Preparation equipment of sodium hydroxamic acid

By combining a screw feeder and a stirring motor, the initial mixing and subsequent full reaction of materials in the sodium hydroxamate preparation equipment are achieved, solving the problems of long mixing time and uneven mixing in existing equipment, and improving the reaction rate and preparation effect.

CN223761026UActive Publication Date: 2026-01-06河南德峰新材料有限公司
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Patent Information

Application Number
CN202520044131.3
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-01-08
Publication Date
2026-01-06
Estimated Expiration
2035-01-08

AI Technical Summary

Technical Problem

Existing sodium hydroxamate preparation equipment is time-consuming during material addition and mixing, resulting in limited reaction rates and uneven mixing, which affects the preparation effect.

Method used

Materials are transported using a screw feeder and a conveying pump. The screw blades are used for initial mixing, and the mixture is further stirred and heated by a stirring motor and an electric heater, so as to achieve initial mixing and subsequent full reaction of the materials during the conveying process.

Benefits of technology

It improves the efficiency and uniformity of material mixing, shortens the mixing time, and enhances the reaction rate and preparation effect.

✦ Generated by Eureka AI based on patent content.

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    Figure CN223761026U_ABST
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Abstract

The utility model relates to the technical field of mineral smelting material preparation equipment, in particular to sodium hydroxamic acid preparation equipment which comprises a preparation cylinder, an inclined pipe is fixedly mounted on a top cylinder body of the preparation cylinder, a vertical cylinder is fixedly mounted at the top end of the inclined pipe, and a spiral mixing ring is fixedly mounted on the inner wall of the vertical cylinder. The spiral mixing ring is composed of a plurality of spiral blades, a spiral feeder is arranged on one side of the vertical cylinder, a discharging pipe is fixedly installed at the discharging end of the spiral feeder, the end of the discharging pipe is fixedly installed at the top of the vertical cylinder, a conveying pump is arranged on one side of the vertical cylinder, and a liquid outlet pipe is fixedly installed at the liquid outlet end of the conveying pump. The liquid outlet pipe is fixedly mounted on the top cylinder body of the vertical cylinder, a stirring motor is fixedly mounted in the center of the upper surface of the top cover, a long shaft is fixedly mounted at the tail end of an output shaft of the stirring motor, and stirring blades are fixedly mounted on the long shaft. According to the utility model, full mixing preparation operation is facilitated, and the preparation speed is increased.
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Description

Technical Field

[0001] This utility model relates to the technical field of mineral smelting material preparation equipment, and more specifically, to a preparation equipment for sodium hydroxamate. Background Technology

[0002] Sodium hydroxamate, as an important mineral smelting material, is widely used in the field of mineral processing, especially in the collection of metal oxides, where it exhibits excellent performance. The preparation method of sodium hydroxamate usually involves the hydroxamication reaction of salicylates and hydroxylamine sulfate under specific conditions, followed by solid-liquid separation to obtain the target product.

[0003] The preparation of sodium hydroxamate is usually carried out in a corresponding preparation equipment. There are many types of sodium hydroxamate preparation equipment on the market. Most of these preparation equipment first transports the material to the corresponding mixing equipment through corresponding pipelines or conveying components, and then the raw materials are mixed by the rotation of the stirring blades to achieve the effect of mixing and preparation reaction.

[0004] However, when using this type of equipment, it takes time to add a certain amount of material to the preparation equipment. When multiple materials are added sequentially to their respective devices and then mixed, a considerable amount of time is required. Furthermore, to ensure thorough and uniform mixing, a prolonged mixing time is necessary. This design lacks the ability to pre-mix multiple raw materials during material transport, which to some extent limits the reaction rate and may lead to uneven mixing, affecting the preparation effect. Therefore, we propose a preparation device for sodium hydroxamic acid. Utility Model Content

[0005] The purpose of this invention is to provide a preparation apparatus for sodium hydroxamate, so as to solve the defects mentioned in the background art.

[0006] To achieve the above objectives, this utility model provides the following technical solution:

[0007] A preparation apparatus for sodium hydroxamic acid includes a preparation cylinder. An inclined tube is fixedly installed on the top of the preparation cylinder. A vertical cylinder is fixedly installed at the top end of the inclined tube. A spiral mixing ring is fixedly installed on the inner wall of the vertical cylinder. The spiral mixing ring is composed of multiple vertically arranged spiral blades. The spiral blades are spiral-shaped. A spiral feeder is provided on one side of the vertical cylinder. A vertically downward discharge pipe is fixedly installed at the discharge end of the spiral feeder. The end of the discharge pipe is fixedly installed at the top of the vertical cylinder. A transfer pump is provided on one side of the vertical cylinder. A suction pipe is fixedly installed at the inlet end of the transfer pump. A discharge pipe is fixedly installed at the outlet end of the transfer pump. The discharge pipe is fixedly installed on the top of the vertical cylinder.

[0008] Preferably, the liquid outlet pipe is located below the material outlet pipe, and the distance between the top end of the spiral mixing ring and the top wall of the vertical cylinder is greater than 10cm.

[0009] Preferably, a conical hopper is fixedly installed at the bottom of the preparation cylinder, a discharge pipe is fixedly installed at the bottom end of the conical hopper, and a discharge valve is fixedly installed on the discharge pipe.

[0010] Preferably, the plane containing the inner wall of the conical hopper is inclined downward at 45° to 60°, and an electric heater is fixedly installed on the cylinder of the preparation cylinder.

[0011] Preferably, a top cover is fixedly installed on the top surface of the preparation cylinder, a stirring motor is fixedly installed at the center of the upper surface of the top cover, a long shaft is fixedly installed at the end of the output shaft of the stirring motor, and stirring blades are fixedly installed on the long shaft.

[0012] Preferably, the upper half of the stirring blade is located inside the preparation cylinder, and the lower half of the stirring blade is located inside the conical hopper.

[0013] Preferably, an exhaust pipe is fixedly installed on the top cover, and an exhaust valve is fixedly installed on the exhaust pipe.

[0014] Preferably, the inclined tube is inclined upward at 45° to 75°, and the vertical cylinder is vertical.

[0015] Compared with the prior art, the beneficial effects of this utility model are:

[0016] 1. This utility model uses a spiral feeder and a conveying pump to transport materials. As the materials are transported into the vertical cylinder, the fluidity of the liquid materials enables the materials to undergo preliminary mixing under the action of the spiral blades. The mixed materials are then transported into the preparation cylinder for subsequent processing, achieving the effect of preliminary mixing of materials during the material transport process.

[0017] 2. This utility model uses a stirring motor to drive the long shaft and stirring blades to rotate, enabling further stirring and mixing operations. It also uses an electric heater for heating and a discharge pipe for discharging. Attached Figure Description

[0018] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0019] Figure 2 This is a schematic diagram of the exploded structure of this utility model;

[0020] Figure 3This is one of the partial structural schematic diagrams of this utility model;

[0021] Figure 4 This is the second partial structural schematic diagram of the present utility model;

[0022] Figure 5 This is the third partial structural schematic diagram of this utility model;

[0023] The meanings of the labels in the diagram are as follows:

[0024] 1. Preparation cylinder; 10. Conical hopper; 11. Discharge pipe; 12. Discharge valve; 13. Electric heater; 14. Top cover; 15. Inclined pipe; 16. Exhaust pipe; 161. Exhaust valve;

[0025] 2. Stirring motor; 20. Long shaft; 21. Stirring blades;

[0026] 3. Vertical cylinder; 30. Spiral mixing ring; 301. Spiral blade; 31. Spiral feeder; 32. Discharge pipe; 33. Conveying pump; 34. Suction pipe; 35. Liquid outlet pipe. Detailed Implementation

[0027] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0028] Please see Figures 1-5 This utility model provides a technical solution: a preparation device for sodium hydroxamic acid, including a preparation cylinder 1, an inclined tube 15 is fixedly installed on the top cylinder of the preparation cylinder 1, and a vertical cylinder 3 is fixedly installed on the top end of the inclined tube 15. The inclined tube 15 is set at an upward inclination of 45° to 75°, and the vertical cylinder 3 is set vertically, so that the material enters the preparation cylinder 1 more smoothly along the vertical cylinder 3 and the inclined tube 15.

[0029] Specifically, a spiral mixing ring 30 is fixedly installed on the inner wall of the vertical cylinder 3. The spiral mixing ring 30 is composed of multiple vertically arranged spiral blades 301. The spiral blades 301 are spiral in shape and are used for the flow mixing operation between liquids and between liquids and particulate solids during liquid flow.

[0030] Specifically, a screw feeder 31 is installed on one side of the vertical cylinder 3. A vertically downward-oriented discharge pipe 32 is fixedly installed at the discharge end of the screw feeder 31. The end of the discharge pipe 32 is fixedly installed at the top of the vertical cylinder 3 for feeding solid particles from the top. A conveying pump 33 is installed on one side of the vertical cylinder 3. A suction pipe 34 is fixedly installed at the inlet end of the conveying pump 33. A discharge pipe 35 is fixedly installed at the outlet end of the conveying pump 33. The discharge pipe 35 is fixedly installed on the top cylinder of the vertical cylinder 3 and is located below the discharge pipe 32. The distance between the top of the spiral mixing ring 30 and the top wall of the vertical cylinder 3 is greater than 10cm, so that the material can fall down to the spiral blade 301 for mixing. At the same time, it also ensures that the flow of liquid can more thoroughly rinse the spiral mixing ring 30.

[0031] In this embodiment, a conical hopper 10 is fixedly installed at the bottom of the preparation cylinder 1, and a discharge pipe 11 is fixedly installed at the bottom end of the conical hopper 10. A discharge valve 12 is fixedly installed on the discharge pipe 11 to facilitate the discharge operation.

[0032] Specifically, the inner wall of the conical hopper 10 is inclined downward at 45° to 60°, which makes the unloading operation in the conical hopper 10 smoother; an electric heater 13 is fixedly installed on the cylinder of the preparation cylinder 1, and the electric heater 13 is used for heating operation.

[0033] Furthermore, a top cover 14 is fixedly installed on the top surface of the preparation cylinder 1, and a stirring motor 2 is fixedly installed at the center of the upper surface of the top cover 14. A long shaft 20 is fixedly installed at the end of the output shaft of the stirring motor 2, and stirring blades 21 are fixedly installed on the long shaft 20. The upper half of the stirring blade 21 is located inside the preparation cylinder 1, and the lower half of the stirring blade 21 is located inside the conical hopper 10, so as to realize further stirring operation.

[0034] In addition, an exhaust pipe 16 is fixedly installed on the top cover 14, and an exhaust valve 161 is fixedly installed on the exhaust pipe 16 to realize the exhaust operation.

[0035] When using the sodium hydroxamate preparation equipment of this utility model, the discharge valve 12 is closed, the screw feeder 31 is started to transport the solid particles into the vertical cylinder 3, the suction pipe 34 is connected to the liquid delivery pipeline, and the delivery pump 33 is started to transport the liquid into the vertical cylinder 3. Due to the fluidity of the liquid, under the action of the spiral blades 301, the liquid can be initially mixed with the solid particle raw material during the flow process. The mixed material enters the preparation cylinder 1. At this time, the electric heater 13 is connected to the external power supply and put into operation. The electric heater 13 is working to perform the heating operation. The stirring motor 2 is connected to the external power supply and put into operation. The stirring motor 2 is working, and its output shaft rotates to drive the long shaft 20 and the stirring blades 21 to rotate, so as to carry out further mixing and preparation operations. After the reaction preparation is completed, the discharge valve 12 is opened to perform the discharge operation.

[0036] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely preferred examples and are not intended to limit the utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claimed utility model. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. An apparatus for the preparation of sodium hydroxamic acid, comprising a preparation cylinder (1), characterized in that: The top of the preparation cylinder (1) is fixedly installed with an inclined pipe (15), the top end of the inclined pipe (15) is fixedly installed with a vertical cylinder (3), the inner wall of the vertical cylinder (3) is fixedly installed with a spiral mixing ring (30), the spiral mixing ring (30) is composed of a plurality of vertical spiral blades (301), the spiral blades (301) are spiral, one side of the vertical cylinder (3) is provided with a spiral feeder (31), the discharge end of the spiral feeder (31) is fixedly installed with a discharge pipe (32) arranged vertically downward, the end of the discharge pipe (32) is fixedly installed at the top of the vertical cylinder (3), one side of the vertical cylinder (3) is provided with a conveying pump (33), the liquid inlet end of the conveying pump (33) is fixedly installed with a suction pipe (34), the liquid outlet end of the conveying pump (33) is fixedly installed with a liquid outlet pipe (35), and the liquid outlet pipe (35) is fixedly installed on the top of the vertical cylinder (3).

2. The apparatus for preparing sodium hydroxamic acid according to claim 1, characterized by: The liquid outlet pipe (35) is located below the discharge pipe (32), and the distance between the top end of the spiral mixing ring (30) and the top wall of the vertical cylinder (3) is greater than 10 cm.

3. The apparatus for preparing sodium hydroxamic acid according to claim 1, characterized by: The bottom of the preparation cylinder (1) is fixedly installed with a conical hopper (10), the bottom end of the conical hopper (10) is fixedly installed with a discharge pipe (11), and the discharge pipe (11) is fixedly installed with a discharge valve (12).

4. The apparatus for preparing sodium hydroxamic acid according to claim 3, characterized by: The inner wall of the conical hopper (10) is arranged at an angle of 45°-60° downward, and an electric heater (13) is fixedly installed on the cylinder body of the preparation cylinder (1).

5. The apparatus for preparing sodium hydroxamic acid according to claim 3, characterized by: The top surface of the preparation cylinder (1) is fixedly installed with a top cover (14), the upper surface of the top cover (14) is fixedly installed with a stirring motor (2) at the center position, the output shaft end of the stirring motor (2) is fixedly installed with a long shaft (20), and the long shaft (20) is fixedly installed with stirring blades (21).

6. The apparatus for preparing sodium hydroxamic acid according to claim 5, characterized by: The upper half of the stirring blades (21) is located in the preparation cylinder (1), and the lower half of the stirring blades (21) is located in the conical hopper (10).

7. The apparatus for preparing sodium hydroxamic acid according to claim 5, characterized by: The top cover (14) is fixedly installed with an exhaust pipe (16), and the exhaust pipe (16) is fixedly installed with an exhaust valve (161).

8. The apparatus for preparing sodium hydroxamic acid according to claim 1, characterized by: The inclined pipe (15) is arranged at an angle of 45°-75° upward, and the vertical cylinder (3) is arranged vertically.