High-temperature and high-pressure testing device

Through a multi-chamber and multi-component design, the high-temperature and high-pressure test device is solved, and the problems of low reaction efficiency and poor safety in traditional devices are achieved, uniform mixing and safe control of reactants are achieved, and suitable for multi-step chemical reactions.

CN120285869AInactive Publication Date: 2025-07-11YUNNAN OPEN UNIV
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Patent Information

Application Number
CN202510448584.7
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-04-10
Publication Date
2025-07-11
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

Traditional high-temperature and high-pressure reaction devices have problems such as low reaction efficiency, uneven mixing of reactants, lag in gas-liquid interface monitoring, high reaction accuracy, and poor safety, which cannot meet the synchronization and safety control of multi-step reactions.

Method used

A high-temperature and high-pressure test device is designed, adopting a multi-chamber structure and a multi-component system, including feeding, liquid feeding, stirring and heating, pressurization and venting components. By separating the reaction chamber, stirring and heating, liquid level control and pressurization pump and other technical means, the reaction steps can be synchronized and safely controlled.

Benefits of technology

It improves reaction efficiency and accuracy, reduces the risk of gas release, ensures uniform mixing of reactants, enhances safety, and is suitable for the synchronous progress of multi-step chemical reactions.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention belongs to the technical field of chemical engineering, and provides a high-temperature and high-pressure testing device which comprises a box body, a feeding assembly is arranged on the rear side of the upper portion of the box body, a liquid feeding assembly is arranged on the rear side of the box body, a stirring and heating assembly is arranged in an inner cavity of the box body, and a pressurizing assembly is arranged on the outer side of the box body and communicated with the inner cavity of the box body. An emptying assembly is arranged below the rear side of the box body; the reaction chamber is divided into three independent areas, so that different reaction steps are synchronously carried out, the reaction efficiency of the system is improved, the stirring and heating assembly ensures that reactants are uniformly mixed in each reaction chamber and a proper reaction temperature is obtained, the reaction rate is further improved, and the reaction time is shortened. In addition, the feeding assembly and the liquid feeding assembly achieve automatic monitoring and control of the feeding amount of materials and liquid, the experiment accuracy is improved, solutions in all the reaction cavities can be discharged in order through the emptying assembly, and danger caused by excessive liquid is avoided.
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Description

Technical Field

[0001] The present invention belongs to the technical field of chemical engineering, and specifically relates to a high-temperature and high-pressure test device. Background Art

[0002] In the research and industrial applications of chemical reaction processes, high-temperature and high-pressure reaction devices play a crucial role. These devices are commonly used in applications such as the synthesis of new materials, catalytic reactions, drug synthesis, and waste treatment. Traditional high-temperature and high-pressure reaction devices have some technical deficiencies, which limit their efficiency and safety in scientific research and industrial production;

[0003] Many existing high-temperature and high-pressure reaction devices adopt a single reaction chamber design, which only supports linear reaction steps. This design restricts the synchronous progress of multi-step reactions, resulting in an extended reaction time and low reaction efficiency. In addition, reactants at different stages in a single chamber may mix before reaching the optimal reaction conditions, thereby affecting the quality and yield of the final product; moreover, the gas-liquid interface monitoring technology of traditional high-temperature and high-pressure devices lags behind, lacking an effective online monitoring and control system. This leads to the inability to accurately control the feeding amount of materials in real time during the feeding and liquid supply processes, thus affecting the repeatability and accuracy of the reaction. Additionally, the uncertainty of fluid dynamics may cause the liquid level to be unable to be adjusted immediately, increasing the risk of overflow or incomplete reaction.

[0004] In a high-temperature and high-pressure environment, the release of gases and the overflow of liquids are common risks, and many existing devices lack effective safety prevention measures. The release of gases during the reaction process fails to be timely and effectively controlled, which may cause the pressure in the reaction vessel to rise abnormally, thereby triggering an explosion or equipment damage. In addition, the lack of a proper design of the venting system makes the collection and treatment of reaction products complex and unsafe. Moreover, the stirring or heating mechanisms of some existing devices cannot meet the requirements of high reaction rates, resulting in uneven distribution of reactants in the chamber. This unevenness may cause local overheating or incomplete reaction, thus causing side reactions and instability of the product properties.

[0005] Therefore, those skilled in the art have proposed a high-temperature and high-pressure test device, aiming to improve the reaction efficiency and improve the reaction effect by synchronously performing reactions in different steps. Summary of the Invention

[0006] In order to solve the above technical problems, the present invention provides a high-temperature and high-pressure test device to solve the problems raised in the background art.

[0007] A high-temperature and high-pressure test device, comprising a box body. A feeding component is arranged at the rear side above the box body, a liquid supply component is arranged at the upper rear side of the box body, a stirring and heating component is arranged in the inner cavity of the box body, a pressurizing component is arranged outside the box body and is communicated with the inner cavity of the box body, and a venting component is arranged at the lower rear side of the box body.

[0008] Preferably, the inner cavity of the box body is separated into three reaction chambers by a titanium alloy partition board. The reaction chambers are separated into independent chambers with a volume ratio of 1:1.2:1.5. Three groups of observation ports are respectively arranged at the front side above the reaction chambers, and a feeding cup is arranged at the rear side above the box body.

[0009] Preferably, the feeding component includes a feeding hopper arranged at the rear side above the box body. A material cover is installed at the upper end of the feeding hopper, a rotary vane type level switch is installed at the rear side of the feeding hopper, a blade is arranged at the output end of the rotary vane type level switch and is located in the inner cavity of the feeding hopper, a vibrator is arranged at the rear side of the feeding hopper and is located below the rotary vane type level switch, a first motor is fixedly installed at the upper side of the box body and is located at one side of the feeding hopper, a spiral conveyor shaft is fixedly installed at the output end of the first motor and is located in the inner cavity of the feeding hopper, and the outlet of the spiral conveyor shaft is located above the feeding cup.

[0010] Preferably, the liquid supply component includes a liquid infusion port arranged at the rear side of the box body. The rear end of the liquid infusion port is successively communicated with a Y-type filter, a pressure gauge and an electromagnetic valve to form a liquid supply pipeline. A manual union diaphragm valve is installed at the rear end of the liquid supply pipeline, and a pipe clamp is fixedly installed at the rear end of the box body for clamping the liquid supply pipeline. The outlets of the liquid supply pipeline are respectively provided with a first liquid infusion pipe and a second liquid infusion pipe. The first liquid infusion pipe is directly communicated with the reaction chamber above the box body, and the second liquid infusion pipe is communicated with one side of the feeding cup.

[0011] Preferably, the stirring and heating component includes a second motor arranged at the front side above the box body. There are three groups of the second motors, which are respectively located above the reaction chambers. A stirring shaft is fixedly installed at the output end of the second motor and is located in the corresponding reaction chamber. Stirring blades are arranged on the stirring shaft. Heating plates are respectively arranged at the bottoms of the reaction chambers. The inner cavity of the box body is separated into three reaction chambers by a titanium alloy partition board. An overflow pipe is arranged at one side of the reaction chamber below the feeding cup, and a C-shaped groove is fixedly installed at one side of the titanium alloy partition board. A flow port is arranged at the lower end of one side of the C-shaped groove and penetrates through the titanium alloy partition board. The height of the overflow pipe is greater than the height of the C-shaped groove. A liquid level controller is fixedly arranged above the reaction chamber communicated with the pressurizing component.

[0012] Preferably, the pressurizing component includes a bracket. A pressure pump is fixedly installed at the upper end of the bracket. A pressurizing pipe is fixedly installed at the output end of the pressure pump. The top end of the pressurizing pipe penetrates through the box body, and a pressurizing port is arranged at the lower end of one side of the reaction chamber.

[0013] Preferably, the venting assembly includes venting openings formed at the lower rear sides of the three reaction chambers of the box body. The venting openings are respectively communicated with a first branch pipe, a second branch pipe and a third branch pipe. The first branch pipe, the second branch pipe and the third branch pipe are communicated through a main venting pipe, and one end of the main venting pipe is provided with a main pipe outlet.

[0014] Compared with the prior art, the present invention has the following beneficial effects:

[0015] 1. By dividing the reaction chamber into three independent regions, the present invention can realize the synchronous progress of different reaction steps, improve the reaction efficiency of the system, and the stirring and heating assembly ensures the uniform mixing of reactants in each reaction chamber and obtains a suitable reaction temperature, further improving the reaction rate. Moreover, the feeding assembly and the liquid feeding assembly are equipped with a variety of sensors and control systems, which can realize the automatic monitoring and control of the feeding amounts of materials and liquids, improving the accuracy of experiments.

[0016] 2. The present invention monitors the liquid level in the reaction chamber through a liquid level controller to ensure an appropriate amount of liquid, prevent overflow and incomplete reaction. At the same time, the pressurizing assembly ensures that the three reactions are in a high-pressure state through a pressure pump, improving the reaction efficiency while reducing the risk of gas release. The design of the venting assembly enables the orderly discharge of the solutions in each reaction chamber, avoiding danger caused by excessive liquid and facilitating subsequent experimental data collection, so that the device can be applicable to different types of chemical reactions, especially reactions that require the combination of high temperature, high pressure and stirring, and is very suitable for research fields such as material synthesis and chemical synthesis. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 is a schematic diagram of the overall structure of the present invention;

[0018] Figure 2 is a schematic diagram of the structure of the feeding assembly of the present invention;

[0019] Figure 3 is a schematic diagram of the structure of the liquid feeding assembly of the present invention;

[0020] Figure 4 is a schematic diagram of the structure of the stirring and heating assembly of the present invention;

[0021] Figure 5 is a schematic diagram of the structure of the venting assembly of the present invention.

[0022] In the figure:

[0023] 100, Box body; 101, Observation port; 102, Feeding cup; 103, Reaction chamber; 200, Feeding assembly; 201, Feeding hopper; 202, Material cover; 203, Rotary vane level switch; 204, Blade; 205, Vibrator; 206, First motor; 207, Screw conveyor shaft; 300, Liquid feeding assembly; 301, Liquid inlet; 302, Y-type filter; 303, Pressure gauge; 304, Solenoid valve; 305, Manual ball valve; 306, Pipe clamp; 307, First liquid pipe; 308, Second liquid pipe; 400, Stirring and heating assembly; 401, Second motor; 402, Stirring shaft; 403, Stirring blade; 404, Heating plate; 405, Overflow pipe; 406, C-shaped groove; 407, Liquid level controller; 500, Pressurizing assembly; 501, Bracket; 502, Pressurizing pump; 503, Pressurizing pipe; 504, Pressurizing port; 600, Venting assembly; 601, Venting port; 602, First branch pipe; 603, Second branch pipe; 604, Third branch pipe; 605, Main venting pipe; 606, Main pipe outlet. Specific embodiments

[0024] The following further describes in detail the embodiments of the present invention in conjunction with the drawings and examples. The following examples are used to illustrate the present invention, but cannot be used to limit the scope of the present invention.

[0025] As shown in the attached Figure 1 to the attached Figure 5 figures:

[0026] Embodiment 1: The present invention provides a high-temperature and high-pressure test device, including a box body 100, a feeding assembly 200 is arranged at the rear side above the box body 100, a liquid feeding assembly 300 is arranged at the upper rear side of the box body 100, a stirring and heating assembly 400 is arranged in the inner cavity of the box body 100, a pressurizing assembly 500 is arranged outside the box body 100 and is communicated with the inner cavity of the box body 100, and a venting assembly 600 is arranged at the lower rear side of the box body 100.

[0027] The inner cavity of the box body 100 is divided into three reaction chambers 103 by a titanium alloy partition, and the reaction chambers 103 are divided into independent chambers with a volume ratio of 1:1.2:1.5. Three groups of observation ports 101 are opened at the front side above the reaction chambers 103, and a feeding cup 102 is opened at the rear side above the box body 100.

[0028] The feeding assembly 200 includes a feeding hopper 201 arranged at the rear side above the box body 100. A material cover 202 is installed at the upper end of the feeding hopper 201. A rotary vane type level switch 203 is installed at the rear side of the feeding hopper 201. The rotary vane type level switch 203 uses a micro motor as the drive. At the output end of the rotary vane type level switch 203 and inside the feeding hopper 201, a blade 204 is arranged. When the blade 204 does not contact the powder used in the test, the motor runs normally and drives the blade 204 to rotate. When the blade 204 contacts the powder, the generated resistance overcomes the tension of the spring, causing the motor to stop rotating. When the powder drops, the resistance received by the blade 204 disappears, and it returns to the original state by relying on the tension of the torsion spring or the spring, preparing to respond to the rise of the powder again. That is, when the material rises to the position of the blade 204, the resistance causes the motor to stop rotating and outputs a signal to cut off the power supply. When the material drops, the resistance of the blade 204 disappears, and the signal detection device returns to the original state by relying on the spring, preparing to detect again. A vibrator 205 is arranged at the rear side of the feeding hopper 201 and below the rotary vane type level switch 203. The vibrator 205 eliminates the material wall sticking at a frequency of 50 Hz. By slightly vibrating the feeding hopper 201, the wall-sticking powder can fall off. A first motor 206 is fixedly installed above the box body 100 and on one side of the feeding hopper 201. At the output end of the first motor 206 and inside the feeding hopper 201, a spiral conveyor shaft 207 is fixedly installed. The outlet of the spiral conveyor shaft 207 is located above the feeding cup 102. The spiral conveyor shaft 207 accurately feeds materials at a rate of 0.5 - 2 kg / min. By operating the first motor 206, the spiral conveyor shaft 207 rotates, and the dropped powder is conveyed to the feeding cup 102 through the spiral conveyor shaft 207, and thus falls into the first reaction chamber 103 for primary reaction.

[0029] The liquid supply assembly 300 includes an infusion port 301 provided at the rear side of the box body 100. A Y-shaped filter 302, a pressure gauge 303, and a solenoid valve 304 are successively connected to the rear end of the infusion port 301 to form a liquid supply pipeline. A manual ball diaphragm valve 305 is installed at the rear end of the solenoid valve 304 on the liquid supply pipeline. And a pipe clamp 306 is fixedly installed at the rear end of the box body 100 for clamping the liquid supply pipeline. The outlets of the liquid supply pipeline are respectively provided with a first infusion tube 307 and a second infusion tube 308. The first infusion tube 307 is directly connected to the reaction chamber 103 above the box body 100, and the second infusion tube 308 is connected to one side of the feeding cup 102. The reaction liquid is input through the infusion port 301, passes through the Y-shaped filter 302, is detected by the pressure gauge 303 and controlled by the solenoid valve 304, so that the reaction liquid can be detected and controlled for input. Then, the flow rate and pressure of the liquid medium are controlled by the manual ball diaphragm valve 305. The output reaction liquid is directly input into the first reaction chamber 103 through the first infusion tube 307, and also combines with the powder dropped from the screw conveyor shaft 207 in the feeding cup 102 through the second infusion tube 308 and then drops into the first reaction chamber 103. Multiple groups of ball valves are provided on the liquid supply assembly 300 for controlling the liquid flow and transportation.

[0030] The stirring and heating assembly 400 includes a second motor 401 disposed on the front side above the box body 100. There are three groups of the second motors 401, which are respectively located above the three reaction chambers 103. A stirring shaft 402 is fixedly installed at the output end of the second motor 401 and located in the corresponding reaction chamber 103. Stirring blades 403 are arranged on the stirring shaft 402. The stirring blades 403 adopt an asymmetric airfoil design. Referring to the GB / T 19077-2016 standard, the measured mixing efficiency reaches 98.7%. Heating plates 404 are arranged at the bottom of each reaction chamber 103. The inner cavity of the box body 100 is divided into three reaction chambers 103 by a titanium alloy partition. An overflow pipe 405 is arranged on one side of the reaction chamber 103 below the feed cup 102. And C-shaped grooves 406 are fixedly installed on one side of the titanium alloy partition. A flow port is arranged at one side of the lower end of the C-shaped groove 406 through the titanium alloy partition. The height of the overflow pipe 405 is greater than the height of the C-shaped groove 406. A liquid level controller 407 is fixedly arranged above the reaction chamber 103 communicating with the pressurizing assembly 500. By starting the heating plate 404, the reaction liquid and the powder are fused and reacted. And by starting the second motor 401, the stirring shaft 402 drives the stirring blades 403 to stir in the reaction chamber 103, accelerating the reaction rate. And the excess liquid is discharged through the overflow pipe 405 to prevent the liquid in the reaction chamber 103 from being too much, resulting in the risk of swelling. And through the C-shaped groove 406 on one side of the titanium alloy partition, the fused liquid after the initial reaction in the first reaction chamber 103 is introduced into the second reaction chamber 103. After being heated by the heating plate 404 and stirred by the stirring shaft 402, a secondary reaction is carried out. After the reaction, it flows into the third reaction chamber 103 through the C-shaped groove 406 on one side of the titanium alloy partition. The temperatures of the heating plates 404 in the three reaction chambers 103 can be set independently, so as to carry out a three-stage reaction. And a pressurizing assembly 500 is connected in the third reaction chamber 103 for high-pressure treatment.

[0031] The pressurizing assembly 500 includes a bracket 501. A pressurizing pump 502 is fixedly installed at the upper end of the bracket 501. A pressurizing pipe 503 is fixedly installed at the output end of the pressurizing pump 502. The top end of the pressurizing pipe 503 penetrates through the box body 100, and a pressurizing port 504 is opened at the lower end on one side of the reaction chamber 103. By starting the pressurizing pump 502, the third reaction chamber 103 connected thereto is in a high-pressure state. At the same time, the overall reaction chamber 103 is in a high-pressure state through the C-shaped groove 406. Thus, all three reactions are in a high-pressure state. Due to the volume of the reaction chamber 103, the pressurizing method adopts a three-stage progressive pressurization design, which is 5MPa → 15MPa → 30MPa. After being verified by ANSYS simulation, the pressure distribution uniformity is increased by 42%.

[0032] The venting assembly 600 includes vent openings 601 provided at the lower rear sides of three reaction chambers 103 of the box body 100. The vent openings 601 are respectively communicated with a first branch pipe 602, a second branch pipe 603, and a third branch pipe 604. The first branch pipe 602, the second branch pipe 603, and the third branch pipe 604 are communicated through a vent main pipe 605, and one end of the vent main pipe 605 is provided with a main pipe outlet 606. By combining the overflow pipe 405 with the venting assembly 600, dual redundant pressure relief is formed for effective safety protection. The reaction solution in each chamber is controlled to flow out through the ball valves on all branch pipes, so as to orderly collect the solutions at different stages in the three reaction chambers 103.

[0033] Based on the verification of the pilot production line, the following experimental data are obtained:

[0034] index A traditional device Device of the present invention Improvement rate Reaction efficiency 72% 93% 29.2% Energy intensity 8.7kW·h / kg 5.2kW·h / kg 40.2% Product consistency ±6.8% ±1.5% 78%

[0035] It has been implemented in a certain special polymer synthesis project (with an annual output of 5,000 tons), achieving: the reaction cycle is shortened from 14 hours to 9.5 hours, the annual accident rate is reduced from 1.2% to 0.15%, and the qualified rate of product crystal form is increased from 82% to 97%.

[0036] As can be seen from the above, by dividing the reaction chamber into three independent areas, the device can realize the synchronous progress of different reaction steps, improve the reaction efficiency of the system, and the stirring and heating assembly ensures that the reactants are evenly mixed in each reaction chamber and obtain a suitable reaction temperature, further improving the reaction rate. And the feeding assembly and the liquid supply assembly are equipped with a variety of sensors and control systems, which can realize the automatic monitoring and control of the feeding amounts of materials and liquids, improve the accuracy of the experiment. The liquid level controller monitors the liquid level in the reaction chamber to ensure an appropriate amount of liquid, prevent overflow and incomplete reaction. At the same time, the pressurizing assembly ensures that the three reactions are in a high-pressure state through a pressure pump, improving the reaction efficiency while reducing the risk of gas release. The design of the venting assembly enables the solutions in each reaction chamber to be discharged orderly, avoiding danger caused by excessive liquid, and facilitating subsequent experimental data collection. Therefore, the device can be applied to different types of chemical reactions, especially reactions that require the combination of high temperature, high pressure and stirring, and is very suitable for research fields such as material synthesis and chemical synthesis.

[0037] Importantly, it should be noted that the construction and arrangement of the present application shown in multiple different exemplary embodiments are merely illustrative. Although only a few embodiments are described in detail in this disclosure, those who refer to this disclosure should easily understand that many modifications are possible without materially departing from the novel teachings and advantages of the subject matter described in this application (e.g., changes in the dimensions, scales, structures, shapes and proportions of various elements, as well as parameter values (such as temperature, pressure, etc.), installation arrangements, use of materials, colors, orientations, etc.). For example, an element shown as integrally formed may be composed of multiple parts or elements, the position of the element may be inverted or otherwise changed, and the nature, number or position of discrete elements may be altered or changed. Accordingly, all such modifications are intended to be included within the scope of the present invention. The order or sequence of any process or method steps may be changed or re-ordered according to alternative embodiments. In the claims, any "means-plus-function" clause is intended to cover the structures that perform the recited function herein, and not only structural equivalents but also equivalent structures. Other substitutions, modifications, changes and omissions may be made in the design, operating conditions and arrangement of the exemplary embodiments without departing from the scope of the present invention. Accordingly, the present invention is not limited to a particular embodiment, but extends to various modifications that still fall within the scope of the appended claims.

[0038] In addition, to provide a concise description of the exemplary embodiments, not all features of the actual embodiments may be described (i.e., those features that are not relevant to the currently contemplated best mode of carrying out the present invention or those features that are not relevant to implementing the present invention).

[0039] It should be understood that in the development of any actual implementation, in any engineering or design project, numerous specific implementation decisions may be made. Such development efforts may be complex and time-consuming, but for those of ordinary skill in the art who benefit from this disclosure, without undue experimentation, such development efforts will be a routine task of design, manufacturing and production.

[0040] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention and not to limit them. Although the present invention has been described in detail with reference to the preferred embodiments, those of ordinary skill in the art should understand that the technical solutions of the present invention may be modified or equivalently replaced without departing from the spirit and scope of the technical solutions of the present invention, and they should all be covered within the scope of the claims of the present invention.

Claims

1. A high-temperature and high-pressure test device, characterized in that: It includes a box body (100), a feeding component (200) is arranged at the rear side above the box body (100), a liquid feeding component (300) is arranged at the upper rear side of the box body (100), a stirring and heating component (400) is arranged in the inner cavity of the box body (100), a pressurizing component (500) is arranged outside the box body (100) and is communicated with the inner cavity of the box body (100), and a venting component (600) is arranged at the lower rear side of the box body (100).

2. The high-temperature and high-pressure test device according to claim 1, wherein: The inner cavity of the box body (100) is divided into three reaction chambers (103) by a titanium alloy partition board. The reaction chambers (103) are divided into independent chambers with a volume ratio of 1:1.2:1.

5. Three groups of observation ports (101) are arranged at the front side above the reaction chambers (103), and a feeding cup (102) is arranged at the upper rear side of the box body (100).

3. The high-temperature and high-pressure test device according to claim 1, characterized in that: The feeding component (200) includes a feeding hopper (201) arranged at the rear side above the box body (100). A material cover (202) is installed at the upper end of the feeding hopper (201). A rotary vane type level switch (203) is installed at the rear side of the feeding hopper (201). A blade (204) is arranged at the output end of the rotary vane type level switch (203) and is located in the inner cavity of the feeding hopper (201). A vibrator (205) is arranged at the rear side of the feeding hopper (201) and is located below the rotary vane type level switch (203). A first motor (206) is fixedly installed above the box body (100) and on one side of the feeding hopper (201). A spiral conveyor shaft (207) is fixedly installed at the output end of the first motor (206) and is located in the inner cavity of the feeding hopper (201). The outlet of the spiral conveyor shaft (207) is located above the feeding cup (102).

4. The high-temperature and high-pressure test device according to claim 1, characterized in that: The liquid feeding component (300) includes a liquid infusion port (301) arranged at the rear side of the box body (100). The rear end of the liquid infusion port (301) is sequentially communicated with a Y-type filter (302), a pressure gauge (303) and a solenoid valve (304) to form a liquid feeding pipeline. A manual union diaphragm valve (305) is installed at the rear end of the liquid feeding pipeline. And a pipe clamp (306) is fixedly installed at the rear end of the box body (100) for clamping the liquid feeding pipeline. The outlets of the liquid feeding pipeline are respectively provided with a first liquid infusion pipe (307) and a second liquid infusion pipe (308). The first liquid infusion pipe (307) is directly communicated with the reaction chamber (103) above the box body (100), and the second liquid infusion pipe (308) is communicated with one side of the feeding cup (102).

5. The high-temperature and high-pressure test device according to claim 1, wherein: The stirring and heating assembly (400) includes a second motor (401) disposed on the front side above the box body (100). There are three groups of the second motors (401), which are respectively located above the reaction chambers (103). A stirring shaft (402) is fixedly installed at the output end of the second motor (401) and in the corresponding reaction chamber (103). Stirring blades (403) are arranged on the stirring shaft (402). Heating plates (404) are arranged at the bottoms in the reaction chambers (103). The inner cavity of the box body (100) is divided into three reaction chambers (103) by a titanium alloy partition. An overflow pipe (405) is arranged on one side in the reaction chamber (103) below the feed cup (102). C-shaped grooves (406) are fixedly installed on one side of the titanium alloy partition. A circulation port is arranged at one side of the lower end of the C-shaped groove (406) penetrating through the titanium alloy partition. The height of the overflow pipe (405) is greater than the height of the C-shaped groove (406). A liquid level controller (407) is fixedly arranged above the reaction chamber (103) communicated with the pressurizing assembly (500).

6. The high-temperature and high-pressure test device according to claim 1, wherein: The pressurizing assembly (500) includes a bracket (501). A pressurizing pump (502) is fixedly installed at the upper end of the bracket (501). A pressurizing pipe (503) is fixedly installed at the output end of the pressurizing pump (502). The top end of the pressurizing pipe (503) penetrates through the box body (100), and a pressurizing port (504) is opened at the lower end on one side of the reaction chamber (103).

7. The high-temperature and high-pressure test device according to claim 1, characterized in that: The emptying assembly (600) includes emptying ports (601) opened at the lower ends of the rear sides of the three reaction chambers (103) of the box body (100). The emptying ports (601) are respectively communicated with a first branch pipe (602), a second branch pipe (603) and a third branch pipe (604). The first branch pipe (602), the second branch pipe (603) and the third branch pipe (604) are communicated through an emptying main pipe (605). A main pipe outlet (606) is arranged at one end of the emptying main pipe (605).