Heating reaction kettle

Abstract

The utility model relates to the technical field of reaction kettles and discloses a heating reaction kettle which comprises a reaction kettle body, an electromagnetic heating mechanism is mounted at the bottom of the outer side of the reaction kettle body, a supporting plate is fixedly connected to the inner side of the reaction kettle body, a driving assembly is mounted on the right side of the top of the supporting plate, and a transmission assembly is mounted on the back face of the supporting plate. The middle of the top of the supporting plate is movably sleeved with a rotating rod, a mounting assembly is mounted at the bottom of the rotating rod, and a stirring assembly is mounted at the bottom of the mounting assembly. The reaction kettle main body is rapidly heated to the required temperature through the electromagnetic heating mechanism, the driving assembly and the transmission assembly are arranged to drive the rotating rod to rotate, the rotating rod drives the mounting assembly to rotate in a reciprocating mode, then ammonia gas is sprayed into liquid sodium through the gas spraying holes, and the stirring pipe can stir the liquid sodium at the same time; the ammonia gas sprayed from the gas spraying holes can be in full contact with the liquid sodium, so that the reaction efficiency is improved.

Description

TECHNICAL FIELD

[0001] The present application relates to the technical field of reaction kettles, and more particularly to a heating reaction kettle. BACKGROUND

[0002] A reaction kettle for liquid sodium and ammonia is generally used to synthesize some chemicals, such as sodium nitride, sodium amide, etc. The working principle of this kind of reaction kettle involves the reaction of liquid sodium and ammonia gas under high temperature conditions. Liquid sodium is put into a sodium ammonia kettle, the feed inlet of the sodium ammonia kettle is closed, and ammonia gas is quantitatively and constantly fed through a flowmeter after being heated to 360-400℃ by electricity. Liquid sodium reacts with ammonia gas to generate sodium amide, which is used for the next reaction. Liquid sodium amide can also be dried by a roller, cooled and sliced, and then sold as a sodium amide product. Hydrogen generated by the reaction is sent to an alkali pot for combustion through a water seal tank. The chemical equation for the reaction of liquid sodium and ammonia gas is as follows:

[0003] 2Na + 2NH3→ 2NaNH2 + H2.

[0004] The existing reaction kettle for liquid sodium and ammonia can only stir liquid sodium, and ammonia gas can only be delivered to a certain position of the reaction kettle, which cannot allow ammonia gas to be input in a large area and in a three-dimensional manner. This will result in a small contact area between ammonia gas and liquid sodium, and a low reaction rate of ammonia gas and liquid sodium, and an uneven reaction process. CONTENT OF THE UTILITY MODEL

[0005] In order to overcome the shortcomings of the prior art, the present application provides a heating reaction kettle.

[0006] To achieve the above-mentioned purpose, the present application provides the following technical scheme: a heating reaction kettle, a liquid inlet pipe is installed on the left side of the reaction kettle body, a gas inlet hose is installed on the right side of the reaction kettle body, an electromagnetic heating mechanism is installed on the bottom of the outside of the reaction kettle body, a support plate is fixedly connected to the inside of the reaction kettle body, a driving assembly is installed on the right side of the top of the support plate, a transmission assembly is installed on the back of the support plate, the driving assembly is connected to the transmission assembly, a rotating rod is movably sleeved on the top of the support plate, the top of the outside of the rotating rod is connected to the transmission assembly, an installation assembly is installed on the bottom of the rotating rod, a stirring assembly is installed on the bottom of the installation assembly, the stirring assembly comprises a fixed pipe, a stirring pipe is fixedly connected to the outside of the fixed pipe, gas injection holes are formed in the surface of the stirring pipe, and one end of the gas inlet hose inside the reaction kettle body is fixedly connected to the fixed pipe.

[0007] As a preferred technical scheme of the present application, the installation assembly comprises a top plate fixedly connected to the bottom of the rotating rod, a side plate is fixedly connected to the bottom of the top plate, a bottom plate is fixedly connected to the bottom of the side plate, and a plug rod is fixedly connected to the top of the bottom plate.

[0008] The top of the fixed pipe is sleeved with a mounting plate, and a fixing hole is formed in the surface of the mounting plate.

[0009] As a preferred technical scheme of the present application, the top of the top plate is movably sleeved with a movable rod, the bottom of the movable rod is fixedly connected with a pressing ring, and a pressure spring is sleeved outside the movable rod and located between the top plate and the pressing ring.

[0010] As a preferred technical scheme of the present application, the transmission assembly comprises two fixed blocks fixedly connected to the back of the support plate, a fixed rod fixedly connected between the two fixed blocks, a sliding plate movably sleeved outside the fixed rod, a rack plate fixedly connected to the top of the sliding plate, a transmission gear fixedly sleeved to the top of the outer side of the rotating rod, and the rack plate is engaged with the transmission gear; the rack plate is moved under the driving action of the driving assembly.

[0011] As a preferred technical scheme of the present application, the driving assembly comprises a fixed plate fixedly connected to the top of the support plate, a cylindrical rod movably sleeved with the fixed plate, a rotating disc fixedly connected to the back of the cylindrical rod, a first cylindrical block fixedly connected to the back of one side of the rotating disc, the outer side of the first cylindrical block movably sleeved at one end of a connecting plate, and the other end of the connecting plate connected with the rack plate.

[0012] As a preferred technical scheme of the present application, the right side of the rack plate is fixedly connected with two connecting blocks, a second cylindrical block fixedly connected between the two connecting blocks, and the second cylindrical block movably sleeved at the end of the connecting plate away from the first cylindrical block.

[0013] As a preferred technical scheme of the present application, the driving assembly further comprises a driving motor fixedly connected to the right side of the reaction kettle body, a worm fixedly connected to the output shaft of the driving motor through the reaction kettle body, and a worm gear fixedly sleeved to the front of the cylindrical rod, and the worm is engaged with the worm gear.

[0014] As a preferred technical scheme of the present application, a pressure detector is installed on the top of the reaction kettle body, a gas outlet pipe is installed on the top of the reaction kettle body, and a liquid outlet pipe is installed on the bottom of the reaction kettle body.

[0015] Compared with the prior art, the present application has the following advantages:

[0016] 1. The application is provided with driving assembly, transmission assembly, rotating rod and transmission gear, in the process of ammonia gas, start driving motor to drive the worm rotation, through the meshing effect of worm gear drive cylindrical rod rotation, so that the rotating disc can drive one end of the connecting plate to make circular swing, in turn, the connecting plate can drive the rack plate to move back and forth in left and right direction, through the meshing effect of rack plate and transmission gear, rotating rod drive installation assembly reciprocating rotation, in turn, ammonia gas is sprayed in the liquid sodium through the air jet hole, the stirring pipe can stir the liquid sodium at the same time, the ammonia gas sprayed by the air jet hole can fully contact with the liquid sodium, improve the reaction efficiency.

[0017] 2. The application is provided with installation assembly and mounting plate, the plug rod and the fixed hole are matched with each other, the plug rod is inserted into the inside of the fixed hole, the mounting plate can be fixed in horizontal direction, when the installation assembly rotates, it can drive the stirring assembly to rotate, the pressure spring has downward pressure on the pressing ring, so that the bottom of the mounting plate is attached to the top of the bottom plate, avoiding the separation of the fixed hole and the plug rod, making the installation stable between the stirring assembly and the installation assembly. BRIEF DESCRIPTION OF DRAWINGS

[0018] In order to more clearly illustrate the technical scheme in the embodiments of the application or prior art, the following will briefly introduce the drawings needed to be used in the embodiment or prior art description. Obviously, the drawings in the following description are some embodiments of the application, and those skilled in the art can obtain other drawings according to these drawings without creative labor.

[0019] Figure 1 The structure of the application is shown in the figure;

[0020] Figure 2 The main body of the reaction kettle is shown in the figure;

[0021] Figure 3 The driving assembly structure of the application is shown in the figure;

[0022] Figure 4 The transmission assembly structure of the application is shown in the figure;

[0023] Figure 5 The installation assembly structure of the application is shown in the figure;

[0024] Figure 6 The stirring assembly structure of the application is shown in the figure.

[0025] In the figure: 1, reaction kettle main body; 101, liquid inlet pipe; 102, gas inlet hose; 103, pressure detector; 104, electromagnetic heating mechanism; 105, gas outlet pipe; 106, liquid outlet pipe; 2, support plate; 3, drive assembly; 301, fixed plate; 302, cylindrical rod; 303, rotating disc; 304, first cylindrical block; 305, connecting plate; 306, worm gear; 307, drive motor; 308, worm; 4, transmission assembly; 401, fixed block; 402, fixed rod; 403, sliding plate; 404, rack plate; 405, connecting block; 406, second cylindrical block; 5, rotating rod; 501, transmission gear; 6, mounting assembly; 601, top plate; 602, side plate; 603, bottom plate; 604, insertion rod; 605, movable rod; 606, pressing ring; 607, pressure spring; 7, stirring assembly; 701, fixed pipe; 702, stirring pipe; 703, air injection hole; 704, mounting plate; 705, fixed hole. DETAILED DESCRIPTION

[0026] To make the objectives, technical solutions and advantages of the embodiments of the present application clearer, the technical solutions in the embodiments of the present application are clearly and completely described below. Obviously, the described embodiments are some but not all of the embodiments of the present application. Based on the embodiments in the present application, all other embodiments obtained by those of ordinary skill in the art without creative work fall within the scope of the present application.

[0027] As shown in Figures 1 to 6 The heating reaction kettle provided by the present application comprises a reaction kettle main body 1, a liquid inlet pipe 101 is installed on the left side of the reaction kettle main body 1, a gas inlet hose 102 is installed on the right side of the reaction kettle main body 1, an electromagnetic heating mechanism 104 is installed on the bottom of the outer side of the reaction kettle main body 1, a support plate 2 is fixedly connected to the inner side of the reaction kettle main body 1, a drive assembly 3 is installed on the right side of the top of the support plate 2, a transmission assembly 4 is installed on the back of the support plate 2, the drive assembly 3 is connected to the transmission assembly 4, a rotating rod 5 is movably sleeved on the top of the support plate 2, the top of the outer side of the rotating rod 5 is connected to the transmission assembly 4, a mounting assembly 6 is installed on the bottom of the rotating rod 5, a stirring assembly 7 is installed on the bottom of the mounting assembly 6, the stirring assembly 7 comprises a fixed pipe 701, a stirring pipe 702 is fixedly connected to the outer side of the fixed pipe 701, air injection holes 703 are formed in the surface of the stirring pipe 702, and one end of the gas inlet hose 102 located on the inner side of the reaction kettle main body 1 is fixedly connected to the fixed pipe 701.

[0028] In the embodiment of the present application, liquid sodium is poured into the inside of the reaction kettle body 1 through the liquid inlet pipe 101, and the reaction kettle body 1 is rapidly heated to 360-400°C by the electromagnetic heating mechanism 104. The electromagnetic heating mechanism 104 can refer to the relevant description in the prior art, which will not be described here. The electromagnetic heating mechanism 104 has the effects of energy saving, environmental protection, and rapid heating. The reaction kettle body 1 can be made of metal.

[0029] After being heated to 360-400°C, ammonia gas is added to the inside of the reaction kettle body 1 through the gas inlet hose 102. The ammonia gas passes through the fixed pipe 701 and is sprayed out from the air injection hole 703 of the stirring pipe 702. In the process of adding ammonia gas, the driving assembly 3 drives the transmission assembly 4 to rotate, the transmission assembly 4 drives the rotating rod 5 to rotate, and the rotating rod 5 drives the mounting assembly 6 to rotate reciprocally. Then, the ammonia gas is sprayed into the liquid sodium through the air injection hole 703 of the stirring pipe 702, and the stirring pipe 702 can stir the liquid sodium at the same time, so that the ammonia gas sprayed out of the air injection hole 703 can fully contact with the liquid sodium, thereby improving the reaction efficiency.

[0030] The mounting assembly 6 includes a top plate 601 fixedly connected to the bottom of the rotating rod 5, a side plate 602 fixedly connected to the bottom of the top plate 601, a bottom plate 603 fixedly connected to the bottom of the side plate 602, a plug rod 604 fixedly connected to the top of the bottom plate 603, and a mounting plate 704 fixedly sleeved with the top of the fixed pipe 701. The surface of the mounting plate 704 is provided with a fixed hole 705.

[0031] The plug rod 604 and the fixed hole 705 are mutually matched. The mounting plate 704 is connected with the bottom plate 603 by inserting the plug rod 604 into the inside of the fixed hole 705, so as to fix the mounting plate 704 in the horizontal direction. When the mounting assembly 6 rotates under the driving of the rotating rod 5, the mounting plate 704 can rotate, thereby driving the fixed pipe 701 to rotate.

[0032] The top of the top plate 601 movably sleeved with an active rod 605, the bottom of the active rod 605 is fixedly connected with a pressing ring 606, the outer side of the active rod 605 is sleeved with a pressure spring 607, and the pressure spring 607 is located between the top plate 601 and the pressing ring 606.

[0033] The pressure spring 607 has a downward pressure on the pressing ring 606, so that the bottom of the mounting plate 704 is attached to the top of the bottom plate 603, avoiding the separation of the fixed hole 705 and the plug rod 604, and improving the stability of the mounting assembly 6 when driving the stirring assembly 7 to rotate.

[0034] The transmission assembly 4 comprises two fixed blocks 401 fixedly connected to the back of the support plate 2, a fixed rod 402 fixedly connected between the two fixed blocks 401, a sliding plate 403 movably sleeved on the outer side of the fixed rod 402, a rack plate 404 fixedly connected to the top of the sliding plate 403, and a transmission gear 501 fixedly sleeved on the top of the outer side of the rotating rod 5, wherein the rack plate 404 is engaged with the transmission gear 501.

[0035] The driving assembly 3 is connected with the rack plate 404 and can drive the rack plate 404 to reciprocate. Since the rack plate 404 is connected between the two fixed blocks 401 through the sliding plate 403 and the fixed rod 402, the rack plate 404 reciprocates horizontally along the fixed rod 402 between the two fixed blocks 401 during movement. Since the rack plate 404 is engaged with the transmission gear 501, the rack plate 404 drives the transmission gear 501 to reciprocate during horizontal reciprocation, so that the rotating rod 5 and the stirring pipe 702 also reciprocate, and the ammonia gas is rotated clockwise or counterclockwise to further improve the sufficiency of contact between the ammonia gas and the liquid sodium.

[0036] The driving assembly 3 comprises a fixed plate 301 fixedly connected to the top of the support plate 2, a cylindrical rod 302 movably sleeved on the fixed plate 301, a rotating disc 303 fixedly connected to the back of the cylindrical rod 302, a first cylindrical block 304 fixedly connected to one side of the back of the rotating disc 303, and a connecting plate 305 movably sleeved on one end of the first cylindrical block 304, wherein the other end of the connecting plate 305 is connected with the rack plate 404.

[0037] When the rotating disc 303 rotates with the cylindrical rod 302, the first cylindrical block 304 also rotates around the cylindrical rod 302 with the rotating disc 303. Since one end of the connecting plate 305 is movably sleeved on the first cylindrical block 304 and the other end is connected with the rack plate 404, the connecting plate 305 drives the rack plate 405 to reciprocate horizontally left and right when the first cylindrical block 304 rotates around the cylindrical rod 302 under the restriction that the rack plate 404 can only move horizontally.

[0038] The rack plate 404 is fixedly connected with two connecting blocks 405 on the right side, the two connecting blocks 405 are fixedly connected with a second cylindrical block 406, and the second cylindrical block 406 is movably sleeved on the end of the connecting plate 305 away from the first cylindrical block 304.

[0039] The end of the connecting plate 305 away from the first cylindrical block 304 is sleeved on the second cylindrical block 406 and located between the two connecting blocks 405, so that the connecting plate 305 drives the rack plate 404 to move through the second cylindrical block 406 and the connecting blocks 405 under the drive of the first cylindrical block 304.

[0040] The driving assembly 3 further comprises a driving motor 307 fixedly connected to the right side of the reaction kettle body 1, the output shaft of the driving motor 307 is fixedly connected with a worm 308 penetrating through the reaction kettle body 1, the front surface of the cylindrical rod 302 is fixedly sleeved with a worm wheel 306, and the worm 308 is engaged with the worm wheel 306.

[0041] The driving motor 307 is started, the driving motor 307 drives the worm 308 to rotate, the worm 308 drives the worm wheel 306 to rotate, and since the worm wheel 306 and the rotating disc 303 are both fixedly sleeved on the cylindrical rod 302, the rotating disc 303 can be driven to rotate, so that the rack plate 404 can be driven to move.

[0042] The top of the reaction kettle body 1 is provided with a pressure detector 103, the top of the reaction kettle body 1 is provided with a gas outlet pipe 105, and the bottom of the reaction kettle body 1 is provided with a liquid outlet pipe 106. The hydrogen obtained after the reaction can be discharged from the top through the gas outlet pipe 105, and the sodium amide can be discharged from the bottom through the liquid outlet pipe 106. The pressure detector 103 can monitor the pressure in the reaction kettle body 1 during the reaction. It should be noted that the top of the reaction kettle body 1 is not sealed by the supporting plate 2, so that the hydrogen generated by the reaction can be discharged from the top.

[0043] The working principle and use process of the present application are as follows:

[0044] The liquid sodium is poured into the inside of the reaction kettle body 1 through the liquid inlet pipe 101, and after being heated to 360-400 DEG C by the electromagnetic heating mechanism 104, the ammonia gas is introduced through the gas inlet hose 102, the fixed pipe 701 and the stirring pipe 702. In the process of introducing the ammonia gas, the driving motor 307 is started to drive the worm 308 to rotate, the cylindrical rod 302 is driven to rotate through the meshing action of the worm wheel 306, so that one end of the connecting plate 305 can be circularly oscillated by the rotating disc 303, and then the connecting plate 305 can drive the rack plate 404 to move back and forth in the left and right directions, the rack plate 404 and the transmission gear 501 are engaged, the rotating rod 5 drives the mounting assembly 6 to rotate back and forth, and then the ammonia gas is sprayed into the liquid sodium through the gas injection hole 703, the stirring pipe 702 can stir the liquid sodium at the same time, so that the ammonia gas sprayed out of the gas injection hole 703 can fully contact with the liquid sodium, and the reaction efficiency is improved.

[0045] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present application, but not to limit them; although the present application has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that the technical solutions recorded in the foregoing embodiments can be modified, or some or all of the technical features can be replaced by equivalents; and these modifications or replacements do not make the essence of the corresponding technical solutions deviate from the scope of the technical solutions of the embodiments of the present application.

Claims

1. A heating reactor comprising a reactor body (1), characterized in that: The left side of the reaction kettle body (1) is provided with a liquid inlet pipe (101), the right side of the reaction kettle body (1) is provided with an air inlet hose (102), the bottom outside of the reaction kettle body (1) is provided with an electromagnetic heating mechanism (104), the inside of the reaction kettle body (1) is fixedly connected with a support plate (2), the right side of the top of the support plate (2) is provided with a driving assembly (3), the back of the support plate (2) is provided with a transmission assembly (4), the driving assembly (3) is connected with the transmission assembly (4), the top of the support plate (2) is movably sleeved with a rotating rod (5), the top of the outside of the rotating rod (5) is connected with the transmission assembly (4), the bottom of the rotating rod (5) is provided with a mounting assembly (6), the bottom of the mounting assembly (6) is provided with a stirring assembly (7), the stirring assembly (7) comprises a fixed pipe (701), the outside of the fixed pipe (701) is fixedly connected with a stirring pipe (702), a plurality of air injection holes (703) are formed in the surface of the stirring pipe (702), and one end of the air inlet hose (102) inside the reaction kettle body (1) is fixedly connected with the fixed pipe (701).

2. The heating reactor of claim 1, wherein: The mounting assembly (6) comprises a top plate (601) fixedly connected to the bottom of the rotating rod (5), the bottom of the top plate (601) is fixedly connected with a side plate (602), the bottom of the side plate (602) is fixedly connected with a bottom plate (603), and the top of the bottom plate (603) is fixedly connected with a plug rod (604). The top of the fixed pipe (701) is movably sleeved with a mounting plate (704), and the surface of the mounting plate (704) is provided with a fixed hole (705).

3. The heated reaction vessel of claim 2, wherein: The top of the top plate (601) is movably sleeved with an elastic rod (605), the bottom of the elastic rod (605) is fixedly connected with a pressing ring (606), the outside of the elastic rod (605) is sleeved with a pressure spring (607), and the pressure spring (607) is located between the top plate (601) and the pressing ring (606).

4. The heating reactor of claim 1, wherein, The transmission assembly (4) comprises two fixed blocks (401) fixedly connected to the back of the support plate (2), a fixed rod (402) fixedly connected between the two fixed blocks (401), a sliding plate (403) movably sleeved outside the fixed rod (402), a rack plate (404) fixedly connected to the top of the sliding plate (403), a transmission gear (501) fixedly sleeved outside the top of the rotating rod (5), and the rack plate (404) is engaged with the transmission gear (501). The rack plate (404) moves under the driving action of the driving assembly (3).

5. The heating reactor of claim 4, wherein, The driving assembly (3) comprises a fixed plate (301) fixedly connected to the top of the support plate (2), the fixed plate (301) movably sleeved with a cylindrical rod (302), the back of the cylindrical rod (302) is fixedly connected with a rotating disc (303), the back of the rotating disc (303) is fixedly connected with a first cylindrical block (304), the outer side of the first cylindrical block (304) is movably sleeved on one end of a connecting plate (305), the other end of the connecting plate (305) is connected with the rack plate (404).

6. The heating reactor of claim 5, wherein, The right side of the rack plate (404) is fixedly connected with two connecting blocks (405), the two connecting blocks (405) are fixedly connected with a second cylindrical block (406) between the two connecting blocks (405), the second cylindrical block (406) is movably sleeved on the end of the connecting plate (305) away from the first cylindrical block (304).

7. The heated reaction vessel of claim 5, wherein: The driving assembly (3) further comprises a driving motor (307) fixedly connected to the right side of the reaction kettle body (1), the output shaft of the driving motor (307) penetrates through the reaction kettle body (1) and is fixedly connected with a worm (308), the front of the cylindrical rod (302) is fixedly sleeved with a worm wheel (306), and the worm (308) is engaged with the worm wheel (306).

8. The heated reaction vessel of any one of claims 1-7, wherein: The top of the reaction kettle body (1) is provided with a pressure detector (103), the top of the reaction kettle body (1) is provided with an air outlet pipe (105), and the bottom of the reaction kettle body (1) is provided with a liquid outlet pipe (106).

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