarks can also be added.

[0079] The transport characterization data storage unit is used to store the following data: sample transport characterization photo, sample transport characterization test data, and transport characterization remarks can also be added.

[0080] The specific heat characterization data storage unit is used to store the following data: sample specific heat characterization photo, sample specific heat characterization mass, sample specific heat characterization test data, and specific heat characterization remarks can also be added.

[0081] The method for recording standardized crystal growth data of the present invention includes:

[0082] Establish experimental input and storage mechanisms for different categories of crystal synthesis methods according to the crystal synthesis method to achieve classified storage of experimental data, facilitating query and management of experimental data.

[0083] Through the use of different standard modules for electronic input and storage of crystal growth experimental data, standardized input of experimental data is achieved.

[0084] Experimental method: Record the start and end time of the experiment, target product, reaction method, and sample number.

[0085] Experimental conditions: Record the crucible type, crucible inner diameter, crucible depth, reaction atmosphere, whether to grind, whether to press tablets, whether to seal tantalum tubes, whether to seal quartz tubes, cooling method, and furnace number.

[0086] Starting materials: Record the material type, ratio, actual mass, and material form.

[0087] Heating program: Record the changes in reaction temperature.

[0088] Experimental results: record the product form, product photos, XRD test data, EDS test data, EDS test results, whether it is the target product, and add notes to the results to supplement the experimental conditions outside the standard. If the obtained product has a standard diffraction card, the product XRD data can be compared with the standard diffraction card to know whether the obtained product is the target product. If the obtained product does not have a standard diffraction card, the EDS test can be used to know whether it is the target product based on the element ratio of the product.

[0089] Structural characterization: record sample photos, powder XRD data, single crystal XRD data, crystal information data, and make notes.

[0090] Component characterization: record photos and eds data of test samples.

[0091] Magnetic characterization: record photos of test samples, sample quality, test data.

[0092] Transport characterization: record photos of test samples and test data.

[0093] Specific heat characterization: record the sample’s photo, quality, and test data.

[0094] The characterized experimental data are then classified and stored according to the material category and associated with the growth data. The recording method is generally manual input, and all data records are uploaded by uploading the test data.

[0095] Example 2

[0096] This embodiment is an exemplary description of the effects of the apparatus and method for recording standardized crystal growth data of the present invention.

[0097] This embodiment takes the flux method as an example. This embodiment will provide a more detailed description of the input contents involved, and the description order refers to Example 1. Some general descriptions made in this embodiment will not be repeated in subsequent embodiments unless there are special circumstances.

[0098] Select the flux method crystal synthesis experiment entry and storage organization, and create a new experimental project in the organization. Including: naming (select the name of the target product to name the project, which needs to be filled in manually), project establishment time, number (need to be filled in manually so that it can be changed at any time), remarks (such as whether the target product is obtained, etc., which needs to be filled in manually so that information can be obtained when browsing the experimental project).

[0099] 1. Enter the experimental protocol in the experimental protocol data storage unit, including: enter the starting time of crystal growth in the format of year / month / day. Generally, the time when this experimental project is established is the default starting time, which can be modified if different. After crystal growth is completed, the ending time of crystal growth can be entered. The reaction method is the flux method, and the name of the target product is the same as the named product. Sample number, number the product after successfully obtaining the target product. Finally, enter the flux used.

[0100] 2. Enter the experimental conditions in the experimental condition data storage unit, including the type of crucible, the inner diameter of the crucible, and the depth of the crucible. The reaction atmosphere is defaulted to vacuum, which can be changed if there are other atmosphere requirements. The cooling method is defaulted to furnace cooling, which can be changed in other cases. Enter the furnace number. Generally, it is defaulted to seal the quartz tube. Whether to grind, press tablets, and seal tantalum tubes are all defaulted to no, which can be changed according to the actual situation in other cases.

[0101] 3. Enter in the starting material data storage unit: starting materials, types, ratios, and material forms.

[0102] 4. Enter the heating and temperature reaction related data in the heating and temperature reaction data storage unit: record the furnace temperature, the holding time in each temperature range, and the total reaction time to obtain the change of the reaction temperature.

[0103] After obtaining the product, it is necessary to perform an XRD test on the obtained product and compare it with the standard spectrum to determine whether the target product is successfully obtained. If it cannot be judged only by the XRD test, then perform an EDS test for auxiliary judgment. If it is judged that the target product is not obtained, the experiment is terminated. If the target product is successfully obtained, continue to record.

[0104] Enter the result recording data in the crystal growth experiment result recording module, including: product form, product photo, XRD test data, EDS test data, EDS test result, and whether it is the target product.

[0105] In the characterization entry storage module, enter the characterization data according to the structure characterization data storage unit, component characterization data storage unit, magnetic characterization data storage unit, transport characterization data storage unit, and specific heat characterization data storage unit respectively.

[0106] Example 3

[0107] This embodiment is an exemplary illustration of the effect of the recording device and method for the standardized crystal growth data of the present invention.

[0108] This embodiment takes the solid-phase reaction method as an example. This embodiment and subsequent embodiments only provide the differences from Embodiment 2, and the same content will not be repeated.

[0109] Select the solid-phase reaction crystal synthesis input and storage mechanism. In terms of the experimental scheme, no cosolvent is used in the solid-phase reaction, so there is no need to input this item.

[0110] Example 4

[0111] This embodiment is an exemplary illustration of the effect of the recording device and method for the standardized crystal growth data of the present invention.

[0112] This embodiment takes the chemical vapor transport method as an example. This embodiment and subsequent embodiments only provide the differences from Embodiment 2, and the same content will not be repeated.

[0113] Select the chemical vapor transport experiment input and storage mechanism. In this method, the cosolvent item is changed to a transport agent. According to the conditions of the vapor transport method, this method must seal the quartz tube. Since there are high and low temperature zones, the temperature changes in the two temperature zones are recorded at the reaction temperature.

[0114] Example 5

[0115] This embodiment is an exemplary illustration of the effect of the recording device and method for the standardized crystal growth data of the present invention.

[0116] This embodiment takes the melting method as an example. This embodiment and subsequent embodiments only provide the differences from Embodiment 2, and the same content will not be repeated.

[0117] Select the melting method crystal synthesis input and storage mechanism. This method has no cosolvent and does not involve any experimental conditions in Embodiment 2. The melting method does not involve the reaction temperature. The melting method involves the arc voltage, which is equivalent to the reaction temperature. The arc voltage is recorded to indirectly record the reaction temperature. Generally, only the voltage used during continuous melting is recorded, and the voltage change is not recorded.

[0118] Example 6

[0119] This embodiment is an exemplary illustration of the effect of the recording device and method for the standardized crystal growth data of the present invention.

[0120] This embodiment takes the high-temperature method as an example. This embodiment and subsequent embodiments only provide the differences from Embodiment 2, and the same content will not be repeated.

[0121] Select the high-temperature method crystal synthesis input and storage mechanism. This method uses a carbon crucible. This method only involves grinding and tablet pressing in the experimental conditions. Since the specific temperature inside the experimental equipment cannot be known, the reaction temperature is indirectly recorded by recording the heating power. The power and time changes are recorded.

[0122] Although the effects of some embodiments are shown above, those skilled in the art should understand that according to the concept of the present invention, the foregoing other embodiments without specifically showing the effects or other technical solutions of the present invention not shown in the embodiments can also achieve the following technical effects stated in the summary of the invention that are equivalent to those of the embodiments:

[0123] 1. The recording device and recording method of the present invention can obtain standardized experimental data for comprehensive crystal material growth and performance characterization.

[0124] 2. The recording device and recording method of the present invention can unify the standard for recording data and improve scientific research efficiency.

[0125] 3. The recording device and recording method of the present invention can make each group of characterization data correspond to a specific experiment, improving the authenticity and reliability.

[0126] Although the present invention has been described to a certain extent, obviously, appropriate changes can be made to various conditions without departing from the spirit and scope of the present invention. It can be understood that the present invention is not limited to the described embodiments, but falls within the scope of the claims, which includes equivalent replacements for each factor described.

Claims

1. A crystal growth data recording device, characterized in that: The recording device comprises: one or more crystal synthesis method experimental recording and storage mechanisms, each of which comprises: A crystal growth experiment process recording and storage module for recording and storing growth experiment process data; and A crystal growth experiment result and characterization recording and storage module for recording and storing growth experiment results and crystal characterization data; Preferably, the crystal growth experiment result and characterization entry storage module comprises: a crystal growth experiment result recording module and a characterization entry storage module.

2. The recording device according to claim 1, characterized in that: The crystal synthesis method experiment recording and storage mechanism is selected from one or more of the following: a flux method crystal synthesis experiment recording and storage mechanism, a Bridgman method crystal synthesis experiment recording and storage mechanism, a solid phase reaction crystal synthesis experiment recording and storage mechanism, a chemical vapor transport method experiment recording and storage mechanism, a melting method crystal synthesis experiment recording and storage mechanism, and a high temperature method crystal synthesis experiment recording and storage mechanism, preferably selected from one or more of the following: a flux method crystal synthesis experiment recording and storage mechanism, a solid phase reaction crystal synthesis experiment recording and storage mechanism, a chemical vapor transport method experiment recording and storage mechanism, a melting method crystal synthesis experiment recording and storage mechanism, and a high temperature method crystal synthesis experiment recording and storage mechanism; and / or The crystal growth experiment process entry and storage module includes one or more data storage units selected from the following: an experimental scheme data storage unit, an experimental condition data storage unit, a starting material data storage unit, and a heating and temperature reaction data storage unit, preferably including one or more data storage units selected from the following: an experimental condition data storage unit, a starting material data storage unit, and a heating and temperature reaction data storage unit.

3. The recording device according to claim 2, characterized in that: The experimental scheme data storage unit is used to store data including one or more selected from the following: crystal growth start time, crystal growth end time, target product, reaction method, sample number, flux, preferably including one or more selected from the following: crystal growth start time, crystal growth end time, target product, reaction method, sample number, more preferably including one or more selected from the following: crystal growth start time, target product, reaction method, sample number; The experimental condition data storage unit is used to store data selected from one or more of the following: crucible type, crucible inner diameter, crucible depth, reaction atmosphere, whether to grind, whether to press, whether to seal tantalum tube, whether to seal quartz tube, cooling method, furnace number, preferably including one or more of the following data selected from the following: crucible type, crucible inner diameter, crucible depth, reaction atmosphere, whether to seal tantalum tube, whether to seal quartz tube, cooling method, furnace number, more preferably including one or more of the following data selected from the following: crucible type, crucible inner diameter, reaction atmosphere, cooling method, furnace number; The starting material data storage unit is used to store data selected from one or more of the following: material type, ratio, actual mass, material form, preferably one or more of the following: material type, ratio, actual mass; and / or The heating and temperature reaction data storage unit is used to store data selected from one or more of the following: furnace temperature, holding time of each temperature interval, total reaction time, preferably including: furnace temperature and / or holding time of each temperature interval.

4. The recording device according to any one of claims 1 to 3, characterized in that The crystal growth experiment result recording module is used to record data selected from one or more of the following: product form, product photo, xrd test data, eds test data, eds test results, whether it is the target product, preferably including one or more of the following data selected from the following: product photo, xrd test data, eds test data, eds test results, whether it is the target product; Preferably, the data recorded by the crystal growth experiment result recording module also includes non-standard experimental data.

5. The recording device according to any one of claims 1 to 4, characterized in that The characterization entry storage module includes one or more data storage units selected from the following: a structural characterization data storage unit, a component characterization data storage unit, a magnetic characterization data storage unit, a transport characterization data storage unit, and a specific heat characterization data storage unit, preferably including one or more data storage units selected from the following: a structural characterization data storage unit, a component characterization data storage unit, a transport characterization data storage unit, and a specific heat characterization data storage unit, and more preferably including one or more data storage units selected from the following: a structural characterization data storage unit, a component characterization data storage unit, a magnetic characterization data storage unit, and a transport characterization data storage unit.

6. The recording device according to claim 5, characterized in that: The structure characterization data storage unit is used to store data selected from one or more of the following: sample structure characterization photos, sample powder XRD data, sample single crystal XRD data, and sample crystal information data; The data stored in the structure representation data storage unit preferably includes structure representation notes; The component characterization data storage unit is used to store: sample component characterization photos and / or sample component eds data; the data stored in the component characterization data storage unit preferably includes component characterization notes; The magnetic characterization data storage unit is used to store data selected from one or more of the following: sample magnetic characterization photos, sample magnetic characterization quality, sample magnetic characterization test data; the data stored in the magnetic characterization data storage unit preferably includes magnetic characterization notes; The transport characterization data storage unit is used to store: sample transport characterization photos and / or sample transport characterization test data; the data stored in the transport characterization data storage unit preferably includes transport characterization notes; and / or The specific heat characterization data storage unit is used to store data selected from one or more of the following: sample specific heat characterization photos, sample specific heat characterization mass, and sample specific heat characterization test data; the data stored in the specific heat characterization data storage unit preferably includes specific heat characterization remarks.

7. A method for recording standardized crystal growth data, characterized in that: The recording method comprises using a recording device as claimed in any one of claims 1 to 6; Preferably, the recording method comprises the following steps: 1) according to the adopted crystal synthesis method, one or more crystal synthesis method experiment recording and storage mechanisms are established, in each of the crystal synthesis method experiment recording and storage mechanisms, crystal synthesis method data is recorded and stored, and the crystal growth experiment process recording and storage module and the crystal growth experiment result and characterization recording and storage module are established; 2) recording and storing growth experiment process data in the crystal growth experiment process recording and storage module; and 3) In the crystal growth experiment result and characterization recording and storage module, the growth experiment result data is recorded and stored. When the growth experiment result data is consistent with the data of the target product, the target product is characterized and the crystal characterization data is recorded; when the growth experiment result data is not consistent with the data of the target product, the experiment is terminated.

8. The recording method according to claim 7, characterized in that: The recording method further comprises after step 3): 4) Associating the crystal synthesis method data entered and stored in step 1) with the crystal characterization data entered and stored in step 3).

9. A computer-readable storage medium, characterized in that: The computer-readable storage medium includes: one or more computer programs; When the computer program is executed by a processor, the recording device according to any one of claims 1 to 6 is constructed and / or the recording method according to claim 7 or 8 is implemented.

10. An electronic device, characterized in that: The electronic device comprises a memory and a processor, wherein: The memory is used to store computer programs; and The processor comprises the recording device according to any one of claims 1 to 6, and the processor is used to implement the recording method according to claim 7 or 8 when executing the computer program stored in the memory.

Images