Filtering and concentrating device for matrine extraction

Through the device with integrated filtration and reduced pressure evaporation and concentration functions, the stainless steel folding filter element and heat exchange system are used to solve the problem of low filtration and concentration efficiency in malpine extraction, and efficient stock solution treatment is achieved.

CN223069216UActive Publication Date: 2025-07-08SHANDONG HEMEIXIN ANIMAL PHARM CO LTD
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Patent Information

Application Number
CN202421733229.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-07-22
Publication Date
2025-07-08
Estimated Expiration
2034-07-22

AI Technical Summary

Technical Problem

During the existing matrine extraction process, the filtration and concentration devices are monomer machines, which are cumbersome and have low filtration and concentration efficiency.

Method used

A device integrating filtration and reduced pressure evaporation and concentration functions is designed, using stainless steel folding filter element and heat exchange system, combined with negative pressure evaporation technology to improve filtration and concentration efficiency.

Benefits of technology

It significantly improves the filtration and concentration efficiency, simplifies the operation process, and improves the filtration speed and concentration efficiency of the stock solution.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a filtering and concentrating device for matrine extraction, which comprises a shell, a sealing cover arranged at the top of the shell, a transversely arranged partition plate fixedly connected to the middle of an inner cavity of the shell, a filtering cavity arranged above the partition plate, a concentrating cavity arranged below the partition plate, and a drainage pipe fixedly arranged along the vertical direction and fixedly arranged at the center position of the partition plate, the top end of the drainage tube is positioned at the bottom of the filtering cavity; the bottom end of the drainage tube extends to the bottom of the concentration cavity; a filter element is mounted in the filter cavity; a heat exchange tube row is arranged in the concentration cavity and is arranged on the periphery of the drainage tube, and the upper end and the lower end of the heat exchange tube row are connected with a heat exchange medium inlet and outlet tube; a heat exchange jacket is arranged outside the concentration cavity, and the upper end and the lower end of the heat exchange jacket are connected with a heat exchange medium inlet and outlet pipe. According to the utility model, the functions of filtration and reduced pressure evaporation concentration are integrated, and the filtration and concentration efficiency is remarkably improved.
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Description

Technical Field

[0001] The utility model relates to a filtering and concentrating device for matrine extraction, belonging to the technical field of matrine extraction. Background Art

[0002] Stainless steel folded filters are widely used in industries such as environmental protection, chemical engineering, pharmaceuticals, medical treatment, and food. Stainless steel folded filters usually adopt 304 or 316L stainless steel, with excellent corrosion resistance and high temperature resistance. The filter media are folded into a wavy shape through a special process, significantly increasing the filtration area (which can be 3 - 5 times larger than traditional filters), reducing the pressure difference, and improving the dirt holding capacity. The filtration accuracy of the folded filter can be selected according to the size of the target particulate matter.

[0003] Matrine is made by extracting the dry roots, plants, and fruits of Sophora flavescens, a leguminous plant, with organic solvents such as ethanol, and it is an alkaloid. Generally, it is total matrine, and its main components include matrine, sophocarpine, oxysophocarpine, sophoridine and other alkaloids, with matrine and oxymatrine having the highest contents. Other sources are Sophora subprostrata and the above-ground parts of Sophora subprostrata. The pure product appears as a white powder. Oxymatrine is widely used in the pharmaceutical and pesticide fields. Oxymatrine is a natural plant pesticide, with low toxicity to humans and livestock, and it is a broad-spectrum insecticide, having contact and stomach toxicity effects.

[0004] During the extraction process of matrine, the original solution needs to be filtered and concentrated to remove the impurities contained in the original solution and concentrate it into a semi-finished product of a certain specification. However, in the existing work, the filtering and concentrating devices are monomeric machines, which are relatively cumbersome during operation, and there is generally a problem of low filtering and concentrating efficiency.

[0005] To sum up, it is obvious that there are inconveniences and defects in the existing technology in actual use, so it is necessary to make improvements. Content of the Utility Model

[0006] Aiming at the deficiencies in the background art, the utility model provides a filtering and concentrating device for matrine extraction, which can integrate the functions of filtering and vacuum evaporation concentration, and significantly improve the filtering and concentrating efficiency.

[0007] To solve the above technical problems, the utility model adopts the following technical solutions:

[0008] A filtering and concentrating device for matrine extraction, including a housing, a sealing cover is arranged at the top of the housing, a horizontally arranged partition is fixedly connected in the middle of the inner cavity of the housing, a filtering chamber is arranged above the partition, and a concentrating chamber is arranged below the partition;

[0009] A vertically arranged drainage pipe is fixedly installed at the central position of the partition, the top end of the drainage pipe is located at the bottom of the filtering chamber, and the bottom end of the drainage pipe extends to the bottom of the concentrating chamber; a filter element is installed in the filtering chamber;

[0010] A heat exchange tube row is installed in the concentration chamber. The heat exchange tube row is installed around the drain pipe, and the upper and lower ends of the heat exchange tube row are connected to the heat exchange medium inlet and outlet pipes; an external heat exchange jacket is provided outside the concentration chamber, and the upper and lower ends of the heat exchange jacket are connected to the heat exchange medium inlet and outlet pipes.

[0011] Furthermore, the filter element is installed vertically at the top end of the drain pipe. The bottom end of the filter element is connected to the top end of the drain pipe by threads, and the top end of the filter element is pressed by a compression spring.

[0012] Furthermore, the filter element is of a stainless steel folded structure.

[0013] Furthermore, a columnar protrusion is fixedly connected to the bottom of the sealing cover, and the columnar protrusion is used for sleeving and fixing the top end of the compression spring.

[0014] Furthermore, a groove is provided at the top end of the filter element, and the bottom end of the compression spring abuts against the groove.

[0015] Furthermore, a liquid inlet pipe is connected to the outer wall of the filtration chamber, and the liquid inlet pipe is used for introducing the stock solution into the filtration chamber.

[0016] Furthermore, an air outlet pipe is provided on one side of the top of the concentration chamber, a vacuum pipe communicating with the air outlet pipe is installed on the air outlet pipe, and valves are installed on both the vacuum pipe and the air outlet pipe.

[0017] Furthermore, a liquid outlet pipe is connected to the bottom of the concentration chamber, and a valve is installed on the liquid outlet pipe.

[0018] After the present utility model adopts the above technical solutions, compared with the prior art, it has the following advantages:

[0019] The stock solution enters the filtration chamber, impurities in the stock solution are intercepted between the filter element and the housing, the filtered clean stock solution converges into the inner cavity of the filter element, and then flows to the concentration chamber through the drain pipe. The internal heat exchange tube row and the external heat exchange jacket in the concentration chamber simultaneously provide heat sources for the evaporation of the stock solution, and the evaporation and concentration efficiency is relatively high; the inside of the concentration chamber is in a negative pressure state, which can not only enable the stock solution to achieve reduced-pressure evaporation and concentration in the concentration chamber, but also significantly improve the filtration speed of the stock solution.

[0020] The present utility model will be described in detail below with reference to the accompanying drawings and embodiments. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] Figure 1 is a schematic structural diagram of the present utility model;

[0022] Figure 2 is a schematic internal structural diagram of the present utility model;

[0023] Figure 3 is Figure 2 an enlarged view of the N position in

[0024] In the figure, 1 is the housing, 2 is the partition plate, 3 is the filtration chamber, 4 is the concentration chamber, 5 is the filter element, 6 is the drain pipe, 7 is the groove, 8 is the compression spring, 9 is the columnar protrusion, 10 is the liquid inlet pipe, 11 is the heat exchange jacket, 12 is the heat exchange tube row, 13 is the liquid outlet pipe, 14 is the gas outlet pipe, 15 is the vacuum pipe, and 16 is the sealing cover. Specific embodiments

[0025] For a clearer understanding of the technical features, objectives, and effects of the present utility model, the specific embodiments of the present utility model will now be described with reference to the accompanying drawings.

[0026] As Figures 1-3 As shown together, the present utility model provides a filtration and concentration device for matrine extraction, including a housing 1. A sealing cover 16 is provided at the top of the housing 1. A horizontally arranged partition plate 2 is fixedly connected to the middle of the inner cavity of the housing 1. A filtration chamber 3 is arranged above the partition plate 2, and a concentration chamber 4 is arranged below the partition plate 2.

[0027] A vertically arranged drain pipe 6 is fixedly installed at the central position of the partition plate 2. The top end of the drain pipe 6 is located at the bottom of the filtration chamber 3, and the bottom end of the drain pipe 6 extends to the bottom of the concentration chamber 4.

[0028] A filter element 5 is installed in the filtration chamber 3. The filter element 5 is of a stainless steel folded structure. The filter element 5 is installed vertically at the top end of the drain pipe 6, and the bottom end of the filter element 5 is threadedly connected to the top end of the drain pipe 6. The top end of the filter element 5 is pressed tightly by a compression spring 8 to prevent the filter element 5 from tilting under force during use.

[0029] A columnar protrusion 9 is fixedly connected to the bottom of the sealing cover 16 for sleeving and fixing the top end of the compression spring 8; a groove 7 is provided at the top end of the filter element 5, and the bottom end of the compression spring 8 abuts against the groove 7.

[0030] A liquid inlet pipe 10 is connected to the outer wall of the filtration chamber 3 for introducing the original liquid into the filtration chamber 3.

[0031] A heat exchange tube row 12 is installed in the concentration chamber 4. The heat exchange tube row 12 is installed around the drain pipe 6, and the upper and lower ends of the heat exchange tube row 12 are connected to the heat exchange medium inlet and outlet pipes.

[0032] A heat exchange jacket 11 is provided outside the concentration chamber 4. The upper and lower ends of the heat exchange jacket 11 are connected to the heat exchange medium inlet and outlet pipes.

[0033] The heat exchange medium flows in the heat exchange tube row 12 and the heat exchange jacket 11, providing a heat source for the evaporation of the original liquid in the concentration chamber 4.

[0034] One side of the top of the concentration chamber 4 is provided with an air outlet pipe 14, and the steam generated during the concentration process is output therefrom. A vacuum pipe 15 communicating with the air outlet pipe 14 is installed on the air outlet pipe 14, and valves are installed on both the vacuum pipe 15 and the air outlet pipe 14.

[0035] The outer end of the vacuum pipe 15 is connected to a negative pressure suction device, which can form a negative pressure inside the concentration chamber 4 to achieve reduced-pressure evaporation.

[0036] The bottom of the concentration chamber 4 is connected with a liquid outlet pipe 13, and a valve is installed on the liquid outlet pipe 13. The liquid outlet pipe 13 is used to output the concentrated liquid after reduced-pressure evaporation concentration.

[0037] The specific working principle of the present utility model:

[0038] The original liquid enters the filtering chamber 3 from the liquid inlet pipe 10. The impurities in the original liquid are intercepted in the clamping cavity between the filter element 5 and the housing 1. The filtered clean original liquid converges into the inner cavity of the filter element 5 and then flows to the concentration chamber 4 through the diversion pipe 6. The heat exchange tube row 12 inside the concentration chamber 4 and the heat exchange jacket 11 outside the concentration chamber 4 simultaneously provide heat sources for the evaporation of the original liquid, with a relatively high evaporation efficiency. The evaporated water is led out from the air outlet pipe 14, and the concentrated liquid after evaporation is led out from the liquid outlet pipe 13.

[0039] The inside of the concentration chamber is in a negative pressure state, which can not only enable the original liquid to achieve reduced-pressure evaporation concentration in the concentration chamber, but also significantly improve the filtering speed of the original liquid.

[0040] The bottom of the filter element in the present utility model is connected by threads, and the top is pressed by a compression spring, which is convenient for installation, disassembly and subsequent maintenance.

[0041] The above is an example of the best implementation mode of the present utility model, and the parts not described in detail are all common general knowledge of those skilled in the art. The protection scope of the present utility model is subject to the content of the claims, and any equivalent transformation based on the technical revelation of the present utility model is also within the protection scope of the present utility model.

Claims

1. Filter and concentration device for matrine extraction, characterized in that: It includes a housing (1), a sealing cover (16) is provided at the top of the housing (1), a horizontally arranged partition (2) is fixedly connected to the middle of the inner cavity of the housing (1), a filtration chamber (3) is arranged above the partition (2), and a concentration chamber (4) is arranged below the partition (2); A drain pipe (6) arranged vertically is fixedly installed at the central position of the partition (2), the top end of the drain pipe (6) is located at the bottom of the filtration chamber (3), and the bottom end of the drain pipe (6) extends to the bottom of the concentration chamber (4); A filter element (5) is installed in the filtration chamber (3); A heat exchange tube row (12) is installed in the concentration chamber (4), the heat exchange tube row (12) is installed on the periphery of the drain pipe (6), and the upper and lower ends of the heat exchange tube row (12) are connected to the heat exchange medium inlet and outlet pipes; A heat exchange jacket (11) is provided outside the concentration chamber (4), and the upper and lower ends of the heat exchange jacket (11) are connected to the heat exchange medium inlet and outlet pipes.

2. The filtering and concentrating device for matrine extraction according to claim 1, wherein: The filter element (5) is installed vertically at the top end of the drain pipe (6), the bottom end of the filter element (5) is threadedly connected to the top end of the drain pipe (6), and the top end of the filter element (5) is pressed by a compression spring (8).

3. The filtering and concentrating device for matrine extraction according to claim 2, characterized in that: The filter element (5) is of a stainless steel folded structure.

4. The filtering and concentrating device for matrine extraction according to claim 3, wherein: A columnar protrusion (9) is fixedly connected to the bottom of the sealing cover (16), and the columnar protrusion (9) is used for sleeving and fixing the top end of the compression spring (8).

5. The filtering and concentrating device for matrine extraction according to claim 4, characterized in that: A groove (7) is provided at the top end of the filter element (5), and the bottom end of the compression spring (8) abuts against the groove (7).

6. The filtering and concentrating device for matrine extraction according to claim 1, characterized in that: A liquid inlet pipe (10) is connected to the outer wall of the filtration chamber (3), and the liquid inlet pipe (10) is used for introducing the original liquid into the filtration chamber (3).

7. The filtration and concentration device for matrine extraction according to claim 1, characterized in that: An air outlet pipe (14) is provided on one side of the top of the concentration chamber (4), a vacuum pipe (15) communicated with the air outlet pipe (14) is installed on the air outlet pipe (14), and valves are installed on both the vacuum pipe (15) and the air outlet pipe (14).

8. The filtering and concentrating device for matrine extraction according to claim 1, wherein: A liquid outlet pipe (13) is connected to the bottom of the concentration chamber (4), and a valve is installed on the liquid outlet pipe (13).