Purifying device for developing titanate coupling agent

Abstract

The utility model relates to the technical field of coupling agent purification, and discloses a titanate coupling agent purification device which comprises a reaction kettle, a fixed base and a heating and stirring mechanism, the fixed base comprises a first bottom plate, a hydraulic cylinder, a second bottom plate and a baffle, and a rear fixed frame is fixedly arranged on one side of the upper end of the first bottom plate; a plurality of second supporting blocks are fixedly arranged at the upper end of the baffle, balls are arranged at the upper ends of the second supporting blocks, the reaction kettle comprises a kettle body, a front fixing frame and two sliding rails, the heating and stirring mechanism comprises a motor and a spiral sliding groove, and a rotating shaft is fixedly arranged at the output end of the motor. And connecting columns are arranged around the rotating shaft in a sliding manner. When the reaction kettle is used, raw materials in the reaction kettle can be uniformly heated through the heating and stirring mechanism, so that the reaction effect of the reaction kettle is better, and in addition, the reaction kettle can be very conveniently assembled and disassembled through the fixed base.

Description

Technical Field

[0001] The utility model relates to the technical field of coupling agent purification, in particular to a purification device for developing titanate coupling agents. Background Technique

[0002] Titanate coupling agents have good coupling effects in filler systems such as thermoplastics, thermosetting plastics, and rubbers. Titanate coupling agents can be roughly divided into four categories according to their structures: monoalkoxy type, monoalkoxy pyrophosphate type, chelating type, and coordination type. When applied in the rubber industry, they can play a reinforcing role in filler modification, reduce the usage of rubber and anti-aging agents, improve the wear resistance and anti-aging ability of products, and significantly improve their gloss.

[0003] When the existing device is in use, in order to achieve uniform heating of the materials inside the reaction kettle, a heating component with heating and stirring functions is usually set to heat the materials, and then an additional power mechanism needs to be added to drive the heating component to move up and down to achieve uniform heating. However, this will not only increase the cost but also reduce the space inside the reaction kettle. The power device of the first heating and stirring component is arranged inside the reaction kettle, which is not convenient for maintenance. Therefore, this application provides a purification device for developing titanate coupling agents to solve the problems raised in the above background technique. Content of the Utility Model

[0004] The purpose of the utility model is to solve the deficiencies existing in the prior art, and a purification device for developing titanate coupling agents is proposed. When the device is in use, the motor drives the rotating shaft to rotate, the rotating shaft drives the connecting column to rotate, the connecting column drives the heating component to rotate, and the heating component drives the fixed block to rotate. The fixed ring block is slidably clamped inside the spiral chute. When the heating component rotates, it can move up and down through the fixed block, which is beneficial to heating the materials more uniformly, making the reaction effect better and improving its purity.

[0005] To achieve the above purpose, the utility model provides the following technical solution: A purification device for developing titanate coupling agents, including a reaction kettle, a fixed base, and a heating and stirring mechanism. The fixed base includes a first bottom plate, a hydraulic cylinder, a second bottom plate, and a baffle. A rear fixed frame is fixedly arranged on one side of the upper end of the first bottom plate. A plurality of second support blocks are fixedly arranged on the upper end of the baffle. Ball beads are arranged on the upper ends of the plurality of second support blocks. The reaction kettle includes a kettle body, a front fixed frame, and two slide rails;

[0006] The heating and stirring mechanism includes a motor and a spiral chute. A rotating shaft is fixedly arranged at the output end of the motor. A connecting column is slidably arranged around the rotating shaft. A heating component is fixedly arranged on one side of the connecting column. Conical blocks are fixedly arranged on both sides of the heating component. A fixing block is fixedly arranged at the end of the heating component away from the connecting column. The heating component, the two conical blocks and the fixing block are all provided in three groups. The sliding blocks on the mutually separated sides of the three fixing blocks are all arranged inside the spiral chute;

[0007] Through the above technical solution, when the device is in use, the motor drives the rotating shaft to rotate, and the rotating shaft drives the connecting column, the heating component and the fixing block to rotate together. Since the fixing block is slidably clamped inside the spiral chute, the heating component will move up and down while rotating, which is beneficial to heating the material more evenly, making its reaction effect better and improving its purity. In addition, since the three groups of heating components have different heights, there is a larger stirring space during rotation, which is beneficial to improving the stirring effect and making the material heating more uniform.

[0008] Further, four support legs are fixedly arranged at the upper end of the second bottom plate. The first bottom plate is fixedly arranged at the upper ends of the four support legs. A groove is formed on one side of the first bottom plate away from the rear fixing frame;

[0009] Through the above technical solution, the four support legs are beneficial to supporting the first bottom plate and leaving a space for installing the hydraulic cylinder. The first bottom plate is beneficial to supporting the reaction kettle. The groove is beneficial to fixing the front fixing frame.

[0010] Further, a hydraulic cylinder is fixedly arranged in the middle at the upper end of the second bottom plate. The baffle is fixedly arranged at the upper end of the hydraulic cylinder. The first bottom plate is provided with a plurality of through holes in a penetrating manner. A plurality of balls are all arranged inside the through holes;

[0011] Through the above technical solution, the hydraulic cylinder is beneficial to pushing the baffle, and the baffle pushes the balls to make the balls higher than the upper end surface of the first bottom plate, facilitating the movement of the reaction kettle.

[0012] Further, two sliding rails are fixedly arranged at the lower end of one side of the kettle body. The front fixing frame is slidably clamped at the lower end of one side of the kettle body through the two sliding rails. A clamping block is fixedly arranged at the lower end of the front fixing frame. Two first support blocks are fixedly arranged at the lower end of the kettle body;

[0013] Through the above technical solution, the front fixing frame is beneficial to being connected with the rear fixing frame, and is beneficial to fixing the kettle body at the upper end of the first bottom plate so that it will not move. The two first support blocks are beneficial to supporting the front fixing frame so that it will not fall off. The fixing block is beneficial to making the front fixing frame more stable.

[0014] Furthermore, a handle is fixedly arranged at the upper end of the front fixing frame on the side far away from the kettle body, and a through hole is formed in the middle of the side of the front fixing frame far away from the kettle body;

[0015] Through the above technical solution, the handle is beneficial to lift the front fixing frame to separate it from the rear fixing frame, facilitating the disassembly of the reactor. Through the through hole, it is beneficial to connect the pipeline and take out the material.

[0016] Furthermore, a protective cover is fixedly arranged at the upper end of the kettle body, and a feed inlet is fixedly arranged on the upper side of the front end of the reactor;

[0017] Through the above technical solution, the protective cover is beneficial to protect the motor. Through the feed inlet, it is beneficial to convey raw materials into the kettle body, facilitating the subsequent purification steps.

[0018] Furthermore, the front fixing frame and the rear fixing frame are slidably clamped together, and the heights of the three heating components, the fixing blocks and the conical blocks are inconsistent;

[0019] Through the above technical solution, it is beneficial to very conveniently separate the front fixing frame and the rear fixing frame, beneficial to having a larger stirring space and avoiding heat concentration.

[0020] The utility model has the following beneficial effects:

[0021] 1. The purification device for developing titanate coupling agent proposed by the utility model, when in use, drives the rotating shaft to rotate through the motor, the rotating shaft drives the connecting column to rotate, the connecting column drives the heating component and the fixing block to rotate, and one end of the fixing block is slidably clamped inside the spiral chute. When the fixing block rotates, the spiral chute will drive the fixing block to move up and down, which is beneficial to making the material heat more evenly, making its reaction effect better, improving its purity. Through the conical blocks on both sides of the heating component, it is beneficial to make the resistance of the heating component smaller when rotating, reducing the burden on the motor, and only one motor is needed, saving cost and reducing energy consumption. And the motor is installed outside the reactor, facilitating the maintenance of the motor and reducing the occupation of the space inside the reactor.

[0022] 2. The purification device for developing titanate coupling agent proposed by the utility model, when disassembling the reactor, can lift the front fixing frame through the handle, then push the baffle through the hydraulic cylinder, push the second support block and the ball through the baffle, so that the ball lifts the reactor. At this time, the reactor is at the upper end of multiple balls. At this time, lift the front fixing frame through the handle to separate it from the rear fixing frame, and then the reactor can be moved more easily, which is beneficial to more conveniently disassembling and installing the reactor. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 It is the rear axonometric schematic diagram of the utility model;

[0024] Figure 2 It is the front view axonometric schematic diagram of the present utility model;

[0025] Figure 3 It is the exploded schematic diagram of the fixed base of the present utility model;

[0026] Figure 4 It is the axonometric schematic diagram of the reaction kettle of the present utility model;

[0027] Figure 5 It is the sectional view schematic diagram of the reaction kettle of the present utility model.

[0028] Legend description:

[0029] 1. Protection cover; 2. Reaction kettle; 3. Fixed base; 4. Feed inlet; 5. Heating and stirring mechanism; 201. Kettle body; 202. Slide rail; 203. First support block; 204. Clamping block; 205. Front fixing frame; 206. Handle; 207. Through hole; 301. Rear fixing frame; 302. First bottom plate; 303. Second support block; 304. Hydraulic cylinder; 305. Ball; 306. Groove; 307. Support leg; 308. Baffle; 309. Second bottom plate; 501. Motor; 502. Spiral chute; 503. Heating component; 504. Fixed block; 505. Tapered block; 506. Connecting column; 507. Rotating shaft. Specific embodiments

[0030] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all the embodiments. Based on the embodiments in the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present utility model.

[0031] Refer to Figures 1-5 , the purification device for developing titanate coupling agent provided by this application includes a reaction kettle 2, a fixed base 3, and a heating and stirring mechanism 5. The fixed base 3 includes a first bottom plate 302, a hydraulic cylinder 304, a second bottom plate 309, and a baffle 308. A rear fixing frame 301 is fixedly arranged on one side of the upper end of the first bottom plate 302. A plurality of second support blocks 303 are fixedly arranged on the upper end of the baffle 308. A ball 305 is arranged on the upper end of each of the plurality of second support blocks 303. The reaction kettle 2 includes a kettle body 201, a front fixing frame 205, and two slide rails 202;

[0032] Through a plurality of balls 305, it is beneficial to make the reaction kettle 2 move more easily. Through the rear fixing frame 301, it is beneficial to combine with the front fixing frame 205 to form a whole and fix the kettle body 201 so that it will not move.

[0033] The heating and stirring mechanism 5 includes a motor 501 and a spiral chute 502. A rotating shaft 507 is fixedly arranged at the output end of the motor 501. A connecting column 506 is slidably arranged around the rotating shaft 507. A heating component 503 is fixedly arranged on one side of the connecting column 506. Conical blocks 505 are fixedly arranged on both sides of the heating component 503. A fixing block 504 is fixedly arranged at the end of the heating component 503 away from the connecting column 506. The heating component 503, the two conical blocks 505 and the fixing block 504 are all provided in three groups. The mutually remote sides of the three fixing blocks 504 are all slidably arranged inside the spiral chute 502.

[0034] The motor 501 is beneficial to drive the rotation of the rotating shaft 507. Through the rotating shaft 507, it is beneficial to drive the rotation of the connecting column 506 and the heating component 503. Through the heating component 503, it is beneficial to heat the material so that the material undergoes a chemical reaction. Through the two conical blocks 505, it is beneficial to reduce the resistance when the heating component 503 rotates and reduce the burden on the motor 501. Through the spiral chute 502, it is beneficial to drive the fixing block 504 and the heating component 503 to move up and down, making the heating effect more uniform.

[0035] Four support legs 307 are fixedly arranged at the upper end of the second bottom plate 309, which is beneficial to support the first bottom plate 302 and leave a space for installing the hydraulic cylinder 304. The first bottom plate 302 is fixedly arranged at the upper ends of the four support legs 307, which is beneficial to support the reaction kettle 2. A groove 306 is opened on one side of the first bottom plate 302 away from the rear fixing frame 301, which is beneficial to make the front fixing frame 205 more stable. A hydraulic cylinder 304 is fixedly arranged in the middle at the upper end of the second bottom plate 309, which is beneficial to push the baffle 308. The baffle 308 is fixedly arranged at the upper end of the hydraulic cylinder 304, which is beneficial to push a plurality of balls 305 simultaneously. A plurality of through holes are penetrated through the first bottom plate 302, which is beneficial to store a plurality of balls 305 and prevent them from extruding the bottom of the kettle body 201 and causing deformation. A plurality of balls 305 are all arranged inside the through holes, which is beneficial to move the reaction kettle 2. Two slide rails 202 are fixedly arranged at the lower end of one side of the kettle body 201, which is beneficial to install the front fixing frame 205. The front fixing frame 205 is slidably clamped on the lower end of one side of the kettle body 201 through the two slide rails 202, which is beneficial to be connected with the rear fixing frame 301 to fix the reaction kettle 2. A clamping block 204 is fixedly arranged at the lower end of the front fixing frame 205, which is beneficial to make the front fixing frame 205 more stable. Two first support blocks 203 are fixedly arranged at the lower end of the kettle body 201 to prevent the front fixing frame 205 from falling.

[0036] On the upper end of the side of the front fixing frame 205 away from the kettle body 201, a handle 206 is fixedly arranged, which is beneficial to lifting the front fixing frame 205. A through hole 207 is opened in the middle of the side of the front fixing frame 205 away from the kettle body 201, which is beneficial to installing pipelines and releasing raw materials. A protective cover 1 is fixedly arranged on the upper end of the kettle body 201. On the upper side of the front end of the reaction kettle 2, a feed inlet 4 is fixedly arranged, which is beneficial to conveying raw materials for processing. The front fixing frame 205 and the rear fixing frame 301 are slidably and snap-fitted together. The heights of the three heating components 503, the fixing blocks 504 and the conical blocks 505 are inconsistent, which is beneficial to enabling the heating and stirring mechanism 5 to have a larger stirring space, enhancing the stirring effect and making the heating more uniform.

[0037] Working principle: When the device is in use, start the motor 501 to drive the rotating shaft 507 to rotate. The rotating shaft 507 drives the connecting column 506 to rotate. The connecting column 506 drives the heating component 503 and the fixing block 504 to rotate. Since one end of the fixing block 504 is slidably and snap-fitted inside the spiral chute 502, when the fixing block 504 rotates, the spiral chute 502 will drive the fixing block 504 and the heating component 503 to move upward, which is beneficial to heating the materials inside the reaction kettle 2 more evenly, improving the reaction effect and its purity. In addition, when the reaction kettle 2 needs to be disassembled, the hydraulic cylinder 304 can be used to push the baffle 308. The baffle 308 simultaneously pushes a plurality of balls 305 through a plurality of first support blocks 203, making the balls 305 higher than the upper end surface of the first bottom plate 302. Then, lift the front fixing frame 205 to separate it from the rear fixing frame 301. At this time, since the reaction kettle 2 is on the upper ends of the plurality of balls 305, the reaction kettle 2 can be moved relatively easily.

[0038] Finally, it should be noted that the above are only the preferred embodiments of the present invention and are not used to limit the present invention. Although the present invention has been described in detail with reference to the foregoing embodiments, for those skilled in the art, they can still modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements for some of the technical features. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principle of the present invention shall be included within the protection scope of the present invention.

Claims

1. A device for preparing a titanate coupling agent purification device, comprising a reaction kettle (2), a fixed base (3) and a heating and stirring mechanism (5), characterized in that: The fixed base (3) comprises a No. 1 bottom plate (302), a hydraulic cylinder (304), a No. 2 bottom plate (309) and a baffle (308); a rear fixing frame (301) is fixedly arranged on one side of the upper end of the No. 1 bottom plate (302); a plurality of No. 2 support blocks (303) are fixedly arranged on the upper end of the baffle (308); and a ball bearing (305) is arranged on the upper ends of the plurality of No. 2 support blocks (303); and the reaction kettle (2) comprises a kettle body (201), a front fixing frame (205) and two slide rails (202); The heating and stirring mechanism (5) comprises a motor (501) and a spiral slide groove (502); a rotating shaft (507) is fixedly provided at the output end of the motor (501); a connecting column (506) is slidably provided around the rotating shaft (507); a heating component (503) is fixedly provided on one side of the connecting column (506); conical blocks (505) are fixedly provided on both sides of the heating component (503); a fixed block (504) is fixedly provided at one end of the heating component (503) away from the connecting column (506); the heating component (503), the two conical blocks (505) and the fixed block (504) are all provided in three groups; the sides of the three fixed blocks (504) away from each other are all slidably provided inside the spiral slide groove (502).

2. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: Four supporting legs (307) are fixedly arranged on the upper end of the No. 2 bottom plate (309), the No. 1 bottom plate (302) is fixedly arranged on the upper ends of the four supporting legs (307), and a groove (306) is provided on a side of the No. 1 bottom plate (302) away from the rear fixing frame (301).

3. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: A hydraulic cylinder (304) is fixedly arranged in the middle of the upper end of the second bottom plate (309), the baffle (308) is fixedly arranged at the upper end of the hydraulic cylinder (304), a plurality of through holes are penetrated through the first bottom plate (302), and a plurality of the balls (305) are arranged inside the through holes.

4. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: The two slide rails (202) are fixedly arranged at the lower end of one side of the kettle body (201); the front fixed frame (205) is slidably connected to the lower end of one side of the kettle body (201) through the two slide rails (202); a connecting block (204) is fixedly arranged at the lower end of the front fixed frame (205); and two No. 1 support blocks (203) are fixedly arranged at the lower end of the kettle body (201).

5. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: A handle (206) is fixedly provided on the upper end of the side of the front fixing frame (205) away from the kettle body (201), and a through hole (207) is provided in the middle of the side of the front fixing frame (205) away from the kettle body (201).

6. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: A protective cover (1) is fixedly provided on the upper end of the kettle body (201), and a feed port (4) is fixedly provided on the upper front end of the reaction kettle (2).

7. The device for preparing and purifying titanate coupling agent according to claim 1, characterized in that: The front fixing frame (205) and the rear fixing frame (301) are slidably connected together, and the heights of the three groups of heating components (503), fixing blocks (504) and conical blocks (505) are inconsistent.

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