Octacosanol short molecule distillation extraction device
By setting the heating chamber and the cooling chamber separately and using semiconductor refrigeration sheets in the cooling chamber, the problem of poor condensation effect in the existing devices is solved, and a more efficient condensation effect is achieved.
Patent Information
- Application Number
- CN202422048735.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-08-23
- Publication Date
- 2025-08-01
- Estimated Expiration
- 2034-08-23
AI Technical Summary
In the existing octadecanol distillation extraction device, the heating chamber and the condensing chamber share one chamber, resulting in the heating temperature affecting the condensing temperature, the contact area of the condensing tube is small, and the condensing effect is poor.
The heating chamber and the cooling chamber are arranged separately, and the inner storage tank and square through holes are designed separately to gather heat and condense respectively, and a semiconductor refrigeration sheet is used to improve the condensation effect.
The condensation effect is improved, the mutual influence of heating and condensation functions is avoided, and the condensation effect of the condensation tube is enhanced.
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Figure CN223170347U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of distillation extraction, in particular to a short molecular distillation extraction device for octacosanol. Background Technique
[0002] Octacosanol is an organic compound, soluble in organic solvents such as hot ethanol, ether, benzene, toluene, chloroform, dichloromethane, petroleum ether, etc., and is stable to light and heat, not easy to absorb moisture. In the extraction process of octacosanol, the extraction liquid needs to be mixed into ether, so that the ether and octacosanol in the extraction liquid are dissolved and mixed, and after extraction, only the mixed liquid of ether and octacosanol is left in the mixed liquid.
[0003] However, in the existing technology, a molecular distillation extraction device for octacosanol is disclosed, and its publication number is CN208694281U. The heating chamber and the condensation chamber in this device share a chamber, which may cause the heating temperature of the heating chamber to affect the condensation temperature of the condenser tube; and the contact area during the condensation of the condenser tube is small, resulting in poor condensation effect of the overall device. Therefore, it does not meet the existing requirements, and for this reason, we propose a short molecular distillation extraction device for octacosanol. Content of the Utility Model
[0004] The purpose of the utility model is to provide a short molecular distillation extraction device for octacosanol, so as to solve the problems in the above background technique that the heating chamber and the condensation chamber in the existing technology share a chamber, which may cause the heating temperature of the heating chamber to affect the condensation temperature of the condenser tube, and the contact area during the condensation of the condenser tube is small, resulting in poor condensation effect of the overall device.
[0005] To achieve the above purpose, the utility model provides the following technical solution: A short molecular distillation extraction device for octacosanol, including a heating chamber, a first side groove is arranged in the middle of the upper end of the heating chamber, a liquid inlet is arranged through the middle of the bottom end of the first side groove, a second connecting frame is fixedly connected to the bottom end of the first side groove, a spring is connected to the upper end inside the second connecting frame, an upper end of the spring is connected to a blocking ball, an upper end of the blocking ball is connected to a column, and an inner storage tank is suspended inside the heating chamber, and ventilation waist holes are arranged on both sides of the upper end of the inner storage tank;
[0006] The heating chamber is fixedly connected to a cooling chamber at the lower end, a first connecting frame is connected to the front end of the cooling chamber, fans are arranged on both sides of the front end of the first connecting frame, a square through hole runs through the front and back of the cooling chamber, second side grooves are arranged on both end faces of the square through hole, and a semiconductor refrigerating sheet is inserted into the second side groove.
[0007] Preferably, a liquid outlet pipe A penetrates and is connected to one side of the lower end of the heating chamber, one end of the liquid outlet pipe A is connected to a hydraulic pump, and the other end of the liquid outlet pipe A is connected and communicated with the inner storage tank.
[0008] Preferably, a plurality of heating sheets are fixedly connected to the inner end wall of the heating chamber and the outer end wall of the inner storage tank.
[0009] Preferably, a liquid outlet pipe B is provided on one side of the lower end of the cooling chamber.
[0010] Preferably, the first side groove has a funnel-shaped structure.
[0011] Preferably, the blocking ball presses against the bottom of the liquid inlet, and the bottom end of the blocking ball and the bottom end inside the second connecting frame are connected by a spring.
[0012] Preferably, openings are provided on both sides of the second connecting frame.
[0013] Compared with the prior art, the beneficial effects of the present utility model are as follows:
[0014] 1. By separately arranging the heating chamber and the cooling chamber, the inner storage tank for heating and the square through-hole for condensation of the present utility model are separated. This arrangement enables the heat generated by heating to accumulate inside the heating chamber, while the low temperature generated by condensation accumulates inside the cooling chamber, so that the heating function and the condensation function no longer affect each other, thereby improving the condensation effect of the square through-hole and the semiconductor refrigeration sheet in the cooling chamber;
[0015] 2. By penetratingly arranging a plurality of square through-holes at the front and rear ends of the cooling chamber, the inner surface of the cooling chamber is increased due to the arrangement of the square through-holes. Second side grooves are arranged on both sides of the surface of the square through-hole, so that the semiconductor refrigeration sheet can be inserted into the second side groove. The operation of the semiconductor refrigeration sheet reduces the temperature of the overall cooling chamber, and the arrangement of the square through-holes improves the condensation effect of the semiconductor refrigeration sheet. BRIEF DESCRIPTION OF THE DRAWINGS
[0016] Figure 1 is a schematic three-dimensional structure diagram of the whole of the present utility model;
[0017] Figure 2 is a three-dimensional view of the whole of the present utility model after separation of the first connecting frame and the semiconductor refrigeration sheet;
[0018] Figure 3 is a front sectional view of the whole of the present utility model;
[0019] Figure 4 is of the present utility model Figure 3 is an enlarged sectional view of part A in the present utility model.
[0020] In the figure: 1. Heating chamber; 2. Cooling chamber; 3. First connecting frame; 4. Fan; 5. Liquid outlet pipe A; 6. Hydraulic pump; 7. Liquid outlet pipe B; 8. Square through hole; 9. First side groove; 10. Vertical column; 11. Second side groove; 12. Semiconductor refrigeration plate; 13. Internal storage tank; 14. Heating plate; 15. Ventilation waist hole; 16. Blocking ball; 17. Second connecting frame; 18. Spring; 19. Liquid inlet. DETAILED DESCRIPTION
[0021] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.
[0022] See also Figures 1 to 4 The utility model provides an embodiment: an octacosanol short molecule distillation extraction device, comprising a heating bin 1, a first side groove 9 is provided in the middle of the upper end of the heating bin 1, a liquid inlet 19 is penetrated in the middle of the bottom end of the first side groove 9, a second connecting frame 17 is fixedly connected to the bottom end of the first side groove 9, a spring 18 is connected to the upper end of the second connecting frame 17, a blocking ball 16 is connected to the upper end of the spring 18, a column 10 is connected to the upper end of the blocking ball 16, an inner storage tank 13 is hoisted inside the heating bin 1, and ventilation holes 15 are provided on both sides of the upper end of the inner storage tank 13;
[0023] The blocking ball 16 and the column 10 are pressed upward as a whole by the stretching force of the spring 18, which causes the blocking ball 16 to move upward under the stretching force of the spring 18, and the upper end of the blocking ball 16 is squeezed on the lower end surface of the liquid inlet 19. At this time, the blocking ball 16 blocks the liquid inlet 19, making it difficult for the gas inside the heating chamber 1 to flow out through the liquid inlet 19.
[0024] The lower end of the heating chamber 1 is fixedly connected to the cooling chamber 2, the front end of the cooling chamber 2 is connected to the first connecting frame 3, and fans 4 are provided on both sides of the front end of the first connecting frame 3. The cooling chamber 2 is penetrated by square through holes 8 at the front and back, and the end surfaces of both sides of the square through holes 8 are provided with second side grooves 11, and semiconductor cooling fins 12 are inserted into the second side grooves 11;
[0025] By setting a plurality of square through holes 8 through the front and rear ends of the cooling bin 2, the setting of the square through holes 8 increases the inner surface of the cooling bin 2, and second side grooves 11 are set on both sides of the surface of the square through holes 8, so that the semiconductor refrigeration plate 12 can be inserted into the second side grooves 11. The operation of the cooling end of the semiconductor refrigeration plate 12 reduces the temperature of the entire cooling bin 2, and a fan 4 is provided at the front end of the first connecting frame 3 to dissipate heat from the heating end of the semiconductor refrigeration plate 12.
[0026] One side at the lower end of the heating chamber 1 is connected through and provided with a liquid outlet pipe A5. One end of the liquid outlet pipe A5 is connected with a hydraulic pump 6, and the other end of the liquid outlet pipe A5 is connected through and communicated with the inner storage tank 13. A plurality of heating sheets 14 are fixedly connected to the inner end wall of the heating chamber 1 and the outer end wall of the inner storage tank 13. One side at the lower end of the cooling chamber 2 is provided with a liquid outlet pipe B7. The first side groove 9 is in a funnel-shaped structure, and this setting makes the extraction liquid not easy to spill out.
[0027] Among them, the blocking ball 16 presses against the bottom of the liquid inlet 19. The bottom end of the blocking ball 16 and the bottom end inside the second connecting frame 17 are connected through a spring 18. Openings are provided on both sides of the second connecting frame 17. The opening setting of the second connecting frame 17 enables the extraction liquid to enter the inner storage tank 13 from the first side groove 9;
[0028] Among them, the separate setting of the heating chamber 1 and the cooling chamber 2 separates the inner storage tank 13 for heating and the square through hole 8 for condensation. This setting makes the heat generated by heating gather inside the heating chamber 1, while the low temperature generated by condensation gathers inside the cooling chamber 2, so that the heating function and the condensation function no longer affect each other, thereby improving the condensation effect of the square through hole 8 and the semiconductor refrigeration sheet 12 in the cooling chamber 2.
[0029] During use, first pour the final mixed liquid into the first side groove 9. At this time, under the action of the stretching elastic force of the spring 18, the blocking ball 16 blocks the bottom end of the liquid inlet 19 to prevent the final mixed liquid from entering the heating sheet 14 in advance;
[0030] Then press down the overall column 10. Then, during the downward movement of the column 10, the column 10 drives the blocking ball 16 to move downward. The downward movement of the blocking ball 16 presses the overall spring 18, thereby overcoming the stretching elastic force of the spring 18, so that the spring 18 no longer squeezes the blocking ball 16 upward. At this time, the liquid inlet 19 is in an open state, and the extraction liquid inside the first side groove 9 flows downward through the liquid inlet 19. The final mixed liquid flows through both sides of the second connecting frame 17, and the final mixed liquid enters the inner storage tank 13;
[0031] Then, the heating sheet 14 on the end wall of the inner storage tank 13 heats the overall inner storage tank 13. Then, the heating sheet 14 raises the temperature to 34.5 degrees Celsius. Under standard atmospheric pressure, at this time, the ether in the mixed liquid is heated to the boiling point. At this time, the ether in the mixed liquid becomes a gas and continuously rises upward from the ventilation waist hole 15 into the inside of the heating chamber 1. Also, a heating sheet 14 is provided on the end wall of the heating chamber 1. Then, the heating sheet 14 continuously heats the ether gas inside the heating chamber 1;
[0032] The ether gas inside the heating chamber 1 will gradually enter the cooling chamber 2 under the action of gravity. The square through holes 8 are provided to increase the contact area between the cooling chamber 2 and the ether gas. Both sides of the square through holes 8 are provided with thermoelectric coolers 12, so the thermoelectric coolers 12 continuously cool the inner surface of the cooling chamber 2. This setting reduces the temperature of the ether gas inside the cooling chamber 2 below 0 °C, and further makes the ether in the cooling chamber 2 in a liquid state;
[0033] When the inner storage tank 13 and the heating element 14 are heated up, the liquid inside the inner storage tank 13 stops boiling. Then the liquid left inside the inner storage tank 13 is octacosanol. Next, the hydraulic pump 6 on the liquid outlet pipe A5 is turned on, and the outside of the liquid outlet pipe A5 is connected to the beaker storage device to store the octacosanol inside the inner storage tank 13. The liquid outlet pipe B7 is connected to an external diversion pipe to store the ether liquid inside the cooling chamber 2, and then the ether liquid can be reused.
[0034] For those skilled in the art, it is obvious that the present invention is not limited to the details of the above exemplary embodiments, and can be implemented in other specific forms without departing from the spirit or basic characteristics of the present invention. Therefore, from any point of view, the embodiments should be regarded as exemplary and non-limiting. The scope of the present invention is defined by the appended claims rather than the above description. Therefore, all changes falling within the meaning and scope of the equivalent elements of the claims are intended to be embraced within the present invention. Any reference signs in the claims should not be regarded as limiting the claimed invention.
Claims
1. A docosanol short molecular distillation extraction device, comprising a heating chamber (1), characterized in that: In the middle of the upper end of the heating chamber (1), a first side groove (9) is provided. At the middle of the bottom end of the first side groove (9), a liquid inlet (19) penetrates through. The bottom end of the first side groove (9) is fixedly connected to a second connecting frame (17). At the upper end inside the second connecting frame (17), a spring (18) is connected. The upper end of the spring (18) is connected to a blocking ball (16). The upper end of the blocking ball (16) is connected to a column (10). An inner storage tank (13) is suspended inside the heating chamber (1). On both sides of the upper end of the inner storage tank (13), air vent waist holes (15) are provided. The heating chamber (1) is fixedly connected to a cooling chamber (2) at the lower end. The front end of the cooling chamber (2) is connected to a first connecting frame (3). On both sides of the front end of the first connecting frame (3), fans (4) are provided. A square through hole (8) runs through the cooling chamber (2) from front to back. On both end faces of the square through hole (8), second side grooves (11) are provided. Inside the second side grooves (11), semiconductor refrigeration sheets (12) are inserted.
2. The octacosanol short molecular distillation extraction device according to claim 1, wherein: On one side of the lower end of the heating chamber (1), a liquid outlet pipe A (5) penetrates and is connected. One end of the liquid outlet pipe A (5) is connected to a hydraulic pump (6). The other end of the liquid outlet pipe A (5) is connected to the inner storage tank (13) in a through manner.
3. The octacosanol short molecular distillation extraction device according to claim 2, wherein: On the inner end wall of the heating chamber (1) and the outer end wall of the inner storage tank (13), a plurality of heating sheets (14) are fixedly connected.
4. A docosanol short molecular distillation extraction device according to claim 3, characterized in that: On one side of the lower end of the cooling chamber (2), a liquid outlet pipe B (7) is provided.
5. The octacosanol short molecular distillation extraction device according to claim 4, characterized in that: The first side groove (9) has a funnel-shaped structure.
6. The octacosanol short molecular distillation extraction device according to claim 1, wherein: The blocking ball (16) presses against the bottom of the liquid inlet (19). The bottom end of the blocking ball (16) and the bottom end inside the second connecting frame (17) are connected by a spring (18).
7. An octacosanol short molecular distillation extraction device according to claim 6, characterized in that: Openings are provided on both sides of the second connecting frame (17).
Citation Information
Patent Citations
Octacosanol molecular distillation extraction element
CN208694281U