Efficient curing agent reaction kettle

By combining internal and external coil countercurrent heating with a temperature regulator, the problem of uneven temperature in the reactor was solved, achieving efficient temperature control and stirring, and improving the production efficiency and quality of the curing agent.

CN223641825UActive Publication Date: 2025-12-09NASURFAR BIOMATERIAL TECH (CHANGSHU) CO LTD
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Patent Information

Application Number
CN202422408509.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-09-30
Publication Date
2025-12-09
Estimated Expiration
2034-09-30

AI Technical Summary

Technical Problem

Existing reactors suffer from uneven temperature distribution, especially in exothermic chemical reactions, resulting in long cooling times, low product quality and production efficiency, and slow heating efficiency.

Method used

The reactor employs a counter-current heating structure with internal and external coils and multiple temperature regulators. Combined with the stirring system and temperature regulators, it achieves uniform temperature control within the reactor. The reactor temperature is regulated by introducing hot steam and cooling water through the internal and external coils, while the stirring system ensures uniform mixing of the reaction materials.

Benefits of technology

It achieves uniform temperature and rapid response within the reactor, improving production efficiency and product quality. Its simple and compact structure makes it easy to operate and ensures the stability and safety of the reaction process.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of reaction kettles, in particular to an efficient curing agent reaction kettle. According to the technical scheme, the reaction kettle is characterized by comprising a shell, a reaction kettle body is included, a stirring system is arranged on the reaction kettle body, an outer coil pipe is arranged on the outer side of the reaction kettle body, a heat source inlet is formed in the bottom end of the outer coil pipe, a heat source outlet is formed in one side of the outer layer of the outer coil pipe, and supporting angle steel is arranged on one side of the inner wall of the reaction kettle body; connecting angle steel is arranged at the end of the supporting angle steel in the direction parallel to the reaction kettle body, one end of the connecting angle steel is arranged on the reaction kettle body, an inner coil pipe is arranged on the connecting angle steel, an inlet is connected to the upper end of the inner coil pipe, an outlet is formed in the lower end of the inner coil pipe, and a plurality of temperature control mechanisms are further arranged on the connecting angle steel. The utility model provides an efficient curing agent reaction kettle, in order to realize uniform temperature of reaction materials in the reaction kettle and improve the operation efficiency and quality, the efficient curing agent reaction kettle can ensure the heating efficiency and uniform temperature of the reaction materials according to the temperature requirement of a production process, and is beneficial to proceeding of chemical reaction; and in addition, the structure is simple and compact, and the operation is convenient.
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Description

TECHNICAL FIELD

[0001] The utility model relates to the technical field of reaction kettle, especially relates to a high -efficient curing agent reaction kettle. BACKGROUND

[0002] The reaction kettle is a container for physical or chemical reaction. Through the structure design and parameter configuration of the container, the functions of heating, evaporation, cooling and low-speed mixing are realized. The reaction kettle is mainly used for processing and treating curing agent.

[0003] The reaction kettle in the prior art usually comprises a kettle body, a jacket is arranged on the outer wall of the kettle body, a reaction cavity is arranged in the kettle body, and the temperature in the reaction cavity is usually cooled by the conduction of the fluid in the jacket to the kettle body wall. Since the heat transfer efficiency at the center position of the reaction cavity is much lower than that near the peripheral wall, there is a problem of uneven temperature in the reaction kettle, which makes it impossible to uniformly heat and cool the chemicals in the reaction kettle. Especially for chemical reactions with a large amount of heat release during the reaction, since the internal temperature can only be cooled by peripheral conduction, not only is the temperature uneven, but also the cooling time is long, which greatly reduces the reaction effect of the product and affects the product quality. Moreover, for curing agent products, different reaction temperatures, reaction pressures, reaction times of materials and reaction conversion rates have a direct impact. Some special material reactions must be carried out in a specific temperature range to achieve sufficient reaction, optimal conversion rate and reaction time. The operator exchanges heat by the conduction of the fluid in the jacket to the kettle body wall to realize the heating and warming of the cylinder body. The heating efficiency is slow, and the reaction efficiency needs to be improved. This makes the curing agent discharge uneven, which undoubtedly greatly reduces the production efficiency and quality. SUMMARY

[0004] In order to realize uniform temperature of reaction materials in the reaction kettle, improve work efficiency and quality, the application provides a high -efficient curing agent reaction kettle, which can realize uniform temperature of reaction materials according to the temperature requirement of production process, is beneficial to chemical reaction, improves production efficiency and product quality, and has simple and compact structure and convenient operation.

[0005] The application provides a high -efficient curing agent reaction kettle, which adopts the following technical scheme:

[0006] The utility model provides a high -efficient curing agent reaction kettle, including the reaction kettle body, is provided with stirring system on the reaction kettle body, the outside of reaction kettle body is provided with the outer coil pipe, the bottom of outer coil pipe is provided with heat source import, one side of outer coil pipe outer layer is provided with heat source export, one side of reaction kettle body inner wall is provided with support angle steel, the end of support angle steel and the parallel direction of reaction kettle body is provided with connecting angle steel, and one end of connecting angle steel is arranged in the reaction kettle body, and the inner coil pipe is arranged on the connecting angle steel, and the import is connected to the upper end of inner coil pipe, and the export is arranged in the lower end of inner coil pipe, a plurality of temperature regulators are further arranged on the connecting angle steel.

[0007] Through the above technical scheme, when producing curing agent, the curing agent raw materials in the reaction kettle body are stirred by the stirring system, the curing agent reaction kettle is provided with the inner coil pipe and the outer coil pipe, the inner coil pipe and the outer coil pipe are both connected with hot steam when heating, the inner and outer steam inlets are opposite, the inner and outer steam flows in opposite directions, so that the temperature of the reaction kettle is more uniform, and the heating efficiency is higher, the reaction kettle is further provided with multiple temperature regulators, the temperature regulator can be connected with steam, cooling water or refrigerated water according to the actual reaction working requirement to adjust the working temperature in the kettle body, so as to achieve the effects of heating, heat preservation, cooling and temperature reduction, the working efficiency of producing curing agent is improved, the quality of the product is improved, the kettle body is heated by the inner and outer coil pipes, the overall temperature control is fast and direct, the temperature in the kettle body is kept in a stable state, and the temperature in the kettle body will not change sharply due to external factors, when cooling, the inner coil pipe is connected with cooling water, the cooling efficiency is higher, and the structure is simple and compact, and the operation is convenient.

[0008] In a specific embodiment, the stirring system includes a mounting base disposed on the top of the reaction kettle body, a special-shaped rack disposed on the mounting base, a motor disposed on the special-shaped rack, a speed reducer disposed on the output shaft of the motor, a coupling connected to the output shaft of the speed reducer, a stirring shaft connected to the coupling, a mechanical seal disposed between the coupling and the stirring shaft, a plurality of stirrers equidistantly disposed on the stirring shaft, and a bottom bearing disposed on the other end of the stirring shaft.

[0009] By adopting the above technical scheme, the mounting base is disposed on the top of the reaction kettle body, the mounting rack and the motor are connected to the speed reducer through the output shaft of the motor, the stirring rate can be adjusted, the coupling, the stirring shaft and the stirrers enable the motor to drive the stirrers to rotate, the curing agent raw materials are stirred, the bottom bearing is fixed to keep the stirring uniform, and each reaction raw material is heated uniformly.

[0010] In a specific embodiment, the stirring shaft is provided with a coupling flange, and the mounting base is provided with a flange flange.

[0011] By adopting the above technical solution, the stirring shaft can be disassembled by setting a connecting flange on the stirring shaft, which facilitates the replacement or maintenance of the blades and ensures the stirring effect of the stirred reactor. The flange also allows the stirring system to be disassembled, making it possible to replace the motor and reducer, thereby improving the service life of the reactor body and adapting to extreme reaction temperatures and stirring conditions.

[0012] The agitator is a curved fan-shaped two-bladed impeller.

[0013] By adopting the above-mentioned technical solution, the curved surface helps to reduce air resistance. The blade-shaped paddle ensures uniform mixing and consistent temperature inside the mixing vessel. The curved fan blades can lift and stir the material at the bottom of the reaction vessel, ensuring that the material reacts fully and does not damage the resin that needs to be cured.

[0014] In one specific implementation scheme, a handhole, solvent feed port, helium port, resin feed port, reflux port, liquid feed port, spare port, pressure gauge, and vacuum port are arranged on one side of the top of the reactor body along a circumference of the same diameter circle centered around the center of the top of the reactor body, and a sight glass and a manhole are provided on the other side.

[0015] By adopting the above technical solution and setting, the equipment's working status can be monitored and tracked in real time. Furthermore, since the reactor needs to operate under high pressure, the safety of the equipment is improved, it is convenient for staff to add materials, and the design of the manhole facilitates the later maintenance of the equipment.

[0016] In one specific implementation, the reactor body is further provided with an ear-type support, and the ear-type support is further provided with an electrostatic grounding plate.

[0017] By adopting the above technical solution, the installation and disassembly of the reactor body can be facilitated by the lug-type support, and the electrostatic grounding plate can ensure the electrostatic safety of the entire reactor body, preventing static electricity from affecting the production efficiency of the curing agent and the health of the staff.

[0018] In one specific implementation, the bottom of the reactor body is provided with a discharge port.

[0019] After processing, the material is discharged through the finished product discharge pipe.

[0020] In one specific implementation scheme, the inner coil is provided with U-bolts, which are used to connect to the connecting angle steel.

[0021] By adopting the above technical solution, the inner coil is fixed to the connecting angle steel with U-bolts to prevent pressure, temperature and other factors from affecting the thermal conductivity of the inner coil.

[0022] In summary, this application includes at least one of the following beneficial technical effects:

[0023] 1. During the production of curing agents, the curing agent raw materials in the reactor are stirred by a stirring system. This curing agent reactor is equipped with inner and outer coils, so that hot steam is introduced into both the inner and outer coils during heating, with the inner and outer hot steam inlets facing opposite directions, causing the steam to flow counter-currently. This helps to maintain a more uniform temperature in the reactor. The reactor is also equipped with multiple temperature regulators, which can be supplied with steam, cooling water, or chilled water according to the actual reaction requirements to adjust the working temperature inside the reactor, achieving effects such as heating, heat preservation, cooling, and cooling down. This improves the efficiency of curing agent production and enhances product quality. The reactor is heated by connecting the inner and outer coils to a heat source, allowing for quick and direct overall temperature control and ensuring a stable internal temperature that is not subject to drastic changes due to external factors. When cooling is required, the inner coil uses cooling water, resulting in higher cooling efficiency. The reactor also features a simple and compact structure, making it easy to operate.

[0024] 2. The mounting base plate set on the top of the reactor body is used to install the frame and motor. The motor output shaft is connected to the reducer, which can adjust the stirring speed. The coupling, stirring shaft and stirrer enable the electrical components to drive the stirrer to rotate and stir the curing agent raw materials. The bottom bearing is fixed to keep the stirring uniform and ensure that the reactants are heated evenly.

[0025] 3. The lug-type support facilitates the installation and disassembly of the reactor body. The electrostatic grounding plate ensures the electrostatic safety of the entire reactor body, preventing static electricity from affecting the production efficiency of the curing agent and the health of the staff. Attached Figure Description

[0026] Figure 1 This is a structural schematic diagram of an embodiment of this application.

[0027] Figure 2 This is a diagram showing the arrangement of the top nozzles of the reactor body in an embodiment of this application.

[0028] Figure 3 This is an enlarged view of part A of the embodiments of this application.

[0029] Figure 4 This is an enlarged view of part B of the embodiment of this application.

[0030] Explanation of reference numerals in the attached drawings: 1. Reactor body; 11. External coil; 112. Heat source inlet; 121. Heat source outlet; 122. Supporting angle steel; 12. Connecting angle steel; 13. Internal coil; 14. Inlet; 15. Outlet; 151. Temperature regulator; 16. Mounting base plate; 17. Irregular frame; 18. Motor; 183. Reducer; 19. Coupling; 20. Stirring shaft; 21. Mechanical seal; 22. 23. Stirrer; 29. ​​Bottom bearing; 29. ​​Connecting flange; 291. Flange flange; 30. Manhole; 31. Solvent inlet; 32. Helium inlet; 33. Resin inlet; 34. Reflux inlet; 35. Liquid inlet; 36. Spare inlet; 37. Pressure gauge; 38. Vacuum inlet; 44. Sight glass; 45. Manhole; 55. Ear support; 62. Electrostatic grounding plate; 71. Discharge port; 81. U-bolt. Detailed Implementation

[0031] The following is in conjunction with the appendix Figures 1-3 This application will be described in further detail.

[0032] This application discloses a high-efficiency curing agent reactor.

[0033] See reference Figure 1 and Figure 3 A high-efficiency curing agent reactor includes a reactor body 1, a stirring system on the reactor body 1, a motor 18, a reducer 183 connected to the output shaft of the motor 18, a coupling 19 connected to the output shaft of the reducer 183, a stirring shaft 20 connected to the coupling 19, a mechanical seal 21 between the coupling 19 and the stirring shaft 20, a plurality of stirrers 22 equidistantly arranged on the stirring shaft 20, a bottom bearing 23 at the other end of the stirring shaft 20, a mounting base plate 16 on the reactor body 1, a special-shaped frame 17 on the mounting base plate 16, the coupling 19 and the mechanical seal 21 are both located in the special-shaped frame 17, a flange 291 on the mounting base plate 16, a connecting flange 29 on the stirring shaft 20, and three equidistant stirrers 22 on the stirring shaft 20, the stirrers 22 being curved fan-shaped two-bladed impellers.

[0034] When repairing or replacing the mixing system, simply loosen the flange 291 on the mounting base plate 16 to remove the motor 18 and reducer 183. To replace the mixer 22, simply insert the new component through the connecting flange 29 and tighten the flange nut.

[0035] Reference Figure 1 and Figure 4An outer coil 11 is provided on the outside of the reactor body 1. A heat source inlet 112 is provided at the bottom of the outer coil 11. A heat source outlet 121 is provided on one side of the outer layer of the outer coil 11. A supporting angle steel 122 is provided on one side of the inner wall of the reactor body 1. A connecting angle steel 12 is provided at the end of the supporting angle steel 122 in a direction parallel to the reactor body 1. One end of the connecting angle steel 12 is provided on the reactor body 1. An inner coil 13 is provided on the connecting angle steel 12. A U-bolt is provided on the inner coil 13 and connected to the connecting angle steel 12 by the U-bolt. An inlet 14 is connected to the upper end of the inner coil 13 and an outlet 15 is provided at the lower end of the inner coil 13. Two temperature regulators 151 are also provided on the connecting angle steel 12.

[0036] Reference Figure 1 and Figure 2 The top of the reactor body 1 is provided with a hand hole 30, a solvent feed port 31, a helium gas port 32, a resin feed port 33, a reflux port 34, a liquid feed port 35, a spare port 36, a pressure gauge 37, and a vacuum port 38 arranged on a circumference of the same diameter circle centered around the center of the top of the reactor body. The other side is provided with a sight glass 44 and a manhole 45. The bottom of the reactor body 1 is provided with a discharge port 71. The reactor body 1 is also provided with an ear-type support 55, and an electrostatic grounding plate 62 is also provided on the ear-type support 55.

[0037] The implementation principle of this embodiment is as follows: When using this high-efficiency curing agent reactor, the motor 18 is first started to drive the reducer 183 to rotate, which can adjust the stirring speed, drive the coupling 19 and the stirring shaft 20 to make the stirrer 22 rotate, and feed is added through the feeding port. At the same time, according to the actual reaction work requirements, steam is introduced into the bottom outer coil 11, and then steam is introduced into the top inner coil 13. The temperature controller is adjusted to ensure that the temperature of the system is uniform. After the reaction is completed, the temperature regulator 151 can introduce steam, cooling water or chilled water according to the actual reaction discharge requirements to adjust the working temperature inside the reactor, so as to achieve the effects of heating, heat preservation, cooling and cooling, ensuring the working efficiency of curing agent production, improving product quality, and the overall temperature control is quick and direct, ensuring that the internal temperature is in a stable state and will not change drastically due to external factors. When cooling is required, the inner coil 13 is cooled by cooling water, which has higher cooling efficiency, and the structure is simple and compact, and the operation is convenient.

[0038] The above are all preferred embodiments of this application, and are not intended to limit the scope of protection of this application. Therefore, all equivalent changes made in accordance with the structure, shape and principle of this application should be covered within the scope of protection of this application.

Claims

1. A high-efficiency curing agent reaction vessel, characterized in that, The reactor includes a reactor body (1), which is equipped with a stirring system. An outer coil (11) is provided on the outside of the reactor body (1). A heat source inlet (112) is provided at the bottom end of the outer coil (11). A heat source outlet (121) is provided on one side of the outer layer of the outer coil (11). A supporting angle steel (122) is provided on one side of the inner wall of the reactor body (1). A connecting angle steel (12) is provided at the end of the supporting angle steel (122) in a direction parallel to the reactor body (1). One end of the connecting angle steel (12) is provided on the reactor body (1). An inner coil (13) is provided on the connecting angle steel (12). An inlet (14) is connected to the upper end of the inner coil (13). An outlet (15) is provided at the lower end of the inner coil (13). Several temperature control mechanisms are also provided on the connecting angle steel (12).

2. The high-efficiency curing agent reactor according to claim 1, characterized in that, The stirring system includes a mounting base plate (16), which is set on the top of the reactor body (1). A special-shaped frame (17) is set on the mounting base plate (16), and a motor (18) is set on the special-shaped frame (17). A reducer (183) is set on the output shaft of the motor (18). A coupling (19) is connected to the output shaft of the reducer (183). A stirring shaft (20) is connected to the coupling (19). A mechanical seal (21) is set between the coupling (19) and the stirring shaft (20). Several stirrers (22) are equidistantly arranged on the stirring shaft (20). A bottom bearing (23) is set at the other end of the stirring shaft (20).

3. The high-efficiency curing agent reactor according to claim 2, characterized in that, A connecting flange (29) is provided on the stirring shaft (20), and a flange flange (291) is provided on the mounting base plate (16).

4. The high-efficiency curing agent reactor according to claim 2, characterized in that, The agitator (22) is a curved fan-shaped two-blade impeller.

5. The high-efficiency curing agent reactor according to claim 1, characterized in that, The reactor body (1) has a handhole (30), a solvent feed port (31), a helium gas port (32), a resin feed port (33), a reflux port (34), a liquid feed port (35), a spare port (36), a pressure gauge (37), and a vacuum port (38) arranged on a circumference of the same diameter circle centered around the top center of the reactor body on one side. The other side has a sight glass (44) and a manhole (45).

6. The high-efficiency curing agent reactor according to claim 1, characterized in that, The reactor body (1) is also provided with an ear-type support (55), and the ear-type support (55) is also provided with an electrostatic grounding plate (62).

7. The high-efficiency curing agent reactor according to claim 1, characterized in that, The bottom of the reactor body (1) is provided with a discharge port (71).

8. The high-efficiency curing agent reactor according to claim 1, characterized in that, The inner coil (13) is provided with U-bolts, which are connected to the connecting angle steel (12).