Reaction system suitable for vacuum insulation

Abstract

A reaction system suitable for vacuum heat insulation comprises a reactor and a pump body, the reactor is arranged in a box body, a vacuum extraction opening is formed in the box body, and the pump body is connected with the vacuum extraction opening to vacuumize the box body. The reactor is in a vacuum adiabatic environment, and the problem of inaccurate experimental data caused by air heat transfer is solved.

Description

Technical Field

[0001] This patent relates to the field of chemical equipment, specifically to a reaction system suitable for vacuum insulation. Background Technology

[0002] Microchannel reactors, as an advanced reaction device, have been applied in many industrial scenarios. Research on microchannels themselves and their application in scientific research and applied experiments have also been carried out. However, the current problem is that when conducting heat transfer-related research on microchannel reactors, the reactor itself will lose heat to the outside, resulting in inaccurate experimental data. Utility Model Content

[0003] In view of the problems in the background art, the present invention provides a reaction system suitable for vacuum insulation, including a reactor and a pump body. The reactor is set in a box, and the box body is provided with a vacuum extraction port. The pump body is connected to the vacuum extraction port to realize the vacuuming of the box body.

[0004] In one embodiment, the reactor is installed on the inner wall of the tank, and the connection is made of an insulating material, such as aerogel felt.

[0005] In one embodiment, a cover that can be opened and closed is provided on one side of the box body. One side of the cover is hinged to the box body by a hinge, which is selected from a combination of a hinge or a bearing and a pin. A handle is provided on the other side of the cover. On the box body, the side where the handle is located is opposite to the side where the hinge is located.

[0006] As one implementation, a sealing strip is provided at the contact position between the lid and the box body to enhance the sealing performance of the box body when the lid is closed.

[0007] As one implementation, the lid can be made of a transparent material to facilitate observation of the sides of the internal reactor.

[0008] In one embodiment, an air purge valve and / or a back pressure valve are provided on the other side of the housing.

[0009] As one implementation, the other side of the housing is made of transparent material to facilitate observation of the front of the internal reactor.

[0010] As one implementation, a display screen is also included, which is disposed on the top of the outer side of the housing.

[0011] In one implementation, the display screen is located on the same side as the purge valve and / or back pressure valve.

[0012] In one embodiment, the housing is provided with a material inlet, a material outlet, a heat exchange medium inlet, and a heat exchange medium outlet. The reactor is connected to the material inlet, material outlet, heat exchange medium inlet, and heat exchange medium outlet of the housing via a pipeline. Temperature sensors are provided at each of the material inlet, material outlet, heat exchange medium inlet, and heat exchange medium outlet for temperature measurement. Alternatively, the housing is made of heat-insulating material.

[0013] Beneficial effects:

[0014] 1. The reaction system provided by this utility model sets the microchannel reactor inside the chamber, and the chamber can be vacuumed during the experiment to block heat transfer. This reduces external interference and accurately obtains experimental data when conducting research on heat transfer in microreactors.

[0015] 2. This utility model allows for convenient disassembly and installation of the reactor by providing an openable and closable side wall for the housing.

[0016] 3. The side wall of the box of this utility model is made of transparent material, which can realize the real-time understanding of the reaction status of the internal reactor and deal with abnormalities in a timely manner.

[0017] 4. In order to prevent the reactor from contacting the tank and transferring heat to the tank, which would affect the experimental research, this utility model provides heat insulation material at the connection between the reactor and the tank to reduce heat transfer. Attached Figure Description

[0018] To more clearly illustrate the specific embodiments of this utility model or the technical solutions in the prior art, the drawings used in the description of the specific embodiments or the prior art will be briefly introduced below. Obviously, the drawings described below are some embodiments of this utility model. For those skilled in the art, other drawings can be obtained from these drawings without creative effort.

[0019] Figure 1 This is a schematic diagram of the reaction system of this utility model;

[0020] Figure 2 yes Figure 1 Enlarged view of point A in the middle.

[0021] Explanation of reference numerals in the attached figures:

[0022] 1. Reactor; 2. Pump body; 3. Housing; 4. Vacuum extraction port; 5. Cover; 6. Hinge; 7. Handle; 8. Purge valve; 9. Back pressure valve; 10. Display screen; 11. Material inlet; 12. Material outlet; 13. Heat exchange medium inlet; 14. Heat exchange medium outlet. Detailed Implementation

[0023] The technical solution of this utility model will now be clearly and completely described with reference to the accompanying drawings. Obviously, the described embodiments are only some, not all, of the embodiments of this utility model. Based on the embodiments of this utility model, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this utility model.

[0024] In the description of this utility model, it should be noted that the terms "upper," "lower," "left," "right," "inner," and "outer," etc., indicating the orientation or positional relationship, are based on the orientation or positional relationship shown in the accompanying drawings and are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and should not be construed as indicating or implying relative importance.

[0025] Furthermore, the technical features involved in the different embodiments of this utility model described below can be combined with each other as long as they do not conflict with each other.

[0026] The present invention will be further described below with reference to the accompanying drawings and embodiments.

[0027] Please refer to Figures 1-2 This utility model provides a reaction system suitable for vacuum insulation, and the preferred embodiment is as follows:

[0028] Example 1: A vacuum-insulated reaction system includes a reactor 1 and a pump 2. The reactor 1 is housed within a housing 3. The housing 3 has a vacuum extraction port 4. The pump 2 is connected to the vacuum extraction port 4 to evacuate the housing 3. One side of the housing 3 has a lid 5 that can be opened and closed. One side of the lid 5 is hinged to the housing 3 via a hinge. The other side of the lid 5 has a handle 7. The side of the handle 7 on the housing 3 is opposite to the side of the hinge 6. The lid 5 can be opened or closed using the handle 7. To achieve a seal, a sealing strip is provided at the contact point between the lid 5 and the housing 3, enhancing the sealing performance of the housing 3 when the lid 5 is closed. To facilitate observation of the internal reactor 1, the other side of the housing 3 and the lid 5 can be made of transparent material. The system is equipped with a material inlet 11, a material outlet 12, a heat exchange medium inlet 13, and a heat exchange medium outlet 14, all connected to reactor 1 via pipelines. Temperature sensors are installed at each of these locations to detect the temperature during the experiment, facilitating experimental research. A purge valve 8 and a back pressure valve 9 are located on the other side of the chamber 3. The purge valve 8 is used to clean the channels of reactor 1, while the back pressure valve 9 regulates the pressure required during the reaction. Both the back pressure valve 9 and the purge valve 8 are located on the outside of the chamber 3, a design that is more convenient to use than placing them inside. The reaction system also includes a display screen 10, which is located on the top of the outside of the chamber 3, on the same side as the back pressure valve 9 and the purge valve 8.

[0029] Example 2: The difference from Example 1 is that one side of the cover 5 is hinged to the box body 3 by a bearing and a pin, and the other side of the box body 3 is made of transparent material, with a back pressure valve 9 located below the transparent material.

[0030] Example 3: The difference from Example 2 is that a purge valve 8 is provided under the transparent material on the other side of the box.

[0031] Example 4: The difference from Example 1 is that the material used for the box body 3 is heat insulation material.

[0032] Example 5: The difference from Example 1 is that the reactor 1 is set on the side wall inside the box 3, and the connection between the reactor 1 and the box 3 is made of aerogel felt, which reduces the heat transfer from the reactor 1 to the side wall of the box 3 and thus reduces the impact on the experimental results.

[0033] Operating Procedure: Close the lid 5, then connect the pump body 2 to the vacuum port 4 to create a vacuum inside the chamber 3. Once a vacuum is formed, the material and heat exchange medium enter the reactor 2 through the material inlet 11 and heat exchange medium inlet 13 respectively, and are then discharged through the material outlet 12 and heat exchange medium outlet 14 respectively, thus completing the experiment. During this process, the reactor 2 is in a vacuum state, and heat cannot be transferred through the medium, thus creating an adiabatic environment, reducing the impact on experimental data, and ensuring the accuracy of research results.

[0034] The above description is merely a specific embodiment of this disclosure, enabling those skilled in the art to understand or implement it. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of this disclosure. Therefore, this disclosure is not to be limited to the embodiments described herein, but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A reaction system suitable for vacuum insulation, comprising a reactor (1) and a pump body (2), characterized in that, The reactor (1) is located inside the box (3), and the box (3) is provided with a vacuum extraction port (4). The pump (2) is connected to the vacuum extraction port (4) to realize the vacuum extraction of the box (3).

2. The reaction system suitable for vacuum insulation according to claim 1, characterized in that, The reactor (1) is installed on the inner wall of the box (3), and the connection is made of an insulating material, such as aerogel felt.

3. A reaction system suitable for vacuum insulation according to claim 2, characterized in that, The box (3) has a cover (5) that can be opened and closed on one side. One side of the cover (5) is hinged to the box (3) by a hinge, which is selected from a hinge (6) or a combination of bearing and pin. The other side of the cover (5) is provided with a handle (7). On the box (3), the side where the handle (7) is located is opposite to the side where the hinge is located.

4. A reaction system suitable for vacuum insulation according to claim 3, characterized in that, A sealing strip is provided at the contact position between the cover (5) and the box body (3) to enhance the sealing performance of the box body (3) when the cover (5) is closed.

5. A reaction system suitable for vacuum insulation according to claim 3 or 4, characterized in that, The cover (5) can be made of transparent material to facilitate observation of the side of the internal reactor (1).

6. A reaction system suitable for vacuum insulation according to claim 2, characterized in that, The other side of the housing (3) is provided with an air purge valve (8) and / or a back pressure valve (9).

7. A reaction system suitable for vacuum insulation according to claim 6, characterized in that, The other side of the box (3) is made of transparent material to facilitate observation of the front of the internal reactor (1).

8. A reaction system suitable for vacuum insulation according to claim 7, characterized in that, It also includes a display screen (10), which is located on the top of the outer side of the housing (3).

9. A reaction system suitable for vacuum insulation according to claim 8, characterized in that, The display screen (10) is located on the same side as the purge valve (8) and / or the back pressure valve (9).

10. A reaction system suitable for vacuum insulation according to claim 1, characterized in that, The housing (3) is provided with a material inlet (11), a material outlet (12), a heat exchange medium inlet (13), and a heat exchange medium outlet (14). The reactor (1) is connected to the material inlet (11), material outlet (12), heat exchange medium inlet (13), and heat exchange medium outlet (14) on the housing (3) through a pipeline. Temperature sensors are provided at each of the material inlet (11), material outlet (12), heat exchange medium inlet (13), and heat exchange medium outlet (14) for temperature measurement. Alternatively, the housing (3) is made of heat insulation material.

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