Real-time detection equipment for recovering metals from circulating mother liquor by Bayer process

By designing a Bayer method recycling mother liquor recovery metal detection equipment with automatic sampling and real-time detection, the mother liquor leakage and manpower waste caused by manual sampling are solved, and efficient and safe gallium metal detection is achieved.

CN222979145UActive Publication Date: 2025-06-13GUIZHOU HAIHAO NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202421904448.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-08-07
Publication Date
2025-06-13
Estimated Expiration
2034-08-07

AI Technical Summary

Technical Problem

During the detection of gallium metal in the Bayer method of circulating mother liquor, the prior art requires manual sampling of samples, resulting in mother liquor leakage and waste of manpower.

Method used

A real-time detection device for recycling mother liquor recycling metal was designed, and the sampling ring was driven by a water wheel to automatically take samples. The shell was designed to avoid manual extraction and mother liquor leakage.

Benefits of technology

Automatic sampling and real-time detection of mother liquor is realized, avoiding mother liquor leakage and waste of manpower, and improving detection efficiency and safety.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model provides real-time detection equipment for recovering metals from circulating mother liquor by a Bayer process, and relates to the technical field of detection devices. A sampling detection shell is welded at the top of the mother liquor circulating pipeline; a water wheel is rotationally mounted on the inner side of the sampling detection shell; six connecting rods are annularly arranged and fixed on the front side of a central shaft of the water wheel; a sampling ring is fixed on the front sides of the six connecting rods; and a metal detection sensor is also fixed in the middle of the front side of the sampling detection shell. According to the detection equipment, an opening for extracting mother liquor does not need to be formed in the pipeline, mother liquor leakage is avoided, manual mother liquor extraction is not needed, and more time and labor are saved during detection.
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Description

Technical Field

[0001] The utility model relates to the technical field of detection devices, in particular to a real-time detection device for recovering metals from Bayer process circulating mother liquor. Background Art

[0002] Gallium metal is an excellent semiconductor material, widely used in the fields of electronics industry, integrated circuits, infrared detection, etc. It is a supporting material for the information industry. When extracting gallium metal, it is mostly extracted and recovered from bauxite by relying on the circulation of Bayer process mother liquor. During the extraction process, it is often necessary to detect the gallium metal in the mother liquor.

[0003] Currently, when detecting gallium metal in Bayer mother liquor, it is necessary to sample the mother liquor first. When sampling, workers need to manually extract it from the pipeline. In this way, the pipeline needs to be provided with an opening for extracting the mother liquor, which is prone to mother liquor leakage. Moreover, the operation of manually extracting samples for detection is also relatively labor-consuming. Summary of the Invention

[0004] The utility model provides a real-time detection device for recovering metals from Bayer process circulating mother liquor, which does not need to set an opening for extracting mother liquor on the pipeline, avoids mother liquor leakage, and does not require manual extraction of mother liquor, saving time and effort during detection.

[0005] In the first aspect of the present disclosure, a real-time detection device for recovering metals from Bayer process circulating mother liquor is provided, specifically including: a mother liquor circulation pipeline;

[0006] A sampling and detection housing is welded to the top of the mother liquor circulation pipeline; a water wheel is rotatably installed inside the sampling and detection housing; six connecting rods are fixedly arranged in a circular arrangement on the front side of the central axis of the water wheel; a sampling ring is fixed to the front sides of the six connecting rods; a metal detection sensor is also fixed at the middle position on the front side of the sampling and detection housing.

[0007] In at least some embodiments, four through holes are arranged in a circular arrangement on the sampling ring, and the lower part of the sampling ring is also located in the cavity inside the mother liquor circulation pipeline.

[0008] In at least some embodiments, the cavity inside the sampling and detection housing is communicated with the cavity inside the mother liquor circulation pipeline, and the blades at the bottom of the water wheel are located in the cavity inside the mother liquor circulation pipeline.

[0009] In at least some embodiments, a through hole is arranged on the front outer wall of the sampling and detection housing, and when the through holes on the sampling ring rotate to the uppermost position, they will be vertically aligned with the through hole on the front outer wall of the sampling and detection housing.

[0010] In at least some embodiments, the rear side of the sampling and detection housing is a cylindrical cavity, and the water wheel can rotate in the cylindrical cavity, and the front side of the sampling and detection housing is a circular ring cavity.

[0011] In at least some embodiments, the metal detection sensor is located directly below the circular hole on the front outer wall of the sampling and detection housing.

[0012] In at least some embodiments, the front outer wall of the sampling ring is in close contact with the front inner wall of the sampling detection shell, and the inner wall and outer wall of the sampling ring are in close contact with the inner wall of the annular cavity on the front side of the sampling detection shell.

[0013] The utility model provides a real-time detection device for recovering metal from circulating mother liquor of the Bayer process, which has the following beneficial effects:

[0014] The circular hole arranged on the sampling ring in the utility model can sample the mother liquor. When the mother liquor flows in the mother liquor circulation pipeline, the sampling ring will be driven to rotate by the water wheel, so that the sampling ring can automatically sample the mother liquor, and when the circular hole on the sampling ring rotates to the top, the collected mother liquor will automatically flow out for detection. The detection equipment does not need to set an opening for extracting the mother liquor on the pipeline to avoid leakage of the mother liquor, and does not need to manually extract the mother liquor, which saves time and effort during detection. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] In order to more clearly illustrate the technical solution of the embodiment of the utility model, the drawings of the embodiment will be briefly introduced below.

[0016] The drawings described below only relate to some embodiments of the present invention, but are not intended to limit the present invention.

[0017] In the attached picture:

[0018] Figure 1 A schematic diagram showing the main shaft side of the overall structure of the present application;

[0019] Figure 2 A schematic diagram of the front left axle side after cutting of the present application is shown;

[0020] Figure 3 Another schematic diagram of the main shaft side after cutting of the present application is shown;

[0021] Figure 4 It shows the axial schematic diagram of the sampling and detection housing after partial sectioning in the present application;

[0022] Figure 5 A schematic diagram of the main shaft side of the water wheel and the sampling ring in the present application is shown;

[0023] Figure 6 A schematic diagram of the rear axle side of the water wheel and the sampling ring in the present application is shown;

[0024] List of Reference Numerals

[0025] 1. Mother liquor circulation pipeline; 2. Sampling and detection housing; 3. Water wheel; 4. Connecting rod; 5. Sampling ring; 6. Metal detection sensor. Detailed Implementation Manner

[0026] To make the objectives, technical solutions and advantages of the embodiments of the present utility model clearer, the technical solutions of the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are some, but not all, of the embodiments of the present utility model. All other embodiments obtained by those of ordinary skill in the art based on the described embodiments of the present utility model without creative efforts shall fall within the scope of protection of the present utility model.

[0027] Embodiment 1: Please refer to Figures 1 to 6 :

[0028] The present utility model provides a real-time metal detection device for recycling mother liquor in the Bayer process, including: a mother liquor circulation pipeline 1;

[0029] A sampling and detection housing 2 is welded to the top of the mother liquor circulation pipeline 1. When extracting and recycling gallium metal by the Bayer process, the mother liquor can flow from left to right in the mother liquor circulation pipeline 1. The sampling and detection housing 2 is used to rotationally support the water wheel 3 and the sampling ring 5, and can seal the cavity inside the mother liquor circulation pipeline 1 to prevent the mother liquor in the mother liquor circulation pipeline 1 from leaking out; A water wheel 3 is rotatably installed inside the sampling and detection housing 2. When the mother liquor flows in the mother liquor circulation pipeline 1, it will contact the blades on the outer side of the water wheel 3 at the bottom. Therefore, the blades on the outer side of the water wheel 3 can drive the water wheel 3 to rotate inside the sampling and detection housing 2, and when the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously through the connecting rod 4; Six connecting rods 4 are fixedly arranged in a circular array on the front side of the central axis of the water wheel 3. When the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously through the connecting rod 4; A sampling ring 5 is fixed to the front side of the six connecting rods 4. When the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously. When the circular hole on the sampling ring 5 rotates to the lowest position, this circular hole will be located in the cavity inside the mother liquor circulation pipeline 1. Therefore, the mother liquor in the mother liquor circulation pipeline 1 can enter the circular hole on the sampling ring 5 to complete sampling; A metal detection sensor 6 is also fixed at the middle position on the front side of the sampling and detection housing 2. When the circular hole on the sampling ring 5 rotates to the highest position, this circular hole will be aligned vertically with the circular hole on the outer wall of the front side of the sampling and detection housing 2. Therefore, the mother liquor in this circular hole will flow down to the metal detection sensor 6 through the circular hole on the outer wall of the front side of the sampling and detection housing 2. Therefore, it can be detected whether the mother liquor contains metal through the metal detection sensor 6.

[0030] In the embodiments of the present disclosure, as Figure 2 , Figure 3 , Figure 5 and Figure 6 shown, four through holes penetrating inside and outside are arranged in a circular pattern on the sampling ring 5, and the lower part of the sampling ring 5 is also located in the cavity inside the mother liquor circulation pipeline 1. When the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously. When the through hole on the sampling ring 5 rotates to the lowest position, this through hole will be located in the cavity inside the mother liquor circulation pipeline 1. Therefore, the mother liquor in the mother liquor circulation pipeline 1 can enter the through hole on the sampling ring 5 to complete sampling.

[0031] In the embodiments of the present disclosure, as Figure 2 and Figure 3 shown, the cavity inside the sampling and detection housing 2 is communicated with the cavity inside the mother liquor circulation pipeline 1. The blades at the bottom of the water wheel 3 are located in the cavity inside the mother liquor circulation pipeline 1. When the mother liquor flows in the mother liquor circulation pipeline 1, it will contact the blades on the outer side and at the bottom of the water wheel 3. Therefore, the water wheel 3 can be driven to rotate inside the sampling and detection housing 2 by the blades on the outer side of the water wheel 3, and when the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously through the connecting rod 4.

[0032] In the embodiments of the present disclosure, as Figures 2 to 4 shown, a through hole penetrating inside and outside is provided on the front outer wall of the sampling and detection housing 2, and when the through hole on the sampling ring 5 rotates to the highest position, it will be aligned vertically with the through hole on the front outer wall of the sampling and detection housing 2. When the through hole on the sampling ring 5 rotates to the highest position, this through hole will be aligned vertically with the through hole on the front outer wall of the sampling and detection housing 2. Therefore, the mother liquor in this through hole will flow downward through the through hole on the front outer wall of the sampling and detection housing 2 to the metal detection sensor 6. Therefore, it can be detected whether there is metal in the mother liquor through the metal detection sensor 6.

[0033] In the embodiments of the present disclosure, as Figure 2 and Figure 4 shown, the rear side of the sampling and detection housing 2 is a cylindrical cavity, and the water wheel 3 can rotate in this cylindrical cavity. The front side of the sampling and detection housing 2 is an annular cavity. When the mother liquor flows in the mother liquor circulation pipeline 1, it will contact the blades on the outer side and at the bottom of the water wheel 3. Therefore, the water wheel 3 can be driven to rotate inside the sampling and detection housing 2 by the blades on the outer side of the water wheel 3, and when the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously in the annular cavity on the front side of the sampling and detection housing 2 through the connecting rod 4.

[0034] In the embodiments of the present disclosure, as Figure 2 and Figure 3As shown, the front outer wall of the sampling ring 5 is in close contact with the front inner wall of the sampling and detection housing 2. Both the inner wall and the outer wall of the axial ring of the sampling ring 5 are in close contact with the inner wall of the front circular cavity of the sampling and detection housing 2. When the circular hole on the sampling ring 5 rotates to the lowest position, this circular hole will be located in the cavity inside the mother liquor circulation pipe 1. Therefore, the mother liquor in the mother liquor circulation pipe 1 can enter the circular hole on the sampling ring 5. Then, the sampling ring 5 will continue to rotate. When the circular hole on the sampling ring 5 is located inside the sampling and detection housing 2, the inner wall of the front circular cavity of the sampling and detection housing 2 will seal the circular hole to prevent the mother liquor collected in the circular hole from leaking outwards.

[0035] Embodiment 2, on the basis of Embodiment 1, as Figures 1 to 6 shown, the metal detection sensor 6 is located directly below the circular hole on the front outer wall of the sampling and detection housing 2. When the circular hole on the sampling ring 5 rotates to the highest position, this circular hole will be aligned vertically with the circular hole on the front outer wall of the sampling and detection housing 2. Therefore, the mother liquor in this circular hole will flow down through the circular hole on the front outer wall of the sampling and detection housing 2 to the metal detection sensor 6. Therefore, it can be detected by the metal detection sensor 6 whether there is metal in the mother liquor.

[0036] The working principle of this embodiment: When extracting and recovering gallium metal by the Bayer process, the mother liquor can flow from left to right in the mother liquor circulation pipe 1. When the mother liquor flows in the mother liquor circulation pipe 1, it will contact the blades located at the bottom on the outside of the water wheel 3. Therefore, the blades on the outside of the water wheel 3 can drive the water wheel 3 to rotate inside the sampling and detection housing 2. When the water wheel 3 rotates, it will drive the sampling ring 5 to rotate synchronously through the connecting rod 4. When the circular hole on the sampling ring 5 rotates to the lowest position, this circular hole will be located in the cavity inside the mother liquor circulation pipe 1. Therefore, the mother liquor in the mother liquor circulation pipe 1 can enter the circular hole on the sampling ring 5. Then, the sampling ring 5 will continue to rotate. When the circular hole on the sampling ring 5 is located inside the sampling and detection housing 2, the inner wall of the front circular cavity of the sampling and detection housing 2 will seal the circular hole to prevent the mother liquor collected in the circular hole from leaking outwards. When this circular hole rotates to the highest position, this circular hole will be aligned vertically with the circular hole on the front outer wall of the sampling and detection housing 2. Therefore, the mother liquor in this circular hole will flow down through the circular hole on the front outer wall of the sampling and detection housing 2 to the metal detection sensor 6. Therefore, it can be detected by the metal detection sensor 6 whether there is metal in the mother liquor, and thus the extraction progress of gallium metal can be obtained.

[0037] In this article, the following points need to be noted:

[0038] 1. The drawings of the embodiments of the present disclosure only relate to the structures involved in the embodiments of the present disclosure. Other structures can refer to the general design.

[0039] 2. Without conflict, the embodiments of the present disclosure and the features in the embodiments can be combined with each other to obtain new embodiments.

[0040] The above are only specific embodiments of the present disclosure, but the protection scope of the present disclosure is not limited thereto. Any person skilled in the art within the technical scope disclosed by the present disclosure can easily think of changes or substitutions, which should all be covered within the protection scope of the present disclosure. Therefore, the protection scope of the present disclosure shall be subject to the protection scope of the claims.

Claims

1. A real-time detection device for recovering metals from circulating mother liquor of the Bayer process, comprising: The mother liquid circulation pipeline (1) is characterized by: A sampling detection shell (2) is welded to the top of the mother liquid circulation pipeline (1); a water wheel (3) is rotatably mounted inside the sampling detection shell (2); six connecting rods (4) are fixed in a circular arrangement in front of the central axis of the water wheel (3); a sampling ring (5) is fixed in front of the six connecting rods (4); and a metal detection sensor (6) is also fixed in the middle position of the front side of the sampling detection shell (2).

2. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The cavity inside the sampling and detection housing (2) is communicated with the cavity inside the mother liquid circulation pipeline (1), and the blades at the bottom of the water wheel (3) are located in the cavity inside the mother liquid circulation pipeline (1).

3. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The rear side of the sampling and detection housing (2) is a cylindrical cavity, and the water wheel (3) can rotate in the cylindrical cavity; the front side of the sampling and detection housing (2) is a circular ring cavity.

4. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The front outer wall of the sampling ring (5) is in close contact with the front inner wall of the sampling detection shell (2), and the inner wall and outer wall of the shaft ring of the sampling ring (5) are both in close contact with the inner wall of the annular cavity on the front side of the sampling detection shell (2).

5. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The sampling ring (5) is provided with four circular holes arranged in a ring shape and penetrating inside and outside, and the lower part of the sampling ring (5) is also located in the cavity inside the mother liquid circulation pipeline (1).

6. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The front outer wall of the sampling detection housing (2) is provided with a circular hole penetrating inside and outside, and when the circular hole on the sampling ring (5) is rotated to the uppermost position, it will be aligned with the circular hole on the front outer wall of the sampling detection housing (2) in the upper and lower directions.

7. A real-time detection device for recovering metals from Bayer process circulating mother liquor according to claim 1, characterized in that: The metal detection sensor (6) is located directly below the circular hole on the front outer wall of the sampling detection housing (2).