Lithium sulfate solution finish machining defluorination equipment

Abstract

The utility model discloses lithium sulfate solution finish machining defluorination equipment which comprises a reaction kettle which is of a hollow cylindrical shell structure, and the bottom of the reaction kettle is fixedly connected with a supporting frame; a rotating mechanism is arranged in the reaction kettle, and the rotating mechanism is characterized in that an observation plate is embedded in the surface of the reaction kettle, a motor is mounted on the surface of the reaction kettle, and a rotating shaft is fixedly connected to the tail end of an output shaft of the motor. The lithium sulfate solution finish machining defluorination equipment is provided with the rotating mechanism, through the rotating mechanism, an internal solution is driven to be stirred, meanwhile, a discharging port is cleaned, the discharging port is prevented from being blocked, a rotating shaft is driven to rotate through clicking, the rotating shaft drives a stirring rod on the surface and a scraping plate to rotate at the same time, and the stirring rod mixes the solution; the scraper blade can clean the interior of the reaction kettle to prevent sediments from being accumulated on the inner wall of the reaction kettle, and the cleaning rod blocks the discharge port to prevent the sediments from being accumulated at the discharge port during discharging.

Description

Technical Field

[0001] The utility model relates to the technical field of lithium sulfate solution processing, in particular to a fine processing defluorination device for lithium sulfate solution. Background Technique

[0002] Lithium sulfate is an anhydrous salt, which is a white crystal. Monohydrate lithium sulfate is a colorless monoclinic crystal and is very stable. It is soluble in water and insoluble in absolute ethanol and acetone. At the same time, lithium sulfate can be used as a raw material for special high-strength glass, an analytical reagent and the pharmaceutical industry. In the production of lithium ion battery materials, lithium sulfate solution often contains trace fluoride impurities, and these impurities will have an adverse impact on the subsequent products. Defluorination of lithium sulfate is a common water treatment method. Its principle is to use the chemical reaction between aluminum sulfate and fluoride ions to convert the fluoride ions in water into aluminum fluoride compounds that are insoluble in water and precipitate, so as to achieve the purpose of defluorination. However, when the existing defluorination equipment is used, it is not convenient to remove the precipitate, which easily causes the precipitate to adhere to the inner bottom surface of the reaction kettle, and at the same time, it easily causes the precipitate to block during feeding, which is not convenient for the use of the reaction kettle. Content of the Utility Model

[0003] The purpose of the utility model is to provide a fine processing defluorination device for lithium sulfate solution, so as to solve the problems put forward in the above background technique that it is not convenient to remove the precipitate, which easily causes the precipitate to adhere to the inner bottom surface of the reaction kettle, and at the same time, it easily causes the precipitate to block during feeding, which is not convenient for the use of the reaction kettle.

[0004] To achieve the above purpose, the utility model provides the following technical scheme: A fine processing defluorination device for lithium sulfate solution, including a reaction kettle which is set as a hollow cylindrical shell structure, and a support frame is fixedly connected to the bottom of the reaction kettle;

[0005] A rotating mechanism is arranged inside the reaction kettle, and the rotating mechanism includes: An observation board is embedded on the surface of the reaction kettle, and a motor is installed on the surface of the reaction kettle. The end of the output shaft of the motor is fixedly connected with a rotating shaft, and the rotating shaft is inserted into the reaction kettle and connected with a stirring rod. A scraper is fixedly connected to the surface of the rotating shaft, and the scraper is arranged inside the reaction kettle. A rotating rod is fixedly connected to the bottom of the rotating shaft, and a cleaning rod is fixedly connected to the surface of the rotating rod. An outlet is installed at the bottom of the reaction kettle, and a blocking plate is embedded at the bottom of the outlet. An inlet pipe is installed on the surface of the reaction kettle.

[0006] Preferably, a drainage mechanism is arranged inside the reaction kettle, and the drainage mechanism includes: A feed box is fixedly connected to the surface of the reaction kettle, and a plurality of feeding ports are fixedly connected to the bottom of the feed box. A drainage plate is fixedly connected to the surface of the rotating shaft, and the drainage plate is arranged inside the reaction kettle.

[0007] With the above technical solution, through the drainage mechanism, the reaction solution can be quickly fused with the internal lithium sulfate solution, improving the efficiency.

[0008] Preferably, an opening is embedded on the surface of the reaction kettle, and the end of the feeding port is inserted into the opening of the reaction kettle.

[0009] With the above technical solution, the reaction solution can enter the interior of the reaction kettle through the feeding port.

[0010] Preferably, the observation plate is made of a transparent material, the reaction kettle is rotatably connected to the rotating shaft, and the bottom of the reaction kettle is provided with an arc-shaped structure.

[0011] With the above technical solution, the internal solution is observed through the observation plate, which is convenient for observing the reaction progress of the solution.

[0012] Preferably, the scraper is provided with an arc-shaped structure, and the end of the scraper is attached to the bottom surface of the reaction kettle, and the reaction kettle is rotatably connected to the scraper.

[0013] With the above technical solution, the scraper can clean the inner bottom surface of the reaction kettle to prevent sediment from accumulating at the bottom of the reaction kettle.

[0014] Preferably, the end of the rotating rod is inserted into the discharge port, and the cleaning rod is arranged inside the discharge port, and a sealing cover is connected to the surface of the inlet pipe.

[0015] With the above technical solution, the rotating rod rotates inside the discharge port, and at the same time, the rotating rod drives the cleaning rod to clean inside the discharge port.

[0016] Preferably, the drainage plate is provided in a spiral blade shape, and the drainage plate is rotatably connected to the reaction kettle.

[0017] With the above technical solution, the solution falls on the surface of the drainage plate and falls along the surface of the drainage plate, which can quickly mix the reaction solution with the lithium sulfate solution.

[0018] Compared with the prior art, the beneficial effects of the present utility model are: This lithium sulfate solution fine processing and defluorination equipment:

[0019] 1. A rotating mechanism is provided. Through the rotating mechanism, the internal solution is driven to stir, and at the same time, the discharge port is cleaned to prevent the discharge port from being blocked. Click to drive the rotating shaft to rotate, and the rotating shaft drives the stirring rod and the scraper on the surface to rotate simultaneously. The stirring rod mixes the solution, and the scraper can clean the inside of the reaction kettle to prevent sediment from accumulating on the inner wall of the reaction kettle. The cleaning rod blocks the discharge port to prevent sediment from accumulating at the discharge port during feeding;

[0020] 2. A drainage mechanism is provided, which can quickly bring the reaction solution into contact with the lithium sulfate solution. Pour the reaction solution into the inside of the feeding box. At this time, the solution falls onto the surface of the drainage plate through the blanking port, causing the reaction solution to flow down along the drainage plate. At the same time, the motor drives the drainage plate to rotate. At this time, the drainage plate rotates above the lithium sulfate solution, enabling the solution on the surface of the drainage plate to flow smoothly onto the surface of the lithium sulfate solution, increasing the contact area of the reaction solution and improving the efficiency of the mixing reaction. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] Figure 1 is a three-dimensional structural schematic diagram of the present utility model;

[0022] Figure 2 is a three-dimensional structural schematic diagram of the installation of the blanking port of the present utility model;

[0023] Figure 3 is a three-dimensional structural schematic diagram of the installation inside the reaction kettle of the present utility model;

[0024] Figure 4 is a three-dimensional structural schematic diagram of the installation of the drainage plate of the present utility model;

[0025] Figure 5 is a three-dimensional structural schematic diagram of the installation of the stirring rod of the present utility model;

[0026] Figure 6 is a three-dimensional structural schematic diagram of the installation of the scraper of the present utility model.

[0027] In the figure: 10, reaction kettle; 101, support frame;

[0028] 20, observation plate;

[0029] 30, motor; 301, rotating shaft; 303, stirring rod; 304, scraper; 305, cleaning rod; 306, discharge port; 307, plug plate; 308, inlet pipe; 309, rotating rod;

[0030] 40, feeding box; 401, blanking port; 402, drainage plate. DETAILED DESCRIPTION OF THE EMBODIMENTS

[0031] Next, the technical solutions in the embodiments of the present utility model will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present utility model. Obviously, the described embodiments are only a part of the embodiments of the present utility model, rather than all of the embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present utility model.

[0032] Please refer to Figure 1-6, the present utility model provides a technical solution: a fine processing and defluorination device for lithium sulfate solution, comprising a reaction kettle 10, a support frame 101, an observation board 20, a motor 30, a rotating shaft 301, a stirring rod 303, a scraper 304, a cleaning rod 305, a discharge port 306, a blocking plate 307, an inlet pipe opening 308, a rotating rod 309, a feed box 40, a blanking port 401 and a diversion plate 402;

[0033] This fine processing and defluorination device for lithium sulfate solution is convenient for mixing materials and increasing the contact area of the reaction solution. The specific implementation method is as follows:

[0034] A diversion mechanism is arranged inside the reaction kettle 10, and the diversion mechanism includes: the surface of the reaction kettle 10 is fixedly connected with a feed box 40, and the bottom of the feed box 40 is fixedly connected with a plurality of blanking ports 401. The surface of the rotating shaft 301 is fixedly connected with a diversion plate 402, and the diversion plate 402 is arranged inside the reaction kettle 10. An opening is embedded on the surface of the reaction kettle 10, and the end of the blanking port 401 is inserted into the opening inside the reaction kettle 10. The diversion plate 402 is arranged in a spiral blade shape, and the diversion plate 402 is rotatably connected to the reaction kettle 10.

[0035] Pour the reaction solution into the inside of the feed box 40. At this time, the reaction solution enters the inside of the blanking port 401 through the feed box 40 and enters the inside of the reaction kettle 10 through the blanking port 401. At this time, the reaction solution falls on the surface of the diversion plate 402 through the blanking port 401, causing the reaction solution to move downward along the surface of the diversion plate 402, so that the reaction solution falls on the surface of the lithium sulfate solution through the diversion plate 402. When starting the motor 30, the motor 30 drives the rotating shaft 301 to rotate inside the reaction kettle 10. At the same time, the rotating shaft 301 drives the diversion plate 402 on its surface to rotate, so that the end of the diversion plate 402 rotates on the surface of the lithium sulfate solution. At this time, the reaction solution falls on the surface of the lithium sulfate solution through the end of the diversion plate 402, enabling it to quickly contact the lithium sulfate solution.

[0036] This fine processing and defluorination device for lithium sulfate solution can facilitate stirring and prevent blockage of the discharge port 306 during blanking. The specific implementation method is as follows:

[0037] The reactor 10 is set as a hollow cylindrical shell structure, and a support frame 101 is fixedly connected to the bottom of the reactor 10; a rotating mechanism is arranged inside the reactor 10, and the rotating mechanism includes: an observation plate 20 is embedded on the surface of the reactor 10, and a motor 30 is installed on the surface of the reactor 10. The end of the output shaft of the motor 30 is fixedly connected to a rotating shaft 301, and the rotating shaft 301 is inserted into the reactor 10 and connected to a stirring rod 303. A scraping plate 304 is fixedly connected to the surface of the rotating shaft 301, and the scraping plate 304 is arranged inside the reactor 10. The bottom of the rotating shaft 301 is fixedly connected to a rotating rod 309, and a cleaning rod 305 is fixedly connected to the surface of the rotating rod 309. An outlet 306 is installed at the bottom of the reactor 10, and a blocking plate 307 is embedded at the bottom of the outlet 306. An inlet pipe 308 is installed on the surface of the reactor 10. The observation plate 20 is made of a transparent material. The reactor 10 is rotatably connected to the rotating shaft 301, and the bottom of the reactor 10 is set as an arc-shaped structure. The scraping plate 304 is set as an arc-shaped structure, and the end of the scraping plate 304 is attached to the bottom surface of the reactor 10. And the reactor 10 is rotatably connected to the scraping plate 304. The end of the rotating rod 309 is inserted into the outlet 306, and the cleaning rod 305 is arranged inside the outlet 306. A sealing cover is connected to the surface of the inlet pipe 308.

[0038] Start the motor 30. The motor 30 drives the rotating shaft 301 to rotate inside the reactor 10. At the same time, the rotating shaft 301 drives the stirring rod 303 on its surface to rotate. The stirring rod 303 can stir the lithium sulfate solution, making the reaction between the lithium sulfate solution and the reaction solution more uniform. At the same time, the rotating shaft 301 drives the scraping plate 304 to rotate, so that the scraping plate 304 rotates on the bottom surface of the reactor 10 to clean the inner wall of the reactor 10 and prevent sediment from accumulating and sticking to the inner wall. At this time, the solution inside the reactor 10 can be observed through the observation plate 20. When the reaction is completed, let it stand still, and pump out the reacted solution above through the pumping mechanism. Take out the blocking plate 307 from the bottom of the outlet 306. At this time, the blocking plate 307 loses its blockage of the outlet 306, and the sediment inside the reactor 10 can be discharged through the outlet 306. At this time, start the motor 30. The motor 30 drives the rotating shaft 301 to rotate. The rotating shaft 301 drives the rotating rod 309 on its surface to rotate. The rotating rod 309 drives the cleaning rod 305 on its surface to rotate, so that the cleaning rod 305 cleans the inside of the outlet 306 and prevents sediment from accumulating on the inner wall of the outlet 306.

[0039] Working principle: When using the fine processing defluorination equipment for lithium sulfate solution, a feeding box 40, a discharging port 401 and a drainage plate 402 are provided to facilitate the mixing of materials and increase the contact area of the reaction solution. An observation plate 20, a motor 30, a rotating shaft 301, stirring rods 303 and a scraper 304 are provided to facilitate stirring, prevent blockage of the discharging port 306, and increase the overall practicability.

[0040] Although the embodiments of the present invention have been shown and described, those of ordinary skill in the art can understand that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principle and spirit of the present invention. The scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A lithium sulfate solution finishing defluorination device, comprising a reaction kettle (10) configured as a hollow cylindrical shell structure, and a support frame (101) is fixedly connected to the bottom of the reaction kettle (10); Features: The reactor (10) is provided with a rotating mechanism inside, and the rotating mechanism comprises: an observation plate (20) is embedded in the surface of the reactor (10), and a motor (30) is installed on the surface of the reactor (10); the end of the output shaft of the motor (30) is fixedly connected to a rotating shaft (301), and the rotating shaft (301) is inserted into the reactor (10) and connected to a stirring rod (303); a scraper (304) is fixedly connected to the surface of the rotating shaft (301), and the scraper (304) is arranged inside the reactor (10); a rotating rod (309) is fixedly connected to the bottom of the rotating shaft (301), and a cleaning rod (305) is fixedly connected to the surface of the rotating rod (309); a discharge port (306) is installed at the bottom of the reactor (10), and a blocking plate (307) is embedded in the bottom of the discharge port (306); and a pipe inlet (308) is installed on the surface of the reactor (10).

2. A lithium sulfate solution finishing defluorination equipment according to claim 1, characterized in that: A drainage mechanism is arranged inside the reactor (10), and the drainage mechanism comprises: a feed box (40) is fixedly connected to the surface of the reactor (10), and a plurality of discharge ports (401) are fixedly connected to the bottom of the feed box (40); a drainage plate (402) is fixedly connected to the surface of the rotating shaft (301), and the drainage plate (402) is arranged inside the reactor (10).

3. A lithium sulfate solution finishing defluorination equipment according to claim 2, characterized in that: An opening is embedded in the surface of the reaction kettle (10), and the end of the feed port (401) is inserted into the opening of the reaction kettle (10).

4. A lithium sulfate solution finishing defluorination equipment according to claim 1, characterized in that: The observation plate (20) is made of a transparent material, the reaction kettle (10) is rotatably connected to the rotating shaft (301), and the bottom of the reaction kettle (10) is arranged in an arc-shaped structure.

5. The lithium sulfate solution finishing defluorination equipment according to claim 1, characterized in that: The scraper (304) is configured as an arc-shaped structure, and the end of the scraper (304) is in contact with the bottom surface of the reaction kettle (10), and the reaction kettle (10) and the scraper (304) are rotatably connected.

6. A lithium sulfate solution finishing defluorination equipment according to claim 1, characterized in that: The end of the rotating rod (309) is inserted into the inside of the discharge port (306), and the cleaning rod (305) is arranged inside the discharge port (306). The surface of the pipe inlet (308) is connected to a sealing cover.

7. A lithium sulfate solution finishing defluorination equipment according to claim 2, characterized in that: The guide plate (402) is configured in the shape of a spiral blade, and the guide plate (402) is rotatably connected to the reaction kettle (10).

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