Continuous rectification purification device
By incorporating a stirring mechanism and a continuous processing mechanism into the distillation and purification unit, the problem of uneven heating of materials was solved, achieving uniform heating of materials, reducing energy consumption, and improving separation and production efficiency.
Patent Information
- Application Number
- CN202520046252.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-09
- Publication Date
- 2025-12-16
- Estimated Expiration
- 2035-01-09
AI Technical Summary
Existing distillation and purification equipment lacks a stirring mechanism, resulting in uneven heating of the distillation material, which necessitates increased heating power and extended heating time, thus increasing energy consumption.
The installation mechanism includes a motor-driven rotating shaft and a stirring shell to achieve uniform mixing of materials, and a connecting mechanism to achieve continuous distillation. It also utilizes an electric heater and a spiral tube to generate steam for continuous processing.
It improves the uniformity of material heating, reduces energy consumption and operating costs, enhances separation and production efficiency, and reduces waiting time between batches.
Smart Images
Figure CN223668681U_ABST
Abstract
Description
Technical Field
[0001] This utility model belongs to the technical field of distillation and purification equipment, and in particular relates to a continuous distillation and purification equipment. Background Technology
[0002] Distillation is a separation process that uses the different volatility of components in a mixture to separate the components. Evaporative distillation apparatus is a widely used sample separation and purification instrument in the laboratory. It achieves the separation and purification of products through processes such as solvent evaporation and concentration of trace components.
[0003] In existing distillation purification devices, the heating material is usually heated directly by the heater. Due to the lack of a stirring mechanism, the material entering the distillation device is easily heated unevenly. In order to compensate for the decrease in separation efficiency caused by this uneven heating, it is necessary to increase the heating power and extend the heating time, thereby increasing energy consumption. Utility Model Content
[0004] The purpose of this invention is to provide a continuous distillation purification device. By setting up an installation mechanism, it solves the problem that, in conventional methods, the distillation material is directly heated by a heater. Due to the lack of a stirring mechanism, this often leads to uneven heating of the material entering the distillation device. To compensate for the decrease in separation efficiency caused by this uneven heating, it is necessary to increase the heating power and extend the heating time, thereby increasing energy consumption.
[0005] To solve the above-mentioned technical problems, this utility model is achieved through the following technical solution:
[0006] This utility model relates to a continuous distillation and purification device, comprising a mounting shell, a storage tank fixedly connected to the bottom of the inner wall of the mounting shell, and a mounting mechanism. The mounting mechanism includes a limiting shell fixedly connected to the outer wall of the storage tank, a first motor fixedly connected to the bottom of the inner wall of the limiting shell, a reciprocating screw fixedly connected to the output end of the first motor via a coupling, a sliding shell threaded onto the outer wall of the reciprocating screw, the outer wall of the sliding shell slidably connected to the inner wall of the limiting shell, a second motor fixedly connected to the top of the inner wall of the sliding shell, a rotating shaft fixedly connected to the output end of the second motor via a coupling, the bottom end of the rotating shaft slidingly extending into the interior of the storage tank, a stirring shell fixedly connected to the outer wall of the rotating shaft, a first connecting pipe fixedly connected to the bottom of the storage tank, a first valve fixedly connected to the outer wall of the first connecting pipe, and an inlet pipe fixedly connected to the top of the storage tank, with a cover hinged to the top end of the inlet pipe.
[0007] Furthermore, a connecting mechanism is provided on the top of the storage bin, the connecting mechanism including a fixed pipe that is connected to and fixedly connected to the top of the storage bin, and a second connecting pipe that is connected to and fixedly connected to the outer wall of the fixed pipe.
[0008] Further, the front side of the mounting shell is fixedly connected with a first rectifying head, the other end of the second connecting pipe is in communication with the outer wall of the first rectifying head and is fixedly connected, and the front side of the mounting shell is fixedly connected with two material storage shells.
[0009] Further, the bottom of each of the two material storage shells is in communication with and fixedly connected with a third connecting pipe, and the outer wall of each of the two third connecting pipes is fixedly connected with a second valve.
[0010] Further, the front side of the mounting shell is fixedly connected with a second rectifying head, one end of the second rectifying head is in communication with and fixedly connected with the top of the left material storage shell.
[0011] Further, the other end of the second rectifying head is in communication with and fixedly connected with the top of the right material storage shell, and the bottom end of the first rectifying head is in communication with and fixedly connected with a fourth connecting pipe.
[0012] Further, the other end of the fourth connecting pipe is in communication with and fixedly connected with the top of the left material storage shell, and the inner wall of the left material storage shell is fixedly connected with a second electric heater.
[0013] Further, the outer wall of the second electric heater is fixedly connected with a spiral pipe, and the other end of the fourth connecting pipe extends into the inside of the spiral pipe.
[0014] The utility model has the advantages of the following beneficial effects:
[0015] 1. By setting up the mounting mechanism, the material is heated by starting two first electric heaters, then the material is stirred by starting the second motor to drive the rotating shaft and the stirring shell to rotate, then the reciprocating screw rod is driven to rotate by starting the first motor, the reciprocating screw rod drives the sliding shell and the second motor and the rotating shaft and the stirring shell to move up and down reciprocatingly, so that the stirring shell rotates and stirs the material while moving up and down, so that the material is evenly heated, the above operation makes the material improve the heating uniformity, can carry out rectification processing to the material without increasing the heating power and prolonging the heating time, which helps to reduce the energy consumption and operation cost, and the material is heated more evenly, the mass transfer and heat transfer efficiency in the rectification process will be improved, and the overall separation efficiency will be improved.
[0016] 2. By setting the connecting mechanism, by starting the second electric heater to heat the spiral pipe, then by the installation mechanism to heat the material, the steam generated by heating enters the inside of the first rectification head through the fixed pipe and the second connecting pipe to condense into water droplets, the condensed water droplets slide on the inner wall of the spiral pipe in the inside of the left storage shell and evaporate, the evaporated steam enters the inside of the second rectification head to condense into water droplets and then enters the inside of the right storage shell for storage, through the above operation, the material can be continuously rectified, this continuous processing method improves the production efficiency, reduces the waiting time between batch processing, thereby improving the overall production efficiency.
[0017] Of course, it is not necessary for any product implementing the present application to achieve all the advantages mentioned above at the same time. BRIEF DESCRIPTION OF DRAWINGS
[0018] In order to more clearly illustrate the technical scheme of the embodiments of the present application, the following will briefly introduce the drawings needed to be used in the embodiment description. Obviously, the drawings in the following description are only some embodiments of the present application, and other drawings can also be obtained by those skilled in the art without creative labor.
[0019] Figure 1 It is a schematic diagram of the overall structure of the present application;
[0020] Figure 2 It is a schematic diagram of the overall partial cross-sectional structure of the present application;
[0021] Figure 3 It is a schematic diagram of the installation mechanism structure of the present application;
[0022] Figure 4 It is a schematic diagram of the connecting mechanism structure of the present application;
[0023] Figure 5 It is Figure 4 It is an enlarged structure schematic diagram of A in the middle.
[0024] In the drawings, the component list represented by each number is as follows:
[0025] 1, installation shell; 11, storage barrel; 2, installation mechanism; 21, limiting shell; 22, first motor; 23, reciprocating screw; 24, sliding shell; 25, second motor; 26, rotating shaft; 27, stirring shell; 28, first electric heater; 29, first connecting pipe; 210, first valve; 211, feeding pipe; 212, cover shell; 3, connecting mechanism; 31, fixed pipe; 32, second connecting pipe; 33, first rectification head; 34, storage shell; 35, third connecting pipe; 36, second valve; 37, second rectification head; 38, fourth connecting pipe; 39, second electric heater; 310, spiral pipe. DETAILED DESCRIPTION
[0026] The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments in the present application, all other embodiments obtained by those skilled in the art without creative labor fall within the scope of protection of the present application.
[0027] Please refer to Figures 1-5 As shown in the drawings, the present application is a continuous rectification purification device, which comprises a mounting shell 1, the inner wall bottom of the mounting shell 1 is fixedly connected with a material storage barrel 11, and further comprises;
[0028] The mounting mechanism 2 comprises a limiting shell 21 fixedly connected to the outer wall of the storage barrel 11, the inner wall bottom of the limiting shell 21 is fixedly connected with a first motor 22, the output end of the first motor 22 is fixedly connected with a reciprocating lead screw 23 through a shaft coupling, the outer wall of the reciprocating lead screw 23 is threadedly sleeved with a sliding shell 24, the outer wall of the sliding shell 24 is slidably connected with the inner wall of the limiting shell 21, the inner wall top of the sliding shell 24 is fixedly connected with a second motor 25, the output end of the second motor 25 is fixedly connected with a rotating shaft 26 through a shaft coupling, the bottom end of the rotating shaft 26 slides and extends into the interior of the storage barrel 11, the outer wall of the rotating shaft 26 is fixedly connected with a stirring shell 27, the bottom of the storage barrel 11 is communicated and fixedly connected with a first connecting pipe 29, the outer wall of the first connecting pipe 29 is fixedly connected with a first valve 210, the top of the storage barrel 11 is communicated and fixedly connected with a feeding pipe 211, the top end of the feeding pipe 211 is hingedly connected with a cover shell 212, the material is poured into the interior of the storage barrel 11 through the feeding pipe 211 by opening the cover shell 212, then the two first electric heaters 28 are started to heat the material, then the second motor 25 is started, the second motor 25 drives the rotating shaft 26 and the stirring shell 27 to rotate to stir the material, then the first motor 22 is started, the first motor 22 drives the reciprocating lead screw 23 to rotate, the reciprocating lead screw 23 drives the sliding shell 24 and the second motor 25 and the rotating shaft 26 and the stirring shell 27 to move up and down reciprocatingly in the interior of the storage barrel 11, so that the stirring shell 27 rotates to stir the material while moving up and down, so that the material is evenly heated, the two first electric heaters 28 are started to heat the material, then the second motor 25 is started to drive the rotating shaft 26 and the stirring shell 27 to rotate to stir the material, then the first motor 22 is started to drive the reciprocating lead screw 23 to rotate, the reciprocating lead screw 23 drives the sliding shell 24 and the second motor 25 and the rotating shaft 26 and the stirring shell 27 to move up and down reciprocatingly, so that the stirring shell 27 rotates to stir the material while moving up and down, so that the material is evenly heated, the above operation can improve the heating uniformity of the material, can rectify the material without increasing the heating power and prolonging the heating time, which helps to reduce the energy consumption and operation cost, and the material is heated more evenly, the mass transfer and heat transfer efficiency in the rectification process is improved, thereby improving the overall separation efficiency, the unprocessed material needs to be taken out, the first valve 210 is opened, and the material flows out through the first connecting pipe 29.
[0029] The top of the storage barrel 11 is provided with a connecting mechanism 3, the connecting mechanism 3 comprises a fixed pipe 31 communicated and fixedly connected to the top of the storage barrel 11, the outer wall of the fixed pipe 31 is communicated and fixedly connected with a second connecting pipe 32, the second electric heater 39 is started to heat the spiral pipe 310, then the material is heated by the mounting mechanism 2, the steam generated by heating enters the interior of the first rectification head 33 through the fixed pipe 31 and the second connecting pipe 32 to condense into water droplets.
[0030] The front side of the installation shell 1 is fixedly connected with a first rectifying head 33, the other end of the second connecting pipe 32 is in communication with the outer wall of the first rectifying head 33 and is fixedly connected, the front side of the installation shell 1 is fixedly connected with two material storage shells 34, the condensed water beads slide on the inner wall of the spiral pipe 310 in the left material storage shell 34 and evaporate, the evaporated steam enters the inside of the second rectifying head 37 and condenses into water beads and then enters the inside of the right material storage shell 34 for storage.
[0031] The bottom of each of the two material storage shells 34 is in communication with and fixedly connected with a third connecting pipe 35, the outer wall of each of the two third connecting pipes 35 is fixedly connected with a second valve 36, and the preliminary processed material and the processed material are collected by flowing out of the third connecting pipe 35 by opening the second valve 36 respectively.
[0032] The front side of the installation shell 1 is fixedly connected with a second rectifying head 37, one end of the second rectifying head 37 is in communication with and fixedly connected with the top of the left material storage shell 34, the evaporated steam enters the inside of the second rectifying head 37 and condenses into water beads and then enters the inside of the right material storage shell 34 for storage.
[0033] The other end of the second rectifying head 37 is in communication with and fixedly connected with the top of the right material storage shell 34, the bottom end of the first rectifying head 33 is in communication with and fixedly connected with a fourth connecting pipe 38, the condensed water beads slide on the inner wall of the spiral pipe 310 in the left material storage shell 34 and evaporate by entering the fourth connecting pipe 38.
[0034] The other end of the fourth connecting pipe 38 is in communication with and fixedly connected with the top of the left material storage shell 34, a second electric heater 39 is fixedly connected with the inner wall of the left material storage shell 34, the spiral pipe 310 is heated by starting the second electric heater 39, the condensed water beads slide on the inner wall of the spiral pipe 310 in the left material storage shell 34 and evaporate by entering the fourth connecting pipe 38, the evaporated steam enters the inside of the second rectifying head 37 and condenses into water beads and then enters the inside of the right material storage shell 34 for storage.
[0035] The outer wall of the second electric heater 39 is fixedly connected with a spiral pipe 310, the other end of the fourth connecting pipe 38 extends to the inside of the spiral pipe 310, the spiral pipe 310 is heated by starting the second electric heater 39, then the material is heated by the mounting mechanism 2, the steam generated by heating enters the inside of the first rectifying head 33 through the fixed pipe 31 and the second connecting pipe 32 to condense into water droplets, the water droplets condense into the inside of the spiral pipe 310 of the left storage shell 34 through the fourth connecting pipe 38 and slide on the inner wall of the spiral pipe 310 and evaporate, the evaporated steam enters the inside of the second rectifying head 37 to condense into water droplets and then enters the inside of the right storage shell 34 for storage, through the above operation, the material can be continuously rectified and processed, this continuous processing method improves the production efficiency and reduces the waiting time between batch processing, thereby improving the overall production efficiency.
[0036] One specific application of the embodiment is: the first electric heater 28, in the continuous rectification and purification device, the electric heater is a key component, its main role is to provide heat to make the rectification material begin to vaporize, the electric heater is a device that converts electrical energy into heat energy, usually composed of resistance wire or heating pipe and other elements. In the continuous rectification and purification device, the electric heater is mainly used for heating the liquid mixture to make it reach the boiling state, so as to generate steam.
[0037] When using the device, open the cover shell 212 to pour the material into the inside of the storage barrel 11 through the feeding pipe 211, then start the two first electric heaters 28 to heat the material, then start the second motor 25, the second motor 25 drives the rotating shaft 26 and the stirring shell 27 to rotate, and the material is stirred, then start the first motor 22, the first motor 22 drives the reciprocating lead screw 23 to rotate, the reciprocating lead screw 23 drives the sliding shell 24 and the second motor 25 and the rotating shaft 26 and the stirring shell 27 to move up and down in the storage barrel 11, so that the stirring shell 27 rotates to stir the material while moving up and down, so that the material is evenly heated, the two first electric heaters 28 are started to heat the material, then the second motor 25 is started to drive the rotating shaft 26 and the stirring shell 27 to rotate, and the material is stirred, then the first motor 22 is started to drive the reciprocating lead screw 23 to rotate, the reciprocating lead screw 23 drives the sliding shell 24 and the second motor 25 and the rotating shaft 26 and the stirring shell 27 to move up and down, so that the stirring shell 27 rotates to stir the material while moving up and down, so that the material is evenly heated, through the above operation, the material improves the uniformity of heating, which can be rectified and processed without increasing the heating power and prolonging the heating time, which helps to reduce energy consumption and operating cost, and the material is heated more evenly, the mass transfer and heat transfer efficiency in the rectification process will be improved, thereby improving the overall separation efficiency.
[0038] When the device is used, the second electric heater 39 is started to heat the spiral pipe 310, then the material is heated between the installation mechanism 2, the steam generated by heating enters the inside of the first rectifying head 33 through the fixed pipe 31 and the second connecting pipe 32 to condense into water droplets, the water droplets condensing through the fourth connecting pipe 38 slide on the inner wall of the spiral pipe 310 in the inside of the left storage shell 34 and evaporate, the evaporated steam enters the inside of the second rectifying head 37 to condense into water droplets and then enters the inside of the right storage shell 34 for storage, so that the material can be continuously rectified, and through the above operation, the material can be continuously rectified, and the continuous processing mode improves the production efficiency and reduces the waiting time between batch processing, thereby improving the overall production efficiency.
[0039] In the description of the present specification, the description referring to the terms "one embodiment", "an example", "a specific example" and the like means that the specific features, structures, materials or characteristics described in connection with the embodiment or example are contained in at least one embodiment or example of the present application. In the present specification, the illustrative description of the above terms does not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.
[0040] The preferred embodiments of the above disclosed application are only used to help explain the application. The preferred embodiments do not describe all the details, nor limit the application to the specific embodiments described. Obviously, according to the content of the present specification, many modifications and changes can be made. The present specification selects and specifically describes these embodiments in order to better explain the principles and practical applications of the application, so that those skilled in the art can well understand and utilize the application. The application is limited by the claims and their entire scope and equivalents.
Claims
1. A continuous rectification purification device, comprising a mounting shell (1), the inner wall bottom of the mounting shell (1) is fixedly connected with a storage barrel (11), characterized in that: Also includes; The installation mechanism (2) includes a limiting shell (21) fixedly connected to the outer wall of the storage barrel (11), the inner wall bottom of the limiting shell (21) is fixedly connected with a first motor (22), the output end of the first motor (22) is fixedly connected with a reciprocating lead screw (23) through a shaft coupling, the outer wall of the reciprocating lead screw (23) is threadedly sleeved with a sliding shell (24), the outer wall of the sliding shell (24) is slidingly connected with the inner wall of the limiting shell (21), the inner wall top of the sliding shell (24) is fixedly connected with a second motor (25), the output end of the second motor (25) is fixedly connected with a rotating shaft (26) through a shaft coupling, the bottom end of the rotating shaft (26) slidingly extends to the inside of the storage barrel (11), the outer wall of the rotating shaft (26) is fixedly connected with a stirring shell (27), the bottom of the storage barrel (11) is communicated and fixedly connected with a first connecting pipe (29), the outer wall of the first connecting pipe (29) is fixedly connected with a first valve (210), the top of the storage barrel (11) is communicated and fixedly connected with a feeding pipe (211), the top end of the feeding pipe (211) is hingedly connected with a cover shell (212).
2. A continuous rectification purification apparatus according to claim 1, wherein, The top of the storage barrel (11) is provided with a connecting mechanism (3), the connecting mechanism (3) includes a fixed pipe (31) communicated and fixedly connected to the top of the storage barrel (11), and the outer wall of the fixed pipe (31) is communicated and fixedly connected with a second connecting pipe (32).
3. A continuous rectification purification apparatus according to claim 2, wherein, The front side of the mounting shell (1) is fixedly connected with a first rectifying head (33), the other end of the second connecting pipe (32) is communicated and fixedly connected with the outer wall of the first rectifying head (33), and the front side of the mounting shell (1) is fixedly connected with two storage shells (34).
4. A continuous rectification purification apparatus according to claim 3, wherein, The bottom of each of the two storage shells (34) is communicated and fixedly connected with a third connecting pipe (35), and the outer wall of each of the two third connecting pipes (35) is fixedly connected with a second valve (36).
5. A continuous rectification purification apparatus according to claim 4, wherein, The front side of the mounting shell (1) is fixedly connected with a second rectifying head (37), one end of the second rectifying head (37) is communicated and fixedly connected with the top of the left storage shell (34).
6. A continuous rectification purification apparatus according to claim 5, wherein, The other end of the second rectifying head (37) is communicated and fixedly connected with the top of the right storage shell (34), and the bottom end of the first rectifying head (33) is communicated and fixedly connected with a fourth connecting pipe (38).
7. A continuous rectification purification apparatus according to claim 6, wherein The other end of the fourth connecting pipe (38) is communicated and fixedly connected with the top of the left storage shell (34), and the inner wall of the left storage shell (34) is fixedly connected with a second electric heater (39).
8. A continuous rectification purification apparatus according to claim 7, wherein, The outer wall of the second electric heater (39) is fixedly connected with a spiral pipe (310), and the other end of the fourth connecting pipe (38) extends to the inside of the spiral pipe (310).