Efficient reaction kettle for producing ammonium bifluoride

By introducing a water pump and nozzle system into the ammonium bifluoride production reactor for internal wall cleaning and utilizing a motor-driven stirring system to improve mixing efficiency, the problems of difficult cleaning and uneven mixing in the prior art have been solved, and the high-efficiency use of the reactor has been achieved.

CN223587140UActive Publication Date: 2025-11-25FUJIAN SHUNCHANG FUBAO TENGDA CHEM
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Patent Information

Application Number
CN202422698813.4
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-06
Publication Date
2025-11-25
Estimated Expiration
2034-11-06

AI Technical Summary

Technical Problem

Existing hydrogen fluoride reactors are difficult to clean during use, have low stirring efficiency and poor mixing uniformity, which affects their subsequent performance.

Method used

A high-efficiency reactor for the production of ammonium bifluoride was designed. The reactor uses a water pump, a water storage tank, a hollow ring, and a nozzle structure for internal wall rinsing. The mixing efficiency is improved by a motor-driven stirring shaft and stirring roller. The reactor is combined with an auxiliary material tank and a feeding pipe to achieve stable addition of various auxiliary materials.

Benefits of technology

This method effectively cleans the inner wall of the reactor, improves stirring efficiency and material mixing uniformity, and ensures the reactor's reusability.

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Abstract

The utility model belongs to the technical field of reaction kettles, and particularly relates to an efficient reaction kettle for ammonium bifluoride production, which comprises a mounting table, a reaction kettle body mounted in the mounting table, a hollow ring fixedly connected to the inner wall of the reaction kettle body, nozzles fixedly connected to the inside of the hollow ring at equal intervals, and a fixing plate fixedly connected to the outside of the mounting table. The top of the fixing plate is fixedly connected with a water pump, the output end of the water pump is fixedly connected with a water guide pipe, and the other end of the water guide pipe penetrates through the reaction kettle body and communicates with the hollow ring. Water in the water storage tank is pumped through the water pump and the water pumping pipe, then guided into the hollow ring through the water guide pipe and finally sprayed to the inner wall of the reaction kettle body from the nozzles, so that attachments on the inner wall of the reaction kettle body are washed, the reaction effect of reuse of the reaction kettle body is prevented from being influenced, and the service life of the reaction kettle body is prolonged. The motor drives the plurality of stirring shafts to rotate at the same time, so that the material mixing efficiency and the material mixing uniformity in the reaction kettle body are improved.
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Description

TECHNICAL FIELD

[0001] The utility model relates to the technical field of reaction kettle, concretely to a high -efficient reaction kettle for ammonium bifluoride production. BACKGROUND

[0002] Ammonium bifluoride, molecular formula is NH4HF2, is a kind of inorganic fluorine salt with larger dosage, mainly used as glass etching agent, chemical reagent, boiler cleaning agent, fermentation industry disinfectant and steel plate surface treatment agent etc.

[0003] Prior art has the following defects or problems: Prior art with the publication number CN210700079U discloses a kind of hydrogen fluoride high -efficient reaction kettle, including high -efficient reaction kettle body, the top of high -efficient reaction kettle body is provided with feed pipe, the outer side of feed pipe is equipped with lifting sleeve, handle is arranged on the outer ring surface of lifting sleeve, and the top of lifting sleeve is provided with auxiliary material storage box, the bottom surface of auxiliary material storage box is provided with enclosure pipe, enclosure pipe is connected in the inside of guide groove, guide groove is opened on the top surface of feed pipe, and the bottom surface of auxiliary material storage box is provided with plug plate, leakage port is opened on the surface of plug plate, plug head is inserted in the inside of leakage port.

[0004] The above-mentioned equipment in the process of using, by being provided with multiple feed pipes on hydrogen fluoride high -efficient reaction kettle, auxiliary material storage box is arranged on the lifting of feed pipe, it is convenient for multiple auxiliary materials to be continuously put into reaction kettle interior, compared with sequentially disposable auxiliary material, it is convenient to improve the mixing uniformity of reaction kettle

[0005] The above-mentioned content in actual use process, reaction kettle cannot be cleaned, is not convenient for subsequent use, and its stirring efficiency is low, and the uniformity is poor, therefore, it is necessary to propose a kind of hydrogen fluoride ammonium production high -efficient reaction kettle.

[0006] It should be noted that the above content belongs to the technical cognition of the inventor and does not necessarily constitute the prior art. CONTENT OF UTILITY MODEL

[0007] In view of the deficiencies of the prior art, the utility model provides a kind of hydrogen fluoride ammonium production high -efficient reaction kettle, solves the problems existing today.

[0008] To achieve the above object, the utility model provides the following technical scheme: a kind of hydrogen fluoride ammonium production high -efficient reaction kettle, including installation platform, the inside of installation platform is installed with reaction kettle body, the inner wall of reaction kettle body is fixedly connected with hollow ring, the inside of hollow ring is fixedly connected with spray head at equal intervals, the outside of installation platform is fixedly connected with fixed plate, the top of fixed plate is fixedly connected with water pump, the output of water pump is fixedly connected with water guide pipe, another end of water guide pipe is communicated with hollow ring and passes through reaction kettle body.

[0009] As a preferred technical scheme of the utility model, the bottom of the installation table is provided with a water storage tank, the input end of the water pump is fixedly connected with a water pumping pipe, and the other end of the water pumping pipe extends to the inside of the water storage tank.

[0010] As a preferred technical scheme of the utility model, the inner wall of the hollow ring is fixedly connected with an installation plate, the top of the installation table is fixedly connected with a motor, the output end of the motor extends to the inside of the reaction kettle body and is fixedly connected with a first gear.

[0011] As a preferred technical scheme of the utility model, the inside of the installation plate is rotatably connected with stirring shafts at equal intervals, the top end of each stirring shaft is fixedly connected with a second gear, each first gear is meshingly connected with a first gear, and the outside of each stirring shaft is fixedly connected with a plurality of stirring rollers at equal intervals.

[0012] As a preferred technical scheme of the utility model, the top of the installation table is symmetrically provided with auxiliary material tanks, the bottom of each auxiliary material tank is fixedly connected with a material injection pipe, the other end of each material injection pipe penetrates through the reaction kettle body and extends below the installation plate, the outside of each material injection pipe is provided with a flow valve, and the top of each auxiliary material tank is provided with an auxiliary material feeding opening.

[0013] As a preferred technical scheme of the utility model, the outside of each auxiliary material tank is sleeved with a clamp, the outside of each clamp is fixedly connected with supporting legs at equal intervals, and each supporting leg is fixedly connected with the upper surface of the installation table.

[0014] As a preferred technical scheme of the utility model, the top of the reaction kettle body is fixedly connected with a main material feeding opening, the other end of the main material feeding opening extends below the installation plate, the bottom of the reaction kettle body is provided with a discharging cover, the driving source of the discharging cover is a pneumatic cylinder, the bottom of the installation table is provided with a material receiving box, and the material receiving box is located directly below the reaction kettle body.

[0015] Compared with the prior art, the utility model provides a hydrogen fluoride production efficient reaction kettle, has the following beneficial effects:

[0016] I. The hydrogen fluoride production efficient reaction kettle, through the water pump, the water storage tank, the hollow ring and the spray head, the water in the water storage tank is pumped through the water pump and the water pumping pipe, then is guided into the hollow ring through the water guide pipe, and finally is sprayed from the multiple spray heads to the inner wall of the reaction kettle body, so that the adherents on the inner wall of the reaction kettle body are washed, and the reaction effect of the reuse of the reaction kettle body is prevented;

[0017] II. The efficient reaction kettle for producing ammonium bifluoride is characterized in that the motor, the first gear, the second gear, the stirring shaft and the stirring roller are arranged, the plurality of stirring shafts are driven to rotate simultaneously by the motor, and thus the material mixing efficiency and the material mixing uniformity in the reaction kettle body are improved. BRIEF DESCRIPTION OF DRAWINGS

[0018] Figure 1 It is a whole structure schematic view of the utility model;

[0019] Figure 2 It is a connecting structure schematic view of the hollow ring of the utility model;

[0020] Figure 3 It is an internal structure schematic view of the reaction kettle of the utility model;

[0021] Figure 4 It is a connecting structure schematic view of the auxiliary material tank of the utility model.

[0022] In the drawing: 1, mounting table; 2, reaction kettle body; 3, hollow ring; 4, spray head; 5, fixed plate; 6, water pump; 7, water guide pipe; 8, water storage tank; 9, water suction pipe; 10, mounting plate; 11, motor; 12, first gear; 13, stirring shaft; 14, second gear; 15, stirring roller; 16, auxiliary material tank; 17, material injection pipe; 18, flow valve; 19, auxiliary material feeding opening; 20, clamp; 21, supporting leg; 22, main material feeding opening; 23, discharging cover; 24, material receiving box. DETAILED DESCRIPTION

[0023] In order to make the above objects, features and advantages of the utility model more clearly understood, the utility model will be further described below with the drawings and embodiments. It should be explained that the embodiments and the features in the embodiments of the present application can be combined with each other without conflict.

[0024] The technical scheme in the embodiments of the utility model will be clearly and completely described below with the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by the ordinary skilled in the art without creative labor belong to the protection scope of the utility model.

[0025] Embodiment one

[0026] As Figures 1-4As shown, this utility model provides a technical solution: a high-efficiency reaction vessel for producing ammonium bifluoride, including a mounting platform 1, a reaction vessel body 2 installed inside the mounting platform 1, a hollow ring 3 fixedly connected to the inner wall of the reaction vessel body 2, nozzles 4 fixedly connected at equal intervals inside the hollow ring 3, a fixing plate 5 fixedly connected to the outside of the mounting platform 1, a water pump 6 fixedly connected to the top of the fixing plate 5, a water guide pipe 7 fixedly connected to the output end of the water pump 6, the other end of the water guide pipe 7 passing through the reaction vessel body 2 and communicating with the hollow ring 3, a water storage tank 8 provided at the bottom of the mounting platform 1, a water pumping pipe 9 fixedly connected to the input end of the water pump 6, and the other end of the water pumping pipe 9 extending into the interior of the water storage tank 8.

[0027] In this embodiment, water is drawn from the water storage tank 8 by the water pump 6 and the water pipe 9, then introduced into the hollow ring 3 through the water guide pipe 7, and finally sprayed from multiple nozzles 4 onto the inner wall of the reactor body 2, thereby rinsing off the deposits on the inner wall of the reactor body 2 and preventing them from affecting the reaction effect of the reactor body 2 for reuse.

[0028] Example 2

[0029] like Figures 1-4 As shown, a mounting plate 10 is fixedly connected to the inner wall of the hollow ring 3, a motor 11 is fixedly connected to the top of the mounting platform 1, the output end of the motor 11 extends into the interior of the reactor body 2 and is fixedly connected to a first gear 12, a stirring shaft 13 is rotatably connected at equal intervals inside the mounting plate 10, a second gear 14 is fixedly connected to the top of each stirring shaft 13, each first gear 12 is meshed with the first gear 12, and multiple stirring rollers 15 are fixedly connected at equal intervals to the outside of each stirring shaft 13.

[0030] In this embodiment, the motor 11 drives the first gear 12 to rotate, and the rotation of the first gear 12 drives multiple second gears 14 to rotate, and the rotation of the second gears 14 drives the stirring shaft 13 to rotate, and the rotation of the stirring shaft 13 drives multiple stirring rollers 15 to rotate simultaneously, thereby fully stirring the material inside the reactor body 2. By driving multiple stirring shafts 13 to rotate simultaneously, the mixing efficiency and uniformity of the material inside the reactor body 2 are improved.

[0031] Example 3

[0032] like Figures 1-4As shown, the top of the mounting table 1 is symmetrically provided with auxiliary material tanks 16, the bottom of each auxiliary material tank 16 is fixedly connected with a material injection pipe 17, the other end of each material injection pipe 17 penetrates through the reaction kettle body 2 and extends below the mounting plate 10, the outside of each material injection pipe 17 is provided with a flow valve 18, the top of each auxiliary material tank 16 is provided with an auxiliary material feeding port 19, the outside of each auxiliary material tank 16 is sleeved with a clamp 20, the outside of each clamp 20 is fixedly connected with a support leg 21 at equal intervals, each support leg 21 is fixedly connected with the upper surface of the mounting table 1, the top of the reaction kettle body 2 is fixedly connected with a main material feeding port 22, the other end of the main material feeding port 22 extends below the mounting plate 10, the bottom of the reaction kettle body 2 is provided with a discharge cover 23, the driving source of the discharge cover 23 is a pneumatic cylinder, and the bottom of the mounting table 1 is provided with a material receiving box 24 which is located directly below the reaction kettle body 2.

[0033] In this embodiment, auxiliary materials are added to each auxiliary material tank 16 through the auxiliary material feeding port 19, the clamp 20 and the support leg 21 can provide stability for the auxiliary material tank 16, the main material is injected into the inside of the reaction kettle body 2 through the main material feeding port 22, and the auxiliary materials in the plurality of auxiliary material tanks 16 enter the reaction kettle body 2 through the material injection pipes 17 to be mixed with the main material, the flow valve 18 can control the flow rate of the auxiliary materials and detect the flow of the auxiliary materials, after the mixing is completed, the discharge cover 23 is opened by the pneumatic cylinder, and the mixed materials fall into the material receiving box 24 below under the influence of gravity.

[0034] The working principle of this embodiment is as follows: in use, first, auxiliary materials are added to each auxiliary material tank 16 through the auxiliary material feeding port 19, the clamp 20 and the support leg 21 can provide stability for the auxiliary material tank 16, the main material is injected into the inside of the reaction kettle body 2 through the main material feeding port 22, and the auxiliary materials in the plurality of auxiliary material tanks 16 enter the reaction kettle body 2 through the material injection pipes 17 to be mixed with the main material, the flow valve 18 can control the flow rate of the auxiliary materials and detect the flow of the auxiliary materials;

[0035] Second, the first gear 12 is driven to rotate by the motor 11, the plurality of second gears 14 are driven to rotate when the first gear 12 rotates, the stirring shaft 13 is driven to rotate when the second gear 14 rotates, and the plurality of stirring rollers 15 are simultaneously driven to rotate when the stirring shaft 13 rotates, so that the materials in the inside of the reaction kettle body 2 are fully stirred, the plurality of stirring shafts 13 are simultaneously driven to rotate by the motor 11, so that the material mixing efficiency and the material mixing uniformity in the inside of the reaction kettle body 2 are improved, after the mixing is completed, the discharge cover 23 is opened by the pneumatic cylinder, and the mixed materials fall into the material receiving box 24 below under the influence of gravity;

[0036] Third: after unloading, through the water pump 6 and water suction pipe 9 water tank 8 inside the water extraction, and then through the water pipe 7 into the hollow ring 3, finally from a plurality of spray head 4 to the reactor body 2 of the inner wall, thereby to the reactor body 2 of the inner wall of the attached object is washed, prevent affecting the reactor body 2 again use the reaction effect.

[0037] The above is only the preferred embodiment of the present application, not other forms of the present application for other restrictions, any skilled in the art of the technical personnel may be disclosed by the above technical content to change or modification as equivalent to the equivalent embodiments applied to other fields, but any simple modification, equivalent changes and modification of the above examples, still belong to the present application technical scheme protection scope according to the technical essence of the present application.

Claims

1. A highly efficient reactor for producing ammonium bifluoride, characterized in that: The utility model relates to a reaction kettle, including installation platform (1), the inside installation of installation platform (1) is equipped with reaction kettle body (2), the inner wall fixed connection of reaction kettle body (2) is equipped with hollow ring (3), the inside equidistance fixed connection of hollow ring (3) is equipped with shower head (4), the outside fixed connection of installation platform (1) is equipped with fixed plate (5), the top fixed connection of fixed plate (5) is equipped with water pump (6), the output of water pump (6) is fixedly connected with water guide pipe (7), the other end of water guide pipe (7) passes through reaction kettle body (2) and is communicated with hollow ring (3). ​ 2. The hydrogen fluoride production reactor according to claim 1, characterized in that: The bottom of the installation platform (1) is provided with a water storage tank (8), and the input end of the water pump (6) is fixedly connected with a water suction pipe (9), and the other end of the water suction pipe (9) extends into the inside of the water storage tank (8).

3. The hydrogen fluoride production reactor according to claim 1, characterized in that: The inner wall of the hollow ring (3) is fixedly connected with a mounting plate (10), the top of the installation platform (1) is fixedly connected with a motor (11), and the output of the motor (11) extends into the inside of the reaction kettle body (2) and is fixedly connected with a first gear (12).

4. The hydrogen fluoride production reactor according to claim 3, characterized in that: The inside of the mounting plate (10) is rotatably connected with a stirring shaft (13), the top end of each stirring shaft (13) is fixedly connected with a second gear (14), each first gear (12) is meshingly connected with a first gear (12), and the outside of each stirring shaft (13) is fixedly connected with a plurality of stirring rollers (15).

5. The hydrogen fluoride production reactor according to claim 1, characterized in that: The top of the installation platform (1) is symmetrically provided with an auxiliary material tank (16), the bottom of each auxiliary material tank (16) is fixedly connected with a material injection pipe (17), the other end of each material injection pipe (17) penetrates through the reaction kettle body (2) and extends below the mounting plate (10), the outside of each material injection pipe (17) is provided with a flow valve (18), and the top of each auxiliary material tank (16) is provided with an auxiliary material feeding port (19).

6. The hydrogen fluoride production reactor according to claim 5, characterized in that: The outside of each auxiliary material tank (16) is sleeved with a clamp (20), the outside of each clamp (20) is fixedly connected with a supporting leg (21) at equal intervals, and each supporting leg (21) is fixedly connected with the upper surface of the installation platform (1).

7. The hydrogen fluoride production reactor according to claim 1, characterized in that: The top of the reaction kettle body (2) is fixedly connected with a main material feeding port (22), the other end of the main material feeding port (22) extends below the mounting plate (10), the bottom of the reaction kettle body (2) is provided with a discharge cover (23), the driving source of the discharge cover (23) is a cylinder, the bottom of the installation platform (1) is provided with a receiving box (24), and the receiving box (24) is located directly below the reaction kettle body (2).

Citation Information

Patent Citations

  • High-efficiency hydrogen fluoride reaction kettle

    CN210700079U