Energy-saving gas supply system for autoclave

By using a combination of auger and piston cylinder in the autoclave, the problem of limited movement range of liquid materials was solved, achieving efficient mixing of gas-liquid reactions and reducing reaction time.

CN223602474UActive Publication Date: 2025-11-28丽水惊蛰科技有限公司
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Patent Information

Application Number
CN202423057170.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-12-11
Publication Date
2025-11-28
Estimated Expiration
2034-12-11

AI Technical Summary

Technical Problem

In existing high-pressure reactors, the movement range of liquid materials during gas-liquid reactions is relatively small, resulting in insufficient reaction between gas and liquid materials and increasing reaction time.

Method used

It adopts a combination structure of auger and piston cylinder. The auger is driven by a motor to rotate and push the liquid material to flow. The piston cylinder realizes the recycling of gas through the cooperation of piston rod and spring, ensuring that the gas and liquid material are in full contact.

Benefits of technology

It improves the efficiency of gas-liquid reaction, reduces reaction time, and achieves more thorough material mixing.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model belongs to the technical field of autoclaves, and relates to an autoclave energy-saving air supply system which comprises an autoclave, a rotating shaft is rotatably connected in the autoclave, an auger is fixedly connected to the bottom of the rotating shaft, a motor is fixedly connected to the top of the autoclave, the motor drives the rotating shaft to rotate, and a fixing cylinder is fixedly arranged at the bottom in the autoclave. The auger is rotatably arranged in the fixed cylinder, a breather pipe is fixedly arranged on the fixed cylinder, a feeding hole is formed in the outer side face of the top of the high-pressure kettle, and an exhaust pipe is fixedly connected to the top of the high-pressure kettle. The high-pressure kettle has the advantages that the auger rotates to downwards press a liquid material in the fixed cylinder, so that the liquid material in the fixed cylinder flows downwards, the liquid material is discharged out of the fixed cylinder through the bottom end of the fixed cylinder, and the liquid material at the top in the high-pressure kettle is pressed into the fixed cylinder, so that the flowing of the liquid material is realized; more liquid materials react with gas exhausted by the fourth gas pipe, so that the reaction time is shortened.
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Description

TECHNICAL FIELD

[0001] The utility model belongs to autoclave technical field relates to an autoclave energy -conserving gas supply system. BACKGROUND

[0002] The autoclave is a kind of reactor operated under high pressure, and is used in gas-liquid reaction, which is to extend the air pipe into the liquid material in the autoclave to make the liquid material and reaction gas fully mixed for reaction. Therefore, a gas supply system is needed to supply gas into the autoclave.

[0003] In the Chinese patent CN220194863U, a kind of gas-liquid mixed reaction kettle is disclosed, which includes kettle body, stirring shaft, gas inlet pipe and driver for driving the stirring shaft to rotate, the gas inlet end of the gas inlet pipe is connected with gas supply device, the gas is transported along the gas inlet pipe, hollow stirring shaft and stirring paddle and enters the kettle body through the gas outlet hole on the stirring paddle to fully contact with the rolling material.

[0004] The reaction kettle stirs the material and the gas by the stirring paddle, but the stirring paddle is located at the bottom end of the hollow stirring shaft, which is not convenient for stirring the material at the top of the kettle body, so that the moving range of the material at the top of the kettle body is small, and the gas is not convenient for reacting with more liquid material, which increases the reaction time.

[0005] In the Chinese patent CN210079499U, a kind of circulating gas-liquid phase reaction device for organic synthesis is disclosed, which includes two reaction kettles, each reaction kettle is communicated with reaction gas pipeline through gas supply pipe, each reaction kettle is communicated with vacuum feed pipe through first connecting pipe, the vacuum feed pipe is used for transporting liquid material, and two gas supply pipes are connected through second connecting pipe.

[0006] When using the reaction device, reaction gas is continuously supplied into the first reaction kettle through the reaction gas pipeline and the gas supply pipe, so that the gas reacts with the liquid material. The gas enters the first high-pressure kettle through the top end of the first high-pressure kettle, and the gas reacts with the liquid material at the top first. When the gas is supplied, the moving range of the liquid material is small, and the gas is not convenient for reacting with more liquid material, which increases the reaction time.

[0007] To solve the above problems, the utility model provides a kind of autoclave energy -conserving gas supply system. Utility model content

[0008] To solve the problems in the background art, the utility model provides an autoclave energy -conserving gas supply system.

[0009] In order to achieve the above purpose, the utility model adopts the following technical scheme: including autoclave, the inside rotation of autoclave is connected with shaft, the bottom of shaft is fixedly connected with auger, the top of autoclave is fixedly connected with motor, and motor drives shaft rotation.

[0010] The bottom of the autoclave is fixedly provided with a fixed cylinder, the auger is rotatably arranged in the fixed cylinder, and a vent pipe is fixedly arranged on the fixed cylinder;

[0011] The top of the autoclave is fixedly connected with an exhaust pipe.

[0012] Further, the bottom surface of the fixed cylinder is uniformly fixedly connected with a plurality of support plates, the bottom end of the support plate is fixedly connected to the bottom surface of the inner cavity of the autoclave, and the top end of the auger extends above the fixed cylinder.

[0013] Further, the vent pipe comprises a third air pipe, an annular pipe and a fourth air pipe, the annular pipe is fixedly connected to the top of the fixed cylinder, the fourth air pipe is provided with a plurality of fourth air pipes, the plurality of fourth air pipes are uniformly fixedly connected to the inner wall of the fixed cylinder, the top end of each fourth air pipe is fixedly communicated with the annular pipe, and a plurality of air outlet holes are spaced apart on each fourth air pipe;

[0014] The bottom end of the third air pipe is fixedly communicated with the annular pipe, and the top end of the third air pipe is fixedly penetrated through the top surface of the autoclave.

[0015] Further, the top of the autoclave is fixedly connected with an air pump, one end of the third air pipe is fixedly communicated with the output end of the air pump, and the input end of the air pump is fixedly connected with a first air pipe;

[0016] The end of the first air pipe close to the air pump is fixedly connected with a second air pipe, the second air pipe is fixedly penetrated through the top surface of the autoclave, and the end of the second air pipe extending into the autoclave is fixedly connected with an air inlet head.

[0017] Further, the top of the inner cavity of the autoclave is fixedly connected with a fixed plate, the rotating shaft and the third air pipe pass through the fixed plate, the annular pipe is fixedly communicated with a fifth air pipe, and the other end of the fifth air pipe is provided with an air extraction assembly.

[0018] Further, the air extraction assembly comprises a piston cylinder, the piston cylinder is fixedly connected to the top of the fixed plate, and the top end of the fifth air pipe is communicated with the inner cavity of the piston cylinder after penetrating through the fixed plate;

[0019] The inner part of the piston cylinder is sealingly and slidably connected with a piston rod, the rotating shaft is provided with a driving assembly, and one end of the piston rod is driven to slide in the inner part of the piston cylinder by the driving assembly;

[0020] The end of the piston cylinder away from the piston rod is fixedly connected with a second air pipe, the other end of the second air pipe is fixedly penetrated through the fixed plate, and the other end of the second air pipe is fixedly connected with an air inlet head.

[0021] Further, the driving assembly comprises a rotating disc, the rotating disc is an oval column, the rotating disc is fixedly sleeved on the rotating shaft, and the rotating disc is in abutting and sliding fit with one end of the piston rod.

[0022] One end of the piston cylinder is fixedly connected with a spring, the spring is sleeved on the piston rod, and the other end of the spring is fixedly connected to the end of the piston rod.

[0023] Further, the fifth gas pipe is provided with a first one-way valve, the first one-way valve allows the gas in the piston cylinder to be discharged only through the fifth gas pipe, and the second gas pipe is provided with a second one-way valve, the second one-way valve allows the gas in the piston cylinder to enter only through the second gas pipe.

[0024] Compared with the prior art, the utility model has the following beneficial effects:

[0025] 1. The high-pressure kettle energy-saving gas supply system is provided with an auger, the auger is rotatably arranged in the fixed cylinder, when the gas and the liquid material react in the high-pressure kettle, the auger is driven to rotate by the motor and the rotating shaft, the auger presses the liquid material in the fixed cylinder downwards, the liquid material in the fixed cylinder flows downwards, the liquid material is discharged from the bottom of the fixed cylinder to the outside of the fixed cylinder, and the liquid material at the top of the high-pressure kettle is pressed into the fixed cylinder, thereby realizing the flow of the liquid material, enabling more liquid material to react with the gas discharged from the fourth gas pipe, and reducing the reaction time.

[0026] 2. The high-pressure kettle energy-saving gas supply system is provided with a piston cylinder, the inner cavity of the piston cylinder is communicated with the annular pipe through the fifth gas pipe, when the third gas pipe is used to transport the reaction gas to the inside of the high-pressure kettle, the unreacted gas becomes bubbles and is discharged from the liquid material, and then is discharged to the top end of the inner cavity of the high-pressure kettle, the motor is started to drive the rotating shaft and the rotating disc to rotate, the rotating disc and the spring cooperate to drive one end of the piston rod to reciprocate in the piston cylinder, the gas at the top of the high-pressure kettle enters the piston cylinder through the second gas pipe, and then the gas is discharged again through the fifth gas pipe to react, so that the gas can react sufficiently, and the reaction efficiency is further improved. BRIEF DESCRIPTION OF DRAWINGS

[0027] Figure 1 It is a perspective structural schematic view of the utility model embodiment 1;

[0028] Figure 2 It is a sectional view of the utility model embodiment 1;

[0029] Figure 3 It is a structural schematic view of the fixed cylinder in the utility model embodiment 1;

[0030] Figure 4 It is a perspective structural schematic view of the utility model embodiment 2;

[0031] Figure 5 It is a sectional view of the utility model embodiment 2;

[0032] Figure 6 It is a sectional view of the utility modelFigure 5 Enlarged structural diagram of section A in the middle.

[0033] In the diagram: 1. Support frame; 2. High pressure vessel; 3. Motor; 4. Air pump; 5. First air pipe; 6. Exhaust pipe; 7. Second air pipe; 8. Third air pipe; 9. Rotating shaft; 10. Screwdriver; 11. Fixed cylinder; 12. Annular pipe; 13. Fourth air pipe; 14. Fifth air pipe; 15. Turntable; 16. Piston cylinder; 17. Fixed plate; 18. Piston rod; 19. Spring; 20. First check valve; 21. Second check valve; 22. Feed port. Detailed Implementation

[0034] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0035] Example 1: As Figures 1-3 As shown, the technical solution adopted by this utility model is as follows: an energy-saving gas supply system for a high-pressure reactor includes a high-pressure reactor 2, a rotating shaft 9 is rotatably connected inside the high-pressure reactor 2, and an auger 10 is fixedly connected to the bottom of the rotating shaft 9. The auger 10 is spirally fixed on the outer surface of the rotating shaft 9.

[0036] A motor 3 is fixedly connected to the top of the autoclave 2, and the motor 3 drives the rotating shaft 9 to rotate. The top end of the rotating shaft 9 rotates through the top surface of the autoclave 2 and is fixedly connected to the output shaft of the motor 3. The bottom end of the rotating shaft 9 is rotatably connected to the inner bottom surface of the autoclave 2.

[0037] A fixed cylinder 11 is fixedly installed at the bottom of the autoclave 2, and the auger 10 is rotatably installed inside the fixed cylinder 11. The fixed cylinder 11 is gourd-shaped.

[0038] Several support plates are evenly fixedly connected to the bottom surface of the fixed cylinder 11, and the bottom ends of the support plates are fixedly connected to the bottom surface of the inner cavity of the autoclave 2. This allows the bottom end of the fixed cylinder 11 to communicate with the inner cavity of the autoclave 2, facilitating the transport of liquid materials. The top end of the auger 10 extends above the fixed cylinder 11, allowing the liquid materials to be forced into the fixed cylinder 11 by rotating the auger 10.

[0039] A vent pipe is fixedly installed on the fixed cylinder 11.

[0040] The ventilation pipe comprises a third gas pipe 8, an annular pipe 12 and fourth gas pipes 13. The annular pipe 12 is fixedly connected to the top of the fixed cylinder 11. The fourth gas pipes 13 are provided in plurality, and the fourth gas pipes 13 are uniformly fixedly connected to the inner wall of the fixed cylinder 11. The top end of each fourth gas pipe 13 is fixedly communicated with the annular pipe 12. The gas in the annular pipe 12 enters the fourth gas pipes 13. The fourth gas pipes 13 are provided with gas outlets at intervals. The gas in the fourth gas pipes 13 is discharged through the gas outlets to react with the liquid material in the fixed cylinder 11. The fourth gas pipes 13 at the tightening part of the fixed cylinder 11 are in sliding fit with the outer surface of the auger 10.

[0041] The bottom end of the third gas pipe 8 is fixedly communicated with the annular pipe 12, and the top end of the third gas pipe 8 is fixedly penetrated through the top surface of the autoclave 2.

[0042] The top of the autoclave 2 is fixedly connected with a gas pump 4. One end of the third gas pipe 8 is fixedly communicated with the output end of the gas pump 4, and the input end of the gas pump 4 is fixedly connected with a first gas pipe 5. The other end of the first gas pipe 5 is connected with the gas to be reacted, so that the gas pump 4 can pass the gas to be reacted into the third gas pipe 8.

[0043] The end of the first gas pipe 5 close to the gas pump 4 is fixedly connected with a second gas pipe 7, the second gas pipe 7 is fixedly penetrated through the top surface of the autoclave 2, and the end of the second gas pipe 7 extending into the autoclave 2 is fixedly connected with a gas inlet head. The second gas pipe 7 and the first gas pipe 5 are provided with valves.

[0044] The outer side surface of the top of the autoclave 2 is provided with a feeding hole 22, through which the liquid material is passed into the autoclave 2. The top of the autoclave 2 is fixedly connected with an exhaust pipe 6, and the exhaust pipe 6 is provided with a valve. The bottom end of the autoclave 2 is fixedly connected with a discharge pipe.

[0045] The bottom of the autoclave 2 is fixedly provided with a support frame 1, which supports the autoclave 2.

[0046] Working principle:

[0047] In use, the liquid material is passed into the autoclave 2 through the feeding hole 22, and the liquid material flows over the fixed cylinder 11. One end of the first gas pipe 5 is connected with the gas to be reacted.

[0048] The valve on the second gas pipe 7 is closed, and the valve on the first gas pipe 5 is opened. The gas pump 4 is started, so that the gas enters the inside of the third gas pipe 8 through the first gas pipe 5, and then enters the inside of the annular pipe 12 and the fourth gas pipes 13, and is discharged through the gas outlets to react with the material in the fixed cylinder 11.

[0049] When more gas is passed in, the gas will move out of the liquid material in the form of bubbles and float to the top of the autoclave 2.

[0050] Close the valve on the first gas pipe 5 and open the valve on the second gas pipe 7. This allows the gas from the top of the autoclave 2 to enter the second gas pipe 7, and then re-enter the fixed cylinder 11 through the third gas pipe 8 to carry out the reaction.

[0051] The motor 3 is started, causing the shaft 9 to rotate, which in turn drives the auger 10 to rotate. The rotation of the auger 10 presses the liquid material downwards, causing it to move downwards inside the fixed cylinder 11, and then flow out of the fixed cylinder 11 through its bottom. Meanwhile, the liquid material at the top of the fixed cylinder 11 is forced into the fixed cylinder 11, thus causing the liquid material to flow inside the autoclave 2, allowing more liquid material to come into contact with the gas, thereby reducing the reaction time.

[0052] After the reaction is complete, the material in the high-pressure reactor 2 is discharged through the discharge pipe.

[0053] Example 2: As Figures 4-6 As shown, an energy-saving gas supply system for a high-pressure reactor includes a high-pressure reactor 2. A rotating shaft 9 is rotatably connected inside the high-pressure reactor 2, and an auger 10 is fixedly connected to the bottom of the rotating shaft 9. The auger 10 is spirally fixed to the outer surface of the rotating shaft 9.

[0054] A motor 3 is fixedly connected to the top of the autoclave 2, and the motor 3 drives the rotating shaft 9 to rotate. The top end of the rotating shaft 9 rotates through the top surface of the autoclave 2 and is fixedly connected to the output shaft of the motor 3. The bottom end of the rotating shaft 9 is rotatably connected to the inner bottom surface of the autoclave 2.

[0055] A fixed cylinder 11 is fixedly installed at the bottom of the autoclave 2, and the auger 10 is rotatably installed inside the fixed cylinder 11. The fixed cylinder 11 is gourd-shaped.

[0056] Several support plates are evenly fixedly connected to the bottom surface of the fixed cylinder 11, and the bottom ends of the support plates are fixedly connected to the bottom surface of the inner cavity of the autoclave 2. This allows the bottom end of the fixed cylinder 11 to communicate with the inner cavity of the autoclave 2, facilitating the transport of liquid materials. The top end of the auger 10 extends above the fixed cylinder 11, allowing the liquid materials to be forced into the fixed cylinder 11 by rotating the auger 10.

[0057] A vent pipe is fixedly installed on the fixed cylinder 11.

[0058] The ventilation pipe comprises a third gas pipe 8, a ring pipe 12 and a fourth gas pipe 13. The ring pipe 12 is fixedly connected to the top of the fixed cylinder 11. The fourth gas pipe 13 is provided with a plurality of fourth gas pipes 13 which are uniformly fixedly connected to the inner wall of the fixed cylinder 11. The top end of each fourth gas pipe 13 is fixedly communicated with the ring pipe 12. The gas in the ring pipe 12 enters the plurality of fourth gas pipes 13. A plurality of gas outlets are arranged on each fourth gas pipe 13 at intervals. The gas in the fourth gas pipe 13 is discharged through the gas outlets, so that the gas reacts with the liquid material at different positions in the fixed cylinder 11. The fourth gas pipe 13 at the tightening portion of the fixed cylinder 11 is in sliding fit with the outer surface of the auger 10.

[0059] The bottom end of the third gas pipe 8 is fixedly communicated with the ring pipe 12, and the top end of the third gas pipe 8 is fixedly penetrated through the top surface of the autoclave 2.

[0060] The top of the inner cavity of the autoclave 2 is fixedly connected with a fixed plate 17, and the rotating shaft 9 and the third gas pipe 8 are both penetrated through the fixed plate 17. The rotating shaft 9 is rotatably penetrated through the fixed plate 17, and the third gas pipe 8 is fixedly penetrated through the fixed plate 17.

[0061] The ring pipe 12 is fixedly communicated with a fifth gas pipe 14. The other end of the fifth gas pipe 14 is provided with a gas extraction assembly.

[0062] The gas extraction assembly comprises a piston cylinder 16 which is fixedly connected to the top of the fixed plate 17. The top end of the fifth gas pipe 14 is communicated with the inner cavity of the piston cylinder 16 after being penetrated through the fixed plate 17.

[0063] A first one-way valve 20 is arranged on the fifth gas pipe 14. The first one-way valve 20 allows the gas in the piston cylinder 16 to be discharged only through the fifth gas pipe 14. The fifth gas pipe 14 discharges the gas to the ring pipe 12.

[0064] A piston rod 18 is sealingly and slidably connected to the inside of the piston cylinder 16. One end of the piston rod 18 extends to the outside of the piston cylinder 16. A driving assembly is arranged on the rotating shaft 9, which drives the one end of the piston rod 18 to slide in the inside of the piston cylinder 16. The piston cylinder 16 is used for gas extraction or gas discharge by sliding of the piston rod 18.

[0065] The other end of the piston cylinder 16 is fixedly connected with a second gas pipe 7, and the other end of the second gas pipe 7 is fixedly penetrated through the fixed plate 17. The other end of the second gas pipe 7 is fixedly connected with an air inlet head. The air inlet head is located below the fixed plate 17, and the gas at the top of the autoclave 2 enters the second gas pipe 7 through the air inlet head.

[0066] A second one-way valve 21 is arranged on the second gas pipe 7. The second one-way valve 21 allows the gas in the piston cylinder 16 to enter only through the second gas pipe 7.

[0067] The driving assembly comprises a rotating disc 15 which is an elliptical cylinder. The rotating disc 15 is fixedly sleeved on the rotating shaft 9, and the rotating disc 15 is in abutting sliding fit with one end of the piston rod 18.

[0068] One end of the piston cylinder 16 is fixedly connected with a spring 19, the spring 19 is sleeved on the piston rod 18, and the other end of the spring 19 is fixedly connected to the end of the piston rod 18. The spring 19 abuts the outer surface of the rotating disc 15.

[0069] An inlet hole 22 is formed on the outer side of the top of the autoclave 2, and liquid material is introduced into the autoclave 2 through the inlet hole 22. The top of the autoclave 2 is fixedly connected with an exhaust pipe 6, and the exhaust pipe 6 is provided with a valve. The bottom end of the autoclave 2 is fixedly connected with a discharge pipe.

[0070] The bottom of the autoclave 2 is fixedly provided with a support frame 1, and the support frame 1 supports the autoclave 2.

[0071] Working principle:

[0072] In use, liquid material is introduced into the autoclave 2 through the inlet hole 22, and the liquid material flows over the fixed cylinder 11. One end of the third gas pipe 8 is connected with the gas to be reacted.

[0073] The gas to be reacted enters the inside of the annular pipe 12 and the fourth gas pipe 13 through the third gas pipe 8, and then is discharged through the gas outlet hole to react with the material in the fixed cylinder 11.

[0074] When more gas is introduced, the gas will move out of the liquid material in the form of bubbles and float to the top of the autoclave 2.

[0075] The rotating shaft 9 is driven to rotate by the starting motor 3, and the rotating shaft 9 drives the auger 10 to rotate. The rotation of the auger 10 will press the liquid material downward, so that the liquid material moves downward in the inside of the fixed cylinder 11, and then flows out of the fixed cylinder 11 through the bottom of the fixed cylinder 11. The liquid material at the top of the fixed cylinder 11 is pressed into the fixed cylinder 11, so that the liquid material flows in the inside of the autoclave 2, and more liquid material is contacted with the gas, thereby reducing the reaction time.

[0076] The rotating shaft 9 will also drive the rotating disc 15 to rotate. Since the rotating disc 15 is an elliptical cylinder, when the end of the rotating disc 15 rotates to contact the end of the piston rod 18, the rotating disc 15 will gradually push the piston rod 18 to slide into the inside of the piston cylinder 16 and compress the spring 19. At this time, the gas in the piston cylinder 16 is discharged into the annular pipe 12 through the fifth gas pipe 14, and then into the fixed cylinder 11.

[0077] When the end of the rotating disc 15 rotates away from the end of the piston rod 18, the spring 19 pushes the piston rod 18 to slide the piston rod 18 to the outside of the piston cylinder 16. The end of the piston rod 18 is always in abutting cooperation with the rotating disc 15 under the action of the spring 19. The gas at the top of the autoclave 2 enters the piston cylinder 16 through the second gas pipe 7.

[0078] Further, the piston cylinder 16 is subjected to gas suction and exhaust through the reciprocating sliding of the end of the piston rod 18 in the piston cylinder 16.

[0079] After the reaction is completed, the material in the autoclave 2 is discharged through the discharge pipe.

[0080] Although the utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions recorded in the foregoing embodiments or make equivalent replacement to part of the technical features, and any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the utility model should be included in the protection scope of the utility model.

Claims

1. An autoclave energy-saving gas supply system, characterized by, Including autoclave (2), the inside of autoclave (2) is rotatably connected with rotating shaft (9), the bottom of rotating shaft (9) is fixedly connected with auger (10), the top of autoclave (2) is fixedly connected with motor (3), and motor (3) drives rotating shaft (9) to rotate; The bottom in the autoclave (2) is fixedly provided with a fixed cylinder (11), the auger (10) is rotatably arranged in the fixed cylinder (11), and the fixed cylinder (11) is fixedly provided with a vent pipe on the top thereof; The vent pipe comprises a third air pipe (8), an annular pipe (12) and a fourth air pipe (13), the annular pipe (12) is fixedly connected to the top of the fixed cylinder (11), the fourth air pipe (13) is provided with a plurality of fourth air pipes (13), the plurality of fourth air pipes (13) are fixedly connected to the inner wall of the fixed cylinder (11), the top end of each fourth air pipe (13) is fixedly communicated with the annular pipe (12), and a plurality of air outlet holes are formed in each fourth air pipe (13) at intervals; The bottom end of the third air pipe (8) is fixedly communicated with the annular pipe (12), and the top end of the third air pipe (8) penetrates the top surface of the autoclave (2) fixedly; The top of the inner cavity of the autoclave (2) is fixedly connected with a fixed plate (17), the rotating shaft (9) and the third air pipe (8) penetrate the fixed plate (17), the annular pipe (12) is fixedly communicated with a fifth air pipe (14), and the other end of the fifth air pipe (14) is provided with an air extraction assembly; The air extraction assembly comprises a piston cylinder (16), the piston cylinder (16) is fixedly connected to the top of the fixed plate (17), and the top end of the fifth air pipe (14) is communicated with the inner cavity of the piston cylinder (16) after penetrating the fixed plate (17); The inner cavity of the piston cylinder (16) is sealingly and slidably connected with a piston rod (18), the rotating shaft (9) is provided with a driving assembly, and one end of the piston rod (18) is driven to slide in the inner cavity of the piston cylinder (16) by the driving assembly; The other end of the piston cylinder (16) is fixedly connected with a second air pipe (7), the other end of the second air pipe (7) penetrates the fixed plate (17) fixedly, and the other end of the second air pipe (7) is fixedly connected with an air inlet head; The top of the autoclave (2) is fixedly connected with an exhaust pipe (6).

2. The energy-saving gas supply system for an autoclave according to claim 1, characterized in that: The bottom surface of the fixed cylinder (11) is fixedly connected with a plurality of support plates, the bottom end of the support plate is fixedly connected to the bottom surface of the inner cavity of the autoclave (2), and the top end of the auger (10) extends above the fixed cylinder (11).

3. The energy-saving gas supply system for an autoclave according to claim 1, characterized in that: The driving assembly comprises a rotating disc (15), the rotating disc (15) is an oval column, the rotating disc (15) is fixedly sleeved on the rotating shaft (9), and the rotating disc (15) is in abutting and sliding fit with one end of the piston rod (18); One end of the piston cylinder (16) is fixedly connected with a spring (19), the spring (19) is sleeved on the piston rod (18), and the other end of the spring (19) is fixedly connected to the end of the piston rod (18).

4. The energy-saving gas supply system for an autoclave according to claim 1, characterized by: The fifth gas pipe (14) is provided with a first one-way valve (20) which allows the gas in the piston cylinder (16) to only be discharged through the fifth gas pipe (14), and the second gas pipe (7) is provided with a second one-way valve (21) which allows the gas in the piston cylinder (16) to only enter through the second gas pipe (7).

Citation Information

Patent Citations

  • Circulating gas-liquid phase reaction device for organic synthesis

    CN210079499U

  • Gas-liquid mixing reaction kettle

    CN220194863U