Moxa health air-conditioning quilt
By combining blending and spinning with enzymatic modification and rice bran wax lubrication, the problems of spinnability and antibacterial properties of mugwort quilts have been solved, achieving long-lasting antibacterial, dynamic dehumidification and improved comfort, making them suitable for people with allergies.
Patent Information
- Application Number
- CN202511029463.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-07-25
- Publication Date
- 2025-11-07
AI Technical Summary
Existing mugwort quilts are inadequate in terms of long-lasting antibacterial properties, comfort, and health intervention functions. Furthermore, the brittleness of mugwort fibers results in poor spinnability, and the active substances are prone to volatilization, making it difficult to meet the needs of long-term close-fitting use.
The blended spinning technology is used to mix styrax, spandex and nylon, which are then knitted into a close-fitting outer layer and laid into a filling layer by an air-jet web forming machine. Combined with enzymatic modification treatment and rice bran wax lubrication, a nano-honeycomb pore structure and a three-dimensional protein network are formed, which enhances flexibility and antibacterial properties.
It achieves long-lasting antibacterial properties, dynamic dehumidification, and enhanced comfort in mugwort quilts. The moisture absorption, quick-drying properties, and softness of the fibers are significantly improved, forming a dual antibacterial mechanism, making it suitable for people with allergies.
Abstract
Description
TECHNICAL FIELD
[0001] The application belongs to the technical field of moxa quilt, and particularly relates to a moxa health air-conditioning quilt. BACKGROUND
[0002] With the acceleration of social aging and the continuous expansion of sub-health population, the traditional medical model is gradually changing to the concept of "prevention first, combination of prevention and treatment" of big health. According to the data of the World Health Organization, more than 75% of the global population has different degrees of sleep disorders and chronic strain problems, and the health preservation concept of "warming meridians, dredging collaterals, supporting yang and consolidating the root" shows unique value in improving such health problems.
[0003] Artemisia argyi, as an important component of traditional Chinese medicine, its leaves are rich in eucalyptol, camphor, alpha-terpinene alcohol and other active ingredients, and have significant antibacterial and anti-inflammatory, dampness and cold dispelling, and promoting microcirculation effects. Moxa, as a product processed from the leaves of Artemisia argyi, also has the above properties and the effects of warming the meridians, dispelling cold, relieving pain, and regulating blood. The application of moxa natural health care properties and sleep is the research focus of the application.
[0004] Then, the inherent brittleness of moxa fibers leads to insufficient elongation at break, restricting the spinnability and product durability; the active substances in moxa are prone to loss due to volatilization, and the health care effect is not long-lasting; the natural antibacterial ingredients in moxa are prone to cause itching and hardening of the fabric due to the large fiber rigidity and poor spinnability, and it is difficult to meet the long-term close-to-body use demand, and the ordinary air-conditioning quilt has a low moisture absorption rate, which cannot match the sweat fluctuation in the human sleep cycle, and is prone to increase the hot and humid feeling and the turning frequency. Therefore, how to improve the long-acting antibacterial, body comfort and health intervention functions of the moxa quilt is the research focus of the application. SUMMARY
[0005] The application discloses a moxa health air-conditioning quilt to solve the above and any potential problems in the prior art. In order to solve the above technical problems, the specific preparation process is as follows:
[0006] The moxa, spandex and polyamide are blended and spun to obtain blended yarn as weft yarn, Xinjiang long-staple cotton yarn is used as warp yarn for weft knitting, and the knitted fabric is used as the close-to-body outer layer, and the basis weight of the fabric is 140±5 g / m²; the moxa and the polyamide are mixed in equal quality, and are laid into uniform flake by using an air-laid machine, and are used as the filling layer, and the basis weight is 150-160 g / m², and finally needle punching is used for reinforcement, the needle punching density is 120-150 punctures / cm², and hot air 130℃ is used for reinforcement for 30s to obtain the moxa health air-conditioning quilt.
[0007] The blending spinning includes: after 20-25 parts of the moxa is dry mixed with 0.8% lubricant powder in a mixer for 5 minutes, 8-15 parts of spandex master batch and 10-20 parts of nylon are added, the temperature in the mixer is 140-155 DEG C, 180-220 rpm is premixed and stirred for 15 minutes, spinning forming: screw rotation speed: 120 rpm, conventional melt spinning, spinneret aperture 0.15 mm, hole number: 72 holes, draft ratio 1:3.5, finally treated with water vapor, 100 DEG C for 3 minutes for setting;
[0008] The lubricant is rice chaff wax.
[0009] The moxa further includes modification treatment: five-year-old moxa is selected as raw material, composite biological enzyme hydrolysis technology is adopted, solid-liquid ratio is 1:12, liquid is acetic acid solution with pH 5.0, and 0.5% cellulase, 0.3% pectinase and 0.2% xylanase are added, pH is adjusted to 5.0±0.2 by adding acid salt, 45 DEG C, 150 rpm shock reaction is carried out for 2 hours, then 80 DEG C water bath is carried out for 10 minutes for inactivation, 40 DEG C deionized water is used for rinsing twice, vacuum filtration is carried out at-0.08 MPa until the moisture content is less than or equal to 35%, the moxa is immersed in 4-8% modified solution, the solid-liquid ratio is 1:8, 60 DEG C reaction is carried out for 40 minutes, 80 rpm, then the modified moxa is immersed in 4-8% softener solution, the ratio of the dry weight of the moxa to the weight of the solution is 1:10-15, the temperature is 40-50 DEG C, the time is 20-30 minutes, then 2000 rpm is used for spinning for 10 minutes, the moxa is laid on the environment of 60-85 DEG C for hot air drying for 10 minutes to obtain flexible moxa.
[0010] The modified solution is casein glue solution.
[0011] The softener is distearyl oxy ethyl hydroxy ethyl methyl ammonium methyl sulfate.
[0012] The advantages and beneficial effects of the application are:
[0013] 1. The application fuses the high active components of five-year-old moxa and complex enzymatic hydrolysis technology, significantly improving the release efficiency of antibacterial substances, and through body temperature stimulation to simulate the effect of traditional Chinese medicine moxibustion, achieving deep cold and dampness; The nano honeycomb pore structure formed by enzymatic modification gives the fiber excellent moisture absorption and quick drying performance; Casein glue constructs a three-dimensional protein network on the surface of moxa, greatly enhances the flexibility and compatibility with spandex and nylon, synchronously releases skin-friendly amino acids to neutralize metabolic acidic substances, optimizes the sleep microenvironment combined with distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate for softening treatment; Rice chaff wax, through surface lubrication and γ-oryzanol synergy, not only ensures smooth spinning and uniform distribution of functional components, but also forms a "membrane rupture-kill" dual antibacterial mechanism with moxa active ingredients, and realizes long-acting controlled release through casein glue film, combined with repellent substances to build an anti-mite and anti-allergic barrier, ultimately obtaining a moxa air conditioner quilt that can warm the meridians, dynamically dehumidify, long-acting antibacterial and comfortable.
[0014] 2. The enzymatic moxa and blending spinning process form nano-sized honeycomb pores, which give the fiber the ability to quickly adsorb body sweat and rapidly direct it to the outside of the fiber for evaporation through capillary action and vapor diffusion, preventing moisture from remaining between the skin and the quilt.
[0015] 3. The casein glue crosslinks into a three-dimensional network protein film on the surface of moxa, binds with moxa cellulose through hydrogen bonds, and makes moxa have a certain elasticity, which can improve the processing fluidity and component compatibility of the subsequent blend, and help spandex, nylon and other fibers better exert their elasticity and strength advantages, making the mechanical properties of the overall fiber more optimal and stable, enhancing its spinnability, and ultimately achieving better mechanical properties on the fiber.
[0016] 4. However, after the casein glue treatment enhances the spinnability of the fiber, its softness performance has decreased accordingly, so distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate is added to enhance its softness. Distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate is a high-efficiency and commonly used cationic quaternary ammonium salt. The long-chain alkyl group in its molecular structure can be adsorbed on the surface of the moxa fiber, forming a soft molecular film that effectively reduces the frictional resistance between fibers, directly compensating for the increased fiber rigidity that may be caused by the crosslinking network of casein glue, giving moxa excellent loftiness. This makes the final flexible moxa not only have the strength and spinnability given by casein glue, but also have the soft and comfortable feeling required for close-to-skin products, which is a key attribute for making high-end close-to-skin textiles. This treatment makes the subsequent high-shear intensive mixing and melt spinning with synthetic fiber masterbatch such as spandex and nylon have better processing fluidity, less fiber damage, and higher uniformity of each component, resulting in softer and more breathable textiles with better moisture absorption.
[0017] 5. Rice chaff wax powder is evenly wrapped on the surface of the flexible raw silk during the dry mixing stage, playing a lubricating role, reducing fiber friction and entanglement during the subsequent high-shear intensive mixing process with nylon and spandex masterbatch, and improving the uniformity of dispersion of each component. The lubricity helps to reduce the melt viscosity, making the subsequent melt spinning process smoother, reducing broken filaments, and improving spinning stability and efficiency. As a carrier of functional components, the uniform dispersion of rice chaff wax ensures the effective distribution of antibacterial and other functions in the final fiber. A small amount of wax can slightly plasticize the blended system, helping to further improve the flexibility and processing performance of the fiber.
[0018] 6. The mechanism of action of γ-oryzanol of rice chaff wax and active ingredients of raw silk is complementary, forming a strong and lasting double antibacterial and antiviral barrier. It not only has good antibacterial effect on Escherichia coli, Candida albicans and Staphylococcus aureus, etc., but also has good antiviral activity rate on influenza virus.
[0019] 7. The three-dimensional protein film formed by casein glue not only wraps raw silk, but also effectively fixes rice chaff wax particles on the surface or near-surface area of the blended fiber. This layer of protein film itself also has a certain barrier effect. When contacting microorganisms, the surface layer of the protein film may first act, at the same time, allowing γ-oryzanol and active ingredients of raw silk to be continuously and controllably released, achieving longer and more stable double antibacterial effect, and avoiding rapid loss of effective ingredients. The volatile repellent substances of raw silk and the active ingredients in rice chaff wax work together to form an unsuitable chemical environment for pests to breed inside and on the surface of the fiber, effectively preventing mosquitoes and mites, and having good antibacterial effect, which can improve the hygiene and durability of the product, especially suitable for people prone to allergies. DETAILED DESCRIPTION
[0020] The application will be further described in detail below in combination with examples, in which the five-year-old raw silk is purchased from Nanyang Tianzheng Pharmaceutical Co., Ltd. The rice chaff wax CAS number used below is 8016-60-2, which is purchased from Beijing Likan Weiye.
[0021] Example 1
[0022] Modification of the Eri: Select five-year-old Eri as raw material, adopt composite biological enzymatic hydrolysis technology, solid-liquid ratio = 1:12, liquid is pH 5.0 acetic acid solution, and add 0.5% cellulase, 0.3% pectinase, 0.2% xylanase, add acid salt to adjust pH to 5.0, 45℃, 150rpm shock reaction 2h, then 80℃ water bath 10min inactivation, rinse with 40℃ deionized water 2 times, -0.08MPa vacuum filtration to moisture content of 30%, immerse it in 6% casein glue aqueous solution, solid-liquid ratio of 1:8, 60℃ reaction 40min, 80rpm, then immerse the modified Eri in 6% mass fraction of distearyl oxy ethyl hydroxy ethyl methyl ammonium methyl sulfate solution, according to Eri dry weight:solution weight of 1:12, temperature 45℃, time 25min, then 2000rpm spin dry 10min, flat on 72℃ environment hot air drying 10min to get flexible Eri.
[0023] Example 2
[0024] Modification of the Eri: Select five-year-old Eri as raw material, adopt composite biological enzymatic hydrolysis technology, solid-liquid ratio = 1:12, liquid is pH 5.0 acetic acid solution, and add 0.5% cellulase, 0.3% pectinase, 0.2% xylanase, add acid salt to adjust pH to 5.2, 45℃, 150rpm shock reaction 2h, then 80℃ water bath 10min inactivation, rinse with 40℃ deionized water 2 times, -0.08MPa vacuum filtration to moisture content of 32%, immerse it in 4% casein glue aqueous solution, solid-liquid ratio of 1:8, 60℃ reaction 40min, 80rpm, then immerse the modified Eri in 4% mass fraction of distearyl oxy ethyl hydroxy ethyl methyl ammonium methyl sulfate solution, according to Eri dry weight:solution weight of 1:15, temperature 50℃, time 30min, then 2000rpm spin dry 10min, flat on 85℃ environment hot air drying 10min to get flexible Eri.
[0025] Example 3
[0026] Modification of the raw silk: Select five-year-old raw silk as raw material, adopt composite biological enzymatic hydrolysis technology, solid-liquid ratio = 1:12, liquid is pH 5.0 acetic acid solution, and add 0.5% cellulase, 0.3% pectinase, 0.2% xylanase, add acid salt to adjust pH to 4.8, 45℃, 150rpm shock reaction 2h, then 80℃ water bath 10min inactivation, rinse twice with 40℃ deionized water, -0.08MPa vacuum filtration to moisture content of 35%, immerse in 8% casein glue aqueous solution, solid-liquid ratio of 1:8, 60℃ reaction 40min, 80rpm, then, immerse the modified raw silk in 4-8% distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate solution, according to the weight ratio of raw silk dry weight to solution weight is 1:10, temperature 40℃, time 20min, then 2000rpm spin dry 10min, flatly in 60℃ environment hot air drying 10min to get flexible raw silk.
[0027] Comparative Example 1
[0028] The difference between this comparative example and Example 1 is that the raw silk in this comparative example is not subjected to enzymatic hydrolysis treatment. The specific modification of the raw silk is as follows: select five-year-old raw silk as raw material, immerse it in 6% casein glue aqueous solution, solid-liquid ratio of 1:8, 60℃ reaction 40min, 80rpm, then 2000rpm spin dry 10min, flatly in 72℃ environment hot air drying 10min to get flexible raw silk.
[0029] Comparative Example 2
[0030] The difference between this comparative example and Example 1 is that the casein glue aqueous solution in this comparative example is carboxymethyl cellulose; the rest is the same as Example 1.
[0031] Comparative Example 3
[0032] The difference between this comparative example and Example 1 is that the modification of the raw silk in this example is as follows: select five-year-old raw silk as raw material, adopt composite biological enzymatic hydrolysis technology, solid-liquid ratio = 1:12, liquid is pH 5.0 acetic acid solution, and add 0.5% cellulase, 0.3% pectinase, 0.2% xylanase, add acid salt to adjust pH to 5.0, 45℃, 150rpm shock reaction 2h, then 80℃ water bath 10min inactivation, rinse twice with 40℃ deionized water, -0.08MPa vacuum filtration to moisture content of 30%, immerse it in 6% casein glue aqueous solution, solid-liquid ratio of 1:8, 60℃ reaction 40min, 80rpm, then 2000rpm spin dry 10min, flatly in 72℃ environment hot air drying 10min to get flexible raw silk.
[0033] Comparative Example 4
[0034] The difference between this comparative example and Example 1 is that the distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate is replaced by octadecyl dimethyl ammonium chloride, and the rest is the same as Example 1.
[0035] Test 1: Spinnability test
[0036] According to the standard method of ASTM D5034 for fabric tensile, the uniaxial tensile test was carried out: using a universal material testing machine to measure the stress-strain curve, to obtain the breaking strength (unit: cN / tex), elongation at break (%) and elastic modulus (unit: GPa), and to set the untreated e'er as a blank group for comparison. The results are shown in Table 1.
[0037] Table 1
[0038] Sample group Breaking strength / cN / tex Elastic modulus / GPa Breaking elongation / % Example 1 24.7 7.5 8.7 Example 2 23.8 7.2 8.5 Example 3 24.1 7.3 8.2 Blank group 17.4 3.7 5.5 Comparative Example 1 21.5 6.1 8.0 Comparative Example 2 18.5 4.6 6.3 Comparative Example 3 20.1 6.4 7.6 Comparative Example 4 20.6 6.8 7.9
[0039] From the above table, the untreated e'er blank group showed the worst spinnability, and the spinnability of the e'er without adding casein glue was also poor. Therefore, for the above spinnability test results, the e'er obtained from Example 1, Comparative Example 1, 3 and 4 was selected for further blending and spinning, and its performance was further detected.
[0040] Example 4
[0041] Take 22 parts of e'er prepared in Example 1 and 0.8% rice chaff wax powder, dry mix in an internal mixer for 5 min, then add 12 parts of spandex masterbatch and 15 parts of nylon, the temperature in the internal mixer is 148℃, 200 rpm pre-mixing stirring for 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret hole diameter 0.15mm, hole number: 72 holes, draw ratio 1:3.5, finally treated with water vapor, 100℃ for 3 min, the obtained blended spinning is used as weft yarn, Xinjiang long-staple cotton yarn is used as warp yarn for weft knitting, as the close-fitting outer layer, the greige fabric weight is 140g / m 2 ; The e'er and nylon are mixed according to equal quality, and are laid into uniform flake using an air-laid machine, as the filling layer, the weight is 15g / m², finally reinforced by needling, needling density 135 needles / cm², hot air 130℃ reinforcement for 30s to obtain e'er health air conditioning quilt.
[0042] Example 5
[0043] Take the preparation of 20 parts of the example 1 with 0.8% rice chaff wax powder in the internal mixer dry mixing 5 min, add 15 parts of spandex masterbatch and 10 parts of nylon, the temperature in the internal mixer is 155 DEG C, 180 rpm premix stirring 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret aperture 0.15 mm, hole number: 72 holes, draft ratio 1: 3.5, finally with water vapor, 100 DEG C treatment 3 min setting, the obtained blended spinning as weft yarn, using Xinjiang long hair cotton yarn as warp yarn for weft knitting, as the outer layer, the weight of the grey fabric is 145 g / m 2 ; the eucalyptus and nylon are mixed according to equal quality, using air-laid machine to lay up into uniform flake, as filling layer, the weight is 160 g / m², finally using needle punching reinforcement, needle punching density 120 needles / cm², hot air 130 DEG C reinforcement 30 s to obtain eucalyptus health air conditioning quilt.
[0044] Example 6
[0045] Take the preparation of 25 parts of the example 1 with 0.8% rice chaff wax powder in the internal mixer dry mixing 5 min, add 8 parts of spandex masterbatch and 20 parts of nylon, the temperature in the internal mixer is 140 DEG C, 220 rpm premix stirring 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret aperture 0.15 mm, hole number: 72 holes, draft ratio 1: 3.5, finally with water vapor, 100 DEG C treatment 3 min setting, the obtained blended spinning as weft yarn, using Xinjiang long hair cotton yarn as warp yarn for weft knitting, as the outer layer, the weight of the grey fabric is 135 g / m 2 ; the eucalyptus and nylon are mixed according to equal quality, using air-laid machine to lay up into uniform flake, as filling layer, the weight is 150 g / m², finally using needle punching reinforcement, needle punching density 150 needles / cm², hot air 130 DEG C reinforcement 30 s to obtain eucalyptus health air conditioning quilt.
[0046] Comparative example 5
[0047] The difference between this comparative example and example 4 is that no rice chaff wax is added in this comparative example, specifically: take 22 parts of the example 1 prepared eucalyptus, 12 parts of spandex masterbatch and 15 parts of nylon, the temperature in the internal mixer is 148 DEG C, 200 rpm premix stirring 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret aperture 0.15 mm, hole number: 72 holes, draft ratio 1: 3.5, finally with water vapor, 100 DEG C treatment 3 min setting, the obtained blended spinning as weft yarn, using Xinjiang long hair cotton yarn as warp yarn for weft knitting, as the outer layer, the weight of the grey fabric is 140 g / m 2; the e-rug and the nylon are mixed according to equal quality, laid into uniform flake by air-laid machine as filling layer, the gram weight is 15 g / m2, finally reinforced by needle punching, the needle punching density is 135 spikes / cm2, the hot air 130℃ reinforcement 30s to obtain the e-rug health air conditioner quilt.
[0048] Comparative Example 6
[0049] The difference between this comparative example and Example 4 is that the rice chaff wax powder in this comparative example is glycerin; the rest is the same as Example 4.
[0050] Comparative Example 7
[0051] The difference between this comparative example and Example 4 is that 22 parts of the flexible e-rug prepared in Example 1 and 1.5% rice chaff wax powder are dry mixed in an internal mixer for 5 min, then 12 parts of spandex masterbatch and 15 parts of nylon are added, the temperature in the internal mixer is 148℃, 200 rpm pre-mixed stirring for 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret hole diameter 0.15mm, hole number: 72 holes, draw ratio 1:3.5, finally treated with water vapor, 100℃ for 3 min to set, the obtained blended spinning yarn is used as weft yarn, Xinjiang long-staple cotton yarn is used as warp yarn for weft knitting, as the skin outer layer, the greige fabric gram weight is 140g / m 2 ; the e-rug and the nylon are mixed according to equal quality, laid into uniform flake by air-laid machine as filling layer, the gram weight is 15 g / m2, finally reinforced by needle punching, the needle punching density is 135 spikes / cm2, the hot air 130℃ reinforcement 30s to obtain the e-rug health air conditioner quilt.
[0052] Comparative Example 8
[0053] The difference between this comparative example and Example 4 is that 22 parts of the flexible e-rug prepared in Example 1 and 0.4% rice chaff wax powder are dry mixed in an internal mixer for 5 min, then 12 parts of spandex masterbatch and 15 parts of nylon are added, the temperature in the internal mixer is 148℃, 200 rpm pre-mixed stirring for 15 min, spinning forming: screw speed: 120 rpm, conventional melt spinning, spinneret hole diameter 0.15mm, hole number: 72 holes, draw ratio 1:3.5, finally treated with water vapor, 100℃ for 3 min to set, the obtained blended spinning yarn is used as weft yarn, Xinjiang long-staple cotton yarn is used as warp yarn for weft knitting, as the skin outer layer, the greige fabric gram weight is 140g / m 2 ; the e-rug and the nylon are mixed according to equal quality, laid into uniform flake by air-laid machine as filling layer, the gram weight is 15 g / m2, finally reinforced by needle punching, the needle punching density is 135 spikes / cm2, the hot air 130℃ reinforcement 30s to obtain the e-rug health air conditioner quilt.
[0054] Comparative Example 9
[0055] The above 22 parts of the raw material of the example 1 were mixed with 0.8% of the rice chaff wax powder in a mixer for 5 minutes, then 12 parts of the spandex master batch and 15 parts of the polyamide were added, the temperature in the mixer was 148°C, and the mixer was stirred at 200 rpm for 15 minutes. The spinning was formed by the screw rotation speed of 120 rpm, the conventional melt spinning, the spinneret aperture of 0.15 mm, the hole number of 72, the draft ratio of 1:3.5, and finally the spinning was treated by the water vapor at 100°C for 3 minutes to shape. The obtained blended yarn was used as the weft yarn, and the Xinjiang long-staple cotton yarn was used as the warp yarn to perform the weft knitting, which was used as the skin layer. The weight of the fabric was 140 g / m 2 The raw material of the example 1 was mixed with the polyamide in the equal quality, and the air-laid machine was used to lay the uniform flake as the filling layer with the weight of 15 g / m². Finally, the needle punching was used for reinforcement with the needle punching density of 135 / cm², and the hot air of 130°C was used for reinforcement for 30 seconds to obtain the raw material of the health air conditioner quilt.
[0056] Comparative example 10
[0057] The above 22 parts of the raw material of the example 1 were mixed with 0.8% of the rice chaff wax powder in a mixer for 5 minutes, then 12 parts of the spandex master batch and 15 parts of the polyamide were added, the temperature in the mixer was 148°C, and the mixer was stirred at 200 rpm for 15 minutes. The spinning was formed by the screw rotation speed of 120 rpm, the conventional melt spinning, the spinneret aperture of 0.15 mm, the hole number of 72, the draft ratio of 1:3.5, and finally the spinning was treated by the water vapor at 100°C for 3 minutes to shape. The obtained blended yarn was used as the weft yarn, and the Xinjiang long-staple cotton yarn was used as the warp yarn to perform the weft knitting, which was used as the skin layer. The weight of the fabric was 140 g / m 2 The raw material of the example 1 was mixed with the polyamide in the equal quality, and the air-laid machine was used to lay the uniform flake as the filling layer with the weight of 15 g / m². Finally, the needle punching was used for reinforcement with the needle punching density of 135 / cm², and the hot air of 130°C was used for reinforcement for 30 seconds to obtain the raw material of the health air conditioner quilt.
[0058] Comparative example 11
[0059] The above 22 parts of the raw material of the example 1 were mixed with 0.8% of the rice chaff wax powder in a mixer for 5 minutes, then 12 parts of the spandex master batch and 15 parts of the polyamide were added, the temperature in the mixer was 148°C, and the mixer was stirred at 200 rpm for 15 minutes. The spinning was formed by the screw rotation speed of 120 rpm, the conventional melt spinning, the spinneret aperture of 0.15 mm, the hole number of 72, the draft ratio of 1:3.5, and finally the spinning was treated by the water vapor at 100°C for 3 minutes to shape. The obtained blended yarn was used as the weft yarn, and the Xinjiang long-staple cotton yarn was used as the warp yarn to perform the weft knitting, which was used as the skin layer. The weight of the fabric was 140 g / m 2The e-mulberry and the nylon are mixed according to equal quality, laid up into uniform flake by air laying machine, used as filling layer, the gram weight is 15g / m2, finally reinforced by needle punching, the needle punching density is 135 strokes / cm2, the hot air 130℃ reinforcement 30s, the e-mulberry health air conditioning quilt is obtained.
[0060] Test 2: detection of hygroscopicity and bulkiness
[0061] The hygroscopicity test is carried out according to GB / T 21655.1-2008. 5 pieces of 10cm×10cm samples are cut, and are adjusted for 24 hours under standard temperature and humidity. Soaked in three-stage water for 5 minutes, vertically hung until no dripping water, weighed, and the average value was measured. The results are shown in Table 2.
[0062] The water absorption rate = (wet weight-dry weight) / dry weight×100%
[0063] The e-mulberry quilt is detected for bulkiness according to GB / T 40976-2021 standard, the bulkiness (unit: mm) is calculated by measuring the volume change under gradient pressure. The formula is:
[0064] P moxa =P1-P2
[0065] Wherein, P1 is the height after 50g pressure disc standing for 10 minutes, P2 is the height after adding 500g pressure disc standing for 10 minutes. The results are shown in Table 3.
[0066] Table 2
[0067] Sample group Moisture absorption rate / % Example 4 9.5 Example 5 9.3 Example 6 9.2 Comparative Example 5 7.9 Comparative Example 6 8.1 Comparative Example 7 8.7 Comparative Example 8 8.3 Comparative Example 9 8.8 Comparative Example 10 8.5 Comparative Example 11 8.3
[0068] Table 3
[0069] Sample group Loft / mm Example 4 85 Example 5 83 Example 6 81 Comparative Example 1 69 Comparative Example 5 72 Comparative Example 6 73 Comparative Example 7 78 Comparative Example 8 74 Comparative Example 9 80 Comparative Example 10 76 Comparative Example 11 78
Claims
1. A health air-conditioning quilt of mulberry silk, characterized in that, The specific preparation process is: The moxa, spandex and nylon are blended and spun to obtain blended yarn as weft yarn, Xinjiang long-staple cotton yarn is used as warp yarn for weft knitting, as the outer layer, the weight of the gray fabric is 140±5g / m²; the moxa and nylon are mixed according to equal quality, and are laid into uniform flake by air laying machine, as the filling layer, the weight is 150-160g / m², finally needle punching is used for reinforcement, the needle punching density is 120-150 / cm², hot air 130°C reinforcement for 30s to obtain moxa health air conditioner quilt; The blended yarn comprises: 20-25 parts of moxa and 0.8% lubricant powder are dry mixed in an internal mixer for 5min, then 8-15 parts of spandex master batch and 10-20 parts of nylon are added, the temperature in the internal mixer is 140-155°C, 180-220rpm pre-mixing stirring for 15min, spinning forming: screw speed: 120rpm, conventional melt spinning, spinneret hole diameter 0.15mm, hole number: 72 holes, draw ratio 1:3.5, finally treated with water vapor, 100°C for 3min to set.
2. The air conditioning blanket of claim 1, wherein: The lubricant is rice chaff wax.
3. The air conditioning blanket of claim 1, wherein: The moxa also comprises modification treatment: five-year-old moxa is selected as raw material, composite biological enzyme hydrolysis technology is used, solid-liquid ratio=1:12, liquid is pH 5.0 acetic acid solution, and 0.5% cellulase, 0.3% pectinase and 0.2% xylanase are added, pH is adjusted to 5.0±0.2 by adding acid salt, 45°C, 150rpm shock reaction for 2h, then 80°C water bath for 10min to inactivate, rinsed with 40°C deionized water for 2 times, vacuum filtration at-0.08MPa to the moisture content≤35%, then immersed in 4-8% modified solution, solid-liquid ratio is 1:8, 60°C reaction for 40min, 80rpm, then the modified moxa is immersed in 4-8% softener solution, according to the weight ratio of moxa dry weight to solution weight is 1:10-15, temperature is 40-50°C, time is 20-30min, then 2000rpm spin-drying for 10min, flatly laid in 60-85°C environment for hot air drying for 10min to obtain flexible moxa.
4. The air conditioning blanket of claim 3, wherein: The modified solution is casein glue solution.
5. The air conditioning blanket of claim 3, wherein: The softener is distearyl oxy ethyl hydroxyethyl methyl ammonium methyl sulfate.
Citation Information
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