Earthworm organic water-soluble fertilizer preparation enzyme hydrolysis device
By designing the sampling head, sampler, sealing ring, and gas injection mechanism in the enzymatic hydrolysis device, the problem of increased dissolved oxygen during sampling was solved, thus achieving accurate sample detection and precise monitoring of the enzymatic hydrolysis process.
Patent Information
- Application Number
- CN202511093644.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2025-08-06
- Publication Date
- 2025-10-24
- Estimated Expiration
- 2045-08-06
AI Technical Summary
During the enzymatic hydrolysis of earthworm organic water-soluble fertilizer, residual air in the sampling tube during sampling increases dissolved oxygen, affecting the accuracy of sample hydrolysis degree detection.
An enzymatic hydrolysis device was designed, comprising a sampling head, a sampler, a driving mechanism, an exhaust mechanism, and a gas injection mechanism. The sealing ring and the gas injection mechanism ensure that the gas environment inside the sampler is the same as that inside the enzymatic hydrolysis tank during the sampling process, thus avoiding an increase in dissolved oxygen.
This ensures the accuracy of sample detection, avoids detection errors caused by increased dissolved oxygen, and improves the monitoring accuracy of the enzymatic hydrolysis process.
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Figure CN120590194B_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The application relates to the technical field of earthworm organic water-soluble fertilizer preparation, in particular to an enzymolysis device for preparing earthworm organic water-soluble fertilizer. BACKGROUND
[0002] After being washed and pulped, live earthworms are mixed with water to form uniform slurry, and then fermentation and enzymolysis are carried out to prepare earthworm organic water-soluble fertilizer; fermentation and enzymolysis aim to maximize the retention of active substances (such as enzymes and microbial flora) and nutrient elements in the earthworms.
[0003] During the enzymolysis process of the earthworm organic water-soluble fertilizer, Bacillus natto needs to be added, and the bacteria are facultative anaerobes; low-oxygen environment (DO 0.2-0.5 mg / L) can promote the proliferation and enzyme secretion of the bacteria; and excessive oxygen can cause oxidation of active peptides in earthworm proteins and reduce the biological activity of the fertilizer, so the DO value in the enzymolysis tank needs to be strictly controlled during the enzymolysis process of the earthworm organic water-soluble fertilizer.
[0004] During the enzymolysis process, water-soluble fertilizer in the enzymolysis tank needs to be sampled every 20-30 minutes to measure the degree of hydrolysis; during the sampling operation, air in the sampling tube is difficult to completely discharge, a small amount of air remains in the sampling tube, and the dissolved oxygen content of the sample increases usually 10-15 minutes from the completion of sampling to sample inspection, the sample hydrolysis degree detection will produce error, which is not conducive to the monitoring of the enzymolysis process. SUMMARY
[0005] The purpose of the present application is to provide an enzymolysis device for preparing earthworm organic water-soluble fertilizer to solve the problems raised in the background.
[0006] To achieve the above-mentioned purpose, the present application provides the following technical scheme: an enzymolysis device for preparing earthworm organic water-soluble fertilizer, comprising an enzymolysis tank, a sampling port is arranged on the side wall of the enzymolysis tank, a sampling unit is arranged on the inner side of the sampling port, and the sampling unit can ensure that the sample is in the same environment in the enzymolysis tank after sampling, and the dissolved oxygen is less than or equal to 0.5 mg / L.
[0007] As a further scheme of the present application, the sampling unit comprises a sampling head, a sampler, a driving mechanism, an exhaust mechanism and an air injection mechanism.
[0008] The sampling head is horizontally and slidingly connected with the sampling port; the sampler is inserted into the sampling head; a channel one is formed in the inner side of the sampling head; a feeding port capable of communicating with the channel one is formed on the sampler; and a sealing ring is elastically and slidingly connected with the circumferential side wall of the sampler along the axial direction.
[0009] The driving mechanism is arranged on the side of the sampling head and is used for driving the sampling head to move horizontally.
[0010] The exhaust mechanism is arranged on the inner side of the sampler.
[0011] The gas injection mechanism is arranged inside the sampling port and is used for injecting the protective gas at the top of the enzymatic hydrolysis tank into the sampler before the sampling head moves into the inside of the enzymatic hydrolysis tank, and the air in the sampler is extruded out through the exhaust mechanism so that the sampler is filled with the protective gas.
[0012] As a further scheme of the present application, a piston is slidably arranged in the sampler, the piston is fixedly connected with a return spring, one end of the return spring away from the piston is fixedly connected with the sampler, a limiting mechanism is arranged on the side of the piston, the limiting mechanism is used for limiting the piston and can cancel the limitation of the piston when the sampling head moves into the enzymatic hydrolysis tank.
[0013] As a further scheme of the present application, the limiting mechanism comprises a clamping block, the clamping block is rotatably connected with the sampler, a traction rope is fixedly connected with the clamping block, one end of the traction rope away from the clamping block is fixedly connected with a sliding rod, and the sliding rod is slidably connected with the sampler.
[0014] As a further scheme of the present application, the exhaust mechanism comprises a second channel, the second channel is arranged inside the piston, an elastic stop block is slidably connected in the second channel, a jack is arranged on the side of the stop block and is used for driving the stop block to move, and the jack is fixedly connected with the sampler.
[0015] As a further scheme of the present application, the stop block is arranged in a circular truncated cone shape, and the second channel is arranged in a circular truncated cone shape matched with the stop block at one end close to the stop block.
[0016] As a further scheme of the present application, a slot is arranged on the sampling head, and an insertion block fixedly connected with the sampler can be inserted into the slot.
[0017] As a further scheme of the present application, the driving mechanism comprises a cylindrical cam, the cylindrical cam is coaxially arranged with the sampling head and is rotatably arranged inside the sampling port, a sliding groove is arranged on the inner wall of the cylindrical cam, a sliding column fixedly connected with the sampling head can be slidably matched with the sliding groove, a gear one is fixedly connected with the outer wall of the cylindrical cam, a gear two is engaged with the gear one, and a motor is arranged on the side of the gear two and is used for driving the gear two to rotate.
[0018] As a further scheme of the present application, the gas injection mechanism comprises a gas tube, one end of the gas tube is communicated with the top of the enzymatic hydrolysis tank, the other end of the gas tube is located in the sampling port and can be communicated with the first channel, and a pump body is arranged in the middle of the gas tube.
[0019] Compared with the prior art, the present application has the following beneficial effects:
[0020] The application is characterized in that the sampling head and the sampler are connected, and the sealing ring can ensure the sealing between the sampling head and the sampler; during the movement of the sampling head to the inside of the enzymolysis tank driven by the driving mechanism, the gas injection mechanism injects the protective gas at the top of the enzymolysis tank into the sampler, and the air in the sampler is extruded out through the exhaust mechanism, so that the gas environment in the sampler and the gas environment in the enzymolysis tank are in the same state, the dissolved oxygen content of the sample is prevented from increasing after the sample enters the sampler, and the accuracy of sample detection is ensured. BRIEF DESCRIPTION OF DRAWINGS
[0021] Figure 1 It is a schematic diagram of the overall structure of the application;
[0022] Figure 2 It is a schematic diagram of the sampling unit structure of the application;
[0023] Figure 3 It is a schematic diagram of the overall structure of the application;
[0024] Figure 4 It is Figure 3 It is a local enlarged view of A in the middle;
[0025] Figure 5 It is Figure 4 It is a local enlarged view of B in the middle
[0026] Figure 6 It is a schematic diagram of the cylindrical cam, the sampling head and the slide column structure of the application;
[0027] Figure 7 It is a schematic diagram of the sampling head and the sampler insertion state of the application;
[0028] Figure 8 It is a schematic diagram of the working state of the gas injection mechanism of the application;
[0029] Figure 9 It is a schematic diagram of the working state of the sampling head and the sampler during sampling of the application.
[0030] The reference signs are as follows:
[0031] 1-enzymolysis tank, 2-sampling port, 3-sampling unit, 4-sampling head, 5-channel one, 6-sampler, 7-feeding port, 8-sealing ring, 9-piston, 10-channel two, 11-plug, 12-ejector rod, 13-insertion slot, 14-insertion block, 15-clamping block, 16-sliding rod, 17-pulling rope, 18-cylindrical cam, 19-sliding groove, 20-sliding column, 21-air pipe, 22-pump body, 23-gear one, 24-gear two, 25-motor, 26-return spring. DETAILED DESCRIPTION
[0032] With reference to the drawings of the embodiments of the present application, the technical solutions in the embodiments of the present application will be described clearly and completely. Obviously, the described embodiments are only a part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments of the present application, all other embodiments obtained by those skilled in the art without creative work fall within the scope of the present application.
[0033] With reference to Figures 1-9 The present application provides a technical solution: an enzymolysis device for preparing earthworm organic water-soluble fertilizer, comprising an enzymolysis tank 1, a sampling port 2 arranged on the side wall of the enzymolysis tank 1, a sampling unit 3 arranged on the inner side of the sampling port 2, the sampling unit 3 being capable of ensuring that the sample is in the same environment in the enzymolysis tank 1 after sampling, and the dissolved oxygen being less than or equal to 0.5 mg / L; the sampling unit 3 comprises a sampling head 4, a sampler 6, a driving mechanism, an exhaust mechanism and a gas injection mechanism; the sampling head 4 is horizontally and slidingly connected with the sampling port 2; the sampler 6 is inserted with the sampling head 4; a channel one 5 is arranged on the inner side of the sampling head 4; a feeding port 7 capable of communicating with the channel one 5 is arranged on the sampler 6; a sealing ring 8 is elastically and slidingly connected with the circumferential side wall of the sampler 6 along the axial direction thereof; the driving mechanism is arranged on the side of the sampling head 4 and is used for driving the horizontal movement of the sampling head 4; the exhaust mechanism is arranged on the inner side of the sampler 6; and the gas injection mechanism is arranged on the inner side of the sampling port 2 and is used for injecting the protective gas at the top of the enzymolysis tank 1 into the sampler 6 before the sampling head 4 moves into the inside of the enzymolysis tank 1, so that the air in the sampler 6 is extruded out through the exhaust mechanism and the protective gas is filled in the sampler 6.
[0034] With reference to Figures 1-6 Earthworm paste and water are added into the enzymolysis tank 1 from the feeding port at the top of the enzymolysis tank 1, and the volume ratio of the earthworm paste to the water is 1:5; for example, 10 kg of earthworm paste needs to be added with 50 kg of water; the stirring mechanism in the enzymolysis tank 1 is started to stir (200 rpm); the enzymolysis tank 1 is kept at a constant temperature of 50°C, and then the neutral protease solution is injected; nitrogen gas is introduced into the enzymolysis tank 1 at the top to disperse air, reduce the oxygen concentration in the gas phase in the enzymolysis tank 1, and maintain a positive pressure in the enzymolysis tank 1; nitrogen gas is introduced into the enzymolysis tank 1 at the bottom through the microporous aeration pipe to form gas circulation, homogenize the material and control oxygen; when sampling detection is needed, for example, the sampling head 4 is moved to the sampling port 2, the sampler 6 is inserted into the channel one 5, and the protective gas in the sampler 6 is injected into the enzymolysis tank 1 through the gas injection mechanism, so that the air in the sampler 6 is extruded out through the exhaust mechanism, and the protective gas is filled in the sampler 6. Figure 7As shown, the sampler 6 is inserted into the sampling head 4 and docked with the sampling head 4. At this time, the left side wall of the sealing ring 8 fits with the right side wall of the sampling head 4, and the pre-tightening force applied by the spring 1 can make the sealing ring 8 fit tightly with the sampling head 4 to ensure the sealing between the sampling head 4 and the sampler 6, and the sampler 6 is relatively fixed to the sampling head 4, and the feed port 7 is aligned with the bottom end of the channel 1 5; then the driving mechanism drives the sampling head 4 and the sampler 6 to move synchronously toward the inside of the enzymolysis tank 1; after the sampling head 4 moves a short distance, the top of the channel 1 5 is connected to the gas injection mechanism; the gas injection mechanism injects the protective gas nitrogen at the top of the enzymolysis tank 1 into the sampler 6 through the channel 1 5 and the feed port 7, and the air in the sampler 6 is squeezed out from the exhaust mechanism; at this time, the gas environment in the channel 1 5, the feed port 7 and the sampler 6 is in the same state as the gas environment in the enzymolysis tank 1; then the driving mechanism drives the sampling head 4 and the sampler 6 to continue to move toward the inside of the enzymolysis tank 1, as shown Figure 9 As shown, until the top of channel 1 5 moves into the enzymolysis tank 1, and then the sample slurry enters the sampler 6 from channel 1 5 through the feed port 7; after the sampling is completed, the driving mechanism drives the sampling head 4 and the sampler 6 to move outward to Figure 7 Then remove the sampler 6 from the sampling head 4, seal the feed port 7 again with the sealing ring 8, and then send the sample in the sampler 6 for inspection; Figure 4 As shown, the middle section of channel 1-5 is set to be inclined. After the sampler 6 is separated from the sampling head 4, the slurry remaining in channel 1-5 will flow out of channel 1-5, avoiding the slurry remaining in channel 1-5 and affecting the next sampling. After each sampling, channel 1-5 can be rinsed with clean water to keep channel 1-5 better clean. The present invention is provided with the sampling head 4, sampler 6, sealing ring 8, exhaust mechanism, gas injection mechanism and driving mechanism. After the sampling head 4 and the sampler 6 are docked, the sealing ring 8 can ensure the seal between the sampling head 4 and the sampler 6. During the process of the driving mechanism driving the sampling head 4 to move into the enzymolysis tank 1, the gas injection mechanism injects the protective gas on the top of the enzymolysis tank 1 into the sampler 6 and squeezes out the air in the sampler 6 through the exhaust mechanism, so that the gas environment in the sampler 6 is in the same state as the gas environment in the enzymolysis tank 1, avoiding the increase of dissolved oxygen content after the sample sent for inspection enters the sampler 6, thereby ensuring the accuracy of sample detection.
[0035] Specifically, such as Figures 2-4 As shown, a piston 9 is slidably installed in the sampler 6, and the piston 9 is fixedly connected to a return spring 26, and the return spring 26 is fixedly connected to the sampler 6 at one end away from the piston 9; a limiting mechanism is provided on the side of the piston 9, and the limiting mechanism is used to limit the piston 9, and can cancel the limitation of the piston 9 when the sampling head 4 moves into the enzymatic hydrolysis tank 1; the limiting mechanism includes a clamping block 15, and the clamping block 15 is rotatably connected to the sampler 6; a traction rope 17 is fixedly connected to the clamping block 15, and the traction rope 17 is fixedly connected to a slide rod 16 at one end away from the clamping block 15, and the slide rod 16 is slidably connected to the sampler 6.
[0036] Reference Figure 2 and Figure 4 In the initial state, the left wall of the piston 9 is in close contact with the inner wall of the sampler 6, which can reduce the amount of air in the sampler 6; the reset spring 26 is in a stretched state, and the clamping block 15 limits the piston 9, so that the piston 9 remains in the Figure 4 position shown; when the sampling head 4 and the sampler 6 move to Figure 8 the position shown, the left end of the slide rod 16 is close to the right wall of the cylindrical cam 18; when the sampling head 4 and the sampler 6 continue to move to the inside of the enzymolysis tank 1, the slide rod 16 moves to contact the cylindrical cam 18, and the slide rod 16 moves to the right relative to the sampler 6, and the slide rod 16 drives the clamping block 15 to rotate upward through the traction rope 17, and the clamping block 15 cancels the limitation of the piston 9; the elastic potential energy of the reset spring 26 is released, driving the piston 9 to move to the right, and the left chamber of the piston 9 in the sampler 6 forms a negative pressure; when the top end of the channel one 5 is moved to the inside of the enzymolysis tank 1 by the sampling head 4, the slurry rapidly enters the sampler 6 under the action of negative pressure, thereby improving the sampling efficiency.
[0037] Specifically, as shown in Figures 3-5 , the exhaust mechanism includes a channel two 10, the channel two 10 is arranged in the inside of the piston 9, and the channel two 10 is elastically and slidably connected with a blocking block 11, the blocking block 11 is provided with a jack 12 for driving the blocking block 11 to move, and the jack 12 is fixedly connected with the sampler 6; the blocking block 11 is provided in a circular truncated cone shape, and the channel two 10 close to the blocking block 11 is provided in a circular truncated cone shape matched with the blocking block 11.
[0038] Reference Figure 5 When the left wall of the piston 9 is in close contact with the inner wall of the sampler 6, the jack 12 acts on the blocking block 11, and the channel two 10 is in an open state; when the gas injection mechanism injects the protective gas in the enzymolysis tank 1 into the channel one 5 and the sampler 6, the air in the channel one 5 and the sampler 6 is discharged from the channel two 10; before the sampling head 4 enters the enzymolysis tank 1, the clamping block 15 cancels the limitation of the piston 9, and after the piston 9 moves to the right, the blocking block 11 moves to the left to block the left end of the channel two 10 under the action of the elastic force of the spring two connected with the blocking block 11; the left end of the blocking block 11 and the channel two 10 are both provided in a circular truncated cone shape, and the left end is smaller than the right end, so that the elastic force of the spring two and the air pressure can tightly block the channel two 10, thereby avoiding the air from entering the sampler 6 to pollute the sample.
[0039] Specifically, as shown in Figure 3 and Figure 4As shown, the sampling head 4 is provided with a slot 13, and the sampler 6 is fixedly connected with an insertion block 14 capable of being inserted into the slot 13; the insertion block 14 and the slot 13 are both rectangular, and the insertion of the insertion block 14 and the slot 13 can realize the positioning of the sampler 6. The abutting end portions of the sampling head 4 and the sampler 6 can be provided with magnetic members (such as magnets), and the relative fixation of the sampling head 4 and the sampler 6 can be realized through the mutual attraction of the magnetic poles and the limiting of the insertion block 14.
[0040] Specifically, as shown in Figures 2-4 and Figure 6 , the driving mechanism includes a cylindrical cam 18 coaxially arranged with the sampling head 4 and rotatably installed inside the sampling port 2. A sliding groove 19 is formed on the inner side wall of the cylindrical cam 18, and a sliding column 20 capable of being slidingly matched with the sliding groove 19 is fixedly connected to the side wall of the sampling head 4. A gear one 23 is fixedly connected to the outer side wall of the cylindrical cam 18, the gear one 23 is engaged with a gear two 24, and the gear two 24 is provided with a motor 25 for driving the rotation thereof. The motor 25 drives the gear one 23 to rotate through the gear two 24, the gear one 23 drives the cylindrical cam 18 to rotate, and the cylindrical cam 18 drives the sampling head 4 to reciprocally move in the horizontal direction through the cooperation of the sliding groove 19 and the sliding column 20.
[0041] Specifically, as shown in Figure 3 and Figure 4 , the gas injection mechanism includes a gas pipe 21. One end of the gas pipe 21 is in communication with the top of the enzymolysis tank 1, and the other end is located inside the sampling port 2 and capable of being in communication with the channel one 5. A pump body 22 is arranged in the middle of the gas pipe 21. When the sampling head 4 moves to the inside of the enzymolysis tank 1 to align the channel one 5 with the bottom end of the gas pipe 21, the pump body 22 slowly pumps the protective gas at the top of the enzymolysis tank 1 into the channel one 5, so that the channel one 5 and the sampler 6 are filled with the protective gas, and the gas environment in the sampler 6 is in the same state as that in the enzymolysis tank 1.
[0042] It should be noted that, in this document, relational terms such as first and second and the like can be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises", "comprising", or any other variations thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but can include other elements not expressly listed or inherent to such process, method, article, or apparatus.
[0043] While embodiments of the application have been shown and described, it is to be understood that the embodiments described are merely exemplary of the principles and application of the present application. Numerous modifications and adaptions can be effected without departing from the spirit and scope of the present application, which is not limited to the exact construction and arrangement described. It is intended, therefore, to cover all modifications and adaptions that fall within the scope of the claims and their equivalents.
Claims
1. An enzymatic hydrolysis device for preparing earthworm organic water-soluble fertilizer, comprising an enzymatic hydrolysis tank (1), characterized in that: The sidewall of the enzymolysis tank (1) is provided with a sampling port (2), and the inside of the sampling port (2) is provided with a sampling unit (3); after sampling, the sampling unit (3) can ensure that the sample is in the same environment in the enzymolysis tank (1), and the dissolved oxygen is less than or equal to 0.5 mg / L; The sampling unit (3) comprises a sampling head (4), a sampler (6), a driving mechanism, an exhaust mechanism and an air injection mechanism; the sampling head (4) is horizontally and slidingly connected with the sampling port (2); the sampler (6) is inserted with the sampling head (4); a channel one (5) is formed in the inside of the sampling head (4); a feeding port (7) is formed in the sampler (6) and can be in communication with the channel one (5); a sealing ring (8) is elastically and slidingly connected with the circumferential sidewall of the sampler (6) along the axial direction; the driving mechanism is arranged at the side of the sampling head (4) and is used for driving the horizontal movement of the sampling head (4); the exhaust mechanism is arranged in the inside of the sampler (6); the air injection mechanism is arranged in the inside of the sampling port (2) and is used for injecting the protective gas at the top of the enzymolysis tank (1) into the sampler (6) before the sampling head (4) moves into the inside of the enzymolysis tank (1), and the air in the sampler (6) is extruded out through the exhaust mechanism, so that the sampler (6) is filled with the protective gas.
2. The enzyme hydrolysis device for preparing earthworm organic water-soluble fertilizer according to claim 1, characterized in that: The piston (9) is slidingly installed in the sampler (6), the piston (9) is fixedly connected with a return spring (26), one end of the return spring (26) away from the piston (9) is fixedly connected with the sampler (6); a limiting mechanism is arranged at the side of the piston (9), the limiting mechanism is used for limiting the piston (9), and the limiting of the piston (9) can be cancelled when the sampling head (4) moves into the enzymolysis tank (1).
3. The earthworm organic water-soluble fertilizer preparation enzyme hydrolysis device according to claim 2, characterized in that: The limiting mechanism comprises a clamping block (15), the clamping block (15) is rotationally connected with the sampler (6); the clamping block (15) is fixedly connected with a traction rope (17), one end of the traction rope (17) away from the clamping block (15) is fixedly connected with a sliding rod (16), and the sliding rod (16) is slidingly connected with the sampler (6).
4. The enzyme hydrolysis device for preparing earthworm organic water-soluble fertilizer according to claim 2, characterized in that: The exhaust mechanism comprises a channel two (10), the channel two (10) is formed in the inside of the piston (9), the channel two (10) is elastically and slidingly connected with a blocking block (11), the side of the blocking block (11) is provided with a jack (12) used for driving the movement of the blocking block (11), and the jack (12) is fixedly connected with the sampler (6).
5. The earthworm organic water-soluble fertilizer preparation enzyme hydrolysis device according to claim 4, characterized in that: The blocking block (11) is in the shape of a circular truncated cone, and the channel two (10) is in the shape of a circular truncated cone matched with the blocking block (11) at one end close to the blocking block (11).
6. The enzyme hydrolysis device for preparing earthworm organic water-soluble fertilizer according to claim 1, characterized in that: A slot (13) is formed in the sampling head (4), and the sampler (6) is fixedly connected with a plug (14) which can be inserted with the slot (13).
7. The earthworm organic water-soluble fertilizer enzyme preparation device according to claim 1, characterized in that: The driving mechanism comprises a cylindrical cam (18) coaxially arranged with the sampling head (4) and rotationally mounted inside the sampling port (2); a sliding groove (19) is formed on the inner side wall of the cylindrical cam (18), and a sliding column (20) capable of slidingly cooperating with the sliding groove (19) is fixedly connected to the side wall of the sampling head (4); a gear one (23) is fixedly connected to the outer side wall of the cylindrical cam (18), the gear one (23) is engaged with a gear two (24), and the gear two (24) is provided with a motor (25) for driving the rotation thereof.
8. The enzyme hydrolysis device for preparing earthworm organic water-soluble fertilizer according to claim 1, characterized in that: The gas injection mechanism comprises a gas pipe (21); one end of the gas pipe (21) is in communication with the top of the enzymolysis tank (1), and the other end is located in the sampling port (2) and can be in communication with the channel one (5); a pump body (22) is arranged in the middle of the gas pipe (21).
Citation Information
Patent Citations
Fermentation device for liquid fertilizer
CN213951023U